CN106665627A - Cockroach attractant, preparation method of cockroach attractant and cockroach bait - Google Patents
Cockroach attractant, preparation method of cockroach attractant and cockroach bait Download PDFInfo
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- CN106665627A CN106665627A CN201611239860.6A CN201611239860A CN106665627A CN 106665627 A CN106665627 A CN 106665627A CN 201611239860 A CN201611239860 A CN 201611239860A CN 106665627 A CN106665627 A CN 106665627A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/002—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits
- A01N25/006—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits insecticidal
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
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Abstract
The invention provides a cockroach attractant, which comprises the following ingredient in percentage by weight: 40 to 55 percent of stir-fried cereal, 20 to 40 percent of cereal leftovers, 8 to 30 percent of saccharides, 0.1 to 5 percent of spice and 0.1 to 5 percent of preservatives. A method for preparing the cockroach attractant comprises the following steps of stir-frying cereal until fragrance is given out; after the thorough cooling, crushing the materials to 50 to 100 meshes for use; respectively crushing the cereal leftovers and saccharides into 50 to 100 meshes for use; proportionally mixing the crushed raw material powder; adding a certain proportion of spice and preservatives; uniformly mixing the materials to obtain the cockroach attractant. A cockroach bait comprising the cockroach attractant is formed by mixing the active ingredients and the cockroach attractants. The cockroach attractant provided by the invention has the special fragrance; the attraction effect on the cockroach can be improved by 40 to 50 percent; the cockroach cannot immediately die after eating the cockroach bait; the poisonousness can spread to other contact cockroaches, so that more cockroaches in secluded positions can be killed.
Description
Technical field
The present invention relates to a kind of cockroach prevention and cure field, especially a kind of cockroach attractant, and preparation method thereof and cockroach
Bait formulation.
Background technology
Harm of the cockroach to the mankind is huge, can carry the ovum of pathogenic bacterium, virus, protozoon, fungi and parasitic worm,
And can be used as the intermediate host of various worms, their infringement is wide, feeding habits are miscellaneous, you can in fields such as rubbish, lavatory, washrooms
Institute's activity, can take food on food again, thus they cause the propagation of enteron aisle disease and parasitic ovum can not be ignored.
Cockroach vitality is extremely strong, and fertility is strong, and this brings very big difficulty to the preventing and treating and removing of cockroach.
Agro-chemicals control cockroach is current relatively effective method, and cockroach contacts with medicament or takes food and play drug effect.
Ethiprole, the general entitled fipronil of English, chemical name：(RS) -5- amino -1- (2,6- bis- chloro- a, a, a- tri-
Fluoro- p- tolyl) -4- trifluoromethyl sulfinyl pyrazole -3- nitriles, No. CAS：120068-37-3, structural formula is as follows：
Ethiprole is developed by French Luo Na-Rhone-Poulenc, is wide a kind of Phenylpyrazole insecticides, insecticidal spectrum, to evil
Worm is had concurrently and is tagged and certain systemic action based on stomach poison function, and its mechanism of action is to hinder insect GABA control
The chloride metabolism of system.At present, hygienic insecticide is widely used in, is mainly used in preventing killing the harmful organisms such as cockroach, ant.
D ichlorbenzuron, also known as Diflubenzuron Ⅲ, Soviet Union's urea I, monochloro-benzene are grand, English common name Chlorbenzuron, chemical name
Claim：1- (2- chlorobenzene formacyls) -3- (4- chlorphenyls) urea, No. CAS：196791-54-5, structural formula is as follows：
D ichlorbenzuron is 1976 is synthesized the analog of a chlorine substituted urea by Hormone Inst., Jiangsu Prov and University Of Suzhou first,
Category benzoyl area kind Chitin synthesis inhibitor, is insect hormone, by suppressing insect cuticle chitin synthesis
The activity of enzyme and urine nucleosides coenzyme is dead so as to cause insect normally to cast off a skin to suppress insect chitin synthesis.Influence
DNA and protein metabolism in the respiratory metabolism of ovum and embryo development procedure, make larva in ovum lack chitin and can not hatch
Or it is dead immediately after hatching；Applied in larval phase, form the new epidermis of insect and be obstructed, delayed development, or lack hardness, it is impossible to just
Often cast off a skin and cause dead or form lopsided pupa death.
