CN105560086A - Pure natural multiple-effect nourishing sunscreen cream containing peony seed oil and preparation method thereof - Google Patents
Pure natural multiple-effect nourishing sunscreen cream containing peony seed oil and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a pure natural multiple-effect nourishing sunscreen cream containing peony seed oil and a preparation method thereof. The pure natural multiple-effect nourishing sunscreen cream consists of peony seed oil, high-quality olive emulsified wax, cananga odorata hydrolat, deionized water, trehalose, a 1% macromolecular sodium hyaluronate solution, a 1% lower-molecular sodium hyaluronate solution, an aloe vera gel stock solution, a red pomegranate extract, a Silasoma MEA ultraviolet absorbing inclusion, a particulate titanium dioxide dispersion liquid, pentanediol, 1,3-butanediol, a magnolia bark extract and an antibacterial agent. The pure natural multiple-effect nourishing sunscreen cream can be effectively resistant to ultraviolet radiation damage to the facial skin, prevent the facial skin from being tanned and sunburned, meanwhile nourish the facial skin and infiltrate into facial skin cells while moisturizing the facial skin, is very easily absorbed and utilized by the skin cells, can comprehensively provide various types of nutrition required by the facial skin and can further quickly repair damaged cells, restore the activity of the facial skin cells, decrease wrinkles, restore skin elasticity and white and make the face reappear youthful luster.
Description
Technical field
The invention belongs to daily cosmetics preparing technical field, relate to the compositions that a kind of uvioresistant, the aging of anti-skin oxidative and check melanin are formed, particularly relate to a kind of pure natural multiple-effect containing peony seed oil and nourish sunscreen cream and preparation method thereof.
Background technology
The sun bring to the earth bright and warm while, also create a large amount of ultraviolet, according to the length of wavelength, ultraviolet can be divided into ultraviolet light,long wave (UVA, 320 ~ 400nm), UV-B (UVB, 280 ~ 320nm) and ultraviolet C (UVC, 200 ~ 280nm) three kinds, it is aging that UVA dominates sunlight, and UVB causes the chief-criminal arch-criminal of skin sunburn, UVC then makes people highly carcinogenic, but fortunately, UVC is absorbed by atmosphere.Ultraviolet (UV) A and UVB can penetrate skin corium, by skin sunburn, tanned and produce decortication etc. shine after phenomenon, thus cause skin in advance old and feeble, serve irremediable injury to skin tape, if the long-term impact by UVA and UVB, also likely cause skin carcinoma.
Sunlight is continuous print electromagnetic radiation as waves, along with the high speed development of modern city, appearance of city is maked rapid progress, high buildings and large mansions, curtain wall stand in great numbers, vehicle streams past in an endless flow, the metope of these cladding glass, skyscraper, automotive glazing and surface road all can uv reflectances, thus increase the amount of ultraviolet irradiation of earth surface, therefore sun-proofly just seem particularly important.Correlational study shows, the ultraviolet radiation rate on rainy day is the 21%-54% of fine day, and cloudy ultraviolet irradiation rate is the 81%-95% of fine day, and this explanation throughout the year all should be sun-proof.
Economic fast development, bring people's living standard to improve constantly, the luxury goods that skin care item have maintained from a kind of skin protection become necessary.Face is people outward manifestation the most intuitively, and face skin is comparatively fragile, the most also be the position being the most directly subject to ultraviolet injury, in order to prevent skin by tanned and sunburn, the sunscreen cream product that with the addition of sun-prevention component arises at the historic moment, simultaneously along with people are to the in-depth of ultraviolet radiation harm understanding, sun-proof consciousness and repair maintenance consciousness after shining and constantly strengthen, sun care preparations occupies critical role especially as a kind of caused by cosmetics for special use.Sunscreen product sun care preparations functional component commercially available is at present rich and varied, physical property ultraviolet light screener can be divided into (also to claim inorganic sunscreen from mechanism of action, this kind of material can reflect on skin, scatters ultraviolet) and chemical UV absorbent (also known as Orangic sunscreen, this kind of material can selective absorbing ultraviolet thus play anti-sunlight function, if para-amino benzoic acid and the compound such as derivant, cinnamic acid thereof or natural materials are as plant extracts such as Aloes, also have some bioactive substance and antioxidant reductases etc.).Physical sunscreen frost is thick and heavy, and there is burden in summer to skin, easy fuel-displaced blocking pore, but is not easy to cause skin sensitivity; Chemical sunscreen frost is frivolous, and dermal respiration is smooth and easy, and quality oiliness easily absorbs, but sensitive skin can not adapt to.Meanwhile, some manufacturer, in order to increase white-skinned face function, does not stint and adds heavy metal and the fluorescent whitening agent such as plumbous hydrargyrum, bring injury to skin.And commercially available sunscreen cream function is relatively single, only focuses on sun-proof function, seldom there is the sunscreen cream repairing double effects after having sun-proof and solarization concurrently commercially to sell, therefore there is certain gaps in market.And it should be noted that, certain relation that influences each other may be there is in existing sun-prevention component and rear the reparation between composition of solarization, namely when both make an addition in identical product jointly, certain negative function may be had, sun-proof function is caused to weaken, make the system of sunscreen cream become unstable simultaneously, be difficult to uniform application on skin.
