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CN106085048A - A kind of preparation method of thermal-insulating external-wall coating - Google Patents

A kind of preparation method of thermal-insulating external-wall coating Download PDF

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Publication number
CN106085048A
CN106085048A CN201610422109.3A CN201610422109A CN106085048A CN 106085048 A CN106085048 A CN 106085048A CN 201610422109 A CN201610422109 A CN 201610422109A CN 106085048 A CN106085048 A CN 106085048A
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Prior art keywords
parts
preparation
thermal
slurry
wall coating
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Pending
Application number
CN201610422109.3A
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Chinese (zh)
Inventor
吴彬彬
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ANHUI ZHENXIN PAINT Co Ltd
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ANHUI ZHENXIN PAINT Co Ltd
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Priority to CN201610422109.3A priority Critical patent/CN106085048A/en
Publication of CN106085048A publication Critical patent/CN106085048A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/004—Reflecting paints; Signal paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses the preparation method of a kind of thermal-insulating external-wall coating, raw material includes deionized water, dispersant, wetting agent, defoamer, multifunctional assistant, antimildew disinfectant, ethylene glycol, coalescents, titanium dioxide, infra-red radiation powder, Nano-meter SiO_22Slurry, hollow glass micropearl, elastic emulsion, pure-acrylic emulsion, thickener, levelling agent, composite color paste, propane diols, coloring pigment.The thermal-insulating external-wall coating that the present invention makes has higher solar reflectivity and thermal emissivity rate, not only has reduction exterior wall surface temperature, reduces the effect to indoor conduction, saving air conditioning energy consumption for the heat energy, and meets the color requirements in people's External Wall decoration.

