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CN106189659A - A kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp - Google Patents

A kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp Download PDF

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Publication number
CN106189659A
CN106189659A CN201610583541.0A CN201610583541A CN106189659A CN 106189659 A CN106189659 A CN 106189659A CN 201610583541 A CN201610583541 A CN 201610583541A CN 106189659 A CN106189659 A CN 106189659A
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China
Prior art keywords
weight portion
oil
herba
weight
radiator
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CN201610583541.0A
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Chinese (zh)
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庄可香
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Individual
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Priority to CN201610651899.2A priority Critical patent/CN106189665A/en
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F21—LIGHTING
    • F21S—NON-PORTABLE LIGHTING DEVICES; SYSTEMS THEREOF; VEHICLE LIGHTING DEVICES SPECIALLY ADAPTED FOR VEHICLE EXTERIORS
    • F21S6/00—Lighting devices intended to be free-standing
    • F21S6/001—Lighting devices intended to be free-standing being candle-shaped
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D161/00—Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
    • C09D161/04—Condensation polymers of aldehydes or ketones with phenols only
    • C09D161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/46—Stemonaceae [Stemona family], e.g. croomia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/01—Deodorant compositions
    • A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
    • C08L63/10—Epoxy resins modified by unsaturated compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F21—LIGHTING
    • F21S—NON-PORTABLE LIGHTING DEVICES; SYSTEMS THEREOF; VEHICLE LIGHTING DEVICES SPECIALLY ADAPTED FOR VEHICLE EXTERIORS
    • F21S10/00—Lighting devices or systems producing a varying lighting effect
    • F21S10/04—Lighting devices or systems producing a varying lighting effect simulating flames
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F21—LIGHTING
    • F21V—FUNCTIONAL FEATURES OR DETAILS OF LIGHTING DEVICES OR SYSTEMS THEREOF; STRUCTURAL COMBINATIONS OF LIGHTING DEVICES WITH OTHER ARTICLES, NOT OTHERWISE PROVIDED FOR
    • F21V29/00—Protecting lighting devices from thermal damage; Cooling or heating arrangements specially adapted for lighting devices or systems
    • F21V29/50—Cooling arrangements
    • F21V29/502—Cooling arrangements characterised by the adaptation for cooling of specific components
    • F21V29/503—Cooling arrangements characterised by the adaptation for cooling of specific components of light sources
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F21—LIGHTING
    • F21V—FUNCTIONAL FEATURES OR DETAILS OF LIGHTING DEVICES OR SYSTEMS THEREOF; STRUCTURAL COMBINATIONS OF LIGHTING DEVICES WITH OTHER ARTICLES, NOT OTHERWISE PROVIDED FOR
    • F21V29/00—Protecting lighting devices from thermal damage; Cooling or heating arrangements specially adapted for lighting devices or systems
    • F21V29/50—Cooling arrangements
    • F21V29/70—Cooling arrangements characterised by passive heat-dissipating elements, e.g. heat-sinks
    • F21V29/83—Cooling arrangements characterised by passive heat-dissipating elements, e.g. heat-sinks the elements having apertures, ducts or channels, e.g. heat radiation holes
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F21—LIGHTING
    • F21V—FUNCTIONAL FEATURES OR DETAILS OF LIGHTING DEVICES OR SYSTEMS THEREOF; STRUCTURAL COMBINATIONS OF LIGHTING DEVICES WITH OTHER ARTICLES, NOT OTHERWISE PROVIDED FOR
    • F21V29/00—Protecting lighting devices from thermal damage; Cooling or heating arrangements specially adapted for lighting devices or systems
    • F21V29/85—Protecting lighting devices from thermal damage; Cooling or heating arrangements specially adapted for lighting devices or systems characterised by the material
    • F21V29/87—Organic material, e.g. filled polymer composites; Thermo-conductive additives or coatings therefor
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F21—LIGHTING
    • F21V—FUNCTIONAL FEATURES OR DETAILS OF LIGHTING DEVICES OR SYSTEMS THEREOF; STRUCTURAL COMBINATIONS OF LIGHTING DEVICES WITH OTHER ARTICLES, NOT OTHERWISE PROVIDED FOR
    • F21V29/00—Protecting lighting devices from thermal damage; Cooling or heating arrangements specially adapted for lighting devices or systems
    • F21V29/85—Protecting lighting devices from thermal damage; Cooling or heating arrangements specially adapted for lighting devices or systems characterised by the material
    • F21V29/89—Metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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    • C08K2201/002—Physical properties
    • C08K2201/004—Additives being defined by their length
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    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
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    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/02—Flame or fire retardant/resistant
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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Abstract

The present invention relates to a kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp, including lampshade, heat carrier, radiator and base, described heat carrier is made by aluminum is one-body molded with radiator, described LED illumination assembly is mounted on heat carrier by heat radiation coating, described radiator rear end is hollow cavity, and the present invention not only has all functions of conventional lamp, capable of releasing negative ion, there is the effect removing the finishing pollution things such as formaldehyde, toluene, TVOC, meet the multiple demand of modern user.

Description

A kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp
Technical field
The present invention relates to technical field of lamps, be specifically related to a kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp.