Summary of the invention
In order to overcome the shortcomings and deficiencies of prior art, the object of the present invention is to provide a kind of physical sunscreen and chemical sunscreen being combined effectively can resist the ultraviolet of each wave band, integrate sun-proof, the compositions of sun-proof moisturizing anti aging effect that moisturizing, moisturizing, whitening, antioxidation, prevention pigmentation etc. are repaired after shining, especially provide a kind of pure natural multiple-effect containing peony seed oil to nourish sunscreen cream and preparation method thereof.
In order to realize object of the present invention, inventor is studied by lot of experiments, finally obtains the technical scheme that the following pure natural multiple-effect containing peony seed oil nourishes sunscreen cream:
A kind of all natural ingredients compositions of sun-proof moisturizing anti aging effect, it is by peony seed oil, excellent olive emulsifing wax, fragrant cananga hydrosol, MEIGUI CHUNLU, deionized water, trehalose, polymer hyaluronic acid sodium 1% solution, low-numerator sodium hyaluronate 1% solution, Aloe gel stock solution, red Punica granatum L. extract, SilasomaMEA ultra-violet absorption inclusion enclave, fine particulate titanium dioxide dispersion liquid, lycopene, pentanediol, 1, and 3 butanediols, Magnolia bark extract, antibacterial form.
Preferably, all natural ingredients compositions of above-mentioned sun-proof moisturizing anti aging effect, what wherein said component was counted by weight consists of:
Further preferably, all natural ingredients compositions of above-mentioned sun-proof moisturizing anti aging effect, what wherein said component was counted by weight consists of:
Again further preferably, all natural ingredients compositions of sun-proof moisturizing anti aging effect described above, it is sunscreen cream, and described Magnolia bark extract is the Magnolia bark extract 98 that German cosphatec produces.
In addition, the preparation method of all natural ingredients compositions sunscreen cream of above-mentioned sun-proof moisturizing anti aging effect provided by the present invention, it comprises following steps:
(1) take the Magnolia bark extract of recipe quantity, red Punica granatum L. extract, use 1 respectively, 3 butanediols dissolve, for subsequent use;
(2) get A, B totally 2 beakers, in A beaker, add the peony seed oil of recipe quantity, excellent olive emulsifing wax;
(3) in B beaker, add the fragrant cananga hydrosol of recipe quantity, MEIGUI CHUNLU, deionized water, trehalose and lycopene, be stirred to and dissolve completely;
(4) A beaker and B beaker are heated in a water bath, heat while stirring, until decorating film dissolves, after temperature reaches 75 DEG C, stop heating, pour the solution in B beaker in A beaker rapid stirring according to a small amount of mode repeatedly even;
Etc. (5) when the temperature of mixed liquor drops to 40 DEG C, add polymer hyaluronic acid sodium 1% solution of recipe quantity, low-numerator sodium hyaluronate 1% solution, Aloe gel stock solution, red Punica granatum L. extract solution, SilasomaMEA ultraviolet inclusion enclave, fine particulate titanium dioxide dispersion liquid, pentanediol, Magnolia bark extract solution according to this, after often adding a kind of component, stir 1-3 minute;
(6) finally add the antibacterial of recipe quantity, both stir can.
