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CN107216117A - Volcanic rock ceramic article and preparation method thereof - Google Patents

Volcanic rock ceramic article and preparation method thereof Download PDF

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Publication number
CN107216117A
CN107216117A CN201710559660.7A CN201710559660A CN107216117A CN 107216117 A CN107216117 A CN 107216117A CN 201710559660 A CN201710559660 A CN 201710559660A CN 107216117 A CN107216117 A CN 107216117A
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China
Prior art keywords
volcanic rock
ball milling
ceramic article
preparation
parts
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710559660.7A
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Chinese (zh)
Inventor
牛柏然
王镭
华涛
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Heilongjiang Volcanic Rock Science And Technology Co Ltd
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Heilongjiang Volcanic Rock Science And Technology Co Ltd
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Priority to CN201710559660.7A priority Critical patent/CN107216117A/en
Publication of CN107216117A publication Critical patent/CN107216117A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/04Clay; Kaolin
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/24Manufacture of porcelain or white ware

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

Volcanic rock ceramic article and preparation method thereof, it is related to a kind of ceramic article and preparation method thereof.It is an object of the invention to provide simple and environmentally-friendly volcanic rock ceramic article of a kind of manufacture craft and preparation method thereof.Volcanic rock ceramic article is made up of alkalic volcanic rock, kaolin and Red Stone Ware.Method:First, by alkalic volcanic rock powder and kaolin ball milling, Red Stone Ware is added, liquid handling to humidity is the 10%~15% of primary liquid by ball milling;2nd, press filt, mud refining bar, throwing dries, repaired biscuit, is put into low temperature electrical kiln, fires 5 hours, is fired from 0 DEG C to 800 DEG C, the system of reburning is taken out after cooling 9.5 hours, from 0 DEG C to 1300 DEG C, and cooling obtains volcanic rock ceramic article.The inventive method is simple, the ceramic article environmental protection of preparation.The invention belongs to ceramic field.

