CN107115242A - A kind of maca is combined the preparation method of buckwheat starch moisturizing lotion - Google Patents
A kind of maca is combined the preparation method of buckwheat starch moisturizing lotion Download PDFInfo
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- CN107115242A CN107115242A CN201710400634.XA CN201710400634A CN107115242A CN 107115242 A CN107115242 A CN 107115242A CN 201710400634 A CN201710400634 A CN 201710400634A CN 107115242 A CN107115242 A CN 107115242A
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- maca
- starch
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- buckwheat starch
- buckwheat
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- Medicines Containing Plant Substances (AREA)
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Abstract
A kind of maca is combined the preparation method of buckwheat starch moisturizing lotion, belongs to facial treatment milk preparing technical field, the present invention includes：Extract maca, extract buckwheat starch, prepare graininess cold water solubles buckwheat starch, prepare maca and be combined buckwheat starch moisturizing lotion.Maca produced by the present invention is combined buckwheat starch moisturizing lotion, and moisturizing rate is high, can reduce skin peeling phenomenon, makes skin smooth fine and smooth, and with white-skinned face function.
Description
Technical field
The present invention relates to facial treatment milk preparing technical field, and in particular to a kind of maca is combined buckwheat starch moisturizing lotion
Preparation method.
Background technology
Emulsion is that the active ingredients such as moisturizing, whitening and anti-aging in the most basic step of skin care, emulsion being capable of more preferable quilt
Percutaneous absorption, it is extremely important to possess one bottle of good emulsion, and emulsions many absolutely occurs in now in the market, is all closed containing a large amount of chemistry
Into thing, to skin, there may be certain side effect for long-term use so that the nutritional ingredient in emulsion is difficult to be absorbed, or even meeting
Trigger the adverse reactions such as scytitis, if selection is improper to will result in immeasurable loss, many emulsions are in system on the market
When making, the problem of selection of chemical substance and consumption have very big, and skin effect is not notable, is further improved.
The content of the invention
According to problems of the prior art, the present invention provides a kind of natural component height, and moisturizing rate height has whitening work(
The maca of effect is combined the preparation method of buckwheat starch moisturizing lotion.
The present invention uses following technical scheme：
A kind of maca is combined the preparation method of buckwheat starch moisturizing lotion, comprises the following steps：
Step one：Maca is washed, the impurity on maca surface is removed, is placed at aeration-drying and carries out after washing
Air-dry, the maca after air-drying is placed in micro-wave oven, moderate heat dries 4min；
Step 2：By dried maca, it is put into pulverizer and crushes, the maca after crushing is crossed into 60 mesh sieves, maca is obtained
Powder；
Step 3：Pueraria root powder 20g, pure water 400g are weighed, by solid-liquid ratio 1:20 add in container, are carried in being decocted at 90 DEG C
100min is taken, the material in container is all taken out, room temperature is cooled to, is filtered with cryogenic freezing centrifuge, rotating speed is 3000r/
Min, centrifugation time 5min, collect supernatant, and Maca extract is obtained after filtering；
Step 4：According to the mass fraction, by 4 parts of Maca extracts, 10 parts of glycerine, 4 parts of propane diols, 0.4 part of triethanolamine
It is added in 78 parts of deionized waters, 80 DEG C of heating stirrings are until dissolving, is made aqueous phase liquid；
Step 5：According to the mass fraction, by 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxyethylene sorbitan lists
Laurate, 0.4 part of xanthan gum, uniform stirring 15min, is made oil phase liquid under the conditions of 80 DEG C；
Step 6：By buckwheat fine powder with bath raio 1:2.5 add in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C
2h is soaked, mixed solution is obtained；
Step 7：Mixed solution under 4000r/min is centrifuged into 10min with centrifuge, upper strata dark matter is wiped off, it is heavy to take
Form sediment and wash one time, cleaned 3 times, washed again after filtering 2 times with the sodium hydroxide solution of mass concentration 0.2% after filtering, suction filtration mistake
Filter, is dried overnight in 45 DEG C of baking oven, crushed 100 mesh sieves, and obtained buckwheat starch；
Step 8：By bath raio 1:Buckwheat starch with the ethanol solution of volumetric concentration 80% is mixed to obtain starch suspension by 20,