Preferably, the preparation method of all natural ingredients compositions sunscreen cream of sun-proof moisturizing anti aging effect described above, red Punica granatum L. extract wherein obtains as follows: using Punica granatum L. corium farinosum as raw material, be that the butanediol solution of 50%-66% is as Extraction solvent with volume fraction, adjust pH=3.0, the ultrasonic lixiviate of room temperature after feed liquid mixing, extraction time is 0.5-3h, filter, filter vacuum concentrates and get final product.
It should be noted that, the preparation method of all natural ingredients compositions sunscreen cream of sun-proof moisturizing anti aging effect described above, excellent olive emulsifing wax is wherein the excellent olive liquid crystal Fructus Canarii albi emulsifing wax of the celestial graceful production of France, English name OLDERMCRYSTALMOIST, INCI is sorbitol olive oil acid esters, the hard ester group glucoside of spermaceti; Described fragrant cananga hydrosol is commercially available Madagascar's fragrant cananga hydrosol, and Cananga odorata quintessence oil content is 0.025%; Described MEIGUI CHUNLU is the commercially available organic MEIGUI CHUNLU of Bulgaria, and Flos Rosae Rugosae quintessence oil content is 0.05%; Described polymer hyaluronic acid sodium 1% solution (product code HA-TL) and low-numerator sodium hyaluronate 1% solution (product code HA-TLLM) Jun Shi Bloomage Freda Biopharm Co., Ltd. product; Described Aloe gel stock solution is the good jade Lu Dema Aloe gel stock solution of global healthy group of the U.S., purity > 99%; Described SilasomaMEA ultra-violet absorption inclusion enclave is bag micropartical capsule (Nippon Kasei Chemical Company's production) in commercially available organic uv absorbers; Described fine particulate titanium dioxide dispersion liquid is the micropartical titanium dioxide aqueous dispersions of 60% of Nippon Kasei Chemical Company's production; Described Magnolia bark extract is that high-purity (>=98%) the Magnolia bark extract 98, INCI that German cosphatec produces is called MagnoliaOfficinalisBarkExtract Magnolia bark extract.
Find according to antioxygenic property experimental study, the non-oxidizability simultaneously containing the sample 1 of peony seed oil and red Punica granatum L. extract is significantly higher than only adds the sample 2 that red Punica granatum L. extract does not add peony seed oil, and be significantly higher than and only add peony seed oil and do not add the sample 3 of red Punica granatum L. extract, this illustrate by peony seed oil and red Punica granatum L. extract according to a certain percentage conbined usage there is collaborative effect of removing skin histology excessive free radicals in skin care item.Therefore, present invention also offers the new opplication of two kinds of specific components couplings, that is: peony seed oil and red Punica granatum L. extract are preparing the application in the skin care item removing excessive free radicals in skin histology; Or peony seed oil and red Punica granatum L. extract are preparing the application in skin non-oxidizability skin care item.Preferred further, described skin care item are sunscreen cream.
Compared with prior art, all natural ingredients compositions (pure natural multiple-effect nourishes sunscreen cream) of sun-proof moisturizing anti aging effect of the present invention has technique effect useful as follows:
(1) have sun-proof, antioxidation, scavenging free radicals, desalination mottle, whitening, anti-inflammation and maintenance face skin moisten lastingly and wait multi-efficiency, not only effectively can keep out the injury of ultraviolet to face skin, prevention face skin is tanned and tan severely, face skin can be nourished simultaneously, facial skin cell is permeated while replenishing water and preserving moisture, very easily absorbed by Skin Cell, and the various nutrition required for face skin can be provided all sidedly, more can repair damaged cell rapidly, recover skin of face cytoactive, reduce wrinkle, recover elasticity of skin and pale, face is allowed to reappear brilliance at an early age.
(2) though summer face skin by tanned or sunburn state under, as long as apply the pure natural multiple-effect nourishing sunscreen cream that one deck contains peony seed oil gently, and massaged gently, just intimately can merge with the skin that is hurt, rapid permeability is repaired skin and can be formed protecting film in skin surface, while absorption and shielding of ultraviolet, moisture is allowed to stay veritably on skin, nutrition is allowed really to be absorbed by the skin, away from irradiating because of sunlight and contact wind, the coarse blackening that the reasons such as the stimulation that dirt and color make-up remain occur and the puzzlement that lost its bounce causes to skin, face skin is made to recover elastic force, pale and delicate.