Description

A kind of preparation method of thermal-insulating external-wall coating
Technical field
The present invention relates to coating material production technical field, be specifically related to the preparation method of a kind of thermal-insulating external-wall coating.
Background technology
With the development of coating industry, people in addition to increasingly higher requirement is had to the feature of environmental protection of coating, economy, Other performances to coating, as alkaline-resisting, water-fast, artificial ageing resistance etc. requires more strict.Exterior coating has become decoration of exterior wall Main flow, the raising of people's living standard in recent years, External Wall coating it is also proposed higher requirement, economizes on resources, energy-conservation subtracts Row, ecological, environmental protective, low-carbon circular economy are the basic models of China's economic development, develop solar heat reflecting and heat insulating coating, reduce Building, equipment surface temperature are a kind of methods passively utilizing solar energy, to save the energy, protection environment, create people with from Right harmonious relationships are significant.
Content of the invention
It is an object of the invention to provide the preparation method of a kind of thermal-insulating external-wall coating, the thermal-insulating external-wall coating that the method is made There is higher solar reflectivity and thermal emissivity rate, not only there is reduction exterior wall surface temperature, reduce heat energy to indoor conduction, joint Save the effect of air conditioning energy consumption, and meet the color requirements in people's External Wall decoration.
For achieving the above object, the technical solution used in the present invention is:
The preparation method of a kind of thermal-insulating external-wall coating, comprises the following steps:
S1, choosing raw material, the weight portion of each constitutive material is as follows, deionized water 120-150 part, dispersant 5-7 part, wetting Agent 3-5 part, defoamer 2-3 part, multifunctional assistant 1-2 part, antimildew disinfectant 1-2 part, ethylene glycol 10-15 part, coalescents 5- 10 parts, titanium dioxide 120-150 part, infra-red radiation powder 40-60 part, Nano-meter SiO_22Slurry 60-80 part, hollow glass micropearl 80-120 Part, elastic emulsion 300-400 part, pure-acrylic emulsion 100-200 part, thickener 3-5 part, levelling agent 3-5 part, composite color paste 10-20 Part, propane diols 5-10 part, coloring pigment 30-50 part；
S2, the preparation of mill base, by deionized water 20-30 part, dispersant 2-3 part, wetting agent 1-2 part, defoamer 1 part, increase Thick dose of 1-2 part, propane diols 30-50 part, coloring pigment 30-50 part add in mixer successively, common high speed dispersion, then instead Multiple grinding；
S3, the preparation of insulating moulding coating: add deionized water 100-120 part in dispersion tank, add dispersion under moderate-speed mixer Agent 3-5 part, wetting agent 2-4 part, defoamer 1-2 part, antimildew disinfectant, multifunctional assistant, ethylene glycol, coalescents, titanium dioxide And infra-red radiation powder, become high speed dispersion 30 minutes, polished make slurry；
S4, squeeze into the slurry in S3 in paint mixing tank, under middle stirring at low speed, add Nano-meter SiO_22Slurry and hollow glass Microballon, disperses 20-30 minute, adds elastic emulsion, pure-acrylic emulsion, adds mill base, levelling agent, composite color paste prepared by S1, Finished product barrelling is prepared after filtration.
Further, the weight portion of each constitutive material of described S1 is as follows, deionized water 140 parts, dispersant 6 parts, wetting agent 4 Part, defoamer 3 parts, multifunctional assistant 2 parts, antimildew disinfectant 1 part, ethylene glycol 12 parts, coalescents 8 parts, titanium dioxide 130 parts, 50 parts of infra-red radiation powder, Nano-meter SiO_2270 parts of slurry, hollow glass micropearl 100 parts, elastic emulsion 350 parts, pure-acrylic emulsion 150 Part, thickener 4 parts, levelling agent 4 parts, composite color paste 15 parts, propane diols 8 parts, coloring pigment 40 parts.
Further, described S1 titanium dioxide is rutile titanium white powder.
Further, described S1 elastic emulsion is acrylic emulsion.
Further, described S1 pure-acrylic emulsion is pure-acrylic emulsion AC-261.
Beneficial effects of the present invention: the preparation method of a kind of thermal-insulating external-wall coating, the thermal-insulating external-wall coating that the method is made There is higher solar reflectivity and thermal emissivity rate, not only there is reduction exterior wall surface temperature, reduce heat energy to indoor conduction, joint Save the effect of air conditioning energy consumption, and meet the color requirements in people's External Wall decoration.
Detailed description of the invention
Embodiment 1
The preparation method of a kind of thermal-insulating external-wall coating, comprises the following steps:
S1, choosing raw material, the weight portion of each constitutive material is as follows, deionized water 120 parts, dispersant 5 parts, wetting agent 3 parts, Defoamer 2 parts, multifunctional assistant 1 part, antimildew disinfectant 1 part, ethylene glycol 10 parts, coalescents 5 parts, rutile titanium white powder 120 Part, 40 parts of infra-red radiation powder, Nano-meter SiO_2260 parts of slurry, hollow glass micropearl 80 parts, acrylic elastic emulsion 300 parts, pure third Emulsion (AC-261) 100 parts, thickener 3 parts, levelling agent 3 parts, composite color paste 10 parts, propane diols 5 parts, coloring pigment 30 parts；