Ethiprole and d ichlorbenzuron have certain effect to preventing and treating cockroach, and the compounded combination of the two can improve preventing and treating effect
Really, spraying times are reduced, use cost is reduced.
In actual application, only cockroach contacts or takes food medicament competence exertion drug effect to cockroach killing chemicals.If medicament pair
Not enough, cockroach will not take food the attracting ability of cockroach, cannot play the prevention effect of cockroach killing chemicals.Therefore, lured in cockroach killing chemicals
The selection of agent plays vital effect to the prevention effect of cockroach.
Based on above research background, be badly in need of a kind of cockroach attractant, and preparation method thereof and cockroach bait formulation.
The content of the invention
It is an object of the invention to provide a kind of with special fragrance, the attractant effect to cockroach can improve 40-50%
Cockroach attractant and preparation method thereof.
Another object of the present invention is to provide a kind of cockroach bait formulation containing above-mentioned cockroach attractant, can improve for roach
The prevention effect of dung beetle, and its usage amount and cost can be reduced.
To achieve the above object, the present invention provides a kind of cockroach attractant, and each component comprising following percentage by weight is fried
Cereal is 40~55% after system, and cereal leftover bits and pieces is 20~40%, and carbohydrate is 8~30%, and spices is 0.1~5%, and preservative is
0.1~5%.
A kind of above-mentioned cockroach attractant, wherein, the percentage by weight of each component is, cereal 45~50% after frying, paddy
Thing leftover bits and pieces 25~40%, carbohydrate 9~20%, spices 0.1~2%, preservative 0.1~3%.
A kind of above-mentioned cockroach attractant, wherein, cereal is soya bean, peanut, sesame, corn, buckwheat, swallow after the frying
One kind in wheat, rice or millet or the mixture as made by least two.
A kind of above-mentioned cockroach attractant, wherein, the cereal leftover bits and pieces is wheat bran, dregs of beans, sesame seed meal, peanut meal, jade
One kind in rice core powder, rice hulls powder or the mixture as made by least two.
A kind of above-mentioned cockroach attractant, wherein, the carbohydrate is sucrose, malt glucide powder, maltose syrups, grape
One kind in sugar, fructose, lactose, brown sugar, white granulated sugar, corn sugar residue, sugarcane sugar residue or the mixing as made by least two
Thing.
A kind of above-mentioned cockroach attractant, wherein, the spices be furanone, soy sauce ketone, vegetable fat powder, full fat soybean essence,
Peanut essence, sesame flavor, corn essence, oat essence, butter essence, Caramel aromatic essence, vanillic aldehyde, Ethyl vanillin, malt
One kind in phenol, ethylmaltol or the mixture as made by least two.
A kind of above-mentioned cockroach attractant, wherein, the preservative is Sodium Benzoate, potassium sorbate, P-hydroxybenzoic acid
One kind in propyl ester, sodium Diacetate, dehydroactic acid sodium, D~sodium isoascorbate or the mixture as made by least two.
The present invention also provides a kind of preparation method of cockroach attractant, comprises the following steps：
Step 1, cereal is fried to out fragrance, thoroughly dry in the air it is cool after, be crushed to 50~100 mesh, it is standby；
Step 2, cereal leftover bits and pieces and carbohydrate are crushed to 50~100 mesh respectively, it is standby；
Step 3, the material powder after above-mentioned crushing is mixed in proportion, is added certain proportion spices and preservative,
It is well mixed to obtain the cockroach attractant.
The present invention also provides a kind of cockroach bait formulation, by any described a kind of cockroach in active ingredient and claim 1 to 7
Attractant is mixed.