(3) effective ingredient retains by compositions to greatest extent, its major function is sun-proof and repairs after shining, can absorb and keep out ultraviolet, supplement the nutrient required for face skin, repair damaged cell, effectively suppress facial melanin is formationed, scavenging free radicals, replenishing water and preserving moisture, the delicacy and pale of compacting, accurately act on face skin cell, can effectively active cell metabolism, nourish skin, desalination mottle, effect is lasting and stablize.
(4) can one deck uvioresistant protecting film be formed on face skin surface and fully can penetrate into skin depths imparting skin nutrition and vigor; With the addition of and there are the ultraviolet peony seed oil of high resistance, Aloe gel stock solution and fine particulate titanium dioxide dispersant etc.; With the addition of heigh antioxidation and alimentary red Punica granatum L. extract and water solublity lycopene strong anti-oxidation elite HYDROPOM; With the addition of simultaneously and there is height moistness, humidity-preserving type and infiltrative trehalose, low-numerator sodium hyaluronate 1% solution and polymer hyaluronic acid sodium 1% solution; Also added the MEIGUI CHUNLU and fragrant cananga hydrosol that have and nourish skin, activating cell and natural lock water effect.
(5), after smearing face skin a period of time, skin recovers elastic force and gloss.Because which are added Natural Antioxidants peony seed oil, American Red Punica granatum L. extract, Radix Ginseng extract and water solublity lycopene strong anti-oxidation elite HYDROPOM, can effective scavenging free radicals, thus prevention cell senescence, slow down aging, and extremely strong with the affinity of skin, can play face skin and nourish effect for a long time.
(6) compositions uses pure natural antibacterial composition, the skin that minimizing interpolation synthetic antiseptic brings stimulates and allergic symptom, the pentanediol added is the natural moisture preserving agent of excellent performance and has anti-corrosion function, the Magnolia bark extract added has antibacterial and anti-oxidation efficacy preferably, the bright peptide antibacterial added is the filtrate of Carrot Roots tunning, having very strong sterilization sterilization functions, is all natural anticorrosion composition, non-stimulated to skin.
(7) compositions sunscreen cream is multiple natural, green, secure group point science is composite to be formed, the sunscreen cream prepared has good sun protection, effectively can resist the ultraviolet of each wave band, there is repair function after good solarization simultaneously, antioxidation, skin care moisturizing, Whitening, spot, the feature of nontoxic grade, pure natural multiple-effect containing peony seed oil is nourished sunscreen cream and both can be used for the injury of pre-anti-ultraviolet to skin, can repair and nourish again skin after shining, comprise facial scaly dry skin, pigmentation, skin tanning, wrinkle intensification and colonization when following the string, also can be used as the anti-aging product preventing face skin aging, the development trend of sunlight screening skin-protecting product will be become, there is wide market application foreground and economic worth.
Detailed description of the invention
Be below specific embodiments of the invention, technical scheme of the present invention is done to describing further, but protection scope of the present invention be not limited to these embodiments.Every do not deviate from the present invention's design change or equivalent substituting include within protection scope of the present invention.
It should be noted that, in following examples, excellent olive emulsifing wax is by the celestial graceful production of France, and English name OLDERMCRYSTALMOIST, INCI are sorbitol olive oil acid esters, the hard ester group glucoside of spermaceti; Fragrant cananga hydrosol is commercially available Madagascar's fragrant cananga hydrosol, and Cananga odorata quintessence oil content is 0.025%; MEIGUI CHUNLU is the commercially available organic MEIGUI CHUNLU of Bulgaria, and Flos Rosae Rugosae quintessence oil content is 0.05%; Trehalose is former trehalose trehalose, the purity > 98% of Japanese woods that Qingdao Abel Science and Technology Ltd. sells; Polymer hyaluronic acid sodium 1% solution (HA-TL) and low-numerator sodium hyaluronate 1% solution (HA-TLLM) are Bloomage Freda Biopharm Co., Ltd.'s products; Aloe gel stock solution is training technology--the dew fresh Aloe gel juice of the spy that SATT Aloe process technology produces adopting Global group of U.S. AGHG, and brand is good jade Lu Dema, purity > 99%; SilasomaMEA ultra-violet absorption inclusion enclave be Nippon Kasei Chemical Company produce organic uv absorbers in bag micropartical capsule; Fine particulate titanium dioxide dispersion liquid is the micropartical titanium dioxide aqueous dispersions of 60% of Nippon Kasei Chemical Company's production; Lycopene is commercially available water solublity lycopene strong anti-oxidation elite HYDROPOM, is produced by Italian Phenbiox; Magnolia bark extract is natural organic Magnolia bark extract of German cosphatec high-purity (>=98%), and INCI is called MagnoliaOfficinalisBarkExtract Magnolia bark extract; Antibacterial is the bright string coccus & Radix Raphani root tunning filtrate that U.S. ActiveMotif produces, and production code member is M15008.
