CN106509161A - Oxidation resistant edible oil and preparation method thereof - Google Patents
Oxidation resistant edible oil and preparation method thereof Download PDFInfo
- Publication number
- CN106509161A CN106509161A CN201610925771.0A CN201610925771A CN106509161A CN 106509161 A CN106509161 A CN 106509161A CN 201610925771 A CN201610925771 A CN 201610925771A CN 106509161 A CN106509161 A CN 106509161A
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- Prior art keywords
- oil
- edible oil
- ball milling
- oxidation
- semen lini
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Edible Oils And Fats (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses oxidation resistant edible oil and a preparation method thereof. The oxidation resistant edible oil is made from 30-50wt% of olive oil, 20-40wt% of linseed oil, 20-40wt% of shiny-leaved yellowhorn oil, and C60 which is 0.05-0.15wt% of the olive oil, the linseed oil and the shiny-leaved yellowhorn oil. The oxidation resistant edible oil is good in oxidation resistant efficacies, reasonable in fatty acid compounding ratio and high in nutrient value, and not only can meet requirements of people for nutrition of edible oil usually but also can provide specific health-care functions.
Description
Technical field
The present invention relates to edible oil field, more particularly to a kind of anti-oxidation edible oil and preparation method thereof.
Background technology
Fatty acid includes satisfied fatty acid, monounsaturated fatty acid and polyunsaturated fatty acid.According to the United Nations's grain farmer's group
Knit the balanced fatty acid requirement proposed with World Health Organization (WHO), dietary saturated fatty acids, monounsaturated fatty acid, how unsaturated fat
The ratio of fat acid should reach 1:1:1 just contributes to human nutrition equilibrium.The ratio of ω -6 and ω -3 is recommended by the developed countries such as America and Europe
Should be at (4-6):Less than 1, nutritionist thinks that rational ω -6 advantageously reduces blood pressure, suppresses irregular heart with ω -3 ratios
Bounce, maintains the generation of the energy balance, carbohydrate metabolism and other chronic diseases and promotes normal growth promoter.How unsaturated fat
Fat acid, particularly linoleic acid and alpha-linolenic acid can not synthesize in human body, it is necessary to by food intake.Vegetable oil is that people's acquisition is more
One important channel of unsaturated fatty acid, but the polyunsaturated fatty acid in the vegetable oil of various single kinds can not all reach
To the ratio of nutritionist suggestion, the only mixed oil through scientific allocation could supplement the dietary fatty acid needed for people.
Substantial amounts of reactive oxygen free radical can be produced in the metabolism of itself in organism.Internal surplus is removed in time
Oxygen-derived free radicals, can effectively prevent, associated conditions are mitigated or eliminated, and using antioxidants retard or reduce human body and receive because of oxidation
The harm arrived, is a highly important prevention approach.C60 is a kind of novel antioxidant developed in recent years, and which resists
Oxidation effectiveness is ascorbic 125 times, is called " sponge for absorbing free radical ".
The content of the invention
It is an object of the invention to provide a kind of reasonable with strong anti-oxidation efficacy, Fatty acids composition（Fatty acids composition
For satisfied fatty acid：Unsaturated fatty acid=1：1, linoleic acid：Linolenic acid is less than 4：1）, be of high nutritive value（Containing abundant insatiable hunger
And the essential fatty acids linoleic that can not synthesize of fatty acid, particularly human body and linolenic acid）Edible health-care oil series, Ji Nengman
Demand of the sufficient people to usual edible nourishing, and distinctive health care can be provided.Meanwhile, find the mediation side of a vegetable oil
Formula so as to meet diet nutritional demand and can quickly dissolve C60 again to greatest extent（Under equal conditions, C60 is dissolved in olive oil
65% is needed 12 hours and can only dissolve, continuing lengthening time dissolubility will not increase；And be dissolved in 11 in the mixed oil of the present invention
Hour can dissolve 90%, and the time lengthens and can also continue to dissolving, can reach 95%（24 hours）, C60 introduced plants are sought
Mass production is carried out in supporting oil.
For achieving the above object, the present invention provides a kind of anti-oxidation edible oil, it is characterised in that by olive oil 30～50
Wt %, 20～40 wt % of Semen Lini oil, 20～40 wt % of shinyleaf yellowhorn oil, C60 are olive oil, Semen Lini oil and shinyleaf yellowhorn oil
0.05～0.15 wt % are constituted.
Further, by 35～50 wt % of olive oil, 25～35 wt % of Semen Lini oil, 20～30 wt % of shinyleaf yellowhorn oil,
C60 is constituted for 0.05～0.15 wt % of olive oil, Semen Lini oil and shinyleaf yellowhorn oil.