A kind of above-mentioned cockroach bait formulation, wherein, the active ingredient account for the percentage by weight of cockroach bait formulation for 0.1~
1.5%；
The active ingredient is 1~2 by mass ratio：1~2 ethiprole and d ichlorbenzuron is made.
Compared with prior art, the present invention has advantages below：
Cockroach attractant provided by the present invention and the cockroach bait formulation containing the cockroach attractant have notable to cockroach
Attractant effect, will not be dead immediately after cockroach is edible, its cockroach bait formulation for carrying and secretion can be broadcast to other contacts
Cockroach, forms chain type and propagates, and can kill the cockroach of more concealment parts, therefore, it can reach a dispenser, can kill within one week
All cockroaches, prevention effect is good.
Specific embodiment
The present invention provides a kind of cockroach attractant, each component comprising following percentage by weight, after frying cereal be 40~
55% (preferred percentage by weight be 45~50%), cereal leftover bits and pieces be 20~40% (preferred percentage by weight is 25~
40%), carbohydrate is 8~30% (preferred percentage by weight is 9~20%), and spices is 0.1~5% (preferred weight percent
Than for 0.1~2%), preservative is 0.1~5% (preferred percentage by weight is 0.1~3%).
Wherein, after frying cereal be soya bean, peanut, sesame, corn, buckwheat, oat, rice or millet in one kind or
Mixture as made by least two.
Cereal is the one kind or mixed as made by least two in soya bean, peanut, corn, sesame after preferred frying
Compound.
Still more preferably it is the mixture as made by soya bean and sesame.
Wherein, cereal leftover bits and pieces be wheat bran, dregs of beans, sesame seed meal, peanut meal, maize cob meal, rice hulls powder in one kind or
Mixture as made by least two.
Wherein, carbohydrate is sucrose, malt glucide powder, maltose syrups, glucose, fructose, lactose, brown sugar, white granulated sugar, jade
One kind in rice sugar residue, sugarcane sugar residue or the mixture as made by least two.
Wherein, spices is furanone, soy sauce ketone, vegetable fat powder, full fat soybean essence, peanut essence, sesame flavor, corn perfume
One kind in essence, oat essence, butter essence, Caramel aromatic essence, vanillic aldehyde, Ethyl vanillin, maltol, ethylmaltol or
Mixture as made by least two.
Preferred spices is in furanone, soy sauce ketone, vanillic aldehyde, Ethyl vanillin, maltol, ethylmaltol
Plant or the mixture as made by least two.
Wherein, preservative is Sodium Benzoate, potassium sorbate, propylparaben, sodium Diacetate, dehydroactic acid sodium, D
One kind in~sodium isoascorbate or the mixture as made by least two.
The present invention also provides a kind of preparation method of cockroach attractant, comprises the following steps：
Step 1, cereal is fried to out by fragrance using small fire, thoroughly dry in the air it is cool after, be crushed to 50~100 mesh, it is standby；
Step 2, cereal leftover bits and pieces and carbohydrate are crushed to 50~100 mesh respectively, it is standby；
Step 3, the material powder after above-mentioned crushing is mixed in proportion, is added certain proportion spices and preservative,
It is well mixed to obtain the cockroach attractant.
The present invention also provides a kind of cockroach bait formulation, is mixed with cockroach attractant by active ingredient.
Wherein, the percentage by weight that active ingredient accounts for cockroach bait formulation is 0.1~1.5%；
Active ingredient is 1~2 by mass ratio：1~2 ethiprole and d ichlorbenzuron is made.
Embodiment 1
The present invention provides a kind of cockroach attractant, is measured with 100g, wherein, soya bean 50g, dregs of beans 40g, malt saccharin
Powder 9g, spices (in furanone, sesame flavor, butter essence, vanillic aldehyde, ethylmaltol any one) 0.1g, benzoic acid
Sodium 0.9g.
