CN105289024B - A kind of vacuum concentration equipment and method for concentration - Google Patents
A kind of vacuum concentration equipment and method for concentration Download PDFInfo
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- CN105289024B CN105289024B CN201510818132.XA CN201510818132A CN105289024B CN 105289024 B CN105289024 B CN 105289024B CN 201510818132 A CN201510818132 A CN 201510818132A CN 105289024 B CN105289024 B CN 105289024B
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Abstract
The invention discloses a kind of concentrator, more particularly to a kind of vacuum concentration equipment and method for concentration.A kind of vacuum concentration equipment, feed spray system is connected by the first conveying pipeline with film concentration systems, film concentration systems bottom is provided with continuous discharge system, continuous discharge system is connected with film concentration systems, continuous discharge system is connected with feed spray system and finished product discharging opening respectively, continuous discharge system is connected by secondary vacuum-pumping tube with vacuum system, heating and cooling system is provided with outside film concentration systems and the preheater of feed spray system, the second thin film concentrator of film concentration systems is connected by main vacuum-pumping tube with vacuum system.The present invention passes through spraying and two vacuum concentration systems of film, improve thickening efficiency, cocnentration factor, concentration continuous operation, shorten concentration time, avoid injury of the high temperature to material, solvent evaporation amount maximum is up to more than 90%, and the more conventional concentration time can shorten more than 70%, reduce concentrated cost.
Description
Technical field
The present invention relates to a kind of concentrator, more particularly to a kind of vacuum concentration equipment and method for concentration.
Background technology
Concentration is a kind of technological operation for being commonly used in production, in medical and health, food chemistry, environmental protection and organic
Purposes is very wide in many industries such as synthesis.At present, conventional concentrator mainly has the concentration of nature film forming and inside and outside circulation dense
Contracting.But, the concentration of natural film forming and interior circulation concentration have that thickening efficiency is low, cocnentration factor is small, poor for applicability, intermittently operated etc.
Problem；Although the first two that outer circulation concentration concentrated effect compares improves notable, he still has heat time length, concentration effect
The low technical problem of rate.Although having been developed for efficiently rising film, falling liquid film, knifing and plate evaporation concentrator, together
When also increase the complexity and volume of equipment, and need to consume the substantial amounts of energy, equipment cost is high, and use cost is high.Cause
The evaporation concentration equipment that this develops efficient, low energy consumption, equipment is simple, operation is gentleer turns into those skilled in the art's urgent need and solved
Technical problem certainly.
The content of the invention
The invention aims to overcome above-mentioned deficiency, and a kind of operation provided is continuous, energy consumption is low, thickening efficiency
The high, vacuum concentration equipment and method for concentration that cocnentration factor is big, technique is simple, processing time is short.
In order to realize foregoing invention purpose, technical scheme is as follows：
A kind of vacuum concentration equipment, it is cold by feed spray system, film concentration systems, continuous discharge system, heating
But system and vacuum system are formed by connecting.
Above-mentioned vacuum concentration equipment, its concrete structure is as follows：Feed spray system is dense by the first conveying pipeline and film
Compression system is connected, and film concentration systems bottom is provided with continuous discharge system, continuous discharge system by the second conveying pipeline with it is thin
Film concentration systems are connected, and continuous discharge system is connected with feed spray system and finished product discharging opening respectively by the 3rd conveying pipeline,
Continuous discharge system is connected by secondary vacuum-pumping tube with vacuum system, outside the preheater of film concentration systems and feed spray system
Heating and cooling system is provided with, the second thin film concentrator of film concentration systems is connected by main vacuum-pumping tube with vacuum system.
The structure of above-mentioned feed spray system is as follows：Material storage tank is connected by the first conveying pipeline with atomizer, atomization
Device is arranged on the top of the first film inspissator of film concentration systems, the first conveying pipeline and is provided with preheater, the first conveying
The first valve is provided with pipe.