The preparation of embodiment 1-3 sunscreen cream
Formula is in table 1:
The formula of table 1 sunblock compositions
Above-mentioned formulated technique is as follows:
(1) preparation of red Punica granatum L. extract
Get Mengzi Yunnan fresh pomegranate → cleaning → 45 DEG C constant temperature drying → pulverizing → accurately take 10g powder → add 200ml volume fraction be 60% butanediol solution (solid-liquid ratio 1:20, pH=3.0) → supersound extraction 40min (extracting 3 times) → filtering vacuum concentrated → red Punica granatum L. extract finished product.
(2) solution preparation
A, Magnolia bark extract solution are prepared
Accurate title Magnolia bark extract 1g, with 1,3 butanediols dissolve, and the butanediol solution being mixed with 1:20 is for subsequent use.
B, red Punica granatum L. extract solution preparation
Accurately take red Punica granatum L. extract 1g, with 1,3 butanediols dissolve, and the butanediol solution being mixed with 1:9 is for subsequent use.
(3) deionized water processing procedure:
1. impurities in water is filtered;
2. high pressure passes through reverse osmosis membrane;
3. ultraviolet-sterilization;
4. ion exchange process maximum resistance rate 18,000,000 is carried out.
(4) beaker getting A, B2 only clean is stand-by, adds the peony seed oil of recipe quantity, excellent olive in A beaker
tMliquid crystal moisturizer agent;
(5) in B beaker, add the fragrant cananga hydrosol of recipe quantity, MEIGUI CHUNLU, deionized water, trehalose and water solublity lycopene strong anti-oxidation elite HYDROPOM, be stirred to and dissolve completely;
(6) beaker A and beaker B is placed on constant temperature water proof heating on electromagnetic oven, heat while stirring, until decorating film dissolves, temperature is lifted down beaker A, B after reaching 75 DEG C immediately, the water preparation in B beaker is poured in beaker A rapid stirring even, approximate time about 20 minutes according to a small amount of method repeatedly;
(7) after stirring, when temperature in mixture drops to 40 DEG C, add polymer hyaluronic acid sodium 1% solution of recipe quantity, low-numerator sodium hyaluronate 1% solution, good jade Lu Dema Aloe gel stock solution, American Red Punica granatum L. extract, Radix Ginseng extract, SilasomaMEA ultraviolet inclusion enclave, 60% micropartical titanium oxide dispersion, pentanediol, Magnolia bark extract according to this, additive often adds a kind of needs stirring 2 minutes;
(8) finally add the antibacterial of recipe quantity, both stir can;
(9) preserve under the sunscreen cream sealing room temperature that Packs sterilized installs, 12 months effect duration.
The pure natural multiple-effect containing peony seed oil utilizing above-mentioned composition and engineering to prepare is nourished sunscreen cream and is had following effect:
(1) injury that the ultraviolet effectively resisting each wave band causes skin, has excellent sun-proof performance;
(2) nourish skin comprehensively, repair damaged cell, effective scavenging free radicals, recover skin of face cytoactive, keeps the colour of skin pale lastingly, allow face reappear delicate water profit at an early age, rear skin ageing is shone in antagonism, has repairing effect after good solarization;
(3) form protecting film in skin surface while rapid permeability face skin, the injury that effective shielding of ultraviolet and wind, dirt and color make-up cause skin, make face skin recovery elastic force, compact He Shuirun;
(4) effectively suppress the activity of Skin Cell tryrosinase, stop that melanin is formed, prevention pigementation;
(5) effectively activated cell is active, promotes cellular metabolism regeneration, reduces wrinkle, delaying skin aging.