The preparation method of above-mentioned cockroach attractant, comprises the following steps：
Step 1, that using small fire the soya bean of above-mentioned weight is fried to out into beans is fragrant, thoroughly dry in the air it is cool after, using the omnipotent powder of high speed
Broken machine is crushed to 50~100 mesh, standby；
Step 2, the dregs of beans of above-mentioned weight and malt glucide powder are crushed to 50~100 using high speed Universal pulverizer respectively
Mesh, it is standby；
Step 3, the material powder after above-mentioned crushing is mixed, and it is 0.9g's to add spices and the weight that weight is 0.1g
Sodium Benzoate, it is to be mixed it is uniform after, reuse high speed Universal pulverizer and crushed, finally give with fragrant and sweet beany flavour
Powdered cockroach attractant.
By by powdered cockroach attractant and active ingredient with fragrant and sweet beany flavour obtained by above-mentioned preparation method
Mixing, to obtain cockroach bait formulation.
Wherein, cockroach attractant and active ingredient 99.5:0.5 mass ratio is mixed.
Wherein, active ingredient is 1 by mass ratio:1 ethiprole and d ichlorbenzuron is mixed.
Embodiment 2
The present invention provides a kind of cockroach attractant, is measured with 100g, wherein, soya bean 35g, sesame 15g, wheat bran 40g,
Brown sugar 9g, vanillic aldehyde 0.1g, potassium sorbate 0.9g.
The preparation method of above-mentioned cockroach attractant, comprises the following steps：
Step 1, the soya bean of above-mentioned weight and sesame be fried to out fragrance using small fire respectively, thoroughly dry in the air it is cool after, point
50~100 mesh are not crushed to using high speed Universal pulverizer, it is standby；
Step 2, the wheat bran and brown sugar of above-mentioned weight are crushed to 50~100 mesh using high speed Universal pulverizer respectively, it is standby
With；
Step 3, the material powder after above-mentioned crushing is mixed, and it is 0.9g to add vanillic aldehyde and the weight that weight is 0.1g
Potassium sorbate, it is to be mixed it is uniform after, reuse high speed Universal pulverizer and crushed, finally give with fragrant and sweet beany flavour
With the powdered cockroach attractant of sesame taste.
By by the powdered cockroach attractant with fragrant and sweet beany flavour and sesame taste obtained by above-mentioned preparation method with
Active ingredient mixes, to obtain cockroach bait formulation.
Wherein, cockroach attractant and active ingredient 99:1 mass ratio is mixed.
Wherein, active ingredient is 2 by mass ratio:1 ethiprole and d ichlorbenzuron is mixed.
Embodiment 3
The present invention provides a kind of cockroach attractant, is measured with 100g, wherein, soya bean 35g, peanut 15g, wheat bran 40g,
Brown sugar 9g, vanillic aldehyde 0.1g, potassium sorbate 0.9g.
The preparation method of above-mentioned cockroach attractant, comprises the following steps：
Step 1, the soya bean of above-mentioned weight and peanut be fried to out fragrance using small fire respectively, thoroughly dry in the air it is cool after, point
50~100 mesh are not crushed to using high speed Universal pulverizer, it is standby；
Step 2, the wheat bran and brown sugar of above-mentioned weight are crushed to 50~100 mesh using high speed Universal pulverizer respectively, it is standby
With；
Step 3, the material powder after above-mentioned crushing is mixed, and it is 0.9g to add vanillic aldehyde and the weight that weight is 0.1g
Potassium sorbate, it is to be mixed it is uniform after, reuse high speed Universal pulverizer and crushed, finally give with fragrant and sweet beany flavour
With the powdered cockroach attractant of peanut fragrance.
By by the powdered cockroach attractant with fragrant and sweet beany flavour Yu peanut fragrance obtained by above-mentioned preparation method
Mix with active ingredient, to obtain cockroach bait formulation.
Wherein, cockroach attractant and active ingredient 98.5:1.5 mass ratio is mixed.
Wherein, active ingredient is 1 by mass ratio:2 ethiprole and d ichlorbenzuron is mixed.