It is placed in 70 DEG C of thermostat water baths, while concentration is slowly dropped into starch suspension for 10.5g/100mL sodium hydroxide solution
In liquid, starch suspension pH value is remained at 7-7.5, and be stirred continuously, suction filtration after reaction 80min；
Step 9：Starch obtained by suction filtration is neutralized to neutrality with 3mol/L hydrochloric acid solution, with the second of volumetric concentration 70%
Alcoholic solution is cleaned twice, and supernatant is discarded after precipitation, then is cleaned twice with the ethanol solution of volumetric concentration 85%, is discarded after precipitation
Supernatant, is finally cleaned once with the ethanol solution of volumetric concentration 95% again, and suction filtration crushed 100 mesh after 45 DEG C of oven for drying
Sieve, obtains graininess cold water solubles buckwheat starch；
Step 10：Under conditions of being stirred continuously, oil phase liquid made from step 5 is added slowly to step 4 and is made
Aqueous phase liquid in, using high speed disperser stir 5min, then add 3 mass parts graininess cold water solubles buckwheat starch, continue
3min is stirred using high speed disperser, cooling discharging had both obtained maca and has been combined buckwheat starch moisturizing lotion.
It is preferred that, the mixing speed of the high speed disperser described in step 10 is 5000r/min.
The beneficial effects of the present invention are：
1) maca is it is verified that containing the composition such as polysaccharide, Polyphenols and alkaloid, macamide, maca ene, this
A little compositions are widely used in cosmetics.Such as polysaccharide composition, the composition such as hyaluronic acid, glucan, biological carbohydrate gum, oneself
Through the synonym as cosmetics moisture-keeping efficacy, and maca has excellent white-skinned face function rich in several amino acids.
2) protein of buckwheat seed, fat content are higher than rice and wheat, and vitamin B2 content is higher than other grains
4-24 times, and containing chlorophyll and rutin, have functions that to moisten and repair skin for making emulsion.
3) buckwheat starch is used as a kind of natural biological macromolecular therein, aboundresources, and cheap, easy biological drop
Solve, do not result in pollution, be a kind of green raw material.
4) emulsion prepared using this method has natural component high, and moisturizing rate is high, can reduce skin peeling phenomenon, make skin
The smooth exquisiteness of skin, and with white-skinned face function.
Embodiment
Below with reference to specific embodiment, the present invention is described further.
Embodiment 1
A kind of maca is combined the preparation method of buckwheat starch moisturizing lotion, comprises the following steps：
Step one：Maca is washed, the impurity on maca surface is removed, is placed at aeration-drying and carries out after washing
Air-dry, the maca after air-drying is placed in micro-wave oven, moderate heat dries 4min；
Step 2：By dried maca, it is put into pulverizer and crushes, the maca after crushing is crossed into 60 mesh sieves, maca is obtained
Powder；
Step 3：Pueraria root powder 20g, pure water 400g are weighed, by solid-liquid ratio 1:20 add in container, are carried in being decocted at 90 DEG C
100min is taken, the material in container is all taken out, room temperature is cooled to, is filtered with cryogenic freezing centrifuge, rotating speed is 3000r/
Min, centrifugation time 5min, collect supernatant, and Maca extract is obtained after filtering；
Step 4：According to the mass fraction, by 4 parts of Maca extracts, 10 parts of glycerine, 4 parts of propane diols, 0.4 part of triethanolamine
It is added in 78 parts of deionized waters, 80 DEG C of heating stirrings are until dissolving, is made aqueous phase liquid；
Step 5：According to the mass fraction, by 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxyethylene sorbitan lists
Laurate, 0.4 part of xanthan gum, uniform stirring 15min, is made oil phase liquid under the conditions of 80 DEG C；
Step 6：By buckwheat fine powder with bath raio 1:2.5 add in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C
2h is soaked, mixed solution is obtained；
Step 7：Mixed solution under 4000r/min is centrifuged into 10min with centrifuge, upper strata dark matter is wiped off, it is heavy to take
Form sediment and wash one time, cleaned 3 times, washed again after filtering 2 times with the sodium hydroxide solution of mass concentration 0.2% after filtering, suction filtration mistake
Filter, is dried overnight in 45 DEG C of baking oven, crushed 100 mesh sieves, and obtained buckwheat starch；
Step 8：By bath raio 1:Buckwheat starch with the ethanol solution of volumetric concentration 80% is mixed to obtain starch suspension by 20,