Description

Volcanic rock ceramic article and preparation method thereof
Technical field
The present invention relates to a kind of ceramic article and preparation method thereof.
Background technology
Ceramics, English:china.Chinese have just invented pottery early in about B.C. 8000-2000 (Neolithic Age) Device.The vessel fired with clay are pottery, and the vessel fired with china clay are porcelain.It is ceramic then be pottery, stoneware and porcelain it is total Claim.Every is raw material with clay and china clay both clays of different nature, by the technique stream such as dispensing, shaping, drying, roasting The implements that journey is made can be ceramics.
Contemporary people focus on the health of oneself, to contain food vessel whether environment protection health is paid special attention to.
The content of the invention
It is an object of the invention to provide a kind of simple and environmentally-friendly volcanic rock ceramic article of manufacture craft and its preparation side Method.
Volcanic rock ceramic article is by weight by 1 part~11.9 parts of alkalic volcanic rock, 88.1 parts~99 parts of kaolinite Soil and 20 parts of Red Stone Ware are made.
The preparation method of volcanic rock ceramic article, the preparation method is as follows:
First, Volcanic Region ground surface is chosen to the Alkaline Volcano rock of the next meter of depth in ground, is rejected impurity, is crushed, be put into star Border ball mill, 2 ± 0.1h of ball milling, sieving obtains the alkalic volcanic rock powder of 200 mesh, Alkaline Volcano rock wherein in ball grinder, The mass ratio of water and ball milling is 1:1:1.5;
2nd, the alkalic volcanic rock powder and 88.1 parts~99 parts of kaolin for weighing 1 part~11.9 parts by weight are filled Enter in rubber ball grinder, add ball milling, 3 ± 0.1h of ball milling takes out ball milling liquid, crosses 250 mesh sieves, go the removal of impurity, ball grinder The mass ratio of interior alkalic volcanic rock powder and kaolin gross mass, the quality of water and ball milling is 1:1:1.5;
3rd, the Red Stone Ware of 20 parts by weight is added into the product obtained by step 2, then mixture is put into ball mill, Ball milling takes out ball milling liquid after 2 hours, cross 250 mesh sieves, go the removal of impurity, liquid is placed in drying baker, in 30 DEG C of bar of constant temperature Handled under part to 10%~15% that humidity is primary liquid;
4th, step 3 products therefrom is put into slip drying press and carries out press filt, taken out the mud cake that slip drying press has been squeezed, mud cake is put Enter in vacuum pugmill, carry out vacuum mud refining operation, take out the mud bar refined, be placed again into vacuum pugmill, repeatedly operation Until the shale feel produced is fine and smooth, the mud refined is placed on Blank drawing machine rotating disk, artificial hand throwing is carried out, by the base drawn Body, which is placed, to dry in the air on base frame, is dried, while keeping humidity to be the 25%~35% of original base substrate humidity, base substrate is repaiied Base, the side wall thickness for keeping the base substrate vertical tangent plane fixed is 0.3cm~0.8cm;
5th, the base substrate fixed in step 4 is put into low temperature electrical kiln, fired 5 hours, fired from 0 DEG C to 800 DEG C, cooling After take out base substrate;
6th, the base substrate that will be handled by step 5, is fired 9.5 hours, from 0 DEG C to 1300 DEG C, cooling, obtains volcanic rock pottery Porcelain articles for use.
Advantages of the present invention:
Volcanic Region surface is generally volcanic agglomerate to the deep alkalic volcanic rock in next meter of ground, is black, the volcano of aubergine Clastic rock, and almost it is all the several centimetres to tens centimetres of basaltic foam chip and particle diameter, irregular of black or aubergine The volcano dust do not remembered is divided into identical, finer and smoother volcano gravel Filling Cementation, and degree of consolidation is not high, and rock is loosely easy It is broken.It is easy to gather, the work such as ball milling.By investigating, relative to the volcanic rock in other orientation, floor surface to next meter of ground depth Alkalic volcanic rock have one it is important and it is obvious the characteristics of, be exactly in rock generally containing potassium height, other oxide contents between Between 4.28~5.80%, average 5.28%;Sodium oxide content is between 3.25~4.52% or so;Averagely 3.63%;Oxidation Sodium and potassium oxide sum are more than 8%, and potassium oxide content is more than sodium oxide molybdena.In this alkali basalt more regional than other Potassium oxide content is higher by 1~4 times, and sodium oxide molybdena then the content more regional than other close to or it is relatively low.In a word, the selected fire of works Mountain area surface is to be rich in alkaline potassium matter volcano with oneself uniqueness on chemical feature to the volcanic rock of the next meter of depth in ground The chemical group and property of rock, the Typical Representative-Japan's lava for deviateing so-called ' Pacific type ' calcic rock stone are more farther, together When, the mineral matter element that the works produced are sustained out also depends on the selection of material.
First sintering of the present invention, improves base substrate hardness, it is unnecessary that reduction is produced in experimentation because of external force Breakage, meanwhile, it is once sintered to contribute to second of sinter molding, increase the success rate burnt till.