Background technology
Along with the development and progress of society, the environmental protection idea of people is increasingly stronger, thus the illumination dress of environmental protection Put and can more be favored by people, day by day ripe LED technology due to its have efficiently, energy-saving and environmental protection, length in service life, merit The advantages such as rate is low, LED illumination lamp the most gradually starts to replace traditional lighting.
LED electricity-saving lamp is actually a kind of compact, carries the LED of ballast, and lamp tube ends voltage is directly over Plasma state turns on and sends the ultraviolet of 253.7nm, and ultraviolet evokes light-emitting phosphor, due to filament during fluorescent lamp operation Temperature at about 1160K, more much lower than temperature 2200-2700K of electric filament lamp work, thus its life-span the most significantly prolong Long, arrive more than 5000 hours, due to the electric ballast that its operation efficiency is higher, there is not electric current as electric filament lamp simultaneously Heat effect, the energy conversion efficiency of fluorescent material is the highest, arrives more than every watt of 50 lumens, saves energy.
On the one hand, along with the continuous rising of Global Temperature, the population of mosquito and quantity all will be greatly improved, the most day by day threaten The health of the mankind.Mosquito, in addition to directly stining thorn and sucking blood, harass sleep, more seriously propagates multiple disease.The mosquito of China passes disease Having malaria, Filariasis, epidemic encephalitis type B and dengue fever (or dengue hemorrhagic fever) four class, mosquito passes more important virosis Also have yellow fever and various equine encephalitis etc..
On the other hand, by negative aeroion Technology application in electricity-saving lamp product, the electricity-saving lamp after using is long-term in indoor Release negative aeroion, especially negative oxygen ion.Owing to it is structurally similar to ultra-oxygen anion free radical, therefore there is phase As biological activity, it is possible to make live biological cell electronegative, so that virus loses the attacking ability to cell；Meanwhile, Negative oxygen ion can react with the finishing pollution thing such as formaldehyde, toluene, TVOC, product be nonpoisonous and tasteless carbon dioxide and Water, the generation of non-secondary pollution, there is certain effect purified the air of a room, such as, in artificial air's anion environment, In air, mycete, bacterial population can reduce by more than 90% after measured.After negative oxygen ion is inhaled into human body, can regulate neural emerging Put forth energy state, improve the ventilatory of lung, improve blood circulation, enhance metabolism, strengthen immune system ability, make people's spirit shake Putting forth energy, improve work efficiency etc., the numerous diseases such as hypertension, asthma, influenza, insomnia, arthritis are also had certain treatment to make by it With, so people's anion is called " vitamin in air " " long-lived element ".
So far, make conventional lamp product have the Technology design of expelling mosquito and anion releasing health care the most simultaneously Have and see.
Summary of the invention
The deficiency existed for prior art, the technical problem to be solved is to provide a kind of multi-functional remove except aldehyde Phenyl ring protects LED candle lamp, on the basis of not affecting original light fixture radiating effect, makes light fixture have an expelling mosquito, release bear from The function of son, fragrant odour simultaneously, character is gentle, also has certain antibiotic effect, has certain removal formaldehyde, first simultaneously Effect of the finishing pollution thing such as benzene, TVOC, enriches the use function of conventional lamp.
It is an object of the invention to be achieved through the following technical solutions:
A kind of novel LED environmental-protection decorative light fixture, it is characterised in that: include lampshade, LED illumination assembly, heat carrier, radiator, Electric power driving module and base, described electric power driving module device is in described base, and described heat carrier and radiator are by aluminum One-body molded being made, described LED illumination assembly is mounted on heat carrier by heat radiation coating, and described radiator rear end is Hollow cavity, described radiator is connected with base by thread, wherein, is provided with some heat radiations in the leading section of described radiator Hole, the sidewall of described radiator is provided with some radiating grooves, and described radiating groove runs through the sidewall of radiator, in described radiator The inner wall surface even spread of cavity body has heat radiation coating, described heat radiation coating by following component according to parts by weight preparation and Become: hybrid resin 60-75 weight portion, Graphene 5-6.5 weight portion, sodium-based montmorillonite 3-4.5 weight portion, carboxylic styrene butadiene latex 4- 6.5 weight portions, silicones metlyl branching silicone oil 1.5-2 weight portion, Polyethylene Glycol 0.7-1.2 weight portion, pentane 0.7-1.8 weight Amount part, nano silicon 1-2.5 weight portion, polyacrylonitrile-based carbon fibre 7-9 weight portion, aerosil 1-2 weight portion, Fire retardant 5.5-7 weight portion, curing agent 4-6 weight portion, solvent 15-20 weight portion, ceria 0.1-0.15 Weight portion, active mineral matter powder 1.5-2 weight portion, essential oil of traditional Chinese medicine 1.5-2.5 weight portion；Wherein, described hybrid resin is phenolic aldehyde The mass ratio of resin and the mixture of epoxy resin, phenolic resin and epoxy resin is 2:1-3:1；Described polyacrylonitrile-based carbon is fine Tie up a length of 0.01mm；Described fire retardant is the mixture of APP, tripolycyanamide and expanded graphites, described polyphosphoric acid The mass ratio 2:1.5:1.3 of ammonium, tripolycyanamide and expanded graphites；Described solvent is the mixing of DAA and butyl ester Thing, the mass ratio of described DAA and butyl ester is 3:1-3:2；Described active mineral matter powder be germanite, fluorite, tourmaline, Gahnite by weight the mixture of 2.5:3:3.5:1.7, wherein tourmaline be dravite and elbaite by weight The mixture of 4:3, particle diameter≤15 μm of described active mineral matter powder, described heat radiation coating is made by the steps and forms:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender Go out, i.e. prepare mixture A, standby；