Further, by 40 wt % of olive oil, 30 wt % of Semen Lini oil, 30 wt % of shinyleaf yellowhorn oil, C60 be olive oil,
The 0.12 wt % compositions of Semen Lini oil and shinyleaf yellowhorn oil.
Further, the purity of the C60 is more than 99.5%.
Further, the preparation method of the anti-oxidation edible oil is,
Weigh：Olive oil, Semen Lini oil, shinyleaf yellowhorn oil and C60 are weighed respectively by required ratio；
Ball milling：Sample is poured into；
Centrifugation：Transferred product after ball milling is carried out in centrifuge bottle centrifugal treating；
It is degerming：Product after centrifugation carries out bacteria removing by filter plant；
Fill：Product is obtained final product after degerming can directly fill.
Further, the ball milling adopts ball grinder and ball milling pearl；It is preferred that agate pot and agate bead.Using agate pot and Achatess
Pearl can make C60 to greatest extent and prestissimo is dissolved in oils and fatss, and Achatess will not be destroyed, and does not have Achatess residual in finished product
Stay.
Further, the ball milling is that the sample for weighing directly is poured into, it is not necessary to through stirring；Ball
The time of mill is less than 12 hours, and preferred Ball-milling Time is 7-11 hours；Rotating speed is less than 300 r/min, preferably 60-
210r/min.The control of time and rotating speed prevents product from spraying.
Further, the centrifuge speed of the centrifugation is less than 10000 r/min, preferred 5000-8000 r/min；Centrifugation
Time is less than 150min, preferred 100-140min.Time and rotating speed control prevent product from spraying.
Further, the degerming filter plant pore size filter is 0.5 m, and filter effect is obvious and the time is fast, will not indulge in
The assembly line work of production by mistake.
Further, the fill uses high-pressure filling mode.
The proportioning of oils and fatss of the present invention carries out component analyses to raw material through gas chromatogram and gets, to ensure its fatty acid
The stable ratio in satisfied fatty acid and unsaturated fatty acid of ratio be 1：1；Linoleic acid and linolenic ratio are less than 4:1,
The nutrition that so can be only achieved oils and fatss is balanced, and this ratio is that the recommendation of FAO (Food and Agriculture Organization of the United Nation) and NNFA of various countries to oils and fatss is taken the photograph
Enter ratio.0.05～0.15 wt %s of the C60 for olive oil, Semen Lini oil and shinyleaf yellowhorn oil.When the content of C60 is higher than 0.15 wt
Dissolving of the oils and fatss to C60 during % is in saturation, and continuing addition dissolubility will not increase, and waste C60 on the contrary；Less than 0.05
During wt %, antioxidant effect is not obvious.
The present invention gives full play to the distinctive free radical resisting of olive oil, Semen Lini oil and shinyleaf yellowhorn oil, defying age, blood pressure lowering drop
The ability of blood fat, plays booster action with the efficient anti-oxidation functions of C60, and long-term consumption can be with balanced human's fatty acid, removing body
Interior free radical, reduce blood pressure blood fat, slow down aging, enhance immunity, reaches beauty and prophylactic effect.
Description of the drawings
Fig. 1 is anti-oxidation edible oil of the present invention and addition antioxidant BHT, the antioxidant effect comparison diagram of TBHQ.
Fig. 2 is the body weight change figure of each group experimental animal in compliance test result test.
Specific embodiment
Embodiments of the invention are described below in detail, the example of the embodiment is shown in the drawings, wherein from start to finish
Same or similar label represents same or similar element or the element with same or like function.Below with reference to attached
The embodiment of figure description is exemplary, it is intended to for explaining the present invention, and be not considered as limiting the invention.Embodiment
In unreceipted particular technique or condition person, according to the technology or condition described by document in the art or according to the description of product
Book is carried out.Agents useful for same or the unreceipted production firm person of instrument, be can pass through city available from conventional products.
C60 used below is purchased from Xiamen good fortune and takes in the fresh Materials Co., Ltd.
Embodiment 1：The preparation of anti-oxidation edible oil
Raw material dosage：It is shown in Table 1.
1 each embodiment material therefor scale of table（wt%）
Preparation method：210r/min ball millings 7 hours, 8000r/min centrifugation 100min, were carried out from 0.5 m apertures filter element
Filter.
Embodiment 2：The preparation of anti-oxidation edible oil
Raw material dosage：It is shown in Table 1.
Preparation method：60r/min ball millings 11.5 hours, 7500r/min centrifugation 110min. are entered from 0.5 m apertures filter element
Row is filtered.
