CN106433344A - Water-based metal flashing paint and preparation method thereof - Google Patents
Water-based metal flashing paint and preparation method thereof Download PDFInfo
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- CN106433344A CN106433344A CN201610573920.1A CN201610573920A CN106433344A CN 106433344 A CN106433344 A CN 106433344A CN 201610573920 A CN201610573920 A CN 201610573920A CN 106433344 A CN106433344 A CN 106433344A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/38—Paints containing free metal not provided for above in groups C09D5/00 - C09D5/36
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/45—Anti-settling agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/47—Levelling agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a water-based metal flashing paint and a preparation method thereof. The coating part is prepared from, by weight, 30-40 parts of water-dispersible acrylic emulsion, 0.3-1 part of a defoaming agent, 0.4-1 part of a flatting agent, 7-12 parts of a thickening agent, 1.5-3.5 parts of an anti-settling agent, 5-10 parts of water-based aluminum paste, 0.3-1 part of a dispersing agent, 4-6 parts of a cosolvent, 0.02-0.05 part of a pH regulator and 30-45 parts of deionized water. It is needed to conduct dry spraying several times in construction of an existing water-based aluminum powder paint available in the market, plate spray paint mist is poor in wettability and is in a cloud state, and aluminum powder is seriously accumulated. The water-based metal flashing paint easy to smear can be normally constructed with deionized water directly, and the construction performance and the appearance can completely reach the solvent type standard; besides, all performance indexes of a paint film can completely reach the indexes of an oil-based aluminum powder paint coating.
Description
Technical field
The invention belongs to a kind of water-based metal metallic finishe is and in particular to a kind of aqueous aluminum powder of water-dispersed acrylic system
Paint and preparation method thereof.
Background technology
Show according to the statistical data that State Statistics Bureau announces, Chinese coating total output reaches 1648.188 ten thousand tons within 2014, adjusts
Increase by 7.87% on a year-on-year basis after whole.Compare coating total output in 2013 1303.349 ten thousand tons, have newly increased 344.839 ten thousand in 2014
Ton.Record high again.Wherein, Guangdong Province's whole year coating yield is 333.99 ten thousand tons, increases by 6.92% on a year-on-year basis, Shanghai City is annual
187.09 ten thousand tons of coating yield, increases by 10.54% on a year-on-year basis, annual 182.15 ten thousand tons of the coating yield in Jiangsu Province, increases by a year-on-year basis
5.43%.
Calculated with 2013 annual productions, if using oil paint, annual air VOC emission total amount is 1145 tons, and uses water
Property paint after, annual VOC emission total amount is only 19 tons, and the range of decrease up to 98% is it is seen that it is huge to environmental protection, fall haze effect;
Secondly, spraying effective percentage is substantially improved, and the effective percentage of oil paint spraying before is only 35%~40%, and present water paint is coated with
Efficiency rises to more than 79%, has not only effectively reduced cost but also has decreased environmental pollution.
With the popularization of environmental protection concept, water paint obtains more and more consumers as the product with environmental-protecting performance
Accreditation.On January 16th, 2015, National Ministry of Finance combines issue " with regard to imposing the consumption tax to battery, coating with the national taxation bureau
Notice ", environment-friendly water-basedization of coating is irresistible, and market prospect is wide.
Content of the invention
It is an object of the invention to provide a kind of water-based metal metallic finishe, its have excellent ornamental, good weatherability and
Application property, the prominent low VOC feature of environmental protection are it is adaptable to the application of automobile and engineering machinery etc..
The purpose of the present invention can be reached by following measures:
A kind of water-based metal metallic finishe, is mainly formulated by following components in parts by weight:
(1) 0.3~1 part of dispersant;
(2) 4~6 parts of cosolvent;
(3) 5~10 parts of water aluminum-silver slurry;
(4) 30~40 parts of aqueous acrylic emulsion;
(5) 0.3~1 part of defoamer;
(6) 0.4~1 part of levelling agent;
(7) 7~12 parts of thickening agent;
(8) 1.5~3.5 parts of anti-settling agent;
(9) PH regulator 0.02~0.05;
(10) 30~45 parts of deionized water.
Dispersant in the present invention adopts AFCONA 6226.
Cosolvent in the present invention adopts isopropanol.
Water aluminum-silver slurry in the present invention uses the SBCAQJ 6820B3B of star platinum connection.
Aqueous acrylic emulsion in the present invention adopts the E-125 of DSM.
Defoamer in the present invention is the water-based emulsion shape defoamer AFCONA 2501 containing organosilicon.
