CN105456041A - Toothpaste containing particles and transparent viscous substance - Google Patents
Toothpaste containing particles and transparent viscous substance Download PDFInfo
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- CN105456041A CN105456041A CN201510916544.7A CN201510916544A CN105456041A CN 105456041 A CN105456041 A CN 105456041A CN 201510916544 A CN201510916544 A CN 201510916544A CN 105456041 A CN105456041 A CN 105456041A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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Abstract
The invention discloses toothpaste containing particles and a transparent viscous substance. The particles suspend in the transparent viscous substance; the particles include an abrasive, a moisturizer, a foaming agent, a thickening agent, a functional component, an appearance conditioning agent, a flavoring agent, a stabilizing agent, a preservative, spices and de-ionized water, wherein in the particles, the thickening agent accounts for 1.0-10.0% in terms of the mass of the de-ionized water and the de-ionized water accounts for 13.0-59.0% in terms of the total mass of the particles; the transparent viscous substance consists of a moisturizer, a thickening agent, a stabilizing agent, a preservative, a functional component and de-ionized water, wherein in the transparent viscous substance, the thickening agent accounts for 0.1-1.7% in terms of the mass of the de-ionized water and the de-ionized water accounts for 47.0-99.4% in terms of the total mass of the transparent viscous substance; and the appearance conditioning agent is a non-water-soluble appearance conditioning agent. With the existence of the transparent viscous substance, the particles suspend uniformly and cannot settle or dissolve out. The particles, in the transparent viscous substance, are good in stability, and are free from phenomena of dissolution, breakage and precipitation.
Description
Technical field
The invention belongs to household chemicals technical field, be specifically related to a kind of toothpaste comprising particulate matter and clear viscous object.
Background technology
Since entering 21 century, along with the continuous change of people's living habit, taste, consumer is also more and more higher to the requirement of requisite dental care products in this life of toothpaste, to a certain extent, only cleaning of teeth was focused on from the past, gradually to the mouthfeel future development pursuing toothpaste, then develop to all-direction multi-functional.People use toothpaste to be not only fundamental need for meeting oral health, and brushing teeth rises, and the enjoyment become in a kind of psychological factor is experienced, more and more stronger to the individual requirement of toothpaste.In lifting consumer in the acceptance of product and frequency of utilization, good product aesthetic effect has played very important effect.
But toothpaste character mostly in the market is the transparent or colored toothpaste of real color, the improvement of outward appearance is also add the materials such as some particles, tablet or Muscovitum in toothpaste content, effect that these particles, tablet, shimmering powder carry is more single, commonly particle wraps up some extract or fresheners etc., more just as a kind of raw material of aesthetic appeal.
In addition the packaging of toothpaste is commonly single tubular package now, needs uncap during use, with hands squeezing toothpaste on toothbrush, and then cover lid, taken amount cannot be constant, and ease of use is very limited.Meanwhile, existing toothpaste is due to problems such as the restriction of its formula compatibility, mouthfeel restrictions, and achieved toothpaste mouthfeel is relatively single.
Summary of the invention
The object of the invention is to the shortcoming overcoming prior art, provide a kind of toothpaste comprising particulate matter and clear viscous object, clear viscous object can make particulate matter even suspension, and not sedimentation not stripping; Particulate matter is good stability in clear viscous object, not dissolving, broken and precipitation phenomenon.
For achieving the above object, present invention employs following technical proposals:
A kind of toothpaste comprising particulate matter and clear viscous object, particulate matter is suspended in clear viscous object, described particulate matter comprises abrasive, wetting agent, foaming agent, thickening agent, functional component, outward appearance regulator, flavour enhancer, stabilizing agent, antiseptic, spice and deionized water, in particulate matter, thickening agent accounts for the 1.0%-10.0% of ionized water quality, deionized water accounts for the 13.0%-59.0% of particulate matter gross mass, clear viscous object comprises wetting agent, thickening agent, stabilizing agent, antiseptic, functional component and deionized water, thickening agent in clear viscous object accounts for the 0.1%-1.7% of described deionized water quality, deionized water accounts for the 47.0-99.4% of clear viscous object gross mass, described outward appearance regulator is water-insoluble outward appearance regulator.