The structure of above-mentioned film concentration systems is as follows：By being arranged on the first film inspissator on top and being arranged on first
Second thin film concentrator of thin film concentrator lower end is constituted, and the inner chamber of the first film inspissator and the second thin film concentrator is connected
Logical, the feeding mouth of the first film inspissator is the discharging opening of the atomizer of feed spray system, the bottom of the second thin film concentrator
It is provided with clean-up port.
Above-mentioned the first film inspissator and the second thin film concentrator is connected by flange.
The structure of above-mentioned continuous discharge system is as follows：Main the second thin film concentrator by being arranged on film concentration systems
The concentrate temporary storage tank of bottom is constituted, and concentrate temporary storage tank is connected by the discharging opening of the second conveying pipeline and the second thin film concentrator
Connect, the second discharge valve and atmospheric valve are provided with the second conveying pipeline, the discharge end of concentrate temporary storage tank passes through the 3rd conveying pipeline
It is connected respectively with the material storage tank charging aperture and finished product discharging opening of feed spray system, the 3rd is disposed with the 3rd conveying pipeline
Outlet valve, delivery pump and sub-material switching valve；Concentrate temporary storage tank passes through on secondary vacuum-pumping tube and the main vacuum-pumping tube of vacuum system
Gas-liquid separator connection, be provided with vacuum valve on secondary vacuum-pumping tube.
Above-mentioned heating and cooling system is made up of heat transfer medium transfer pipeline and control valve.
The structure of above-mentioned vacuum system is as follows：Main vacuum-pumping tube is connected with vavuum pump, the vacuum orifice of main vacuum-pumping tube
It is arranged in the second thin film concentrator of film concentration systems, gas-liquid separator is provided with main vacuum-pumping tube.
A kind of vacuum concentration method, its step is as follows：Under the vacuum differential pressure action of vacuum system, material is sprayed by feeding
Mist system is preheated, be atomized concentration after be transported in film concentration systems, secondary film concentration is carried out in film concentration systems,
Material after film is concentrated is entered in the concentrate temporary storage tank of continuous discharge system, and continuous discharge system will be concentrated finally
Material afterwards is respectively outputted to the material storage tank of finished product materials outlet or feed spray system.
Above-mentioned secondary film concentration is comprised the following steps that：It is dense that material carries out secondary film in the first film inspissator
Contracting, the material after the concentration of secondary film, which is entered in the second thin film concentrator, further to be concentrated.
Above-mentioned secondary film concentration is comprised the following steps that：It is dense that material carries out secondary film in the first film inspissator
Contracting, the material after the concentration of secondary film, which is entered, carries out cooling down operation in the second thin film concentrator, temperature of charge can be cold
But extremely<40℃.
Due to using above-mentioned technical proposal so that the invention has the advantages that and effect：
Material is atomized after preheater is heated into atomizer, and the material of spray pattern considerably increases material
Disengagement area, improves evaporation efficiency.When the atomization material having been warmed up enters inside inspissator, due to vacuum action, solvent
Moment reaches that boiling point evaporates, and realizes spray concentration operation, and solvent evaporation capacity in several seconds, up to 68-72%, adds concentration effect
Rate, shortens concentration time；Film concentration systems are mainly made up of the first film inspissator and the second thin film concentrator.First is thin
Membrane concentrator and the second thin film concentrator realize that 4-100 DEG C of temperature is controllable；Material after spray concentration due to the effect of centrifugal force,
Reach the first film inspissator inner wall surface and form uniform thin electrolyte film, and moved down along wall；The more natural film forming concentration of film forming
Film forming is thinner, evenly, improves thickening efficiency, shortens concentration time.The first film inspissator and the second thin film concentrator
Inner wall surface is heating surface, and material realizes that film is concentrated in folding process, concentration is further carried out to material；Second is thin
The inner wall surface of membrane concentrator can also be cooling surface, can realize cooling down operation to thermo-responsive material, it is to avoid in operating process
In, material causes nutritive loss by long-time heating；The first film inspissator and the second thin film concentrator chuck and preheater folder
Set is connected in series, and heating medium is recycled, and improves heat utilization ratio.Vacuum system is mainly that concentration operation provides vacuum
Solvent vapo(u)r is entered in gas-liquid separator by vacuum tube after condition, concentration, and the feed separation carried in solvent vapo(u)r is come out, and
Into concentrate temporary storage tank, material recycle is realized, it is to avoid loss of material, solvent vapo(u)r carries out condensation recycling after separation.