Levelling agent in the present invention is acrylic acid-Organosiliconcopolymere AQ-7130.
Thickening agent in the present invention is the AS-1130 of BASF.
Anti-settling agent in the present invention is polyamide wax salt AQH-800.
PH adjusting agent in the present invention is AMP-95.
The aluminum paint, aqueous preparation method of the present invention is as follows:
(1) by dispersant, cosolvent, deionized water and water aluminum-silver slurry mixing and stirring, soak 15~20min;
(2) aqueous acrylic emulsion, defoamer, levelling agent, thickening agent, anti-settling agent and deionized water mix homogeneously, low
Stir under shearing force;
(3) (2), under stirring at low speed state, add (1), stir when stirring;
(4) with pH adjusting agent, the pH value of (3) is adjusted between 7.5-8.5.
First above-mentioned paint component is stirred during construction, diluted with the deionized water or drinking public water supply of 5-15%, so
Afterwards according to construction requirement, even application is on workpiece to be coated.
The present invention is aluminum paint, aqueous to be had the characteristics that:
(1) coating of the present invention has good application property, consistent even with normal solvent-borne type aluminium paint construction reference
Part surmounts;
(2) coating of the present invention adopts water-dispersible acrylic's emulsion, can give the excellent dicoration of paint film and film property;
(3) coating of the present invention possesses good pliability, can prevent paint film cracking, come off;
(4) coating of the present invention has prominent moisture resistance, can directly coat and apply in wet structure and wet environment
Work;
(5) coating of the present invention, with water as solvent, saves ample resources;
(6) coating of the present invention reduces to atmospheric pollution;
(7) coating of the present invention, only with a small amount of hypotoxicity alcohol ethers organic solvent, improves operating environmental condition;
(8) the paint spraying instrument of the present invention can wash by water, and greatly reduces the consumption of cleaning solvent.
The aluminum paint, aqueous coating of the present invention, compared with oil paint, is all substantially to hear the taste that holds one's breath, construction after can opening
When be with cleaning water-reducible from the beginning, belong to benign chemicals, environmental protection index is free from benzene, heavy metal and high-load
The poisonous and harmful substances such as VOC.The present invention can be obviously improved aluminum paint, aqueous workability, workability is excellent have broader
The demand in market and prospect.
Specific embodiment
The present invention will be further described with reference to embodiments.
Embodiment 1
The aluminum paint, aqueous composition by weight of the present embodiment:0.7 part of dispersant, 4 parts of cosolvent, 5 parts of deionized water, aqueouss aluminum silver
Slurry 5 parts, 35 parts of E-125 acrylic emulsion, 0.4 part of defoamer, 0.4 part of levelling agent, 8 parts of thickening agent, 1.5 parts of anti-settling agent, go from
40 parts of sub- water, appropriate pH adjusting agent.
Its preparation method is:
(1) by 0.7 part of dispersant, 4 parts of cosolvent, 5 parts of deionized water and 5 parts of addition containers of water aluminum-silver slurry, mixing is stirred
Mix uniformly, soak 15~20min;
(2) 35 parts of E-125 acrylic emulsion, 0.4 part of defoamer, 0.4 part of levelling agent, 8 parts of thickening agent, 1.5 parts of anti-settling agent,
35 parts of addition containers of deionized water, stir at low shear;
(3) (2), under stirring at low speed, add (1) when stirring, and pour in (2) with the container that 5 parts of deionized waters wash away (1),
Stirring at low speed 15-20 minute;
(4) with qs pH adjuster, the pH value of (3) is adjusted to 7.8.
During use, paint component presses 100 with deionized water or drinking public water supply:20 weight proportion mix homogeneously, is sprayed on
On tinplate, place when drying in thermostatic constant wet chamber's (23 ± 2 DEG C, 50 ± 5%) and selecting corresponding regulation by technical specification
Between, record all technical and be shown in Table one.
Embodiment 2
The aluminum paint, aqueous composition by weight of the present embodiment:0.6 part of dispersant, 4 parts of cosolvent, 5 parts of deionized water, aqueouss aluminum
6 parts of silver paste, 35 parts of E-125 acrylic emulsion, 0.3 part of defoamer, 0.6 part of levelling agent, 7 parts of thickening agent, 2.5 parts of anti-settling agent, goes
39 parts of ionized water, appropriate pH adjusting agent.
