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CN106007440A - Magnesium gelling product modifier and preparation method thereof - Google Patents

Magnesium gelling product modifier and preparation method thereof Download PDF

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Publication number
CN106007440A
CN106007440A CN201610349086.8A CN201610349086A CN106007440A CN 106007440 A CN106007440 A CN 106007440A CN 201610349086 A CN201610349086 A CN 201610349086A CN 106007440 A CN106007440 A CN 106007440A
Authority
CN
China
Prior art keywords
mixing plant
salt
add
parts
modifier
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610349086.8A
Other languages
Chinese (zh)
Inventor
汪映兴
傅江
何辉
李小彪
尹文彪
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hemujia Chengdu New Material Co Ltd
Original Assignee
Hemujia Chengdu New Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hemujia Chengdu New Material Co Ltd filed Critical Hemujia Chengdu New Material Co Ltd
Priority to CN201610349086.8A priority Critical patent/CN106007440A/en
Publication of CN106007440A publication Critical patent/CN106007440A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B40/00Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
    • C04B40/0028Aspects relating to the mixing step of the mortar preparation
    • C04B40/0039Premixtures of ingredients

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Pretreatment Of Seeds And Plants (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention discloses a magnesium gelling product modifier and a preparation method thereof. The magnesium gelling product modifier comprises the following components in parts by weight: 15-25 parts of rubber powder, 10-20 parts of brine, 25-35 parts of clear water and 1-3 parts of titanium dioxide. The brine is a magnesium chloride water solution in which the mass ratio of magnesium chloride to water is (0.8-0.9):1. The invention also discloses a preparation method of the magnesium gelling product modifier. The preparation method comprises the following steps: S1: weighing the raw materials; S2: manufacturing the brine; S3: primary proportioning; S4: adding the clear water; S5: adding the titanium dioxide; and S6: adding the auxiliary materials. The magnesium gelling product modifier can improve the accumulation state of 5.1.8 crystal seeds and block capillary channels in the system, thereby achieving the goal of halogenide resistance. The magnesium gelling product modifier can enhance the moisture absorption resistance, halogenide resistance and scumming resistance of the magnesite product and enhance the strength and service life of the magnesite product.