It is placed in 70 DEG C of thermostat water baths, while concentration is slowly dropped into starch suspension for 10.5g/100mL sodium hydroxide solution
In liquid, starch suspension pH value is remained at 7-7.5, and be stirred continuously, suction filtration after reaction 80min；
Step 9：Starch obtained by suction filtration is neutralized to neutrality with 3mol/L hydrochloric acid solution, with the second of volumetric concentration 70%
Alcoholic solution is cleaned twice, and supernatant is discarded after precipitation, then is cleaned twice with the ethanol solution of volumetric concentration 85%, is discarded after precipitation
Supernatant, is finally cleaned once with the ethanol solution of volumetric concentration 95% again, and suction filtration crushed 100 mesh after 45 DEG C of oven for drying
Sieve, obtains graininess cold water solubles buckwheat starch；
Step 10：Under conditions of being stirred continuously, oil phase liquid made from step 5 is added slowly to step 4 and is made
Aqueous phase liquid in, using high speed disperser stir 5min, then add 3 mass parts graininess cold water solubles buckwheat starch, continue
3min is stirred using high speed disperser, cooling discharging had both obtained maca and has been combined buckwheat starch moisturizing lotion.
The mixing speed of high speed disperser described in step 10 is 5000r/min.
Claims (2)
1. a kind of maca is combined the preparation method of buckwheat starch moisturizing lotion, it is characterised in that comprise the following steps：
Step one：Maca is washed, the impurity on maca surface is removed, is placed on after washing at aeration-drying and enters sector-style
It is dry, the maca after air-drying is placed in micro-wave oven, moderate heat dries 4min；
Step 2：By dried maca, it is put into pulverizer and crushes, the maca after crushing is crossed into 60 mesh sieves, pueraria root powder is obtained；
Step 3：Pueraria root powder 20g, pure water 400g are weighed, by solid-liquid ratio 1:20 add in container, are extracted in being decocted at 90 DEG C
100min, the material in container is all taken out, room temperature is cooled to, is filtered with cryogenic freezing centrifuge, rotating speed is 3000r/
Min, centrifugation time 5min, collect supernatant, and Maca extract is obtained after filtering；
Step 4：According to the mass fraction, 4 parts of Maca extracts, 10 parts of glycerine, 4 parts of propane diols, 0.4 part of triethanolamine are added
Into 78 parts of deionized waters, 80 DEG C of heating stirrings are until dissolving, is made aqueous phase liquid；
Step 5：According to the mass fraction, by 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxyethylene sorbitan list bays
Acid esters, 0.4 part of xanthan gum, uniform stirring 15min, is made oil phase liquid under the conditions of 80 DEG C；
Step 6：By buckwheat fine powder with bath raio 1:2.5 add mass concentration in 2% sodium sulfite aqueous solution, 50 DEG C are soaked
2h, obtains mixed solution；
Step 7：Mixed solution under 4000r/min is centrifuged into 10min with centrifuge, upper strata dark matter is wiped off, takes precipitation water
Wash one time, cleaned 3 times, washed again after filtering 2 times, filtered off with suction with the sodium hydroxide solution of mass concentration 0.2% after filtering,
It is dried overnight in 45 DEG C of baking oven, crushed 100 mesh sieves, and obtained buckwheat starch；
Step 8：By bath raio 1:Buckwheat starch with the ethanol solution of volumetric concentration 80% is mixed to obtain starch suspension by 20, is placed in
In 70 DEG C of thermostat water baths, while concentration is slowly dropped in starch suspension for 10.5g/100mL sodium hydroxide solution,
Starch suspension pH value is remained at 7-7.5, and be stirred continuously, suction filtration after reaction 80min；
Step 9：Starch obtained by suction filtration is neutralized to neutrality with 3mol/L hydrochloric acid solution, the ethanol with volumetric concentration 70% is molten
Liquid is cleaned twice, and supernatant is discarded after precipitation, then is cleaned twice with the ethanol solution of volumetric concentration 85%, and supernatant is discarded after precipitation
Liquid, is finally cleaned once with the ethanol solution of volumetric concentration 95% again, and suction filtration was crushed 100 mesh sieves, and obtained after 45 DEG C of oven for drying
To graininess cold water solubles buckwheat starch；
Step 10：Under conditions of being stirred continuously, oil phase liquid made from step 5 is added slowly to water made from step 4
In phase liquid, 5min is stirred using high speed disperser, 3 mass parts graininess cold water solubles buckwheat starch is then added, is continuing with
High speed disperser stirs 3min, and cooling discharging had both obtained maca and has been combined buckwheat starch moisturizing lotion.