Embodiment 4 peony seed oil content is on the impact of the sun-proof performance of sunblock compositions
Test arranges 5 samples, the same embodiment of compound method of sample 1-5, wherein peony seed oil content is followed successively by 1 part, 4 parts, 7 parts, 10 parts and 13 parts, other constituent contents are with embodiment 1, so sample 4 is identical with embodiment 1, mainly measures the sun protection of product under 280nm, 290nm, 300nm, 310nm, 320nm and 330nm6 wavelength.Assuming that be the biomaterial such as horny layer, epidermis with piezoid, at the sun-proof sample of coated thereon, ultraviolet spectrophotometer is used to measure their absorbance (light transmittance) value.According to the size of absorbance (light transmittance), evaluate the sun-proof performance of product.Assay method is as follows:
(1) at piezoid even application one deck product on the surface;
(2) then with adhesive tape outside tied up and put into wherein;
(3) on ultraviolet spectrophotometer, survey its light absorption value on each wavelength.Not add the sample of peony seed oil as blank.
According to Lambert-Beer law, measure absorbance for index with ultraviolet spectroscopy, initial reaction sun-proof result.For avoiding random error when adopting single absorbance to be index, ask for UVA, UVB wave band mean light absorbency
give smoothing processing.Sun-proof result evaluation reference Diffey tests the normal data of gained erythema occurrence frequency and wavelength relationship, wavelength has stronger erythemal effect at the UV of 290-330nm, therefore select 280,290,300,310,320 (UVB) and 330 (UVA) nm5 wavelength, measure absorbance, according to the size of absorbance, evaluate the sun-proof performance of product.Absorbance is larger, and sun-proof result is better, and result of the test is in table 2.
The computing formula of absorbance is:
A(UVB)＝(A280+A290+A300+A310+A320)/5
A(UVA)＝A330
The sun protection result of the test of sample is in table 2.
The sun protection development test result of table 2 sample
As can be seen from the test statistics result of table 2, in the scope that wavelength is 280nm-330nm, each sample absorbance difference is remarkable, and is obviously greater than UVA to the absorbance of UVB; Along with the increase of peony seed oil content in sample, absorbance increases gradually, when in sample, peony seed oil content reaches 10, the absorbance of sample 4 (embodiment 1) all shows as maximum at each wave band, and remarkable to ultraviolet absorbance difference with other samples, but when peony seed oil content is 13, sample absorbance shows as reduction, may be because peony seed oil content more than 10 after sunscreen cream thinning, sun protectionly no longer to increase.As can be seen from experimental result, sample 4 i.e. embodiment 1, no matter be all show stronger ultraviolet-absorbing to UVB or UVA.Therefore no matter be ultraviolet B radiation or long wave ultraviolet, sunscreen cream of the present invention can play good resists ultraviolet function, is desirable sunlight screening skin-protecting product.
Embodiment 5 performance of keeping humidity is tested
Embodiment 1-3, glycerol, hyaluronic acid are respectively got 6 parts and is divided into 2 groups, each sample is contained on the surface plate that diameter is 4cm respectively, weighs.First group of sample being dared to hydroscopicity under high humidity measures, and namely putting into relative humidity (RH) under the room temperature (25 DEG C) filling silica gel is accurately weigh after the exsiccator of the saturated ammonium sulfate aqueous solution of 81% processes 24h.Under equally second group of sample being used for low-moisture conditions, hydroscopicity measures, and accurately weighs after namely putting into the vacuum desiccator dried 24h that relative humidity (RH) is 43%, vacuum is-0.1MPa.Of poor quality by sample before and after moisture absorption, obtain hydroscopicity according to following formula:
Hydroscopicity=(Mn-M
0)/M
0× 100% formula (1)
In formula (1): M
0for quality before sample moisture absorption, Mn is quality after moisture absorption 24h.Continue to place 24h after the moisture absorbed reaches capacity, accurately take each sample mass, of poor quality by before and after sample, obtain moisturizing rate according to following formula:
Moisturizing rate=H
n/ H
0× 100% formula (2)
In formula (2): H
nfor sample is containing water quality, H
0for sample after placement 24h is containing water quality
Sample moisture-absorbing moisture-keeping type result of the test is in table 3.