Description

A kind of magnesial gelatinized goods formula of modifier and preparation method thereof
Technical field
The present invention relates to energy-conserving and environment-protective building materials field, a kind of magnesial gelatinized goods formula of modifier and Its preparation method.
Background technology
When producing magnesite product due to raw material, formula, production technology goes wrong, causes Pedicellus et Pericarpium Trapae The disadvantage damp suction surface halide accumulation of magnesium products, it is moist that goods occur returning halogen rear surface, the globule occurs, has a strong impact on dress Decorations quality and Usage parameter control, reduces product strength, shortens product service life.
Summary of the invention
It is an object of the invention to provide a kind of magnesial gelatinized goods formula of modifier and preparation method thereof, with The problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme: a kind of magnesial gelatinized goods modifying agent Formula, including following composition by weight: rubber powder 15-25 part, salt 10-20 part, clear water 25-35 part, Titanium dioxide 1-3 part;
Wherein, described salt is magnesium chloride brine, and magnesium chloride is 0.8-0.9:1 with the mass ratio of water;
Described rubber powder is phosphate and/or sulfate.
Further, described rubber powder is the mixture of ferrous sulfate and sodium phosphate.
The preparation method of a kind of magnesial gelatinized goods modifying agent, comprises the following steps:
S1: weigh raw material, by the raw material of use in need according to certain ratio, weigh, And deposit standby respectively;
S2: make salt, the raw material of salt is placed individually in mixing plant and is stirred, during stirring Between be 10-16 minute, whipping temp is 20-28 degree Celsius, to be mixed complete after, the halogen that will make Water storage is standby;
S3: preliminary dispensing, the salt and the rubber powder that previous step are made are put into mixing plant and are stirred, and stir The time of mixing is 18-24 minute, until the bottom of mixing plant no longer has bubble to produce;
S4: add clear water, when not having bubble to produce in mixing plant, add in mixing plant and weigh Clear water, and continue stirring 5-10 minute;
S5: add titanium dioxide, add load weighted titania powder in mixing plant, and continue Being stirred, mixing time is 3-15 minute;
S6: complete.
Compared with prior art, the invention has the beneficial effects as follows: the present invention can improve 518 crystal seeds Stacking states, the capillary channel in blocking system, thus reach the purpose of anti-halogen, magnesite system can be improved Product anti-moisture absorption returns the ability of halogen, scum, increases magnesite product intensity and service life.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that institute The embodiment described is only a part of embodiment of the present invention rather than whole embodiments.Based on this Embodiment in bright, those of ordinary skill in the art are obtained under not making creative work premise Every other embodiment, broadly falls into the scope of protection of the invention.
Embodiment one
The present invention provides a kind of technical scheme: a kind of magnesial gelatinized goods formula of modifier, including following heavy Amount component: 10 parts of the salt that mass ratio is 0.8:1 of 15 parts of ferrous sulfate powder, magnesium chloride and water, 25 parts of clear water, titania powder 1 part.
The preparation method of a kind of magnesial gelatinized goods modifying agent, comprises the following steps:
S1: weigh raw material, by the raw material of use in need according to certain ratio, weigh, And deposit standby respectively;
S2: make salt, the raw material of salt is placed individually in mixing plant and is stirred, during stirring Between be 10 minutes, whipping temp is 20-28 degree Celsius, to be mixed complete after, the salt made is deposited Deposit is used;
S3: preliminary dispensing, the salt and the rubber powder that previous step are made are put into mixing plant and are stirred, and stir The time of mixing is 18 minutes, until the bottom of mixing plant no longer has bubble to produce;
S4: add clear water, when not having bubble to produce in mixing plant, add in mixing plant and weigh Clear water, and continue to stir 5 minutes;
S5: add titanium dioxide, add load weighted titania powder in mixing plant, and continue Being stirred, mixing time is 3 minutes;
S6: add adjuvant, add load weighted adjuvant in mixing plant, be stirred, mixing time It is 2 minutes, completes.
Embodiment two
The present invention provides a kind of technical scheme: a kind of magnesial gelatinized goods formula of modifier, including following heavy Amount component: ferrous sulfate and sodium phosphate mixed powder 17 parts, 11.013 parts of salt, 28 parts of clear water, dioxy Change titanium powder 1.5 parts, adjuvant 1.106 parts;
Wherein, described salt is magnesium chloride brine, and magnesium chloride is 0.9:1 with the mass ratio of water.
The preparation method of a kind of magnesial gelatinized goods modifying agent, comprises the following steps:
S1: weigh raw material, by the raw material of use in need according to certain ratio, weigh, And deposit standby respectively;
S2: make salt, the raw material of salt is placed individually in mixing plant and is stirred, during stirring Between be 11 minutes, whipping temp is 13 degrees Celsius, to be mixed complete after, will make salt storage Standby;
S3: preliminary dispensing, the salt and the rubber powder that previous step are made are put into mixing plant and are stirred, and stir The time of mixing is 19 minutes, until the bottom of mixing plant no longer has bubble to produce;
S4: add clear water, when not having bubble to produce in mixing plant, add in mixing plant and weigh Clear water, and continue to stir 6 minutes;
S5: add titanium dioxide, add load weighted titania powder in mixing plant, and continue Being stirred, mixing time is 5 minutes;
S6: add adjuvant, add load weighted adjuvant in mixing plant, be stirred, mixing time It is 3 minutes, completes.
Embodiment three
The present invention provides a kind of technical scheme: a kind of magnesial gelatinized goods formula of modifier, including following heavy Amount component: 18 parts of sodium phosphate powder, 13.017 parts of salt, 29 parts of clear water, titania powder 1.8 parts, Adjuvant 1.408 parts;
Wherein, described salt is magnesium chloride brine, and magnesium chloride is 0.9:1 with the mass ratio of water.
The preparation method of a kind of magnesial gelatinized goods modifying agent, comprises the following steps:
S1: weigh raw material, by the raw material of use in need according to certain ratio, weigh, And deposit standby respectively;
S2: make salt, the raw material of salt is placed individually in mixing plant and is stirred, during stirring Between be 13 minutes, whipping temp is 17 degrees Celsius, to be mixed complete after, will make salt storage Standby;
S3: preliminary dispensing, the salt and the rubber powder that previous step are made are put into mixing plant and are stirred, and stir The time of mixing is 20 minutes, until the bottom of mixing plant no longer has bubble to produce;
S4: add clear water, when not having bubble to produce in mixing plant, add in mixing plant and weigh Clear water, and continue to stir 8 minutes;
S5: add titanium dioxide, add load weighted titania powder in mixing plant, and continue Being stirred, mixing time is 7 minutes;
S6: add adjuvant, add load weighted adjuvant in mixing plant, be stirred, mixing time It is 6 minutes, completes.
Embodiment four
The present invention provides a kind of technical scheme: a kind of magnesial gelatinized goods formula of modifier, including following heavy Amount component: ferrous sulfate and magnesium phosphate mixed powder 24 parts, 18.02 parts of salt, 34 parts of clear water, dioxy Changing titanium valve 2.8 parts, wherein, described salt is magnesium chloride brine, and magnesium chloride is 0.9 with the mass ratio of water: 1。
The preparation method of a kind of magnesial gelatinized goods modifying agent, comprises the following steps:
S1: weigh raw material, by the raw material of use in need according to certain ratio, weigh, And deposit standby respectively;
S2: make salt, the raw material of salt is placed individually in mixing plant and is stirred, during stirring Between be 15 minutes, whipping temp is 25 degrees Celsius, to be mixed complete after, will make salt storage Standby;
S3: preliminary dispensing, the salt and the rubber powder that previous step are made are put into mixing plant and are stirred, and stir The time of mixing is 22 minutes, until the bottom of mixing plant no longer has bubble to produce;
S4: add clear water, when not having bubble to produce in mixing plant, add in mixing plant and weigh Clear water, and continue to stir 8 minutes;
S5: add titanium dioxide, add load weighted titania powder in mixing plant, and continue Being stirred, mixing time is 12 minutes;
S6: add adjuvant, add load weighted adjuvant in mixing plant, be stirred, mixing time It is 6 minutes, completes.
By above-mentioned four groups of embodiments being carried out contrast experiment, often group embodiment all can improve magnesite product resist Damp suction surface halide accumulation, the ability of scum, increase magnesite product intensity and service life, the wherein side of embodiment one Case anti-halogen best results.
Although an embodiment of the present invention has been shown and described, for those of ordinary skill in the art Speech, it is possible to understand that these embodiments can be carried out without departing from the principles and spirit of the present invention Multiple change, revising, replace and modification, the scope of the present invention is limited by claims and equivalent thereof Fixed.