Embodiment 4
The present invention provides a kind of cockroach attractant, is measured with 100g, wherein, corn 35g, peanut 15g, wheat bran 40g,
Carbohydrate admixture 9g, spice mixt 0.1g, potassium sorbate 0.9g.
Wherein, carbohydrate admixture is mixed by brown sugar with maltose syrups.
Spice mixt is mixed by vegetable fat powder with vanillic aldehyde.
The preparation method of above-mentioned cockroach attractant, comprises the following steps：
Step 1, the corn and peanut of above-mentioned weight be fried to out fragrance using small fire respectively, thoroughly dry in the air it is cool after, point
50~100 mesh are not crushed to using high speed Universal pulverizer, it is standby；
Step 2, the wheat bran and carbohydrate admixture of above-mentioned weight are crushed to 50~100 using high speed Universal pulverizer respectively
Mesh, it is standby；
Step 3, by after above-mentioned crushing material powder mix, and add weight be 0.1g spice mixt be with weight
The potassium sorbate of 0.9g, it is to be mixed it is uniform after, reuse high speed Universal pulverizer and crushed, finally give with milk
The powdered cockroach attractant of taste, corn fragrance and peanut fragrance.
To be drawn by the powdered cockroach with milk fragrance, corn fragrance and peanut fragrance obtained by above-mentioned preparation method
Lure mixes with active ingredient, to obtain cockroach bait formulation.
Wherein, cockroach attractant and active ingredient 98:2 mass ratio is mixed.
Wherein, active ingredient is 1 by mass ratio:1 ethiprole and d ichlorbenzuron is mixed.
Embodiment 5
The present invention provides a kind of cockroach attractant, is measured with 100g, wherein, corn 35g, sesame 15g, wheat bran 40g,
Carbohydrate admixture 9g, spice mixt 0.1g, potassium sorbate 0.9g.
Wherein, carbohydrate admixture is mixed by brown sugar with maltose syrups.
Spice mixt is mixed by vegetable fat powder with vanillic aldehyde.
The preparation method of above-mentioned cockroach attractant, comprises the following steps：
Step 1, the corn and sesame of above-mentioned weight be fried to out fragrance using small fire respectively, thoroughly dry in the air it is cool after, point
50~100 mesh are not crushed to using high speed Universal pulverizer, it is standby；
Step 2, the wheat bran and carbohydrate admixture of above-mentioned weight are crushed to 50~100 using high speed Universal pulverizer respectively
Mesh, it is standby；
Step 3, by after above-mentioned crushing material powder mix, and add weight be 0.1g spice mixt be with weight
The potassium sorbate of 0.9g, it is to be mixed it is uniform after, reuse high speed Universal pulverizer and crushed, finally give with milk
The powdered cockroach attractant of taste, corn fragrance and peanut fragrance.
To be drawn by the powdered cockroach with milk fragrance, corn fragrance and sesame fragrance obtained by above-mentioned preparation method
Lure mixes with active ingredient, to obtain cockroach bait formulation.
Wherein, cockroach attractant and active ingredient 98:2 mass ratio is mixed.
Wherein, active ingredient is 1 by mass ratio:1 ethiprole and d ichlorbenzuron is mixed.
The comparative example 1 of cockroach attractant
The cockroach attractant of comparative example 1 is measured with 100g, wherein, soya bean 50g, dregs of beans 40g, malt glucide powder 9g,
Sodium Benzoate 1g.
The preparation method of comparative example 1, comprises the following steps：
Soya bean is directly crushed to 50-100 mesh with high speed Universal pulverizer, it is standby；
Dregs of beans, malt glucide powder are crushed to 50-100 mesh using high speed Universal pulverizer respectively, standby；
Above-mentioned raw materials powder is mixed, Sodium Benzoate is added, is well mixed, reuse high speed Universal pulverizer crushing,
Obtain powdered attractant.
The comparative example 2 of cockroach attractant
The cockroach attractant of comparative example 2 is measured with 100g, wherein, soya bean 50g, dregs of beans 40g, malt glucide powder 9g,
Vanillic aldehyde 0.1g, Sodium Benzoate 0.9g.