Preferably, the volume ratio of described particulate matter cumulative volume and clear viscous object cumulative volume is 1:(0.5-5), the average external volume of particulate matter is 4 × 10
-9cubic meter is to 5 × 10
-7cubic meter.
Preferably, the shape of particulate matter is one or more in irregular spheroid, regular spheroid, irregular polyhedrons, regular polyhedron.
Especially preferred, the shape of particulate matter is one or more in spheroid, spheroid, cube and cone.
Preferably, described water-insoluble outward appearance regulator is selected from one or more in Muscovitum, water-insoluble pigment, water-insoluble mill base.
Further preferred, described water-insoluble pigment is selected from titanium dioxide, oil-soluble is blue, oil-soluble is yellow, oil-soluble red in one or more.
Preferred further, described water-insoluble mill base is selected from one or more in red shallow lake, yellow lake, blue shallow lake, green lake.
Preferably, count by weight, described particulate matter component is as follows:
Preferably, count by weight, described clear viscous compositions of matter is as follows:
Further preferred, the described functional component in described particulate matter be selected from sodium phytate, pyrophosphate, Margarita powder, hydroxyapatite, zinc citrate, western arsenic oronain, magnolol extract, fluoride, xylitol, erythritol, potassium nitrate, strontium chloride, hydroxyapatite, paeonol, tranamic acid, 0-p-Cymene-5-alcohol, Rhizoma Euonymus Ilex extract, Flos Lonicerae extract one or more; Described abrasive is selected from one or more in natural whiting, silicon dioxide, dihydrogen phosphate dihydrate calcium, aluminium hydroxide, precipitated calcium carbonate, calcium phosphate dibasic anhydrous, anhydrous calcium pyrophosphate or calcium hydroxy phosphate; Described wetting agent is selected from one or more in sorbitol, glycerol, propylene glycol, Polyethylene Glycol, ethanol; Described foaming agent is selected from one or more in the materials such as sodium lauryl sulfate, sodium lauroyl sarcosine, betanin, alkyl polyglucoside; Described flavour enhancer is selected from one or more in saccharin sodium, sucralose, stevioside, aspartame, acesulfame potassium, Sal; Described stabilizing agent be selected from pyrophosphate, sodium hydroxide, citrate, dibastic sodium phosphate salt one or more; Described antiseptic is selected from one or more in oxybenzene formicester, propyl hydroxybenzoate, benzoic acid, sodium benzoate, sorbic acid, potassium sorbate; Described spice is selected from one or more in the essence such as mint aroma, Herba Menthae Rotundifoliae type, fragrance of a flower odor type, fruital odor type; Described thickening agent is selected from one or more in gellan gum, sodium alginate, agar, xanthan gum, carrageenan, carbomer.
Preferred further, the described wetting agent in described clear viscous object is selected from one or more in sorbitol, glycerol, propylene glycol, Polyethylene Glycol, ethanol; Described functional component be selected from cetylpyridinium chloride, 0-p-Cymene-5-alcohol, magnolol extract, Folium Artemisiae Argyi extract, grapefruit extract one or more; Described antiseptic is selected from one or more in oxybenzene formicester, propyl hydroxybenzoate, benzoic acid, sodium benzoate, sorbic acid, potassium sorbate; Described thickening agent is selected from one or more in gellan gum, carbomer, carrageenan, xanthan gum, sodium carboxymethyl cellulose; Described stabilizing agent is selected from one or more in the materials such as pyrophosphate, sodium hydroxide, citrate, dibastic sodium phosphate salt, calcium chloride.