S2, the preparation of mill base, by deionized water 20 parts, dispersant 2 parts, wetting agent 1 part, defoamer 1 part, thickener 1 part, Propane diols 30 parts, coloring pigment 30 parts add in mixer successively, and then common high speed dispersion grinds repeatedly；
S3, the preparation of insulating moulding coating: add deionized water 100 parts in dispersion tank, add dispersant 3 under moderate-speed mixer Part, wetting agent 2 parts, defoamer 1 part, antimildew disinfectant, multifunctional assistant, ethylene glycol, coalescents, rutile titanium white powder and red External radiation powder, becomes high speed dispersion 30 minutes, polished makes slurry；
S4, squeeze into the slurry in S3 in paint mixing tank, under middle stirring at low speed, add Nano-meter SiO_22Slurry and hollow glass Microballon, disperses 20-30 minute, adds acrylic elastic emulsion, pure-acrylic emulsion (AC-261), adds mill base, stream prepared by S1 Flat agent, composite color paste, prepare finished product barrelling after filtration.
Embodiment 2
The preparation method of a kind of thermal-insulating external-wall coating, comprises the following steps:
S1, choosing raw material, the weight portion of each constitutive material is as follows, deionized water 150 parts, dispersant 7 parts, wetting agent 5 parts, Defoamer 3 parts, multifunctional assistant 2 parts, antimildew disinfectant 2 parts, ethylene glycol 15 parts, coalescents 10 parts, rutile titanium white powder 150 Part, 60 parts of infra-red radiation powder, Nano-meter SiO_2280 parts of slurry, hollow glass micropearl 120 parts, acrylic elastic emulsion 400 parts, pure third Emulsion (AC-261) 200 parts, thickener 5 parts, levelling agent 5 parts, composite color paste 20 parts, propane diols 10 parts, coloring pigment 50 parts；
S2, the preparation of mill base, by deionized water 30 parts, dispersant 3 parts, wetting agent 2 parts, defoamer 1 part, thickener 2 parts, Propane diols 50 parts, coloring pigment 50 parts add in mixer successively, and then common high speed dispersion grinds repeatedly；
S3, the preparation of insulating moulding coating: add deionized water 120 parts in dispersion tank, add dispersant 4 under moderate-speed mixer Part, wetting agent 3 parts, defoamer 2 parts, antimildew disinfectant, multifunctional assistant, ethylene glycol, coalescents, rutile titanium white powder and red External radiation powder, becomes high speed dispersion 30 minutes, polished makes slurry；
S4, squeeze into the slurry in S3 in paint mixing tank, under middle stirring at low speed, add Nano-meter SiO_22Slurry and hollow glass Microballon, disperses 20-30 minute, adds acrylic elastic emulsion, pure-acrylic emulsion (AC-261), adds mill base, stream prepared by S1 Flat agent, composite color paste, prepare finished product barrelling after filtration.
Embodiment 3
The preparation method of a kind of thermal-insulating external-wall coating, comprises the following steps:
S1, choosing raw material, the weight portion of each constitutive material is as follows, deionized water 140 parts, dispersant 6 parts, wetting agent 4 parts, Defoamer 3 parts, multifunctional assistant 2 parts, antimildew disinfectant 1 part, ethylene glycol 12 parts, coalescents 8 parts, rutile titanium white powder 130 Part, 50 parts of infra-red radiation powder, Nano-meter SiO_2270 parts of slurry, hollow glass micropearl 100 parts, acrylic elastic emulsion 350 parts, pure third Emulsion (AC-261) 150 parts, thickener 4 parts, levelling agent 4 parts, composite color paste 15 parts, propane diols 8 parts, coloring pigment 40 parts.
S2, the preparation of mill base, by deionized water 25 parts, dispersant 2 parts, wetting agent 1 part, defoamer 1 part, thickener 1 part, Propane diols 40 parts, coloring pigment 40 parts add in mixer successively, and then common high speed dispersion grinds repeatedly；
S3, the preparation of insulating moulding coating: add deionized water 115 parts in dispersion tank, add dispersant 4 under moderate-speed mixer Part, wetting agent 3 parts, defoamer 2 parts, antimildew disinfectant, multifunctional assistant, ethylene glycol, coalescents, titanium dioxide and infra-red radiation Powder, becomes high speed dispersion 30 minutes, polished makes slurry；
S4, squeeze into the slurry in S3 in paint mixing tank, under middle stirring at low speed, add Nano-meter SiO_22Slurry and hollow glass Microballon, disperses 20-30 minute, adds elastic emulsion, pure-acrylic emulsion, adds mill base, levelling agent, composite color paste prepared by S1, Finished product barrelling is prepared after filtration.
The preparation method of thermal-insulating external-wall coating of the present invention, the thermal-insulating external-wall coating made have higher solar reflectivity and Thermal emissivity rate, not only has reduction exterior wall surface temperature, reduces the effect to indoor conduction, saving air conditioning energy consumption for the heat energy, and Also the color requirements in people's External Wall decoration is met.
Embodiment described above is only to be described the preferred embodiment of the present invention, the not structure to the present invention Think and scope is defined.On the premise of without departing from design concept of the present invention, the technology to the present invention for this area ordinary person Various modification that scheme is made and improvement, all should drop into protection scope of the present invention.

