CN105851090A - Book worm-resist agent and preparing method thereof - Google Patents

Abstract

The invention discloses a book worm-resist agent and a preparing method thereof, and relates to the technical field of worm-resist agent preparation. The preparing method includes the following steps that 1, Chinese prickly ash, Chinese goldthread, Chinese honeylocust fruit, Chinaberry seeds, remote lemongrass herbs, China wood oil and preservative are weighed by weight; 2, juice is extracted, wherein the Chinese prickly ash, the Chinese honeylocust fruit and the Chinaberry seeds are smashed, squeezed and extracted to obtain a first stock solution, and the Chinese goldthread and the remote lemongrass herbs are soaked, broken, squeezed, extracted in a reflux mode, then heated at the temperature of 65-75 DEG C, distilled, filtered, concentrated at the pressure of minus 0.15-minus 0.05 MPa and dissolved with water to obtain a second stock solution; the two stock solutions are mixed, the China wood oil and the preservative are added and heated to 80-90 DEG C, and the mixture is stirred, mixed uniformly, cooled, packaged and stored. Compared with the prior art, the book worm-resist agent is safe, effectively, capable of preventing bookworms from damaging books.

Description

Book mothproofing agent and preparation method

Technical field

The present invention relates to insect-proof agent preparing technical field, a kind of compositions for books insect protected and preparation side thereof Method.

Background technology

Bookworm is big to books infringement, and the domestic antitermite agent that the most many consumers use carries out anti-lepismae saccharinae bookworm, anti- Agent of damaging by worms is paracide goods, and paracide is the by-product during chlorobenzene production, makes through distillation and recrystallization, is A kind of chlorination aromatic hydrocarbon compounds, belongs to the virose VOC of tool, is commonly used for insecticide, mothproofing agent and agriculture Medicine, human body short term contact can cause eyes, skin and respiratory tract, prolonged and repeated contact can cause headache, dyspnea, evil The heart, vomit, suffer from diarrhoea, the symptom such as skin allergy, numbness, be excessively used and also can cause pulmonary dysfunction, liver damage etc..As far back as upper Individual the 80s and 90s in century, the zoopery that the U.S., the related research institutes of Japan are done is just it was demonstrated that paracide is to animal Carcinogenic, suspicious carcinogenic to the mankind.

Summary of the invention

The technical problem to be solved is to provide one safely and effectively book mothproofing agent and preparation method.

The present invention solves the technical scheme that technical problem used: a kind of book mothproofing agent, former by following weight portion Material is made: 35 parts～40 parts of Pericarpium Zanthoxyli, Rhizoma Coptidis 15 parts～20 parts, Fructus Gleditsia 10 parts～12 parts, Fructus Toosendan 5 parts～10 parts, Herba Cymbopogonis 10 Part～12 parts, Oleum Verniciae fordii 1 part～3 parts, preservative 1 part～1.5 parts.

In above-mentioned book mothproofing agent and preparation method technical scheme, more specifically technical scheme is it may also is that a kind of books The preparation method of insect-proof agent, book mothproofing agent is made up of the raw material of following weight portion: 35 parts～40 parts of Pericarpium Zanthoxyli, Rhizoma Coptidis 15 parts～20 Part, Fructus Gleditsia 10 parts～12 parts, Fructus Toosendan 5 parts～10 parts, Herba Cymbopogonis 10 parts～12 parts, Oleum Verniciae fordii 1 part～3 parts, preservative 1 part～ 1.5 part；

Comprise the following steps:

A, weigh following raw material by weight: Pericarpium Zanthoxyli, Rhizoma Coptidis, Fructus Gleditsia, Fructus Toosendan, Herba Cymbopogonis, Oleum Verniciae fordii and preservative；

B, extraction juice: respectively Pericarpium Zanthoxyli, Fructus Gleditsia and Fructus Toosendan are pulverized squeezing extraction and obtains the first stock solution, by the bits of pulverizing again Ethanol heated and stirred with 75% is extracted, and heating-up temperature is 85 DEG C～90 DEG C, extracts 3 times continuously, continues 1 hour～2 little every time Time；

By Rhizoma Coptidis and Herba Cymbopogonis respectively through soaking, broken, squeezing, reflux, extract, then 65 DEG C～75 DEG C heating, distillation, Filter, after pressure is-0.15MPa～-0.05MPa concentrates, then obtain the second stock solution with water dissolution；

C, by the mixing of two kinds of stock solutions, add Oleum Verniciae fordii and preservative be heated to 80 DEG C～90 DEG C, be uniformly mixed, cooling, packaging Store.