Also comprise pigment in described clear viscous object, described pigment accounts for the 0.01%-0.1% of dope weight.Described pigment is preferably water colo(u)r.
Present invention also offers the preparation method of described toothpaste, be first prepare particulate matter and clear viscous object respectively, then blending tank dresses up the toothpaste of clear viscous suspended particulate substance.Described particulate matter is preferably spheroidal particle thing.Described clear viscous object is preferably transparent gel.
Preferably, adopt one-step method to prepare spheroidal particle thing, specifically comprise the steps: functional component, flavour enhancer, stabilizing agent, antiseptic to be added in deionized water, be stirred to and dissolve completely, make aqueous phase solution.In aqueous phase solution, add wetting agent, stirring and dissolving makes liquid solution.Mix homogeneously after abrasive, thickening agent, foaming agent being weighed, adds in the middle of liquid solution, rapid stirring homogenizing 20-60 minute.Load weighted outward appearance regulator and essence are added wherein, stirs, after degassed process completes, give over to the spherical mastic of preparation and use.In closed environment, the toothpaste prepared is carried out heating 60-90 DEG C to mobility liquid, after heating, best viscosity controls in 1000-2000cP scope, in its mobility liquid, drip the silicone oil of (-10)-10 DEG C, pure water or liquid calcium chloride, obtain the spherical toothpaste of uniform diameter 1-10mm with solid drop pill machine.
Preferably, adopt and prepare clear viscous object with the following method, specifically comprise the steps: first weighing part water from formula total Water, under agitation thickening agent is slowly joined in deionized water, stir 30-60 minute, make hydrated gums solution, stand-by.Stabilizing agent, functional component, antiseptic are added in part water, stirs, until make aqueous phase solution, then add wetting agent stirring, make liquid solution, stand-by.The hydrated gums solution made and liquid solution are mixed, stirs after 30-60 minute, after degassed process, be prepared into limpid transparent gel.
Preferably, the method for preparation containing spheroidal particle thing and clear viscous object toothpaste, by the spheroidal particle thing prepared and the mixing of clear viscous object degassed after together be filled in transparent pump line.
The outward appearance of a kind of Novel beautiful of toothpaste not only given by toothpaste provided by the invention, more can realize the many mouth feeling experience to oral cavity and the realization of many effects, meet the user demand of modern to diversification effect of toothpaste.Simultaneously by the novel packaging material of pump type, be not only improving product ease of use, promote user's aesthetic experience by the profile of products innovation and packaging especially, allow consumer brush teeth safeguard oral health from the love of reducing phlegm and internal heat of aspect at heart.
By this dentifrice composition fill in transparent pump type packaging material, not only can present excellent apparent visual effect, pump type gets cream, and to use health convenient, and particulate matter and clear viscous object can be the combinations of different mouthfeel formula, bring the mouth feeling experience of consumer's uniqueness.
Compared with prior art, the present invention has following beneficial effect:
1, include in the present invention in the toothpaste of particulate matter and clear viscous object, particulate matter is good stability in clear viscous object, does not dissolve and separates out phenomenon.Clear viscous object of the present invention adopts aqueous solution systems, the particulate matter adopting non-water-soluble outward appearance regulator to prepare is water-insoluble, the 1.0%-10.0% of ionized water quality and the thickening agent adopted when preparing particulate matter accounts for, deionized water accounts for the 13.0%-59.0% of compositions gross mass, and the thickening agent of employing can make particulate matter not dissolve and separate out phenomenon in clear viscous object with the combined effect of outward appearance regulator.
Meanwhile, well, particulate matter can not produce stripping in clear viscous object, fracture phenomena for particulate matter and clear viscous object compatibility.
2, clear viscous object of the present invention by adopting gellan gum and/or carbomer and/or carrageenan and/or xanthan gum and/or sodium carboxymethyl cellulose, especially gellan gum and carbomer is used, the 0.1%-1.7% of its ionized water quality that accounts for, and deionized water accounts for the 47.0-99.4% of compositions total raw material quality, control the suspending power of clear viscous object, make particulate matter energy even suspension and not sedimentation not stripping.