2. a kind of maca according to claim 1 is combined the preparation method of buckwheat starch moisturizing lotion, it is characterised in that：Step
The mixing speed of high speed disperser described in rapid ten is 5000r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710400634.XA CN107115242A (en) | 2017-05-31 | 2017-05-31 | A kind of maca is combined the preparation method of buckwheat starch moisturizing lotion |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710400634.XA CN107115242A (en) | 2017-05-31 | 2017-05-31 | A kind of maca is combined the preparation method of buckwheat starch moisturizing lotion |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108553375A (en) * | 2018-07-02 | 2018-09-21 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of Whitening, spot lotion |
| CN108653114A (en) * | 2018-08-04 | 2018-10-16 | 芜湖慧宇商贸有限公司 | A kind of preparation method of the moisturizing emulsion containing logwood extract |
| CN108685793A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the moisturizing emulsion of the extract containing passion fruit |
| CN108685836A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the moisturizing emulsion containing Cordyceps |
| CN108685795A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the Whitening, spot lotion of the leaf extract containing chinaberry |
| CN108685794A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the Whitening, spot lotion containing gadol extract |
| CN108743485A (en) * | 2018-08-02 | 2018-11-06 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the after-sun lotion containing yellow fragrant chinaberry extract |
| CN108852965A (en) * | 2018-08-02 | 2018-11-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the Whitening, spot lotion of the extract containing Amomum cardamomum |
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| CN102958496A (en) * | 2010-07-01 | 2013-03-06 | 阿肯马法国公司 | Cosmetic composition comprising peba |
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- 2017-05-31 CN CN201710400634.XA patent/CN107115242A/en active Pending
Patent Citations (4)
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| CN101259095A (en) * | 2008-04-24 | 2008-09-10 | 天津盛世永业科技发展有限公司 | Skin care products for neck and preparation technique thereof |
| CN101824165A (en) * | 2010-05-04 | 2010-09-08 | 西南大学 | Granular cold water soluble porous starch |
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| CN102958496A (en) * | 2010-07-01 | 2013-03-06 | 阿肯马法国公司 | Cosmetic composition comprising peba |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108553375A (en) * | 2018-07-02 | 2018-09-21 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of Whitening, spot lotion |
| CN108685793A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the moisturizing emulsion of the extract containing passion fruit |
| CN108685836A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the moisturizing emulsion containing Cordyceps |
| CN108685795A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the Whitening, spot lotion of the leaf extract containing chinaberry |
| CN108685794A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the Whitening, spot lotion containing gadol extract |
| CN108743485A (en) * | 2018-08-02 | 2018-11-06 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the after-sun lotion containing yellow fragrant chinaberry extract |
| CN108852965A (en) * | 2018-08-02 | 2018-11-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the Whitening, spot lotion of the extract containing Amomum cardamomum |
| CN108653114A (en) * | 2018-08-04 | 2018-10-16 | 芜湖慧宇商贸有限公司 | A kind of preparation method of the moisturizing emulsion containing logwood extract |
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