Embodiment 3：The preparation of anti-oxidation edible oil
Raw material dosage：It is shown in Table 1.
Preparation method：80r/min ball millings 11 hours, 6000r/min centrifugation 140min. are carried out from 0.5 m apertures filter element
Filter.
Embodiment 4：The preparation of anti-oxidation edible oil
Raw material dosage：It is shown in Table 1.
Preparation method：280r/min ball millings 8 hours, 9000r/min centrifugation 100min. are carried out from 0.5 m apertures filter element
Filter.
Embodiment 5：The preparation of anti-oxidation edible oil
Raw material dosage：It is shown in Table 1.
Preparation method：150r/min ball millings 10 hours, 5000r/min centrifugation 148min. are entered from 0.5 m apertures filter element
Row is filtered.
Embodiment 6：Compliance test result is tested
1）With the antioxidant effect comparative test of TBHQ, BHT
To be resisted with the edible oil added with BHT, TBHQ antioxidant obtained by the present embodiment 1-5 using classical baking oven storage method
Oxidation effectiveness compares, with reference to GB/T5538-2005《Animal and plant fat determination of POV》Determine its peroxide value.
The adding method of BHT and TBHQ：It is each 0.1000g to be weighed accurately with the electronic analytical balance that degree of accuracy is 0.0001g
Antioxidant（BHT or TBHQ）, it is added to 10g oily（Olive oil：Semen Lini oil：Shinyleaf yellowhorn oil=4:3:3）In and mix highly concentrated
The mother solution of degree, then takes 1g mother solutions and is added in the same oils and fatss of 49g, make each antioxidant（BHT or TBHQ）Addition be
The 0.02% of oily weight.By baking oven Acceleration study, with 264 hours as time limit, by measuring the change of its peroxide value to its antioxygen
Change effect to be evaluated, result of the test is shown in Fig. 1.Product of the present invention need not still further add non-oxidizability as can be seen from Figure 1, and which resists
Oxidation effectiveness can compare favourably with the non-oxidizability of addition antioxidant.
2）Antioxidation is tested
Experimental subject：From the male rat 50 that 12 monthly ages were in a good state of health.
Feeding environment condition：Daily sterilization ground, table top and metope during test, disinfectant is bromo geramine and ethanol.
Temperature and Humidity Control exists：Temperature 20-25 DEG C, relative humidity 40-70%.Feedstuff and drinking water are freely absorbed, using front Jing High Temperature High Pressure
Steam sterilization.
Experimental technique：Rat is randomly divided into into matched group 1, matched group 2, matched group 3, experimental group 1, experimental group 2, experimental group
3rd, experimental group 4, experimental group 5 10 per group.Experimental group 1, experimental group 2, experimental group 3, experimental group 4, the difference feeding of experimental group 5 are implemented
The product of example 1-5（By 1ml/kg gavage mode feedings）, 1 fed with water of matched group, 2 feeding olive oil of matched group（Fill by 1ml/kg
Stomach mode feeding）, mixed oil of 3 feeding of matched group without C60（Olive oil：Semen Lini oil：Shinyleaf yellowhorn oil=4:3:3）（Press
1ml/kg gavage mode feedings）, feeding 30 days feeds once daily.Experiment adopts tail blood after terminating, and prepares serum.Peroxide in serum
Change degradation of lipid product malonaldehyde（MDA）Assay adopts thiobarbituricacidα-（TBA）Fluorescence spectrophotometry, surpasses in serum
Superoxide dismutase（SOD）Vitality test adopts azanol colorimetry, determines kit specification operation by SOD.
Experimental data carries out variance analyses using SAS statistical softwares.
Experimental result：It is shown in Table 2-3 and Fig. 2.Knowable to table 2-3, compound anti-oxidation nutrition obtained in feeding embodiment 1-5
Oil, can significantly reduce lipid peroxide catabolite malonaldehyde in male rat serum（MDA）Content；The fat of rat can be affected
Matter peroxidation, can significantly improve activity of SOD in serum, improve oxidation effectiveness, reduce the lipid peroxidation of body, so as to
Slow down aging, enhance immunity.Difference has statistical significance.Show that according to result the anti-oxidation edible oil of the present invention has
The antioxidant effect of effect.This product provides the nutrition of abundance for rat as can be seen from Figure 2, maintains the body weight increase of rat, it is ensured that its
Growth promoter.