3, toothpaste of the present invention comprises particulate matter and clear viscous object, and it can each tool different efficacies and different mouthfeel.During use, extrude particulate matter and clear viscous object and be mixed, realizing the collaborative and mouthfeel superposition of effect.
4, include in the present invention in the toothpaste of particulate matter and clear viscous object, particulate matter can have different CFs, can realize toothpaste color or various shapes, reaches effect attractive in appearance.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated, but the scope of protection of present invention is not limited to the scope that embodiment is expressed.
Formula and the clear viscous object formula of spheroidal particle thing refer to following table 1.
The formula of table 1 spheroidal particle thing and clear viscous object formula
The formula of table 2 spheroidal particle thing and clear viscous object formula
The formula of table 3 spheroidal particle thing and clear viscous object formula
Prepare spheroidal particle thing: prepare raw material by each embodiment and comparative example formula in table 1-3, adopt one-step method preparation respectively, specifically comprise the steps:
(1) be added in deionized water by crystalline sodium pyrophosphate, sodium phytate, saccharin sodium, cetylpyridinium chloride, sodium benzoate, wherein, embodiment 5 also needs to add sodium phytate, is stirred to and dissolves completely, make aqueous phase solution.In aqueous phase solution, add sorbitol, Polyethylene Glycol, stirring and dissolving makes liquid solution.
(2) mix homogeneously after hydrated silica, carrageenan, xanthan gum, sodium lauryl sulfate being weighed, adds in the middle of liquid solution, rapid stirring homogenizing 20 minutes.
(3) load weighted oil-soluble is blue and essence adds wherein, stirs 15 minutes, after degassed process completes, gives over to the spherical mastic of preparation and uses.In closed environment, the toothpaste prepared is carried out heating 60 DEG C to mobility liquid, after heating, viscosity controls at 1000cP, drips the silicone oil of-8 DEG C, obtain the spheroidal particle of uniform diameter 3mm with solid drop pill machine in its mobility liquid.
Prepare clear viscous object: prepare raw material by embodiment each in table 1 and comparative example formula, adopt respectively and prepare with the following method, specifically comprise the steps:
(1) under agitation carbomer is slowly joined in deionized water, stir 30 minutes, make hydrated gums solution, stand-by.
(2) sodium hydroxide, 0-p-Cymene-5-alcohol, grapefruit extract, methyl hydroxybenzoate are added in part water, stir, until make aqueous phase solution, then add sorbitol, glycerol stirring, make liquid solution, stand-by.
(3) the hydrated gums solution made and liquid solution are mixed, stir after 30 minutes, after degassed process, be prepared into transparent gel.
Prepare toothpaste: the spheroidal particle thing prepared and transparent gel are chosen volume by the formula of each embodiment in table 1 and comparative example, mixed degassed after be filled in transparent pump line together, prepare the toothpaste comprising spheroidal particle thing and transparent gel respectively.
Tested respectively under the same conditions by the toothpaste that embodiment 1-5 and comparative example 1-6 prepares, test result is as follows respectively in table 4.
Table 4 measurement result
The above results shows; its particulate matter of toothpaste of toothpaste prepared by embodiment 1 and comparative example 1 preparation is perfectly round; particulate matter in toothpaste prepared by embodiment 1 does not occur dissolving and separating out phenomenon relative to its pigment of comparative example 1 owing to adding the pigment " oil-soluble is blue " being insoluble in water; and good stability; place pigment after 3 months all not occur dissolving and separating out phenomenon at room temperature and 45 DEG C; simultaneously in particulate matter energy stable suspersion and transparent gel; there is not distortion in particulate matter, can play well clean and protective effect to tooth.And owing to adding water colo(u)r in particulate matter after the toothpaste preparation of comparative example 1, pigmentolysis and precipitation reach 50%, place dissolving and precipitation after 1 month and reach 90%, and along with extending standing time, deformation effect is obvious.