The preparation method of comparative example 2, comprises the following steps：
Soya bean is directly crushed to 50-100 mesh with high speed Universal pulverizer, standby；
Dregs of beans, malt glucide powder are crushed to 50-100 mesh using high speed Universal pulverizer respectively, standby；
Above-mentioned raw materials powder is mixed, Sodium Benzoate and vanillic aldehyde is added, is well mixed, reuse the omnipotent crushing of high speed
Machine is crushed, and obtains the powdered attractant with fragrant and sweet beany flavour.
The comparative example 3 of cockroach attractant
The cockroach attractant of comparative example 3 is measured with 100g, wherein, soya bean 50g, dregs of beans 40g, malt glucide powder 9g,
Sodium Benzoate 1g.
The preparation method of comparative example 3, comprises the following steps：
Soya bean small fire is fried to out beans fragrant, dry in the air it is cool after, be crushed to 50-100 mesh with high speed Universal pulverizer, it is standby；
Dregs of beans, malt glucide powder are crushed to 50-100 mesh using high speed Universal pulverizer respectively, standby；
Above-mentioned raw materials powder is mixed, Sodium Benzoate is added, is well mixed, reuse high speed Universal pulverizer crushing,
Obtain the powdered attractant with fragrant and sweet beany flavour.
Indoor biometricses are tested
(1) cockroach attractant effect experiment
Sample described in above-described embodiment 1-5 and comparative example is carried out into cockroach attractant effect experiment.
Experimental subjects：Groton bug
Experimental technique：In 10 glass square chests of 70cm × 70cm × 70cm, 100 Groton bugs are delivered respectively (female
Half and half) hero, after normal raising 24h, is respectively put into the sample described in the embodiment 1-5 and comparative example of equal quality in 10 glass
In glass case, using normal diet as control, water is respectively put into case, it is normal to raise and observe, determine a food ingestion within every 24 hours,
And constantly change position of the attractant in case.
Lure rate computational methods：
Experimental result is as follows：
Table 1
Table 2
Can be drawn by the contrast of table 1 and 2, the soya bean and the soya bean of non-frying of spices and frying are added in the soya bean of non-frying
Compare, lure rate to increase, lure rate to be respectively 38.99% and 73.65%, therefore, cereal frying and addition spices pair
Cockroach lures rate to improve and is respectively provided with certain effect.
Table 3
Table 4
Table 5
Table 6
Table 7
Table 8
Table 9
Table 10
Table 11
Attractant is compared with comparative example 3 in can be seen that above-described embodiment by table 3-7 experimental results, and attractant effect is obvious
Increase；The addition of spices and frying analysis for soybean powder (ratio 3) are compared in attractant, and cockroach attractant effect is significantly improved, and lure rate
Between 84.97%-136.25%；Spices increases degree to attractant effect：Vanillic aldehyde ＞ furanone ＞ butter essence ＞ ethyls
Maltitol powder ＞ sesame flavors.
Be can be seen that by table 8-11 experimental results during the frying cereal in attractant combines, soya bean and sesame combination are drawn
It is 168.70% to lure rate, and the rate of luring of soya bean and peanut combination is 152.08%, and the rate of luring of corn and sesame combination is
135.99%, corn and peanut combination lure rate for 126.70%, and rate highest is lured in soya bean and sesame combination, therefore, choosing
Soya bean and sesame are taken as optimum combination.
(2) Toxicity Determination of ethiprole and d ichlorbenzuron compound synergic
Experimental subjects：Groton bug
Experimental technique：Attractant as described in embodiment 2 adds different amounts of active insecticidal components, is configured to content difference
It is the bait formulation of 0.1,0.05,0.025,0.0125,0.00625 (mg/kg).
In the square glass cylinder of 20cm × 20cm, 20 Groton bug female insects are put into, removed after conventinal breeding 24h
Unhealthy individuality, and after doing corresponding supplement, replace bait, normal water supply dead individuals number to be observed and record, with routine with poison bait
Raise as control, each concentration in triplicate, calculates the death rate, averages respectively after 48h.