S2, by material Fructus Xanthii 70-80 weight portion, Folium Symplocoris Caudatae 15-20 weight portion, Pericarpium Zanthoxyli 20-25 weight portion, Folium Viticis Negundo 6-8 weight Part, Herba Hedyotidis Diffusae 3-5 weight portion, beans leaf 8-16 weight portion, Herba Solani Lyrati 25-35 weight portion, Herba Houttuyniae 15-25 weight portion, even Stick up 10-20 weight portion, Radix Salviae Miltiorrhizae 3-4 weight portion, Herba polygoni hydropiperis 3-4 weight portion, Radix Stemonae 5-8 weight portion decontamination, be placed in-20 DEG C together Vacuum still 2-3 hour, be placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 30-40 minute, microwave merit Rate is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Calendula officinalis 3-4 weight portion, Rhizoma Atractylodis 1.5-2 weight portion, Herba Anemones Hupehensis 3-5 weight portion, Herba Menthae 1-3 weight portion, mountain Chicken green pepper 3-5 weight portion, Herba Portulacae 3-4 weight portion, Herba Pogostemonis 3-4 weight portion, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Faeces Leporis 4-8 weight portion, beg Chinese mugwort 3-4 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, then adds deionized water and soaks 5 hours, adds The water yield by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.13-0.2 weight portion and be dried place Reason, i.e. prepares volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 70-80 DEG C, concentrates in blender Stirring mixing 15 minutes, obtains premix material, standby；
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 70-80 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity Agent 3-5 weight portion, diethyltoluamide 0.1-0.2, butyl butyrate 9-15 weight portion, Eucalyptus oil 10-13 weight portion, isopropyl myristate 1-2 weight portion, polyoxyethylenated alcohol sodium sulfate 10-15 weight portion and sodium benzoate 0.1-0.3 weight portion.
It should be noted that the experiment proved that, active mineral matter powder adds appropriate ceria (CeO2), utilize The emittance of this rare earth element is high, the feature of half degradation period limit for length, and the anion that active mineral matter powder can be significantly increased produces Rate, its principle is as follows: the Ce in ceria4+Ce is changed under photoenvironment3+, in conversion process, electron-hole Recombination probability reduces, then in active mineral matter powder under the effect of the material electric field such as tourmaline, part electronics is passively with electric field side To displacement, electron-hole recombination probability reduces, thus at tourmaline/CeO2Substantial amounts of electricity has been gathered on composite powder surface The energy of solution air molecule, and then create the negative aeroion of high concentration, Ce simultaneously3+It is oxidized into again Ce4+, then repeat Aforesaid conversion process；Meanwhile, through practice detection, be combined through the present invention active mineral matter powder of proportioning adds appropriate Ceria component, higher more than 10 times than without the concentration of active mineral matter powder anion adding ceria, r ray with from So environment is identical.
The present invention is based on motherland's traditional medicine, with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine with anti- Reviewing card, give full play to each group of weight portion synergism, the effect brief introduction of the most each raw material is as follows.
Fructus Xanthii: fruit: pungent, bitter, temperature, pain relieving parasite killing, suspension can prevent eliminating aphis, and as camphorated, killing rate is higher, Fructus Xanthii Calx closes liquid can killing aphids.
Folium Symplocoris Caudatae: branch and leaf contain aromatic oil, can make perfumery raw material.All herbal medicine, has the effect of parasite killing.
Pericarpium Zanthoxyli: medicinal part is the dry mature skin of rutaceae Capsicum annuum L. or Pericarpium Zanthoxyli.Acrid in the mouth, warm in nature.Return spleen, stomach, Kidney channel.Warming middle-JIAO to relieve pain, killing parasites for relieving itching.
Folium Viticis Negundo: acrid in the mouth；Bitter；Property flat, expelling pathogenic wind from the body surface, dehumidifying, parasite killing, pain relieving etc..To staphylococcus aureus and anthrax Bacillus has notable antibacterial action, to escherichia coli, group B streptococcus, diphtheria corynebacterium, Bacillus typhi, green pus liver bacterium and dysentery bacterium Deng also there being certain antibacterial action.
Herba Hedyotidis Diffusae: bitter in the mouth, light, cold in nature.Primary efficacy is heat-clearing and toxic substances removing, medicinal powder for relieving pain knot, promoting urination to remove dampness.Outstanding kind treatment All kinds inflammation.In clinical practice, if finding, Herba Hedyotidis Diffusae compatibility is proper, can treat multiple disease.
Beans leaf: medicinal part is the leaf of Piperaceae plant paste.Pungent, temperature.Dispeiling pathogenic wind and removing dampness, killing parasites for relieving itching.
Herba Solani Lyrati: cold in nature, sweet in the mouth, hardship.Return Liver Channel, gallbladder meridian, kidney channel.Effect and effect: heat clearing away, dampness removing, dispel the wind, detoxify.With Treating malaria disease, jaundice, edema, gonorrhea, rheumatic arthritis, erysipelas, furuncle.Main component: containing alkaloids such as solanines.