The present invention improves thickening efficiency, cocnentration factor, the continuous behaviour of concentration by spraying and two vacuum concentration systems of film
Make, shorten concentration time, it is to avoid injury of the high temperature to material, solvent evaporation amount maximum is up to more than 90%, more conventional dense
Contracting processing time can shorten more than 70%, reduce concentrated cost.
Brief description of the drawings
Fig. 1 is the structural representation of vacuum concentration equipment of the present invention.
In figure, 1, feed spray system, 2, film concentration systems, 3, continuous discharge system, 4, heating and cooling system, 5, true
Empty set is united, 101, material storage tank, the 102, first valve, 103, preheater, 104, atomizer, the 105, first conveying pipeline, 201, the
One thin film concentrator, the 202, second thin film concentrator, 203, clean-up port, 301, concentrate temporary storage tank, the 302, second discharge valve,
303rd, atmospheric valve, 304, vacuum valve, the 305, the 3rd outlet valve, 306, delivery pump, 307, sub-material switching valve, the 308, the 3rd conveying
Pipe, 309, secondary vacuum-pumping tube, the 310, second conveying pipeline, 501, main vacuum-pumping tube, 502, gas-liquid separator.
Embodiment
The present invention is explained in further detail with reference to embodiment.Following examples are only the specific reality of the present invention
Example is applied, but the design concept of the present invention is not limited thereto, all changes for carrying out unsubstantiality to the present invention using this design,
The behavior for invading the scope of the present invention should be belonged to.
The present invention relates to a kind of vacuum concentration equipment, it is by feed spray system 1, film concentration systems 2, continuous discharge
System 3, heating and cooling system 4 and vacuum system 5 are formed by connecting.
As shown in figure 1, the concrete structure of vacuum concentration equipment of the present invention is as follows：Feed spray system 1 passes through the first conveying
Pipe 105 is connected with film concentration systems 2, and the bottom of film concentration systems 2 is provided with continuous discharge system 3, and continuous discharge system 3 is led to
Cross the second conveying pipeline 310 to be connected with film concentration systems 2, continuous discharge system 3 is sprayed with charging respectively by the 3rd conveying pipeline 308
Mist system 1 and the connection of finished product discharging opening, continuous discharge system 3 are connected by secondary vacuum-pumping tube 309 with vacuum system 5, and film is dense
Heating and cooling system 4 is provided with outside compression system 2 and the preheater of feed spray system 1 103, the second of film concentration systems 2 is thin
Membrane concentrator 202 is connected by main vacuum-pumping tube 501 with vacuum system 5.