Claims (3)

1. a magnesial gelatinized goods formula of modifier, it is characterised in that include following composition by weight: glue Powder 15-25 part, salt 10-20 part, clear water 25-35 part, titania powder 1-3 part;
Wherein, described salt is magnesium chloride brine, and magnesium chloride is 0.8-0.9:1 with the mass ratio of water;
Described rubber powder is phosphate and/or sulfate.
Magnesial gelatinized goods formula of modifier the most according to claim 1, it is characterised in that described Rubber powder is the mixture of ferrous sulfate and sodium phosphate.
3. a preparation method for the magnesial gelatinized goods modifying agent described in claim 1 or 2, its feature It is, comprises the following steps:
S1: weigh raw material, by the raw material of use in need according to certain ratio, weigh, And deposit standby respectively;
S2: make salt, the raw material of salt is placed individually in mixing plant and is stirred, during stirring Between be 10-16 minute, whipping temp is 20-28 degree Celsius, to be mixed complete after, the halogen that will make Water storage is standby;
S3: preliminary dispensing, the salt and the rubber powder that previous step are made are put into mixing plant and are stirred, and stir The time of mixing is 18-24 minute, until the bottom of mixing plant no longer has bubble to produce;
S4: add clear water, when not having bubble to produce in mixing plant, add in mixing plant and weigh Clear water, and continue stirring 5-10 minute;
S5: add titanium dioxide, add load weighted titania powder in mixing plant, and continue Being stirred, mixing time is 3-15 minute;
S6: complete.
CN201610349086.8A 2016-05-24 2016-05-24 Magnesium gelling product modifier and preparation method thereof Pending CN106007440A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610349086.8A CN106007440A (en) 2016-05-24 2016-05-24 Magnesium gelling product modifier and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106007440A true CN106007440A (en) 2016-10-12

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110540403A (en) * 2018-05-28 2019-12-06 福建同方集成住宅建设有限公司 high-strength bamboo-wood carbon fiber high-magnesium gel structure board and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103553410A (en) * 2013-11-15 2014-02-05 晋江安能建材制造有限公司 Magnesium oxychloride modifying cement and magnesium oxychloride cement
CN103588448A (en) * 2013-09-07 2014-02-19 天津全达科技有限公司 Novel heat-insulation fireproof board

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103588448A (en) * 2013-09-07 2014-02-19 天津全达科技有限公司 Novel heat-insulation fireproof board
CN103553410A (en) * 2013-11-15 2014-02-05 晋江安能建材制造有限公司 Magnesium oxychloride modifying cement and magnesium oxychloride cement

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
李娜等: "氯氧镁水泥耐水性的研究", 《四川水泥》 *
毛敏等: "磷酸镁水泥耐水性能改善的研究", 《非金属矿》 *
汪澜: "《水泥混凝土:组成·性能·应用》", 31 January 2005, 中国建材工业出版社 *
王禹阶: "《无机玻璃钢工艺及应用》", 29 February 2004, 化学工业出版社 *
邓德华等: "可溶性磷酸盐改善氯氧镁水泥耐水性的研究", 《华南建设学院西院学报》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110540403A (en) * 2018-05-28 2019-12-06 福建同方集成住宅建设有限公司 high-strength bamboo-wood carbon fiber high-magnesium gel structure board and preparation method thereof

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CB03 Change of inventor or designer information

Inventor after: Wang Yingxing

Inventor after: Fu Jiang

Inventor after: Yin Wenbiao

Inventor before: Wang Yingxing

Inventor before: Fu Jiang

Inventor before: He Hui

Inventor before: Li Xiaobiao

Inventor before: Yin Wenbiao

CB03 Change of inventor or designer information
RJ01 Rejection of invention patent application after publication

Application publication date: 20161012

RJ01 Rejection of invention patent application after publication