Red Stone Ware is added in the present invention, Red Stone Ware raw material belongs to simple ore original into mud, is the higher mud ore deposit of iron-holder, and have Excellent performance, plasticity can be improved by adding in works, improve the blank strength after shaping, the drying shrinkage phase of base substrate To smaller, make works will not at a temperature of external environment condition season cracking.Sintering temperature is low and degree of crystallizing into is high, and mud weight is husky Property is small, and slip casting performance is good, is conducive to works injection forming.The boccaro porosity after burning till is larger, can be just by works Mineral matter element be fully sustained.The inventive method is simple, the ceramic article environmental protection of preparation.
Embodiment
Technical solution of the present invention is not limited to act embodiment set forth below, in addition between each embodiment Any combination.
Embodiment one:Volcanic rock ceramic article is by weight by 1 part~11.9 parts of alkalic volcanic rock, 88.1 Part~99 parts of kaolin and 20 parts of Red Stone Ware be made.
Embodiment two:Present embodiment and volcanic rock ceramic article unlike embodiment one are by weight Number is made up of 2 parts~10 parts of alkalic volcanic rock, 90 parts~92 parts of kaolin and 20 parts of Red Stone Ware.Other and specific reality Apply mode one identical.
Embodiment three:The preparation method of volcanic rock ceramic article described in embodiment one:
First, Volcanic Region ground surface is chosen to the Alkaline Volcano rock of the next meter of depth in ground, is rejected impurity, is crushed, be put into star Border ball mill (model F-P2000, producer is Fu Kasi companies), 2 ± 0.1h of ball milling, sieving obtains the Alkaline Volcano of 200 mesh Rock dust end, the mass ratio of Alkaline Volcano rock, water and ball milling is 1 wherein in ball grinder:1:1.5;
2nd, the alkalic volcanic rock powder and 88.1 parts~99 parts of kaolin for weighing 1 part~11.9 parts by weight are filled Enter in rubber ball grinder (model F-P2000, producer is Fu Kasi companies), add ball milling, 3 ± 0.1h of ball milling takes out ball Grinding fluid body, crosses 250 mesh sieves, removes alkalic volcanic rock powder and kaolin gross mass, the quality of water and ball milling in the removal of impurity, ball grinder The mass ratio of son is 1:1:1.5;
3rd, the Red Stone Ware of 20 parts by weight is added into the product obtained by step 2, mixture is then put into ball mill (type Number it is F-P2000, producer is Fu Kasi companies) in, ball milling takes out ball milling liquid after 2 hours, cross 250 mesh sieves, go the removal of impurity, general Liquid is placed in drying baker, is handled under conditions of 30 DEG C of constant temperature to 10%~15% that humidity is primary liquid;
4th, step 3 products therefrom is put into slip drying press (model T2500, producer is water meteors pottery art) and squeezed Mud, takes out the mud cake that slip drying press has been squeezed, mud cake is put into vacuum pugmill, carry out vacuum mud refining operation, take out the mud refined Bar, is placed again into vacuum pugmill, and the mud refined is placed Blank drawing machine and turned by operation repeatedly until the shale feel exquisiteness produced On disk, artificial hand throwing is carried out, the base substrate drawn is placed and dried in the air on base frame, is dried, while keeping humidity to be original base The 25%~35% of body humidity, repaired biscuit is carried out by base substrate, keep the side wall thickness of base substrate vertical tangent plane fixed for 0.3cm~ 0.8cm;
5th, the base substrate fixed in step 4 is put into low temperature electrical kiln, fired 5 hours, fired from 0 DEG C to 800 DEG C, cooling After take out base substrate;
6th, the base substrate that will be handled by step 5, is fired 9.5 hours, from 0 DEG C to 1300 DEG C, cooling, obtains volcanic rock pottery Porcelain articles for use.
Embodiment four:Present embodiment from ball milling is described in step one unlike embodiment three Diameter 20mm, diameter 10mm and diameter 5mm ball milling, diameter 20mm, diameter 10mm and the sub quantity ratio of diameter 5mm ball millings are 1:5:25.It is other identical with embodiment three.
Embodiment five:Present embodiment and ball milling described in step one unlike embodiment three or four 2h.It is other identical with embodiment three or four.
Embodiment six:Unlike one of present embodiment and embodiment one to five described in step 2 Ball milling is diameter 20mm, diameter 10mm and diameter 5mm ball milling, and diameter 20mm, diameter 10mm and diameter 5mm ball millings are sub Quantity ratio is 1:5:25.It is other identical with one of embodiment one to five.
Embodiment seven:Unlike one of present embodiment and embodiment one to six described in step 2 Ball milling 3h.It is other identical with one of embodiment one to six.
Embodiment eight:In perseverance in step 3 unlike one of present embodiment and embodiment one to seven Handled under conditions of 30 DEG C of temperature to 12% that humidity is primary liquid.It is other identical with one of embodiment one to seven.
Embodiment nine:In step 4 unlike one of present embodiment and embodiment one to eight simultaneously It is the 30% of original base substrate humidity to keep humidity.It is other identical with one of embodiment one to eight.