The structure of above-mentioned feed spray system 1 is as follows：Material storage tank 101 passes through the first conveying pipeline 105 and atomizer 104
Connection, atomizer 104, which is arranged on the top of the first film inspissator 201 of film concentration systems 2, the first conveying pipeline 105, pacifies
Equipped with preheater 103, the first valve 102 is provided with the first conveying pipeline 105；The structure of film concentration systems 2 is as follows：By setting
The first film inspissator 201 and the structure of the second thin film concentrator 202 for being arranged on the lower end of the first film inspissator 201 on top
Into the intracavity inter-connection of the thin film concentrator 202 of the first film inspissator 201 and second, the feeding mouth of the first film inspissator 201
For the discharging opening of the atomizer 104 of feed spray system 1, the bottom of the second thin film concentrator 202 is provided with clean-up port 203, the
One thin film concentrator 201 and the second thin film concentrator 202 are connected by flange；The structure of continuous discharge system 3 is as follows：It is main by
The concentrate temporary storage tank 301 for being arranged on the bottom of the second thin film concentrator 202 of film concentration systems 2 is constituted, concentrate temporary storage tank
301 are connected by the second conveying pipeline 310 with the discharging opening of the second thin film concentrator 202, and second is provided with the second conveying pipeline 310
Discharge valve 302 and atmospheric valve 303, the discharge end of concentrate temporary storage tank 301 by the 3rd conveying pipeline 308 respectively with feed spray
The charging aperture of material storage tank 101 and finished product discharging opening of system 1 are connected, and the 3rd outlet valve is disposed with the 3rd conveying pipeline 308
305th, delivery pump 306 and sub-material switching valve 307；Concentrate temporary storage tank 301 passes through secondary vacuum-pumping tube 309 and the master of vacuum system 5
Gas-liquid separator 502 on vacuum-pumping tube 501 is connected, and vacuum valve 304 is provided with secondary vacuum-pumping tube 309；Heating and cooling system 4
It is to be made up of heat transfer medium transfer pipeline and control valve.The structure of vacuum system 5 is as follows：Main vacuum-pumping tube 501 and vavuum pump
Connection, the vacuum orifice of main vacuum-pumping tube 501 is arranged in the second thin film concentrator 202 of film concentration systems 2, and master vacuumizes
Gas-liquid separator 502 is provided with pipe 501.Heating and cooling system is identical with existing concentrator, is not described in detail, but this is not
It can be used to limit the scope of the invention.
The first vacuum concentration method of the invention, it is comprised the following steps that：
The heating medium for turning on heating and cooling system enters the first film inspissator 201, the second thin film concentrator 202 and pre-
Hot device 103 is preheated, and heating medium sequentially enters the first film inspissator 201, the second thin film concentrator 202 and preheater
103 chuck, heating-up temperature is controllable in the range of 30-100 DEG C.Upon reaching a predetermined temperature, start vavuum pump, reach predetermined true
After reciprocal of duty cycle, the first valve 102 is opened, material is preheated by preheater 103, turning into fine drop through the atomization of atomizer 104 carries out mist
Change concentration, material moment reaches boiling point, and 30%-70% solvents evaporate rapidly；Material after atomization concentration enters film concentration systems
2, due to the effect of the centrifugal force of atomizer 104, it is uniformly distributed in the inner wall surface of the first film inspissator 201, and along inner wall surface
It is descending, film is formed, material is carried out at secondary film concentration by the thin film concentrator 202 of the first film inspissator 201 and second
Reason, solvent evaporation amount maximum is up to more than 90%；By the two-step enrichment of 201 and second thin film concentrator of the first film inspissator 202
Material afterwards reaches the bottom of film concentration systems 2, enters concentrate temporary storage tank 301 through the second conveying pipeline 310, when concentrate is temporary
After tank 301 is filled, the second discharge valve 302 and vacuum valve 304 are closed, atmospheric valve 303 is opened, when in concentrate temporary storage tank 301
Portion's pressure is reached after normal pressure, opens the 3rd outlet valve 305, starts delivery pump 306, if concentration material reaches requirement, directly will
Concentrate is transported to finished product discharging opening；If material up to requiring, is not transmitted back to material storage tank 101, with delivered fresh by concentration material
Material reenters concentration operation together.After conveying is finished, the outlet valve 305 of atmospheric valve 303 and the 3rd is closed, the second outlet valve is opened
Door 302 and vacuum valve 304, recover vacuum state, are connected with film concentration systems 2, concentrate goes successively to concentrate temporary storage tank
301。
Second of vacuum concentration method of the invention, it is comprised the following steps that：
The heating medium of conducting heating and cooling system enters the first film inspissator 201 and preheater 103 is preheated, plus