Herba Houttuyniae: there is the effects such as antibacterial, antiviral, raising immunity of organisms, to various microorganisms (especially yeast And mycete) all there is inhibitory action, to the streptococcus of hemolytic, staphylococcus aureus, hemophilus influenza, micrococcus catarrhalis, pneumonia ball Bacterium has obvious inhibitory action.Escherichia coli, dysentery bacterium, Bacillus typhi also there is effect.
Fructus Forsythiae: heat-clearing and toxic substances removing, dispersing swelling and dissipating binds, dispelling wind and heat pathogens, there is the title of " persons particularly liable to develop skin infection's panacea ", Bacillus typhi, secondary wound can be suppressed Cold bacillus, escherichia coli, dysentery bacterium, diphtheria corynebacterium and vibrio cholera, staphylococcus, streptococcus etc..
Radix Salviae Miltiorrhizae: nature and flavor are bitter, are slightly cold.GUIXIN, Liver Channel." the southern regions of the Yunnan Province book on Chinese herbal medicine " is recorded: reinforcing the heart sedate, calming heart and tranquilizing mind.Control forgetful seized with terror Punching, palpitation with fear is insomnia, and has stasis-dispelling and pain-killing, promoting blood circulation to restore menstrual flow, the effect of the relieving restlessness that clears away heart-fire, and for menoxenia, amenorrhea dysmenorrhea, lump in the abdomen amasss Poly-, chest and abdomen twinge, pyretic arthralgia pain, skin infection.
Herba polygoni hydropiperis: all have inhibitory action, current clinical medicine research to show in test tube to various dysentery bacteriums, Herba polygoni hydropiperis has There are the effects such as antibacterial, antiviral, antiinflammatory, antioxidation.
The Radix Stemonae: can driving away mosquito, resisting pathogenic microbes effect, to beta hemolytic streptococcus, meningococcus, golden yellow The multiple pathomycetes such as staphylococcus, Staphylococcus albus, Bacillus typhi, pneumobacillus, bacillus pestis, anthrax bacillus have necessarily Inhibitory action, its infusion all has killing action to mosquitos and flies larva, head louse, clothing louse and Cimex bedbug etc..
Calendula officinalis: Compositae Calendula officinalis, is used as medicine with root, flower.Light, flat.Root: promoting blood circulation to remove blood stasis, circulation of qi promoting diuresis.Cure mainly lump in the abdomen hernia Gas, cold syndrome of the stomach pain.Flower: removing heat from blood, hemostasis.Cure mainly discharging fresh blood stool.Flower, leaf have antiinflammatory, an antibacterial action, particularly to staphylococcus, Streptococcus effect is preferable.
Rhizoma Atractylodis: containing volatile oil, mainly atractylol, atractylone and a large amount of vitamin, have a dry abdomen invigorating spleen and dispelling wind-evil, cold expelling, Improving eyesight function；
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " toil, temperature have little Poison." removing toxic substances, evacuation of pus granulation promoting, dissipating blood stasis of subsiding a swelling, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria is little Youngster's infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Herba Menthae: for the dry aerial parts of labiate Herba Menthae, dispelling wind and heat pathogens, the clear profit head, sore-throat relieving rash, soothing the liver row Gas.
Cubeb litsen tree: nature and flavor hardship pungent, micro-, has fragrance, nontoxic.Branch, leaf are respectively provided with fragranced.Root bark and leaf can hyoscines.Tool There is the kidney warming stomach invigorating, effect of promoting QI to circulate and dispersing the agglomeration of the pathogens.For treating the disease such as gastralgic vomitting and innominate toxic swelling.
Herba Portulacae: Portulacaceae annual herb plant.Plump succulence, without hair, high 10-30cm, be born in roadside, field and The area without shade such as ruins, flower garden.All there is distribution domestic various places.This kind is medicine food dual purpose plant.Herb hyoscine, has clearing away heat-damp and promoting diuresis, solution Poison detumescence, antiinflammatory, quench the thirst, diuresis.
Herba Pogostemonis: acrid in the mouth, slightly warm in nature.Effect: removing dampness for regulating stomach, the effect of administration of inducing sweat, solve, cure mainly dampness taste, breast gastral cavity is vexed swollen, Appetite is the most fragrant, Nausea and vomiting；Summer, heat-damp in summer was sleepy, uncomfortable in chest did not relaxed, and affection of exogenous wind-cold. the diseases such as aversion to cold is uncomfortable in chest, and have and have relatively Strong Fungistasis and antibacterial action.
The Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae): the another name river Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), continuous poison, Radix Stellerae, chervil, vexed fresh idea, Re Jiaba, Herba Senecionis Dianthui, Radix scopoliae sinensis, perfume, Medicine sieve foretells, raw pull, flourishing bavin headdress flower, monkey root, Gelsemium elegans Benth., in Chinese medicine with its root eliminate the phlegm, pain relieving, removing food stagnancy, parasite killing.
Faeces Leporis: basis, medicine source is the dry feces of rabbit section animal hare.Pungent, flat.Return lung, Liver Channel.Improving eyesight, parasite killing solution Poison.