Table 2：Lipid peroxide malonaldehyde（MDA）Content table
Note：* represent that each experimental group is compared with matched group, significant difference（P<0.05）
Table 3：Activities of antioxidant enzymes superoxide dismutase（SOD）Active table
Note：* represent that each experimental group is compared with matched group, significant difference（P<0.05）
From the above it can be seen that effect of C60 not only has antioxidation, also Stabilization can be played to oils and fatss, be extended the shelf life, together
When, the anti-oxidation edible oil of the present invention is with the edible oil of addition BHT and TBHQ to suppressing peroxide value to raise with equivalent effect.
And BHT or TBHQ simply has antioxidation to oils and fatss.
Although embodiments of the invention have been shown and described above, it is to be understood that above-described embodiment is example
Property, it is impossible to limitation of the present invention is interpreted as, one of ordinary skill in the art is in the principle and objective without departing from the present invention
In the case of above-described embodiment can be changed within the scope of the invention, change, replace and modification.
Claims (10)
1. a kind of anti-oxidation edible oil, it is characterised in that by 30～50 wt % of olive oil, 20～40 wt % of Semen Lini oil, text
Hat 20～40 wt % of fruit oil, C60 are constituted for 0.05～0.15 wt % of olive oil, Semen Lini oil and shinyleaf yellowhorn oil.
2. anti-oxidation edible oil described in claim 1, it is characterised in that by 35～50 wt % of olive oil, Semen Lini oil 25～35
Wt %, 20～30 wt % of shinyleaf yellowhorn oil, C60 are constituted for 0.05～0.15 wt % of olive oil, Semen Lini oil and shinyleaf yellowhorn oil.
3. anti-oxidation edible oil described in claim 2, it is characterised in that by 40 wt % of olive oil, 30 wt % of Semen Lini oil, text
Hat 30 wt % of fruit oil, C60 are constituted for 0.12 wt % of olive oil, Semen Lini oil and shinyleaf yellowhorn oil.
4. anti-oxidation edible oil described in any one of claim 1-3, it is characterised in that the purity of the C60 is more than 99.5%.
5. anti-oxidation edible oil described in any one of claim 1-4, it is characterised in that preparation method is,
Weigh：Olive oil, Semen Lini oil, shinyleaf yellowhorn oil and C60 are weighed respectively by required ratio；
Ball milling：Sample is poured into；
Centrifugation：Transferred product after ball milling is carried out in centrifuge bottle centrifugal treating；
It is degerming：Product after centrifugation carries out bacteria removing by filter plant；
Fill：Degerming rear products obtained therefrom can directly fill.
6. anti-oxidation edible oil described in claim 5, it is characterised in that the ball milling adopts ball grinder and ball milling pearl；It is preferred that agate
Nao tanks and agate bead.
7. anti-oxidation edible oil described in claim 5, it is characterised in that the ball milling is that the sample for weighing directly pours ball grinder into
In carry out ball milling, it is not necessary to through stirring；The time of ball milling is less than 12 hours, and the time of preferred ball milling is 7-11 hours；Turn
Speed is less than 300 r/min, preferably 60-210r/min.
8. anti-oxidation edible oil described in claim 5, it is characterised in that the rotating speed being centrifuged in centrifugation step is less than 10000 r/
Min, preferred 5000-8000 r/min；Centrifugation time is less than 150min, preferred 100-140min.
9. anti-oxidation edible oil described in claim 5, it is characterised in that degerming 0.5 m of pore size filter.
10. anti-oxidation edible oil described in claim 5, it is characterised in that the fill uses high-pressure filling mode.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610925771.0A CN106509161A (en) | 2016-10-24 | 2016-10-24 | Oxidation resistant edible oil and preparation method thereof |
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| CN201610925771.0A CN106509161A (en) | 2016-10-24 | 2016-10-24 | Oxidation resistant edible oil and preparation method thereof |
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| CN201610925771.0A Pending CN106509161A (en) | 2016-10-24 | 2016-10-24 | Oxidation resistant edible oil and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110301483A (en) * | 2018-03-27 | 2019-10-08 | 厦门福慈生物科技有限公司 | The purposes of fullerene compound and fullerene microcapsule powder and its preparation method and application |
| CN113456673A (en) * | 2021-07-19 | 2021-10-01 | 厦门福纳新材料科技有限公司 | Medicine for treating ulcerative colitis and application of fullerene as active component |
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Cited By (3)
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| CN110301483A (en) * | 2018-03-27 | 2019-10-08 | 厦门福慈生物科技有限公司 | The purposes of fullerene compound and fullerene microcapsule powder and its preparation method and application |
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| CN113456673A (en) * | 2021-07-19 | 2021-10-01 | 厦门福纳新材料科技有限公司 | Medicine for treating ulcerative colitis and application of fullerene as active component |
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Application publication date: 20170322 |