Thermal medium sequentially enters the chuck of the first film inspissator 201 and preheater 103, and heating-up temperature can in the range of 30-100 DEG C
Control；The cooling medium for turning on heating and cooling system enters the second thin film concentrator 202, and chilling temperature can in the range of 4-25 DEG C
Control；Upon reaching a predetermined temperature, start vavuum pump, reach after predetermined vacuum level, open the first valve 102, material is by preheater
103 preheatings, turn into fine drop through the atomization of atomizer 104 and carry out atomization concentration, material moment reaches boiling point, 30%-70% solvents
Rapid evaporation；Material after atomization concentration enters film concentration systems 2, due to the effect of the centrifugal force of atomizer 104, is uniformly distributed
In the inner wall surface of the first film inspissator 201, and it is descending along inner wall surface, film is formed, material passes through the first film inspissator
201 carry out secondary film concentrations, and solvent evaporation amount maximum is up to more than 90%；Thing after secondary film concentration
Material is entered to be cooled down in the second thin film concentrator 202, and temperature of charge can be cooled to<40℃；Passed through after material concentration
Cross the cooling immediately of the second thin film concentrator 202, it is to avoid material continues quilt after concentration in concentrate temporary storage tank 301
The problem of heating and cause active ingredient loss, is adapted to that thickening temperature is too high or heat time unsuitable long material；Through supercooling
But the material after reaches the bottom of film concentration systems 2, enters concentrate temporary storage tank 301 through the second conveying pipeline 310, when concentrate is temporary
Deposit after tank 301 fills, close the second discharge valve 302 and vacuum valve 304, atmospheric valve 303 is opened, when concentrate temporary storage tank 301
Internal pressure is reached after normal pressure, opens the 3rd outlet valve 305, starts delivery pump 306, if concentration material reaches requirement, directly
Concentrate is transported to finished product discharging opening；It is and fresh if material is transmitted back to material storage tank 101 by concentration material not up to requiring
Material reenters concentration operation together.After conveying is finished, the outlet valve 305 of atmospheric valve 303 and the 3rd is closed, second is opened and discharges
Valve 302 and vacuum valve 304, recover vacuum state, are connected with film concentration systems 2, and concentrate goes successively to concentrate and kept in
Tank 301.
Claims (4)
1. a kind of vacuum concentration equipment, it is characterised in that it is by feed spray system（1）, film concentration systems（2）, continuously go out
Material system（3）, heating and cooling system（4）And vacuum system（5）It is formed by connecting；Feed spray system（1）Pass through the first conveying pipeline
（105）With film concentration systems（2）Connection, film concentration systems（2）Bottom is provided with continuous discharge system（3）, continuous discharge
System（3）Pass through the second conveying pipeline（310）With film concentration systems（2）Connection, continuous discharge system（3）Pass through the 3rd conveying pipeline
（308）Respectively with feed spray system（1）And the connection of finished product discharging opening, continuous discharge system（3）Pass through secondary vacuum-pumping tube（309）
With vacuum system（5）Connection, film concentration systems（2）With feed spray system（1）Preheater（103）It is cold that heating is provided with outside
But system（4）, atomizer（104）Installed in film concentration systems（2）The first film inspissator（201）Top, atomization
Device（104）The effect of centrifugal force, is uniformly distributed in the first film inspissator（201）Inner wall surface, film concentration systems（2）
Two thin film concentrators（202）Pass through main vacuum-pumping tube（501）With vacuum system（5）Connection；Described continuous discharge system（3）'s
Structure is as follows：Mainly by being arranged on film concentration systems（2）The second thin film concentrator（202）The concentrate temporary storage tank of bottom
（301）Constitute, concentrate temporary storage tank（301）Pass through the second conveying pipeline（310）With the second thin film concentrator（202）Discharging opening connect
Connect, the second conveying pipeline（310）On be provided with the second discharge valve（302）And atmospheric valve（303）, concentrate temporary storage tank（301）'s
Discharge end passes through the 3rd conveying pipeline（308）Respectively with feed spray system（1）Material storage tank（101）Charging aperture and finished product discharging
Mouth is connected, the 3rd conveying pipeline（308）On be disposed with the 3rd outlet valve（305）, delivery pump（306）And sub-material switching valve
（307）；Concentrate temporary storage tank（301）Pass through secondary vacuum-pumping tube (309) and vacuum system（5）Main vacuum-pumping tube（501）On
Gas-liquid separator（502）Vacuum valve is provided with connection, secondary vacuum-pumping tube (309)（304）；Described vacuum system（5）Knot
Structure is as follows：Main vacuum-pumping tube（501）It is connected with vavuum pump, main vacuum-pumping tube（501）Vacuum orifice be arranged on film concentration system
System（2）The second thin film concentrator（202）It is interior, main vacuum-pumping tube（501）On be provided with gas-liquid separator（502）.