Embodiment ten:Kept in step 4 unlike one of present embodiment and embodiment one to nine The side wall thickness for the base substrate vertical tangent plane fixed is 0.5cm.It is other identical with one of embodiment one to nine.
Using following experimental verifications effect of the present invention:
Experiment one:
The preparation method of volcanic rock ceramic article, it is characterised in that the preparation method is as follows:
First, Volcanic Region ground surface is chosen to the Alkaline Volcano rock of the next meter of depth in ground, is rejected impurity, is crushed, be put into star Border ball mill, ball milling 1.9h, sieving obtains the alkalic volcanic rock powder of 200 mesh, Alkaline Volcano rock, water wherein in ball grinder Mass ratio with ball milling is 1:1:1.5;
2nd, the alkalic volcanic rock powder and 89 parts of kaolin for weighing 1 part by weight are fitted into rubber ball grinder, plus Goal mill, ball milling 2.9h takes out ball milling liquid, crosses 250 mesh sieves, removes alkalic volcanic rock powder and height in the removal of impurity, ball grinder The mass ratio of ridge soil gross mass, the quality of water and ball milling is 1:1:1.5;
3rd, the Red Stone Ware of 20 parts by weight is added into the product obtained by step 2, then mixture is put into ball mill, Ball milling takes out ball milling liquid after 2 hours, cross 250 mesh sieves, go the removal of impurity, liquid is placed in drying baker, in 30 DEG C of bar of constant temperature Handled under part to 12% that humidity is primary liquid;
4th, step 3 products therefrom is put into slip drying press and carries out press filt, taken out the mud cake that slip drying press has been squeezed, mud cake is put Enter in vacuum pugmill, carry out vacuum mud refining operation, take out the mud bar refined, be placed again into vacuum pugmill, repeatedly operation Until the shale feel produced is fine and smooth, the mud refined is placed on Blank drawing machine rotating disk, artificial hand throwing is carried out, by the base drawn Body, which is placed, to dry in the air on base frame, is dried, while keeping humidity to be the 30% of original base substrate humidity, base substrate is carried out into repaired biscuit, kept The side wall thickness for the base substrate vertical tangent plane fixed is 0.5cm;
5th, the base substrate fixed in step 4 is put into low temperature electrical kiln, fired 5 hours, fired from 0 DEG C to 800 DEG C, cooling After take out base substrate;
6th, the base substrate that will be handled by step 5, is fired 9.5 hours, from 0 DEG C to 1300 DEG C, cooling, obtains volcanic rock pottery Porcelain articles for use.
Hot water (100 DEG C), cold water (0 DEG C), (18 DEG C) of raw water are subjected to inductive plasma water quality monitoring point using ICP-MS Analysis test, test result such as following table:
Table 1
Table 2
Shown in report, the water under different temperatures is contained in the vessel of research and development, can obtain different mineral matter effects, Being clearly distinguishable from the market has the product of identical single effect.
Research and develop vessel simultaneously has degradation function to toxic heavy metal element.Beneficial mineral prime element is not influenceed to separate out.
Experiment two:
The preparation method of volcanic rock ceramic article, it is characterised in that the preparation method is as follows:
First, Volcanic Region ground surface is chosen to the Alkaline Volcano rock of the next meter of depth in ground, is rejected impurity, is crushed, be put into star Border ball mill, ball milling 2h, sieving, obtain the alkalic volcanic rock powder of 200 mesh, wherein in ball grinder Alkaline Volcano rock, water with The mass ratio of ball milling is 1:1:1.5;
2nd, the alkalic volcanic rock powder and 90 parts of kaolin for weighing 10 parts by weight are fitted into rubber ball grinder, Ball milling is added, ball milling 3h takes out ball milling liquid, crosses 250 mesh sieves, remove alkalic volcanic rock powder and height in the removal of impurity, ball grinder The mass ratio of ridge soil gross mass, the quality of water and ball milling is 1:1:1.5;
3rd, the Red Stone Ware of 20 parts by weight is added into the product obtained by step 2, then mixture is put into ball mill, Ball milling takes out ball milling liquid after 2 hours, cross 250 mesh sieves, go the removal of impurity, liquid is placed in drying baker, in 30 DEG C of bar of constant temperature Handled under part to 13% that humidity is primary liquid;
4th, step 3 products therefrom is put into slip drying press and carries out press filt, taken out the mud cake that slip drying press has been squeezed, mud cake is put Enter in vacuum pugmill, carry out vacuum mud refining operation, take out the mud bar refined, be placed again into vacuum pugmill, repeatedly operation Until the shale feel produced is fine and smooth, the mud refined is placed on Blank drawing machine rotating disk, artificial hand throwing is carried out, by the base drawn Body, which is placed, to dry in the air on base frame, is dried, while keeping humidity to be the 30% of original base substrate humidity, base substrate is carried out into repaired biscuit, kept The side wall thickness for the base substrate vertical tangent plane fixed is 0.6cm;
5th, the base substrate fixed in step 4 is put into low temperature electrical kiln, fired 5 hours, fired from 0 DEG C to 800 DEG C, cooling After take out base substrate;
6th, the base substrate that will be handled by step 5, is fired 9.5 hours, from 0 DEG C to 1300 DEG C, cooling, obtains volcanic rock pottery Porcelain articles for use.