Experimental result：
Table 12
Note：Mixture ratio is ethiprole：D ichlorbenzuron
According to the criterion of Sun Pei cloud methods：CTC ＜ 80 are antagonism, and 80≤CTC≤120 are summation action, CTC
＞ 120 is synergistic effect.As can be seen from Table 11, ethiprole and d ichlorbenzuron mixture, co-toxicity coefficient are all higher than 120, show as increasing
Effect is acted on, wherein when the two ratio is 1:When 1, co-toxicity coefficient is maximum, and humidification is most strong.Therefore, ethiprole and d ichlorbenzuron
Optimal proportion is 1:1.
(3) sample described in above-described embodiment is carried out into cockroach prevention and cure effect experiment, commercial samples (0.05% ethiprole
Bait formulation, Beijing greenery century daily chemical product Co., Ltd) as control.
Application method：Sample described in embodiment carries out dispenser with commercial samples according to 0.5-2g/m2, and dispenser position is roach
Position or corner that dung beetle often occurs.
Dispenser place：The kitchen that cockroach often occurs.
Cockroach density is investigated：At cockroach corner that may be present, gap, drawer, debris stacking, hand-held compression spraying is used
Device sprays 0.1% Permethrin ethanol solution, and the cockroach number of appearance is observed after 10 minutes.
The computational methods of cockroach density rate of descent：
Before and after cockroach bait formulation is spread fertilizer over the fields, the cockroach number that observation different number of days is inspired calculates cockroach density rate of descent.
Experimental result is as follows：
Table 13
Table 13 test result indicate that, according to method of the present invention prepare cockroach bait formulation to cockroach have draw well
Lure and killing effect, it compares with commercial samples, prevention effect will be higher by 20-30%, killing rate more than 95%, therefore,
Choose active ingredient it is minimum 99.5:0.5 used as best proportion.
In addition, another bright spot of the invention is, the cockroach bait formulation prepared by cockroach attractant after cockroach is applied not
Can be dead immediately, and the bait formulation and secretion of its adhesion can cause other cockroaches to be poisoned in other cockroach contact processes, it is many
Number cockroach can be dead in nest or hidden place, shows as cockroach density decline, and dead cockroach is not almost seen but.
Though the present invention can not eradicate the danger of cockroach within one week or so time by cockroach density reduction by more than 95%
Evil, after general two months, cockroach can stage a comeback, and at that time, need to use product of the present invention as stated above again, reachable
To the purpose of control cockroach.
Presently preferred embodiments of the present invention is the foregoing is only, is merely illustrative for invention, and it is nonrestrictive.
Those skilled in the art understanding, can carry out many changes in the spirit and scope that invention claim is limited to it, change,
It is even equivalent, but fall within protection scope of the present invention.
Claims (10)
1. a kind of cockroach attractant, it is characterised in that each component comprising following percentage by weight, after frying cereal be 40~
55%, cereal leftover bits and pieces is 20~40%, and carbohydrate is 8~30%, and spices is 0.1~5%, and preservative is 0.1~5%.
2. a kind of cockroach attractant according to claim 1, it is characterised in that the percentage by weight of each component is, frying
Cereal 45~50%, cereal leftover bits and pieces 25~40%, carbohydrate 9~20%, spices 0.1~2%, preservative 0.1~3% afterwards.
3. a kind of cockroach attractant according to claim 1 and 2, it is characterised in that cereal is soya bean, flower after the frying
One kind in life, sesame, corn, buckwheat, oat, rice or millet or the mixture as made by least two.
4. a kind of cockroach attractant according to claim 1 and 2, it is characterised in that the cereal leftover bits and pieces is wheat bran, beans
One kind in the dregs of rice, sesame seed meal, peanut meal, maize cob meal, rice hulls powder or the mixture as made by least two.