Artemisia argyi Levl. et Van. var. argyi cv. Qiai: have another name called: containing 17 kinds of known compounds, has and relievings asthma, antitussive, eliminates the phlegm and clear scorching effect, reasonable QI and blood, by cold The effects such as wet, regulating menstruation is antiabortive, warming the meridian for stopping bleeding, clearing and antitussive expectorant.Cure mainly cold type of pain in menoxenia, abdomen, vaginal bleeding during pregnancy hematochezia, fetal movement not The diseases such as peace, infertility.
It should be noted that be proven, after carrying out the Radix Salviae Miltiorrhizae of certain part by weight, Herba polygoni hydropiperis and the Radix Stemonae compounding, no Only it is remarkably improved degerming antibacterial ability, also can produce a kind of delicate fragrance taste having no side effect, refreshing, have certain Effect of refreshing oneself；, it is proven, by the Fructus Xanthii of certain part by weight, Folium Symplocoris Caudatae, Pericarpium Zanthoxyli, beans leaf, Faeces Leporis with break meanwhile After bowl flower carries out compounding, the mosquito dispersing ability of said composition is made to be significantly improved；It addition, it is Folium Viticis Negundo, Herba Hedyotidis Diffusae, white After the components such as English, Herba Houttuyniae, Calendula officinalis and Artemisia argyi Levl. et Van. var. argyi cv. Qiai carry out compatibility, substantially increase the antibacterial degerming ability of compositions, through practice Detection, the compositions after compounding is to staphylococcus aureus, anthrax bacillus, hemophilus influenza, micrococcus catarrhalis, streptococcus pneumoniae, large intestine Bacillus, group B streptococcus, diphtheria corynebacterium, Bacillus typhi, green pus liver bacterium, dysentery bacteriums etc. more than 40 are planted pathogenic bacteria and have certain suppression And killing action.
The effect of the present invention:
The present invention uses Chinese medicine to compound with active mineral matter, makes the present invention not only have preferable radiating effect, it is also possible to drive Mosquito, anion releasing, fresh air, simultaneously fragrant odour, character is gentle, has anophelifuge, antibacterial and effect of health care.
Accompanying drawing explanation
Fig. 1 is radiator structure perspective exploded view of the present invention.
Fig. 2 is overall schematic of the present invention.
Fig. 3 is radiator schematic perspective view of the present invention.
Detailed description of the invention
Embodiment 1:
Refer to shown in Fig. 1 to Fig. 3, a kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp, including lampshade 1, LED illumination assembly 2, heat carrier 3, radiator 4, electric power driving module and base 5, described electric power driving module device in described base 5, institute Stating heat carrier 3 to be made by aluminum is one-body molded with radiator 4, described LED illumination assembly 2 is mounted on by heat radiation coating and leads On hot body 3, described radiator 4 rear end is hollow cavity 42, and described radiator 4 is connected by screw thread 50 with base 5, wherein, Be provided with some louvres 40 in the leading section of described radiator 4, the sidewall of described radiator 4 is provided with some radiating grooves 41, described Radiating groove 41 run through the sidewall of radiator 4, extraneous air can by described radiating groove 4 with in described radiator 4 rear end The inner air of cavity body 42 carries out air exchange, and the inner wall surface even spread at described radiator 4 hollow cavity 43 has scattered Hot coating, described heat radiation coating is prepared from according to parts by weight by following component: hybrid resin 60 weight portion, and sodio covers de- Soil 4.5 weight portions, carboxylic styrene butadiene latex 4 weight portion, silicones metlyl branching silicone oil 2 weight portion, Polyethylene Glycol 0.7 weight portion, Pentane 1.8 weight portion, nano silicon 1 weight portion, polyacrylonitrile-based carbon fibre 9 weight portion, Graphene 5 weight portion, gas Aerosil 2 weight portion, fire retardant 5.5 weight portion, curing agent 6 weight portion, solvent 15 weight portion, titanium dioxide Cerium 0.1 weight portion, active mineral matter powder 2 weight portion, essential oil of traditional Chinese medicine 1.5 weight portion；Wherein, described hybrid resin is phenolic resin It is 3:1 with the mass ratio of the mixture of epoxy resin, phenolic resin and epoxy resin；Described polyacrylonitrile-based carbon fibre is a length of 0.01mm；Described fire retardant is the mixture of APP, tripolycyanamide and expanded graphites, described APP, trimerization The mass ratio 2:1.5:1.3 of cyanamide and expanded graphites；Described solvent is the mixture of DAA and butyl ester, described two The mass ratio of pyruvic alcohol and butyl ester is 3:1；Described active mineral matter powder be germanite, fluorite, tourmaline, gahnite by weight The ratio mixture of 2.5:3:3.5:1.7, wherein tourmaline is dravite and the mixture of elbaite 4:3 by weight, institute Stating particle diameter≤15 μm of active mineral matter powder, described heat radiation coating is made by the steps and forms:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender Go out, i.e. prepare mixture A, standby；
S2, by material Fructus Xanthii 70 weight portion, Folium Symplocoris Caudatae 20 weight portion, Pericarpium Zanthoxyli 20 weight portion, Folium Viticis Negundo 8 weight portion, Herba Hedyotidis Diffusae Grass 3 weight portions, beans leaf 16 weight portion, Herba Solani Lyrati 25 weight portion, Herba Houttuyniae 25 weight portion, Fructus Forsythiae 10 weight portion, Radix Salviae Miltiorrhizae 4 weight Part, Herba polygoni hydropiperis 3 weight portion, the Radix Stemonae 8 weight portion decontamination, it is placed in the vacuum still 2 hours of-20 DEG C together, is placed in microwave the most again Drying machine carries out pretreatment, and wherein drying time is 30 minutes, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Calendula officinalis 3 weight portion, Rhizoma Atractylodis 2 weight portion, Herba Anemones Hupehensis 3 weight portion, Herba Menthae 3 weight portion, cubeb litsen tree 3 weight Part, Herba Portulacae 4 weight portion, Herba Pogostemonis 3 weight portion, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 4 weight portion, Faeces Leporis 4 weight portion, Artemisia argyi Levl. et Van. var. argyi cv. Qiai 4 weight portion are clean dries, Putting in super micron mill together and be crushed to 30 mesh, then add deionized water and soak 5 hours, amount of water is by being soaked crude drug matter 7 times of amount, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.13 weight portion and be dried process, i.e. Prepare volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 70 DEG C, concentrates in blender and stirs Mix mixing 15 minutes, obtain premix material, standby；
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 73 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity Agent 3 weight portion, diethyltoluamide 0. 2 weight portion, butyl butyrate 9 weight portion, Eucalyptus oil 4 weight portion, isopropyl myristate 1 weight Part, polyoxyethylenated alcohol sodium sulfate 15 weight portion and sodium benzoate 0.1 weight portion.