Comparative example 2 prepare toothpaste in its 95% equal sedimentation of particulate matter, can not Effective Suspension in transparent gel, reason is the out of proportion of deionized water in transparent gel.In addition, in comparative example 2, colloidal content is not in optimum range, and the particulate matter of molding is uneven and not perfectly round, and ratio of briquetting only has 30%.
Toothpaste prepared by embodiment 3 is compared with toothpaste prepared by comparative example 3, because deionized water consumption is very few, the geode toothpaste of preparation is really up to the mark, and the phenomenon of can not squeezing occurs in use.
Toothpaste prepared by embodiment 4 is compared with toothpaste prepared by comparative example 4, only containing spheroidal particle in toothpaste prepared by comparative example 4, does not have transparent gel.Spheroidal particle thing more than 98% energy stable suspersion prepared by embodiment 4 is in transparent gel, and its spheroidal particle thing of toothpaste prepared by reference examples 4 is all deposited in together, when toothpaste prepared by the toothpaste prepare embodiment 4 and comparative example 4 is respectively charged into and uses in the bottle with pump line, by toothpaste don't be extruded by pipe during owing to using at every turn, residue in embodiment 4 untapped spheroidal particle thing is all excellent, broken speed is 0, and the pressure that airstrip is come when extruding owing to not having transparent gel to cushion of the residue untapped spheroidal particle thing in comparative example 4, it is easily broken that remaining spheroidal particle thing is subject to air extrusion, standing time is longer, its percentage of damage is higher.
Toothpaste prepared by embodiment 4 is compared with toothpaste prepared by comparative example 5, because the volume ratio of transparent gel consumption and spheroidal particle is 0.2:1, use with comparative example 4 pairs of toothpaste, the pressure that when residue in comparative example 5 untapped spheroidal particle thing is extruded owing to not having enough transparent gels to cushion, airstrip is come, it is easily broken that exposed spheroidal particle thing is subject to air extrusion, standing time is longer, and its percentage of damage is higher.。
Toothpaste prepared by embodiment 5 and toothpaste prepared by comparative example 6 adopt SP62 chromascope to carry out whitening test under the same conditions respectively, Testing index is International Commission on Illumination (CIE) L*a*b standard colorimetric system is colour system the most frequently used in dentistry, L* represents visual sense lightness, its numerical value is 0 to 100, the large person of lightness is close to white, and little color is close to black.The change of front and back tooth L* value of being brushed teeth by record, can reflect that the effect of exogenous mottle removed by toothpaste.Test result is as follows in table 5.
Table 5 whitening test data
Table 5 test result shows, the relative standard deviation RSD<30% of the △ L* of this experiment test, shows that the experimental result of this whitening method of testing has good elaboration.Meanwhile, the △ L-value of matched group toothpaste and experimental group toothpaste is respectively 2.69 ± 2.18 and 2.69 ± 2.18, and both have significant difference, shows that the whitening effect of the toothpaste that embodiment 5 is prepared relative to matched group 6 is better.
Toothpaste prepared by the toothpaste prepare embodiment 6 and comparative example 7 carries out fungistatic effect test under the same conditions respectively, and test result is as follows respectively in table 6.
The antibacterial analysis testing result of table 6
The above results shows, toothpaste prepared by embodiment 6 makes the activity of functional component higher because add transparent gel, reaches more than 99.9% relative to the bacteriostasis rate of the toothpaste of comparative example 7 preparation.
The announcement of book and instruction according to the above description, those skilled in the art in the invention can also change above-mentioned embodiment and revise.Therefore, the present invention is not limited to detailed description of the invention disclosed and described above, also should fall in the protection domain of claim of the present invention modifications and changes more of the present invention.In addition, although employ some specific terms in this description, these terms just for convenience of description, do not form any restriction to the present invention.