2. a kind of vacuum concentration equipment according to claim 1, it is characterised in that described feed spray system（1）Knot
Structure is as follows：Material storage tank（101）Pass through the first conveying pipeline（105）With atomizer（104）Connection, the first conveying pipeline（105）Upper peace
Equipped with preheater（103）, the first conveying pipeline（105）On be provided with the first valve（102）.
3. a kind of vacuum concentration equipment according to claim 1, it is characterised in that described film concentration systems（2）Knot
Structure is as follows：By the first film inspissator for being arranged on top（201）Be arranged on the first film inspissator（201）The second of lower end
Thin film concentrator（202）Constitute, the first film inspissator（201）With the second thin film concentrator（202）Intracavity inter-connection, first
Thin film concentrator（201）Feeding mouth be feed spray system（1）Atomizer（104）Discharging opening, the second thin film concentrator
（202）Bottom be provided with clean-up port.
4. a kind of vacuum concentration equipment according to claim 1, it is characterised in that described heating and cooling system（4）Be by
Heat transfer medium transfer pipeline and control valve are constituted.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510818132.XA CN105289024B (en) | 2015-11-24 | 2015-11-24 | A kind of vacuum concentration equipment and method for concentration |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510818132.XA CN105289024B (en) | 2015-11-24 | 2015-11-24 | A kind of vacuum concentration equipment and method for concentration |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105289024A CN105289024A (en) | 2016-02-03 |
| CN105289024B true CN105289024B (en) | 2017-10-27 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510818132.XA Active CN105289024B (en) | 2015-11-24 | 2015-11-24 | A kind of vacuum concentration equipment and method for concentration |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108905252B (en) * | 2018-06-11 | 2021-02-19 | 江西国药有限责任公司 | Drying method in production process of fermented cordyceps sinensis powder |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2193763Y (en) * | 1994-06-22 | 1995-04-05 | 陈忠东 | Simple falling-film evaporator |
| JP2003508203A (en) * | 1999-09-06 | 2003-03-04 | イネオス フラウアー ホールデイングス リミテッド | Apparatus and method for separating liquid mixture |
| CN201101899Y (en) * | 2007-09-10 | 2008-08-20 | 河南润恒生物能源有限公司 | Film evaporimeter |
| CN203816344U (en) * | 2014-03-23 | 2014-09-10 | 胡森 | Vacuum-separating device of fire resistant oil filtering machine |
| CN205109069U (en) * | 2015-11-24 | 2016-03-30 | 沈阳农业大学 | Vacuum concentration equipment |
-
2015
- 2015-11-24 CN CN201510818132.XA patent/CN105289024B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2193763Y (en) * | 1994-06-22 | 1995-04-05 | 陈忠东 | Simple falling-film evaporator |
| JP2003508203A (en) * | 1999-09-06 | 2003-03-04 | イネオス フラウアー ホールデイングス リミテッド | Apparatus and method for separating liquid mixture |
| CN201101899Y (en) * | 2007-09-10 | 2008-08-20 | 河南润恒生物能源有限公司 | Film evaporimeter |
| CN203816344U (en) * | 2014-03-23 | 2014-09-10 | 胡森 | Vacuum-separating device of fire resistant oil filtering machine |
| CN205109069U (en) * | 2015-11-24 | 2016-03-30 | 沈阳农业大学 | Vacuum concentration equipment |
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| Publication number | Publication date |
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| CN105289024A (en) | 2016-02-03 |
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