Embodiment 2:
A kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp, including lampshade 1, LED illumination assembly 2, heat carrier 3, radiator 4, electricity Source drives module and base 5, described electric power driving module device in described base 5, described heat carrier 3 and radiator 4 by Aluminum is one-body molded to be made, and described LED illumination assembly 2 is mounted on heat carrier 3 by heat radiation coating, described radiator 4 Rear end is hollow cavity 42, and described radiator 4 is connected, wherein, in the front end of described radiator 4 by screw thread 50 with base 5 Portion is provided with some louvres 40, and the sidewall of described radiator 4 is provided with some radiating grooves 41, and described radiating groove 41 runs through radiator The sidewall of 4, the inner wall surface even spread at described radiator 4 hollow cavity 43 has heat radiation coating, described heat radiation coating by Following component is prepared from according to parts by weight: hybrid resin 75 weight portion, sodium-based montmorillonite 3 weight portion, carboxylic styrene butadiene latex 6.5 weight portions, silicones metlyl branching silicone oil 1.5 weight portion, Polyethylene Glycol 1.2 weight portion, pentane 0.7 weight portion, nanometer Silicon dioxide 2.5 weight portion, polyacrylonitrile-based carbon fibre 8 weight portion, Graphene 6 weight portion, aerosil 1.5 weight Part, fire retardant 6 weight portion, curing agent 5 weight portion, solvent 17 weight portion, ceria 0.15 weight portion, activity Mineral powder 1.7 weight portion, essential oil of traditional Chinese medicine 2 weight portion；Wherein, described hybrid resin is the mixing of phenolic resin and epoxy resin The mass ratio of thing, phenolic resin and epoxy resin is 3:1；The a length of 0.01mm of described polyacrylonitrile-based carbon fibre；Described fire-retardant Agent is the mixture of APP, tripolycyanamide and expanded graphites, described APP, tripolycyanamide and intumescent stone The mass ratio 2:1.5:1.3 of ink；Described solvent is the mixture of DAA and butyl ester, described DAA and the matter of butyl ester Amount ratio is 3:2；Described active mineral matter powder is that germanite, fluorite, tourmaline, gahnite are by weight 2.5:3:3.5:1.7 Mixture, wherein tourmaline is dravite and the elbaite mixture by weight 4:3, described active mineral matter powder Particle diameter≤15 μm, described heat radiation coating is made by the steps and forms:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender Go out, i.e. prepare mixture A, standby；
S2, by material Fructus Xanthii 80 weight portion, Folium Symplocoris Caudatae 15 weight portion, Pericarpium Zanthoxyli 25 weight portion, Folium Viticis Negundo 6 weight portion, Herba Hedyotidis Diffusae Grass 5 weight portions, beans leaf 8 weight portion, Herba Solani Lyrati 35 weight portion, Herba Houttuyniae 15 weight portion, Fructus Forsythiae 20 weight portion, Radix Salviae Miltiorrhizae 3 weight Part, Herba polygoni hydropiperis 4 weight portion, the Radix Stemonae 5 weight portion decontamination, it is placed in the vacuum still 3 hours of-20 DEG C together, is placed in microwave the most again Drying machine carries out pretreatment, and wherein drying time is 40 minutes, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Calendula officinalis 4 weight portion, Rhizoma Atractylodis 1.5 weight portion, Herba Anemones Hupehensis 5 weight portion, Herba Menthae 1 weight portion, cubeb litsen tree 5 weight Amount part, Herba Portulacae 3 weight portion, Herba Pogostemonis 4 weight portion, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3 weight portion, Faeces Leporis 8 weight portion, Artemisia argyi Levl. et Van. var. argyi cv. Qiai 3 weight portion are clean dries, Putting in super micron mill together and be crushed to 30 mesh, then add deionized water and soak 5 hours, amount of water is by being soaked crude drug matter 7 times of amount, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.18 weight portion and be dried process, i.e. Prepare volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 75 DEG C, concentrates in blender and stirs Mix mixing 15 minutes, obtain premix material, standby；
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 80 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity Agent 5 weight portion, diethyltoluamide 0.1 weight portion, butyl butyrate 15 weight portion, Eucalyptus oil 7 weight portion, isopropyl myristate 2 weight Part, polyoxyethylenated alcohol sodium sulfate 10 weight portion and sodium benzoate 0.3 weight portion.