Table 3 sample moisture absorbability and moisture retentivity result of the test
As can be seen from the test statistics result of table 3, the hydroscopicity of each sample and moisturizing rate significant difference under high humidity, glycerol and hyaluronic acid show stronger hygroscopicity, and the hygroscopicity of embodiment 1-3 is not given prominence to, but moistening effect is apparently higher than glycerol and hyaluronic acid; Descend hydroscopicity and the moisturizing rate significant difference of each sample under low humidity conditions, embodiment 1-3 moisture absorption, moisture retention are all had outstanding performance, especially embodiment 1 shows superior hygroscopicity and moisture retention, be better than glycerol and hyaluronic acid, especially there is good hygroscopicity, and moisture-absorbing moisture-keeping effect stability.Therefore repair replenishing water and preserving moisture for after solarization, embodiment sunscreen cream can play good moistening effect.
Embodiment 6 antioxygenic property is tested
Test arranges 3 samples, sample 1 is embodiment 1 sunscreen cream, sample 2 is replace peony seed oil (other components are with embodiment 1), sample 3 for replacing American Red Punica granatum L. extract (other components are with embodiment 1) with deionized water with glycerol, and the ethanol compound concentration with 95% is 0.04mg/mlDPPH solution.Pipette 1ml sample solution and 3mlDPPH solution respectively in tool plug test tube, fully after mixing, after lucifuge leaves standstill 30min under room temperature, under 517nm, measure absorbance A
1.Sample solution is replaced to make blank determination absorbance A with 1ml ethanol
0, the absorbance A of DPPH measured in solution sample solution is replaced with 3ml ethanol
2.Calculate the clearance rate (experimental result is in table 4) of DPPH free radical according to the following formula:
Clearance rate=(1-(the A of DPPH free radical
1-A
2)/A
0) × 100%
Table 4 each sample is to the clearance rate of DPPH free radical
DPPH is a kind of free radical of very stable nitrogen center, and its stability, mainly from Resonance Stabilization action and the spatial obstacle of 3 phenyl ring, makes azygous electronics on the nitrogen-atoms that is clipped in the middle can not play its due electronics and acts in pairs.The alcoholic solution of DPPH is darkviolet, because DPPH free radical has strong absorption at place centered by 517nm, when there being free radical scavenger to exist, lone pair electrons in DPPH on nitrogen are paired and solution colour are shoaled, become colorless or light yellow, absorbance is diminished, and therefore absorbance is less, clearance rate is larger, shows that the oxidation resistance of scavenger is stronger.Utilize this characteristic can detect the clearance rate of scavenger to DPPH intuitively.As can be seen from the result of the test of table 4, the clearance rate significant difference to DPPH free radical of 3 sample solutions, the clearance rate of sample 1 is maximum reaches 87.67%, showing stronger oxidation resistance, is secondly sample 2, and clearance rate is 45.06%, the clearance rate of sample 3 is the most weak, is 38.63%.From the component of 3 samples, sample 1 is containing peony seed oil and red Punica granatum L. extract, sample 2 is not containing peony seed oil, all the other components are with sample 1, sample 3 is not containing red Punica granatum L. extract, all the other components are with sample 1, be not difficult to find out to the clearance rate of DPPH free radical, the non-oxidizability of the sample 1 simultaneously containing peony seed oil and red Punica granatum L. extract is significantly higher than only adds red Punica granatum L. extract and does not add the sample 2 of peony seed oil and only add the sample 3 that peony seed oil does not add red Punica granatum L. extract, this illustrate by peony seed oil and red Punica granatum L. extract according to a certain percentage conbined usage there is collaborative effect of removing skin histology excessive free radicals in skin care item.This experiment simultaneously shows, the sunscreen cream of embodiment has comparatively strong anti-oxidation, can effectively delay face skin aging, is more satisfactory nourishing sunscreen cream.