Claims (10)
1. one kind comprises the toothpaste of particulate matter and clear viscous object, it is characterized in that, particulate matter is suspended in clear viscous object, described particulate matter comprises abrasive, wetting agent, foaming agent, thickening agent, functional component, outward appearance regulator, flavour enhancer, stabilizing agent, antiseptic, spice and deionized water, in particulate matter, thickening agent accounts for the 1.0%-10.0% of ionized water quality, deionized water accounts for the 13.0%-59.0% of particulate matter gross mass, clear viscous object comprises wetting agent, thickening agent, stabilizing agent, antiseptic, functional component and deionized water, thickening agent in clear viscous object accounts for the 0.1%-1.7% of described deionized water quality, deionized water accounts for the 47.0-99.4% of clear viscous object gross mass, described outward appearance regulator is water-insoluble outward appearance regulator.
2. toothpaste as claimed in claim 1, it is characterized in that, the volume ratio of described particulate matter cumulative volume and clear viscous object cumulative volume is 1:(0.5-5), the average external volume of particulate matter is 4 × 10
-9cubic meter is to 5 × 10
-7cubic meter, the shape of particulate matter is one or more in irregular spheroid, regular spheroid, irregular polyhedrons, regular polyhedron.
3. toothpaste as claimed in claim 1 or 2, it is characterized in that, described water-insoluble outward appearance regulator is selected from one or more in Muscovitum, water-insoluble pigment, water-insoluble mill base, and the shape of particulate matter is one or more in spheroid, spheroid, cube and cone.
4. toothpaste as claimed in claim 3, is characterized in that, described water-insoluble pigment is selected from titanium dioxide, oil-soluble is blue, oil-soluble is yellow, oil-soluble red in one or more.
5. toothpaste as claimed in claim 3, is characterized in that, described water-insoluble mill base is selected from one or more in red shallow lake, yellow lake, blue shallow lake, green lake.
6. the toothpaste as described in any one of claim 1-5, is characterized in that, counts by weight, and described particulate matter component is as follows:
7. the toothpaste as described in any one of claim 1-5, is characterized in that, counts by weight, and described clear viscous compositions of matter is as follows:
8. toothpaste as claimed in claim 6, is characterized in that: the described functional component in described particulate matter be selected from sodium phytate, pyrophosphate, Margarita powder, hydroxyapatite, zinc citrate, western arsenic oronain, magnolol extract, fluoride, xylitol, erythritol, potassium nitrate, strontium chloride, hydroxyapatite, paeonol, tranamic acid, 0-p-Cymene-5-alcohol, Rhizoma Euonymus Ilex extract, Flos Lonicerae extract one or more; Described abrasive is selected from one or more in natural whiting, silicon dioxide, dihydrogen phosphate dihydrate calcium, aluminium hydroxide, precipitated calcium carbonate, calcium phosphate dibasic anhydrous, anhydrous calcium pyrophosphate or calcium hydroxy phosphate; Described wetting agent is selected from one or more in sorbitol, glycerol, propylene glycol, Polyethylene Glycol, ethanol; Described foaming agent is selected from one or more in the materials such as sodium lauryl sulfate, sodium lauroyl sarcosine, betanin, alkyl polyglucoside; Described flavour enhancer is selected from one or more in saccharin sodium, sucralose, stevioside, aspartame, acesulfame potassium, Sal; Described stabilizing agent be selected from pyrophosphate, sodium hydroxide, citrate, dibastic sodium phosphate salt one or more; Described antiseptic be selected from oxybenzene formicester, propyl hydroxybenzoate, benzoic acid, sodium benzoate, sorbic acid, potassium sorbate one or more; Described spice is selected from one or more in the essence such as mint aroma, Herba Menthae Rotundifoliae type, fragrance of a flower odor type, fruital odor type; Described thickening agent is selected from one or more in gellan gum, sodium alginate, agar, xanthan gum, carrageenan, carbomer.