Remaining is with embodiment 1.
In a preferred embodiment, described lampshade 1 is prepared from according to parts by weight by following component:
Resin 50 weight portion；Glass fibre 13 weight portion；Fire retardant 6 weight portion；Graphene 3 weight portion；Modified aromatic amine solidifies Agent 3 weight portion；Fluorescent material 0.2 weight portion, good solid 754 light trigger 3 weight portions of vapour Ba Yan；Polyetheramine catalyst 0.6 weight portion； Active mineral matter powder 2 weight portion；Essential oil of traditional Chinese medicine 2.5 weight portion；Wherein, described resin is epoxy soybean oil acrylate and bis-phenol The mixture of A type E51 epoxy resin, the mass ratio of described epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 2: 1, described fire retardant is the mixture of APP, tripolycyanamide and expanded graphites, described APP, tripolycyanamide with And the mass ratio 2:1.5:1.3 of expanded graphites, described fluorescent material is Ce and YAG fluorescent powder mixture, described fluorescent material Particle diameter≤15 μm, described active mineral matter powder is that germanite, fluorite, tourmaline, gahnite are by weight 2.5:3:3.7:2 Mixture, wherein tourmaline is dravite and the mixture of elbaite 5:3 by weight, the grain of described active mineral matter powder Footpath≤15 μm, described lampshade shell is made by the steps and forms:
S1, the resin by required parts by weight, fire retardant, Graphene, fluorescent material, vapour Ba Yan are good to be consolidated 754 light triggers and gathers Ether amines catalyst is placed in blender, mixes well in the stirring of 75 DEG C of next part high speeds, and mixing time is 15-30 minute, to be mixed all Take out from blender after even, i.e. prepare resin compound, standby；
S2, by Pu, material mountain race 60 weight portion, Bulbus Lycoridis Radiatae stem 10 weight portion, floral leaf 15 weight portion of walking to and for, shaven head grass roots leaf 6 weight Amount part, Firmiana platanifolia (Linn. f.) Marsili bark 5 weight portion, sheep Cortex Jujubae 3.5 weight portion, Flos lupuli (Flos Humuli Lupuli) 3 weight portion, Herba Violae dissectae 2 weight portion, Radix et Rhizoma Dysosmatis 2.5 Weight portion, Fructus Hordei Germinatus 2 weight portion, the Radix Angelicae Dahuricae 1 weight portion, Herba Lysimachiae foenum-graeci 1.5 weight portion and Flos Caryophylli 1.5 weight portion, decontamination, together Being placed in the vacuum still 2.5 hours of-20 DEG C, be placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 35 minutes, Microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 80 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 31MPa, extraction temperature 40 DEG C, carbon dioxide flow is 1100L/h, and dynamic extraction 2.5 hours directly goes out at separating still Mouth triangular flask collects crude oil, then prepared crude oil is placed in 5 DEG C of environment freezing 65 minutes, then the crude oil after freezing is put It is centrifuged 30 minutes in the High speed refrigerated centrifuge that rotating speed is 18000r/min, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3.5 hours, i.e. prepare essential oil of traditional Chinese medicine, standby；
The resin compound that S5, essential oil of traditional Chinese medicine step S4 prepared and step S1 prepare, at 75 DEG C, concentrates in blender Stirring mixing 35 minutes, obtains compound, then this compound is put into ball mill, adds active mineral matter powder, modified aromatic Amine hardener and glass fibre, carry out concentrating at 85 DEG C and grind 3 hours, filter decontamination, i.e. prepare premix material；
S6, the premix material of step S5 is put into twin-screw extrusion equipment, wherein, the rotating speed of twin-screw extrusion equipment is 200 turns/ Point, extrusion temperature is 200 ° of C, extrusion, cooling, and pelletizing i.e. obtains composite；
S7, the composite that step S6 is prepared through injection machine heating, extruding, molding, cool down, repair, obtain lampshade 1.
The test index of Example 1 and Example 2 of the present invention is as follows:
(1) abnormal smells from the patient inspection: sense organ, nonirritant abnormal flavour.
(2) repelling effect test.
Contrast test is carried out according to the repelling effect of ordinary lamp and lantern of the prior art with above-described embodiment 1 and embodiment 2, Test data ask for an interview table 1.
Conclusion: Example 1 and Example 2 of the present invention all can play preferable mosquito-repelling function, with ordinary lamp and lantern on market
Comparing, the present invention has obviously repelling effect.
(3) anionic textiles.
Use anion test instrument, be primarily directed to timber, Ore, ceramic material, negative ion powder are made to relevant The anion quantity that commodity (such as anion medicated clothing, necklace, woollen blanket) etc. are discharged makes measurement, and test result is shown in Table 2.
Conclusion: the embodiment of the present invention 1, embodiment 2 can be with sustained release negative aeroions, with ordinary lamps of the prior art Tool compares, and the present invention has obviously advantage.