Its preparation method is:
(1) by 0.6 part of dispersant, 4 parts of cosolvent, 5 parts of deionized water and 6 parts of addition containers of water aluminum-silver slurry, mixing is stirred
Mix uniformly, soak 15-20 minute;
(2) 35 parts of E-125 acrylic emulsion, 0.3 part of defoamer, 0.6 part of levelling agent, 7 parts of thickening agent, 2.5 parts of anti-settling agent,
34 parts of addition containers of deionized water, stir at low shear;
(3) (2), under stirring at low speed, add (1) when stirring, and pour in (2) with the container that 5 parts of deionized waters wash away (1),
Stirring at low speed 15-20 minute;
(4) with qs pH adjuster, the pH value of (3) is adjusted to 7.9.
During use, paint component presses 100 with deionized water or drinking public water supply:20 weight proportion mix homogeneously, is sprayed on
On tinplate, place when drying in thermostatic constant wet chamber's (23 ± 2 DEG C, 50 ± 5%) and selecting corresponding regulation by technical specification
Between, record all technical and be shown in Table one.
Embodiment 3
The aluminum paint, aqueous composition by weight of the present embodiment:1 part of dispersant, 4 parts of cosolvent, 5 parts of deionized water, water aluminum-silver slurry
7 parts, 37 parts of E-125 acrylic emulsion, 0.7 part of defoamer, 0.8 part of levelling agent, 7 parts of thickening agent, 3.5 parts of anti-settling agent, deionization
Water 34, appropriate pH adjusting agent.
Its preparation method is:
(1) by 1 part of dispersant, 4 parts of cosolvent, 5 parts of deionized water and 7 parts of addition containers of water aluminum-silver slurry, mix and blend
Uniformly, soak 15-20 minute;
(2) 37 parts of E-125 acrylic emulsion, 0.7 part of defoamer, 0.8 part of levelling agent, 7 parts of thickening agent, 3.5 parts of anti-settling agent,
Deionized water 29 adds container, stirs at low shear;
(3) (2), under stirring at low speed, add (1) when stirring, and pour in (2) with the container that 5 parts of deionized waters wash away (1),
Stirring at low speed 15-20 minute;
(4) with qs pH adjuster, the pH value of (3) is adjusted to 7.8.
During use, paint component presses 100 with deionized water or drinking public water supply:20 weight proportion mix homogeneously, is sprayed on
On tinplate, place when drying in thermostatic constant wet chamber's (23 ± 2 DEG C, 50 ± 5%) and selecting corresponding regulation by technical specification
Between, record all technical and be shown in Table one.
With reference to the countries concerned or industry standard, performance detection is carried out to embodiments above, result such as table one.
Table one.
Claims (11)
1. a kind of water-based metal metallic finishe is it is characterised in that described coating portion is formulated by following components in parts by weight:
2. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the dispersant used by coating,
Including modified polyacrylate high polymer, modified polyacrylate and ethylenic copolymer, the alkanolamine of high molecular weight carboxylic,
One or more of fatty acid modified polyester is with the mixing of arbitrary proportion.
3. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the cosolvent used by coating,
Including ethylene glycol only son's mystery, propylene glycol monomethyl ether, propylene glycol methyl ether acetate, dibasic acid ester mixture, ethanol, butanol, isopropanol,
One or more of butanone, acetone are with the mixing of arbitrary proportion.
4. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the aqueouss aluminum silver used by coating
Starch the non-leafing aluminum paste in 5-80 micron for aluminum argentum powder particle size span.
5. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the aqueous acrylamide used by coating
Yogurt liquid, mixed with arbitrary proportion including one or more of water-borne acrylic resin, Aqueous acrylic urethane's dispersion
Close.
6. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the defoamer used by coating,
Including containing organic-silicon-modified water-based emulsion shape defoamer, organically-modified polydimethylsiloxane, ethylenic copolymer, ethylene
One or more of based polyalcohol is with the mixing of arbitrary proportion.
7. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the levelling agent used by coating,
Including organic silicon modified by polyether polymer, organic silicon modified by polyether, modified polyorganosiloxane emulsion, fluorine-carbon modified preneutralization poly- third
One or more of olefin(e) acid aqueous solution of ester, acrylic acid-Organosiliconcopolymere are with the mixing of arbitrary proportion.
8. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the thickening agent used by coating,
Including association type polyurethane thickener, alkali soluble is swollen acroleic acid polyurethane, cellulose thickener.
9. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the anti-settling agent used by coating,
Including polyamide wax ammonium salt, organobentonite.
10. a kind of water-based metal metallic finishe according to claim 1 it is characterised in that:Prepare the pH regulator used by coating
Agent, including dimethylethanolamine, ammonia, triethylamine.