Claims (10)

1. volcanic rock ceramic article, it is characterised in that:Volcanic rock ceramic article is by weight by 1 part~11.9 parts of alkalescence fire Mountain rock, 88.1 parts~99 parts of kaolin and 20 parts of Red Stone Ware are made.
2. volcanic rock ceramic article according to claim 1, it is characterised in that:Volcanic rock ceramic article is by weight by 2 Part~10 parts of alkalic volcanic rock, 90 parts~92 parts of kaolin and 20 parts of Red Stone Ware be made.
3. the preparation method of volcanic rock ceramic article described in claim 1, it is characterised in that the preparation method is as follows:
First, Volcanic Region ground surface is chosen to the Alkaline Volcano rock of the next meter of depth in ground, is rejected impurity, is crushed, be put into interspace ball Grinding machine, 2 ± 0.1h of ball milling, sieving, obtain the alkalic volcanic rock powder of 200 mesh, wherein in ball grinder Alkaline Volcano rock, water with The mass ratio of ball milling is 1:1:1.5;
2nd, the alkalic volcanic rock powder and 88.1 parts~99 parts of kaolin for weighing 1 part~11.9 parts by weight load rubber In glueballs grinding jar, ball milling is added, 3 ± 0.1h of ball milling takes out ball milling liquid, crosses 250 mesh sieves, remove alkali in the removal of impurity, ball grinder Property volcanic rock powder and kaolin gross mass, the quality of water and ball milling mass ratio be 1:1:1.5;
3rd, the Red Stone Ware of 20 parts by weight is added into the product obtained by step 2, then mixture is put into ball mill, ball milling Ball milling liquid is taken out after 2 hours, 250 mesh sieves is crossed, goes the removal of impurity, liquid is placed in drying baker, under conditions of 30 DEG C of constant temperature Handle to 10%~15% that humidity is primary liquid;
4th, step 3 products therefrom is put into slip drying press and carries out press filt, taken out the mud cake that slip drying press has been squeezed, mud cake is put into very In empty soil kneader, carry out vacuum mud refining operation, take out the mud bar that has refined, be placed again into vacuum pugmill, repeatedly operation until The shale feel produced is fine and smooth, and the mud refined is placed on Blank drawing machine rotating disk, carries out artificial hand throwing, the base substrate drawn is put Put and dry in the air on base frame, dried, while keeping humidity to be the 25%~35% of original base substrate humidity, base substrate is subjected to repaired biscuit, protect The side wall thickness for holding the base substrate vertical tangent plane fixed is 0.3cm~0.8cm;
5th, the base substrate fixed in step 4 is put into low temperature electrical kiln, fired 5 hours, fired to 800 DEG C, taken after cooling from 0 DEG C Go out base substrate;
6th, the base substrate that will be handled by step 5, is fired 9.5 hours, from 0 DEG C to 1300 DEG C, cooling, obtains volcanic rock ceramics use Product.
4. the preparation method of volcanic rock ceramic article according to claim 3, it is characterised in that of ball milling described in step one It is the quantity ratio of diameter 20mm, diameter 10mm and diameter 5mm ball milling, diameter 20mm, diameter 10mm and diameter 5mm ball millings For 1:5:25.
5. the preparation method of volcanic rock ceramic article according to claim 3, it is characterised in that ball milling 2h described in step one.
6. the preparation method of volcanic rock ceramic article according to claim 3, it is characterised in that of ball milling described in step 2 It is the quantity ratio of diameter 20mm, diameter 10mm and diameter 5mm ball milling, diameter 20mm, diameter 10mm and diameter 5mm ball millings For 1:5:25.
7. the preparation method of volcanic rock ceramic article according to claim 3, it is characterised in that ball milling 3h described in step 2.
8. the preparation method of volcanic rock ceramic article according to claim 3, it is characterised in that in 30 DEG C of constant temperature in step 3 Under conditions of handle to humidity be primary liquid 12%.
9. the preparation method of volcanic rock ceramic article according to claim 3, it is characterised in that keep wet simultaneously in step 4 Degree is the 30% of original base substrate humidity.
10. the preparation method of volcanic rock ceramic article according to claim 3, it is characterised in that keep what is fixed in step 4 The side wall thickness of base substrate vertical tangent plane is 0.5cm.
CN201710559660.7A 2017-07-10 2017-07-10 Volcanic rock ceramic article and preparation method thereof Pending CN107216117A (en)

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Cited By (2)

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Publication number Priority date Publication date Assignee Title
CN107721391A (en) * 2017-11-28 2018-02-23 山西晋明堂文化科技有限公司 A kind of boccaro rock mud water tank and preparation method thereof
CN107986749A (en) * 2017-11-28 2018-05-04 山西晋明堂文化科技有限公司 A kind of boccaro rock mud herbal cuisine kettle and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107721391A (en) * 2017-11-28 2018-02-23 山西晋明堂文化科技有限公司 A kind of boccaro rock mud water tank and preparation method thereof
CN107986749A (en) * 2017-11-28 2018-05-04 山西晋明堂文化科技有限公司 A kind of boccaro rock mud herbal cuisine kettle and preparation method thereof

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Application publication date: 20170929