5. a kind of cockroach attractant according to claim 1 and 2, it is characterised in that the carbohydrate is sucrose, malt saccharin
One kind in powder, maltose syrups, glucose, fructose, lactose, brown sugar, white granulated sugar, corn sugar residue, sugarcane sugar residue or by least
Mixture made by two kinds.
6. a kind of cockroach attractant according to claim 1 and 2, it is characterised in that the spices is furanone, soy sauce
Ketone, vegetable fat powder, full fat soybean essence, peanut essence, sesame flavor, corn essence, oat essence, butter essence, Caramel aromatic essence, perfume (or spice)
One kind in Lan Su, Ethyl vanillin, maltol, ethylmaltol or the mixture as made by least two.
7. a kind of cockroach attractant according to claim 1 and 2, it is characterised in that the preservative is Sodium Benzoate, mountain
One kind in potassium sorbate, propylparaben, sodium Diacetate, dehydroactic acid sodium, D~sodium isoascorbate or by least
Mixture made by two kinds.
8. the method for preparing any described a kind of cockroach attractant in claim 1 to 7, it is characterised in that including following step
Suddenly：
Step 1, cereal is fried to out fragrance, thoroughly dry in the air it is cool after, be crushed to 50~100 mesh, it is standby；
Step 2, cereal leftover bits and pieces and carbohydrate are crushed to 50~100 mesh respectively, it is standby；
Step 3, the material powder after above-mentioned crushing is mixed in proportion, added certain proportion spices and preservative, mixing
It is uniform to obtain the cockroach attractant.
9. a kind of cockroach bait formulation containing any described a kind of cockroach attractant in claim 1 to 7, it is characterised in that by
A kind of any described cockroach attractant is mixed active ingredient with claim 1 to 7.
10. a kind of cockroach bait formulation according to claim 9, it is characterised in that the active ingredient accounts for the weight of cockroach bait formulation
Amount percentage is 0.1~1.5%；
The active ingredient is 1~2 by mass ratio：1~2 ethiprole and d ichlorbenzuron is made.
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| CN108991029A (en) * | 2018-09-07 | 2018-12-14 | 成都彩虹电器（集团）股份有限公司 | A kind of two-component Rapid Fermentation cockroach attractant and its preparation and application |
| CN109142635A (en) * | 2018-09-07 | 2019-01-04 | 成都彩虹电器（集团）股份有限公司 | A kind of cockroach attractant simulation field efficacy test method |
| CN109349429A (en) * | 2018-12-04 | 2019-02-19 | 华南农业大学 | A kind of soy sauce ketone extract and its application |
| CN111713513A (en) * | 2020-07-01 | 2020-09-29 | 衢州市农业技术推广中心 | Green pesticide and preparation method thereof |
| CN113317415A (en) * | 2021-07-01 | 2021-08-31 | 广东省中药研究所 | Insect attractant and preparation method and application thereof |
| CN115590041A (en) * | 2022-10-24 | 2023-01-13 | 苏州绿力士生物科技有限公司（Cn） | Cockroach attractant and preparation method thereof |
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| CN108991029A (en) * | 2018-09-07 | 2018-12-14 | 成都彩虹电器（集团）股份有限公司 | A kind of two-component Rapid Fermentation cockroach attractant and its preparation and application |
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| CN108991029B (en) * | 2018-09-07 | 2021-09-21 | 成都彩虹电器（集团）股份有限公司 | Double-component quick-fermentation cockroach attractant and preparation and use methods thereof |
| CN109349429A (en) * | 2018-12-04 | 2019-02-19 | 华南农业大学 | A kind of soy sauce ketone extract and its application |
| CN111713513A (en) * | 2020-07-01 | 2020-09-29 | 衢州市农业技术推广中心 | Green pesticide and preparation method thereof |
| CN113317415A (en) * | 2021-07-01 | 2021-08-31 | 广东省中药研究所 | Insect attractant and preparation method and application thereof |
| CN115590041A (en) * | 2022-10-24 | 2023-01-13 | 苏州绿力士生物科技有限公司（Cn） | Cockroach attractant and preparation method thereof |
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