A kind of preparation method of the water-based metal metallic finishe described in 11. claim 1-10, it comprises the following steps:
(1) by dispersant, cosolvent, deionized water and water aluminum-silver slurry mixing and stirring, soak 15~20min;
(2) aqueous acrylic emulsion, defoamer, levelling agent, thickening agent, anti-settling agent and deionized water mix homogeneously, in low sheraing
Stir under power;
(3) (2), under stirring at low speed state, add (1), stir when stirring;
(4) with pH adjusting agent, the pH value of (3) is adjusted between 7.5-8.5.
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CN201610573920.1A CN106433344A (en) | 2016-07-20 | 2016-07-20 | Water-based metal flashing paint and preparation method thereof |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106916497A (en) * | 2017-03-28 | 2017-07-04 | 常州大学 | A kind of preparation method of the automobile water-based property metal flash paint of stably dispersing type |
CN107057501A (en) * | 2017-06-19 | 2017-08-18 | 安徽康瑞高科新材料技术工程有限公司 | One kind applies water aluminum powder paint |
CN107083136A (en) * | 2017-04-28 | 2017-08-22 | 叶镜枝 | Polyacrylate coating and its coating process |
CN107163828A (en) * | 2017-06-12 | 2017-09-15 | 深圳市绚图新材科技有限公司 | A kind of height of zero VOC adheres to aqueous automobile bottom colored paint and preparation method thereof |
CN109337551A (en) * | 2018-09-10 | 2019-02-15 | 中山永辉化工股份有限公司 | It is a kind of can be with the water-soluble mirror effect coating and preparation method of drying at room temperature |
CN109912959A (en) * | 2019-03-06 | 2019-06-21 | 绍兴奥唯特纳米科技有限公司 | The latex balloon of metallic travel water-based metal mill base and preparation method and latex balloon |
CN110028888A (en) * | 2019-04-19 | 2019-07-19 | 上海福岛新材料科技有限公司 | A kind of environment-friendly water-based metallic paint |
CN111592806A (en) * | 2020-06-29 | 2020-08-28 | 山东鑫亿新材料科技有限公司 | Cold-state aluminum coating method for cold end of silicon carbide rod |
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CN103333575A (en) * | 2013-07-26 | 2013-10-02 | 江苏足迹涂料有限公司 | Water-based automobile metallic flashing paint and preparation technology thereof |
CN105315813A (en) * | 2015-07-02 | 2016-02-10 | 江苏足迹涂料有限公司 | Water-based automobile metal base coat and preparing method thereof |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106916497A (en) * | 2017-03-28 | 2017-07-04 | 常州大学 | A kind of preparation method of the automobile water-based property metal flash paint of stably dispersing type |
CN107083136A (en) * | 2017-04-28 | 2017-08-22 | 叶镜枝 | Polyacrylate coating and its coating process |
CN107083136B (en) * | 2017-04-28 | 2020-04-10 | 叶镜枝 | Polyacrylate paint and coating method thereof |
CN107163828A (en) * | 2017-06-12 | 2017-09-15 | 深圳市绚图新材科技有限公司 | A kind of height of zero VOC adheres to aqueous automobile bottom colored paint and preparation method thereof |
CN107163828B (en) * | 2017-06-12 | 2019-04-09 | 深圳市绚图新材科技有限公司 | A kind of height of zero VOC adheres to aqueous automobile bottom colored paint and preparation method thereof |
CN107057501A (en) * | 2017-06-19 | 2017-08-18 | 安徽康瑞高科新材料技术工程有限公司 | One kind applies water aluminum powder paint |
CN109337551A (en) * | 2018-09-10 | 2019-02-15 | 中山永辉化工股份有限公司 | It is a kind of can be with the water-soluble mirror effect coating and preparation method of drying at room temperature |
CN109912959A (en) * | 2019-03-06 | 2019-06-21 | 绍兴奥唯特纳米科技有限公司 | The latex balloon of metallic travel water-based metal mill base and preparation method and latex balloon |
CN109912959B (en) * | 2019-03-06 | 2022-07-29 | 绍兴奥唯特纳米科技有限公司 | Water-based metal color paste with metal flashing effect for latex balloons, preparation method of water-based metal color paste and latex balloons |
CN110028888A (en) * | 2019-04-19 | 2019-07-19 | 上海福岛新材料科技有限公司 | A kind of environment-friendly water-based metallic paint |
CN111592806A (en) * | 2020-06-29 | 2020-08-28 | 山东鑫亿新材料科技有限公司 | Cold-state aluminum coating method for cold end of silicon carbide rod |
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Application publication date: 20170222 |