(4) except aldehyde is except benzene Indexs measure, test result is shown in Table 3.
Conclusion: the embodiment of the present invention 1, embodiment 2 have certain except aldehyde is except benzene function, with ordinary lamps of the prior art Tool compares, and the present invention has obviously advantage.

Claims (2)

1. one kind multi-functional except aldehyde except phenyl ring protect LED candle lamp, it is characterised in that: include lampshade (1), LED illumination assembly (2), Heat carrier (3), radiator (4), electric power driving module and base (5), described electric power driving module device is in described base (5) In, described heat carrier (3) is made by aluminum is one-body molded with radiator (4), and described LED illumination assembly (2) is by heat radiation Coating is mounted on heat carrier (3), and described radiator (4) rear end is hollow cavity (42), described radiator (4) and base (5) connected by screw thread (50), wherein, be provided with some louvres (40), described radiator in the leading section of described radiator (4) (4) sidewall is provided with some radiating grooves (41), and described radiating groove (41) runs through the sidewall of radiator (4), at described radiator (4) the inner wall surface even spread of hollow cavity (42) has heat radiation coating, described heat radiation coating by following component according to weight Number is prepared from: hybrid resin 60-75 weight portion, Graphene 5-6.5 weight portion, sodium-based montmorillonite 3-4.5 weight portion, carboxyl Styrene-butadiene latex 4-6.5 weight portion, silicones metlyl branching silicone oil 1.5-2 weight portion, Polyethylene Glycol 0.7-1.2 weight portion, positive penta Alkane 0.7-1.8 weight portion, nano silicon 1-2.5 weight portion, polyacrylonitrile-based carbon fibre 7-9 weight portion, gas phase titanium dioxide Silicon 1-2 weight portion, fire retardant 5.5-7 weight portion, curing agent 4-6 weight portion, solvent 15-20 weight portion, dioxy Change cerium 0.1-0.15 weight portion, active mineral matter powder 1.5-2 weight portion, essential oil of traditional Chinese medicine 1.5-2.5 weight portion；Wherein, described mixed Resin be the mass ratio of the mixture of phenolic resin and epoxy resin, phenolic resin and epoxy resin be 2:1-3:1；Described poly- The a length of 0.01mm of acrylonitrile base carbon fiber；Described fire retardant is the mixing of APP, tripolycyanamide and expanded graphites Thing, the mass ratio 2:1.5:1.3 of described APP, tripolycyanamide and expanded graphites；Described solvent is DAA With the mixture of butyl ester, the mass ratio of described DAA and butyl ester is 3:1-3:2；Described active mineral matter powder be germanite, Fluorite, tourmaline, gahnite are by weight the mixture of 2.5:3:3.5:1.7, and wherein tourmaline is dravite and lithium electricity Gas stone is by weight the mixture of 4:3, and particle diameter≤15 μm of described active mineral matter powder, described heat radiation coating is as follows It is prepared from:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender Go out, i.e. prepare mixture A, standby；
S2, by material Fructus Xanthii 70-80 weight portion, Folium Symplocoris Caudatae 15-20 weight portion, Pericarpium Zanthoxyli 20-25 weight portion, Folium Viticis Negundo 6-8 weight Part, Herba Hedyotidis Diffusae 3-5 weight portion, beans leaf 8-16 weight portion, Herba Solani Lyrati 25-35 weight portion, Herba Houttuyniae 15-25 weight portion, even Stick up 10-20 weight portion, Radix Salviae Miltiorrhizae 3-4 weight portion, Herba polygoni hydropiperis 3-4 weight portion, Radix Stemonae 5-8 weight portion decontamination, be placed in-20 DEG C together Vacuum still 2-3 hour, be placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 30-40 minute, microwave merit Rate is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Calendula officinalis 3-4 weight portion, Rhizoma Atractylodis 1.5-2 weight portion, Herba Anemones Hupehensis 3-5 weight portion, Herba Menthae 1-3 weight portion, mountain Chicken green pepper 3-5 weight portion, Herba Portulacae 3-4 weight portion, Herba Pogostemonis 3-4 weight portion, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Faeces Leporis 4-8 weight portion, beg Chinese mugwort 3-4 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, then adds deionized water and soaks 5 hours, adds The water yield by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.13-0.2 weight portion and be dried place Reason, i.e. prepares volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 70-80 DEG C, concentrates in blender Stirring mixing 15 minutes, obtains premix material, standby；
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 70-80 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
One the most according to claim 1 is multi-functional protects LED candle lamp except aldehyde except phenyl ring, it is characterised in that: in step S8 In essential oil of traditional Chinese medicine also include the component of following weight portion: surfactant 3-5 weight portion, diethyltoluamide 0.1-0.2 weight portion, fourth Acid butyl ester 9-15 weight portion, Eucalyptus oil 4-7 weight portion, isopropyl myristate 1-2 weight portion, fatty alcohol-polyoxyethylene ether sulphuric acid Sodium 10-15 weight portion and sodium benzoate 0.1-0.3 weight portion.
CN201610583541.0A 2016-05-23 2016-07-24 A kind of multi-functional except aldehyde is except phenyl ring guarantor's LED candle lamp Pending CN106189659A (en)

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Application publication date: 20161207