Claims (5)

1. the preparation method of a thermal-insulating external-wall coating, it is characterised in that comprise the following steps:
S1, choosing raw material, the weight portion of each constitutive material is as follows, deionized water 120-150 part, dispersant 5-7 part, wetting agent 3- 5 parts, defoamer 2-3 part, multifunctional assistant 1-2 part, antimildew disinfectant 1-2 part, ethylene glycol 10-15 part, coalescents 5-10 part, Titanium dioxide 120-150 part, infra-red radiation powder 40-60 part, Nano-meter SiO_22Slurry 60-80 part, hollow glass micropearl 80-120 part, bullet Property emulsion 300-400 part, pure-acrylic emulsion 100-200 part, thickener 3-5 part, levelling agent 3-5 part, composite color paste 10-20 part, third Glycol 5-10 part, coloring pigment 30-50 part；
S2, the preparation of mill base, by deionized water 20-30 part, dispersant 2-3 part, wetting agent 1-2 part, defoamer 1 part, thickener 1-2 part, propane diols 30-50 part, coloring pigment 30-50 part add in mixer successively, and then common high speed dispersion grinds repeatedly Mill；
S3, the preparation of insulating moulding coating: add deionized water 100-120 part in dispersion tank, add dispersant 3-5 under moderate-speed mixer Part, wetting agent 2-4 part, defoamer 1-2 part, antimildew disinfectant, multifunctional assistant, ethylene glycol, coalescents, titanium dioxide and infrared Radiation powder, becomes high speed dispersion 30 minutes, polished makes slurry；
S4, squeeze into the slurry in S3 in paint mixing tank, under middle stirring at low speed, add Nano-meter SiO_22Slurry and hollow glass micropearl, Dispersion 20-30 minute, adds elastic emulsion, pure-acrylic emulsion, adds mill base, levelling agent, composite color paste prepared by S1, after filtration Prepare finished product barrelling.
2. the preparation method of a kind of thermal-insulating external-wall coating as claimed in claim 1, it is characterised in that: each constitutive material of described S1 Weight portion as follows, deionized water 140 parts, dispersant 6 parts, wetting agent 4 parts, defoamer 3 parts, multifunctional assistant 2 parts, mildew-resistant are killed Microbial inoculum 1 part, ethylene glycol 12 parts, coalescents 8 parts, titanium dioxide 130 parts, 50 parts of infra-red radiation powder, Nano-meter SiO_2270 parts of slurry, sky Heart glass microballoon 100 parts, elastic emulsion 350 parts, pure-acrylic emulsion 150 parts, thickener 4 parts, levelling agent 4 parts, composite color paste 15 parts, Propane diols 8 parts, coloring pigment 40 parts.
3. the preparation method of a kind of thermal-insulating external-wall coating as claimed in claim 1, it is characterised in that: described S1 titanium dioxide is gold Red stone titanium dioxide.
4. the preparation method of a kind of thermal-insulating external-wall coating as claimed in claim 1, it is characterised in that: described S1 elastic emulsion is Acrylic emulsion.
5. the preparation method of a kind of thermal-insulating external-wall coating as claimed in claim 1, it is characterised in that: described S1 pure-acrylic emulsion is Pure-acrylic emulsion AC-261.
CN201610422109.3A 2016-06-08 2016-06-08 A kind of preparation method of thermal-insulating external-wall coating Pending CN106085048A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106833228A (en) * 2017-01-20 2017-06-13 中山市阿里大师新材料有限公司 A kind of multifunctional exterior wall coating
CN106947344A (en) * 2017-02-21 2017-07-14 杭州蓝田涂料有限公司 A kind of reflective heat-insulation paint and preparation method thereof
CN107267011A (en) * 2017-08-01 2017-10-20 合肥择浚电气设备有限公司 A kind of coating with heat insulating reflecting function and preparation method thereof
CN107841218A (en) * 2017-10-18 2018-03-27 广东德工化工有限公司 Heat-insulating coating and preparation method thereof
CN108329780A (en) * 2018-02-08 2018-07-27 合肥市大卓电力有限责任公司 A kind of waterproof and heat-insulating exterior coating and preparation method thereof
CN112210265A (en) * 2020-10-16 2021-01-12 贵州黔鳌信息技术有限公司 Exhaust gas photocatalyst degradation coating for exterior wall of urban building group and manufacturing method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101575472A (en) * 2009-06-04 2009-11-11 无锡市艺博涂料有限公司 Anti-cracking stain-resistant exterior wall latex paint and preparation method thereof
CN105295624A (en) * 2015-12-04 2016-02-03 河北晨阳工贸集团有限公司 Dark-color reflective and heat insulation varnish and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101575472A (en) * 2009-06-04 2009-11-11 无锡市艺博涂料有限公司 Anti-cracking stain-resistant exterior wall latex paint and preparation method thereof
CN105295624A (en) * 2015-12-04 2016-02-03 河北晨阳工贸集团有限公司 Dark-color reflective and heat insulation varnish and preparation method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106833228A (en) * 2017-01-20 2017-06-13 中山市阿里大师新材料有限公司 A kind of multifunctional exterior wall coating
CN106947344A (en) * 2017-02-21 2017-07-14 杭州蓝田涂料有限公司 A kind of reflective heat-insulation paint and preparation method thereof
CN106947344B (en) * 2017-02-21 2019-10-01 杭州蓝田涂料有限公司 A kind of reflective heat-insulation paint and preparation method thereof
CN107267011A (en) * 2017-08-01 2017-10-20 合肥择浚电气设备有限公司 A kind of coating with heat insulating reflecting function and preparation method thereof
CN107841218A (en) * 2017-10-18 2018-03-27 广东德工化工有限公司 Heat-insulating coating and preparation method thereof
CN108329780A (en) * 2018-02-08 2018-07-27 合肥市大卓电力有限责任公司 A kind of waterproof and heat-insulating exterior coating and preparation method thereof
CN112210265A (en) * 2020-10-16 2021-01-12 贵州黔鳌信息技术有限公司 Exhaust gas photocatalyst degradation coating for exterior wall of urban building group and manufacturing method thereof

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