Herba Cymbopogonis, for grass Herba Cymbopogonis. herb, acrid in the mouth, micro-hardship, warm in nature.Then the Herba Cymbopogonis placed in book. Herba Cymbopogonis has the gas of delicate fragrant, accompanies delicate fragrance when the books of Herba Cymbopogonis are opened and attacks people, so claiming " having literary or intellectual fame ".

Pericarpium Zanthoxyli, warming spleen and stomach for dispelling cold, dehumidifying, pain relieving, parasite killing, solve fish raw meat poison.Be possible not only to for oral administration can be with external application to resist mosquito Insect stings and skin disease.

Rhizoma Coptidis, Rhizoma Coptidis petiole base expands embraces stem, lobule and petiole base mulberry in sheath shape.Rhizoma Coptidis itself main Composition is berberine, can heat clearing and damp drying, eliminating fire and detoxication, damp-heat in middle-JIAO, heart channel excess-heat etc. can be removed.

Fructus Gleditsia, containing abundant gleditsin in Fructus Gleditsia sarcocarp, with its preparation agricultural chemical insecticide etc..Saponin is stingless to skin Swashing, harmless, its pure natural detergent product market potential is huge.

Fructus Toosendan, regulate the flow of vital energy, pain relieving, clearing away damp-heat, anthelmintic.

Owing to have employed technique scheme, the present invention compared with prior art has the advantages that and uses these books Insect-proof agent periodically carries out sprinkling and can carry out parasite killing, prevent books from being encroached on by bookworm bookshelf；This book mothproofing agent is nontoxic, environmental protection.

Detailed description of the invention

Below in conjunction with example, the invention will be further described:

Embodiment 1:

A kind of book mothproofing agent, is made up of the raw material of following weight portion: 35 parts of Pericarpium Zanthoxyli, Rhizoma Coptidis 15 parts, Fructus Gleditsia 10 parts, Fructus Toosendan 5 Part, Herba Cymbopogonis 10 parts, Oleum Verniciae fordii 1 part, preservative 1 part.

Embodiment 2:

A kind of book mothproofing agent, is made up of the raw material of following weight portion: 40 parts of Pericarpium Zanthoxyli, Rhizoma Coptidis 20 parts, Fructus Gleditsia 12 parts, Fructus Toosendan 10 Part, Herba Cymbopogonis 12 parts, Oleum Verniciae fordii 3 parts, preservative 1.5 parts.

Embodiment 3:

The preparation method of a kind of book mothproofing agent, book mothproofing agent is made up of the raw material of following weight portion: 35 parts of Pericarpium Zanthoxyli, Rhizoma Coptidis 15 Part, Fructus Gleditsia 10 parts, Fructus Toosendan 5 parts, Herba Cymbopogonis 10 parts, Oleum Verniciae fordii 1 part, preservative 1 part；

Comprise the following steps:

A, weigh following raw material by weight: Pericarpium Zanthoxyli, Rhizoma Coptidis, Fructus Gleditsia, Fructus Toosendan, Herba Cymbopogonis, Oleum Verniciae fordii and preservative；

B, extraction juice: respectively Pericarpium Zanthoxyli, Fructus Gleditsia and Fructus Toosendan are pulverized squeezing extraction and obtains the first stock solution, by the bits of pulverizing again Ethanol heated and stirred with 75% is extracted, and heating-up temperature is 85 DEG C～90 DEG C, extracts 3 times continuously, continues 1 hour every time；

By Rhizoma Coptidis and Herba Cymbopogonis respectively through soaking, broken, squeezing, reflux, extract, then 65 DEG C～75 DEG C heating, distillation, Filter, after pressure is-0.15MPa～-0.05MPa concentrates, then obtain the second stock solution with water dissolution；

C, by the mixing of two kinds of stock solutions, add Oleum Verniciae fordii and preservative be heated to 80 DEG C～90 DEG C, be uniformly mixed, cooling, packaging Store.