Embodiment 7 sense organ physical and chemical index measures
Require to carry out the sunscreen cream that conventional index detects embodiment 1 preparation according to China's skin lotion frost industry QB/T1857-2013 standard index (see table 5), the results are shown in Table 6.From result in table 6, the sunscreen cream indices prepared by the present invention all meets relevant industries standard.
Table 5 sense organ, physical and chemical standards index
Table 6 embodiment sense organ, physical and chemical index measurement result
Claims (10)
1. all natural ingredients compositions of a sun-proof moisturizing anti aging effect, it is by peony seed oil, excellent olive emulsifing wax, fragrant cananga hydrosol, MEIGUI CHUNLU, deionized water, trehalose, polymer hyaluronic acid sodium 1% solution, low-numerator sodium hyaluronate 1% solution, Aloe gel stock solution, red Punica granatum L. extract, SilasomaMEA ultra-violet absorption inclusion enclave, fine particulate titanium dioxide dispersion liquid, lycopene, pentanediol, 1, and 3 butanediols, Magnolia bark extract and antibacterial form.
2. all natural ingredients compositions of sun-proof moisturizing anti aging effect according to claim 1, it is characterized in that, what described each component was counted by weight consists of:
3. all natural ingredients compositions of sun-proof moisturizing anti aging effect according to claim 2, it is characterized in that, what described each component was counted by weight consists of:
4. all natural ingredients compositions of sun-proof moisturizing anti aging effect according to claim 1 or 2 or 3, is characterized in that, described Magnolia bark extract is the Magnolia bark extract 98 that German cosphatec produces.
5. all natural ingredients compositions of sun-proof moisturizing anti aging effect according to Claims 2 or 3, it is characterized in that, described compositions is sunscreen cream.
6. a preparation method for all natural ingredients compositions sunscreen cream of sun-proof moisturizing anti aging effect according to claim 5, it is characterized in that, the method comprises following steps:
(1) take the Magnolia bark extract of recipe quantity, red Punica granatum L. extract, use 1 respectively, 3 butanediols dissolve, for subsequent use;
(2) get A, B totally 2 beakers, in A beaker, add the peony seed oil of recipe quantity, excellent olive emulsifing wax;
(3) in B beaker, add the fragrant cananga hydrosol of recipe quantity, MEIGUI CHUNLU, deionized water, trehalose and lycopene, be stirred to and dissolve completely;
(4) A beaker and B beaker are heated in a water bath, heat while stirring, until decorating film dissolves, after temperature reaches 75 DEG C, stop heating, pour the solution in B beaker in A beaker rapid stirring according to a small amount of mode repeatedly even;
Etc. (5) when the temperature of mixed liquor drops to 40 DEG C, add polymer hyaluronic acid sodium 1% solution of recipe quantity, low-numerator sodium hyaluronate 1% solution, Aloe gel stock solution, red Punica granatum L. extract solution, SilasomaMEA ultraviolet inclusion enclave, fine particulate titanium dioxide dispersion liquid, pentanediol, Magnolia bark extract solution according to this, after often adding a kind of component, stir 1-3 minute;
(6) finally add the antibacterial of recipe quantity, both stir can.
7. the preparation method of all natural ingredients compositions sunscreen cream of sun-proof moisturizing anti aging effect according to claim 6, it is characterized in that, described red Punica granatum L. extract obtains as follows: using Punica granatum L. corium farinosum as raw material, be that the butanediol solution of 50%-66% is as Extraction solvent with volume fraction, adjust pH=3.0, the ultrasonic lixiviate of room temperature after feed liquid mixing, extraction time is 0.5-3h, filter, filter vacuum concentrates and get final product.
8. peony seed oil and red Punica granatum L. extract are preparing the application in the skin care item removing excessive free radicals in skin histology.
9. peony seed oil and red Punica granatum L. extract are preparing the application in skin non-oxidizability skin care item.
10. will go the application described in 8 or 9 according to right, it is characterized in that, described skin care item are sunscreen cream.
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| WO2021116616A1 (en) * | 2019-12-12 | 2021-06-17 | L V M H Recherche | Cosmetic composition comprising extracts of pomegranate and peony |
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| WO2021116616A1 (en) * | 2019-12-12 | 2021-06-17 | L V M H Recherche | Cosmetic composition comprising extracts of pomegranate and peony |
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