9. toothpaste as claimed in claim 7, it is characterized in that, the described wetting agent in described clear viscous object is selected from one or more in sorbitol, glycerol, propylene glycol, Polyethylene Glycol, ethanol; Described functional component be selected from cetylpyridinium chloride, 0-p-Cymene-5-alcohol, magnolol extract, Folium Artemisiae Argyi extract, grapefruit extract one or more; Described antiseptic be selected from oxybenzene formicester, propyl hydroxybenzoate, benzoic acid, sodium benzoate, sorbic acid, potassium sorbate, one or more; Described thickening agent is selected from one or more in gellan gum, carbomer, carrageenan, xanthan gum, sodium carboxymethyl cellulose; Described stabilizing agent is selected from one or more in the materials such as pyrophosphate, sodium hydroxide, citrate, dibastic sodium phosphate salt, calcium chloride.
10. toothpaste as claimed in claim 7, it is characterized in that, also comprise pigment in described clear viscous object, described pigment accounts for the 0.01%-0.1% of dope weight.
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| CN112891228A (en) * | 2021-02-02 | 2021-06-04 | 桂林市啄木鸟医疗器械有限公司 | Dental glaze sealing agent and preparation method and application thereof |
| CN114010569A (en) * | 2021-11-11 | 2022-02-08 | 江苏罗来雅实业股份有限公司 | Anhydrous whitening paste and preparation method thereof |
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| CN106890103A (en) * | 2017-03-06 | 2017-06-27 | 广州薇美姿实业有限公司 | A kind of toothpaste suitable for pump type packaging material and preparation method thereof |
| CN106890103B (en) * | 2017-03-06 | 2020-06-16 | 广州薇美姿实业有限公司 | Toothpaste suitable for pump type packing material and preparation method thereof |
| CN107693392B (en) * | 2017-03-07 | 2020-11-06 | 广州薇美姿实业有限公司 | Toothpaste containing enzyme preparation and preparation method thereof |
| CN107693392A (en) * | 2017-03-07 | 2018-02-16 | 广州薇美姿实业有限公司 | A kind of toothpaste of enzyme-containing formulation and preparation method thereof |
| CN107308077A (en) * | 2017-07-04 | 2017-11-03 | 湖南云从科技有限公司 | A kind of formulation of tooth-paste of clean tooth-whitening and preparation method thereof |
| CN107343871A (en) * | 2017-07-22 | 2017-11-14 | 李映波 | A kind of halitosis-removing toothpaste of American-cockroach-extract-containing |
| CN107485584A (en) * | 2017-07-28 | 2017-12-19 | 鹰仕达（中国）有限公司 | A kind of oral care composition |
| CN108553358A (en) * | 2018-05-21 | 2018-09-21 | 浙江泰康生物科技有限公司 | A kind of whitening stains removing toothpaste and preparation method thereof |
| CN111135127A (en) * | 2020-01-19 | 2020-05-12 | 广东立爽生物科技有限公司 | Allergy-relieving and bleeding-stopping toothpaste and preparation method thereof |
| CN112891228A (en) * | 2021-02-02 | 2021-06-04 | 桂林市啄木鸟医疗器械有限公司 | Dental glaze sealing agent and preparation method and application thereof |
| CN114010569A (en) * | 2021-11-11 | 2022-02-08 | 江苏罗来雅实业股份有限公司 | Anhydrous whitening paste and preparation method thereof |
| CN116942579A (en) * | 2023-09-01 | 2023-10-27 | 狮王口腔用品(广州)有限公司 | Gum protecting toothpaste and preparation method thereof |
| CN116942579B (en) * | 2023-09-01 | 2024-01-30 | 狮王口腔用品(广州)有限公司 | Gum protecting toothpaste and preparation method thereof |
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