Embodiment 4:

The preparation method of a kind of book mothproofing agent, book mothproofing agent is made up of the raw material of following weight portion: 40 parts of Pericarpium Zanthoxyli, Rhizoma Coptidis 20 Part, Fructus Gleditsia 12 parts, Fructus Toosendan 10 parts, Herba Cymbopogonis 12 parts, Oleum Verniciae fordii 3 parts, preservative 1.5 parts；

Comprise the following steps:

A, weigh following raw material by weight: Pericarpium Zanthoxyli, Rhizoma Coptidis, Fructus Gleditsia, Fructus Toosendan, Herba Cymbopogonis, Oleum Verniciae fordii and preservative；

B, extraction juice: respectively Pericarpium Zanthoxyli, Fructus Gleditsia and Fructus Toosendan are pulverized squeezing extraction and obtains the first stock solution, by the bits of pulverizing again Ethanol heated and stirred with 75% is extracted, and heating-up temperature is 85 DEG C～90 DEG C, extracts 3 times continuously, continues 2 hours every time；

By Rhizoma Coptidis and Herba Cymbopogonis respectively through soaking, broken, squeezing, reflux, extract, then 65 DEG C～75 DEG C heating, distillation, Filter, after pressure is-0.15MPa～-0.05MPa concentrates, then obtain the second stock solution with water dissolution；

C, by the mixing of two kinds of stock solutions, add Oleum Verniciae fordii and preservative be heated to 80 DEG C～90 DEG C, be uniformly mixed, cooling, packaging Store.

Claims (2)

1. a book mothproofing agent, it is characterised in that: it is made up of the raw material of following weight portion: 35 parts～40 parts of Pericarpium Zanthoxyli, Rhizoma Coptidis 15 Part～20 parts, Fructus Gleditsia 10 parts～12 parts, Fructus Toosendan 5 parts～10 parts, Herba Cymbopogonis 10 parts～12 parts, Oleum Verniciae fordii 1 part～3 parts, preservative 1 part～1.5 parts.

2. the preparation method of a book mothproofing agent, it is characterised in that: book mothproofing agent is made up of the raw material of following weight portion: flower Green pepper 35 parts～40 parts, Rhizoma Coptidis 15 parts～20 parts, Fructus Gleditsia 10 parts～12 parts, Fructus Toosendan 5 parts～10 parts, Herba Cymbopogonis 10 parts～12 parts, Oleum Verniciae fordii 1 part～3 parts, preservative 1 part～1.5 parts；

Comprise the following steps:

A, weigh following raw material by weight: Pericarpium Zanthoxyli, Rhizoma Coptidis, Fructus Gleditsia, Fructus Toosendan, Herba Cymbopogonis, Oleum Verniciae fordii and preservative；

B, extraction juice: respectively Pericarpium Zanthoxyli, Fructus Gleditsia and Fructus Toosendan are pulverized squeezing extraction and obtains the first stock solution, by the bits of pulverizing again Ethanol heated and stirred with 75% is extracted, and heating-up temperature is 85 DEG C～90 DEG C, extracts 3 times continuously, continues 1 hour～2 little every time Time；

By Rhizoma Coptidis and Herba Cymbopogonis respectively through soaking, broken, squeezing, reflux, extract, then 65 DEG C～75 DEG C heating, distillation, Filter, after pressure is-0.15MPa～-0.05MPa concentrates, then obtain the second stock solution with water dissolution；

C, by the mixing of two kinds of stock solutions, add Oleum Verniciae fordii and preservative be heated to 80 DEG C～90 DEG C, be uniformly mixed, cooling, packaging Store.