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CN105267123A - Whitening and hydrating toner and method for manufacturing same - Google Patents

Whitening and hydrating toner and method for manufacturing same Download PDF

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Publication number
CN105267123A
CN105267123A CN201510799233.7A CN201510799233A CN105267123A CN 105267123 A CN105267123 A CN 105267123A CN 201510799233 A CN201510799233 A CN 201510799233A CN 105267123 A CN105267123 A CN 105267123A
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parts
aloe
water
extract
skin
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樊利平
陈洁娣
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A61K8/986Milk; Derivatives thereof, e.g. butter
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Zoology (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to whitening and hydrating toner and a method for manufacturing the same. The whitening and hydrating toner comprises, by weight, 40-60 parts of water, 2-5 parts of glycerin, 2-5 parts of butylene glycol, 1-3 parts of pearl powder, 0.5-1 part of sorbitol, 0.5-1.5 parts of milk proteins, 2-5 parts of hyaluronic acid, 0.01-0.02 part of essence and 10-35 parts of traditional Chinese medicine extract. The traditional Chinese medicine extract comprises eucommia ulmoides, rhodiola crenulata roots, aloe and saposhnikovia divaricata, and a weight ratio of the eucommia ulmoides to the rhodiola crenulata roots to the aloe to the saposhnikovia divaricata is 3-8:3-8:3-8:3-8. The whitening and hydrating toner and the method have the advantages that the whitening and hydrating toner is mild, skin friendly, safe and anti-aging, is free of irritation and can be used for a long time, the skins of users can be effectively whitened and hydrated and are moist, smooth and elastic, and wrinkles can be repaired by the aid of the whitening and hydrating toner.

Description

A kind of whitening skin and preserving moisture cosmetic water and preparation method thereof
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of whitening skin and preserving moisture cosmetic water and preparation method thereof.
Background technology
Along with growth in the living standard, people more and more focus on the maintenance of skin, but the reason such as inherent and external causes various skin problem.Immanent cause: be wrinkle, crows-feet, microgroove, temporal wrinkle be all because the inhomogenous contraction of skin epidermis is subsided and caused.First, skin is made up of three-decker, epidermal area, skin corium, subcutaneous fat respectively, skin corium contains collagen protein, elastin and other fibers and constitutes the skeleton supporting skin, also be that skin that these elements make seems smooth youth, these elements are also the damages being subject to UVA, UVB and ozone or other oxidative factors equally.Extrinsic factor: modern's life stress is large, overtime work is stayed up late, long-time to computer, smoking, do not have enough sleep, stay in air-conditioned room for a long time, drink, excess eye-using etc. becomes life normality, adds air pollution.According to the U.S. beautiful scientific center research of Dior Christian Dior, every day, the each layer of skin can accumulate the cellular elements toxin in a large number caused by inherent or extrinsic factor, skin cell can be caused to suffocate, and have impact on the Dusuqing removing solid capacity of skin self, thus just create the worries such as the colour of skin is obscure, shortage gloss, tired state are showed fully, increase the weight of the burden of skin, accelerate skin aging.Therefore, the cosmetics for the various problems of skin existence also arise at the historic moment.Cosmetic water also claims firming lotion, astringent etc., and its effect is just the pH-value again cleaning to recover skin surface, and nurses one's health horny layer, and skin is absorbed better, and prepares for application maintenance product.So after washed, use cosmetic water, can keep the skin wet rapidly.
" hydropenia " is that skin becomes more poor and more poor and one of aging main arch-criminal, replenishing water and preserving moisture is not the patent of responsive skin, various skin all can because of factors such as environment, age, nutrition, health hydropenia, when human body skin horny layer moisture lower than 10% time, skin will lose fine and soft, elasticity, then becomes coarse, dry, occur various skin abnormality, correct if can not get for a long time, skin easily aging, long speckle becomes responsive, so also will note moisturizing while anti-ageing.
Chinese patent application 201510361533.7 discloses a kind of humidity-preserving type cosmetic water efficiently, this cosmetic water is by spermol, potassium hydroxide, sodium alginate, arbutin, licochalcone, polyoxyethylene hardened castor oil, propylene glycol, Dodecyl Polyglucosides, wheat plantule protein, trimethyl glycine, phloretin, hyaluronic acid, citric acid, salicylic acid forms, the problems such as this cosmetic water can solve and cause that sensitivity is high due to air pollution to the skin of people, corse sweat pore and xerosis cutis hydropenia, but its whitening skin and preserving moisture effect need to improve.
Therefore, be necessary to research and develop a kind of whitening skin and preserving moisture cosmetic water, its whitening, moistening effect are good, and effectively level and smooth skin microgroove, delay skin aging.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of whitening skin and preserving moisture cosmetic water, its gentle pro-skin, easy absorption, antiallergic is safe and non-stimulating, and whitening skin and preserving moisture effect is good, effectively level and smooth skin microgroove, makes skin keep water tender and smooth, can life-time service.
The present invention is by following technical solution to realize above-mentioned purpose:
A kind of whitening skin and preserving moisture cosmetic water, comprise the raw material of following weight parts: 40 ~ 60 parts, water, glycerol 2 ~ 5 parts, butanediol 2 ~ 5 parts, Margarita powder 1 ~ 3 part, sorbitol 0.5 ~ 1 part, milk protein 0.5 ~ 1.5 part, hyaluronic acid 2 ~ 5 parts, 0.01 ~ 0.02 part, essence and Chinese medicine extract 10 ~ 35 parts, the raw materials of described Chinese medicine extract is made up of by the weight ratio of 3 ~ 8:3 ~ 8:3 ~ 8:3 ~ 8 Cortex Eucommiae, Radix Rhodiolae root, Aloe, Radix Saposhnikoviae.
Preferably, described whitening skin and preserving moisture cosmetic water comprises the raw material of following weight parts: 40 parts, water, glycerol 2 parts, butanediol 2 parts, Margarita powder 1 part, sorbitol 0.5 part, milk protein 0.5 part, Chinese medicine extract 12 parts, hyaluronic acid 2 parts and 0.01 part, essence.
Preferably, described whitening skin and preserving moisture cosmetic water comprises the raw material of following weight parts: 60 parts, water, glycerol 5 parts, butanediol 5 parts, Margarita powder 3 parts, sorbitol 1 part, milk protein 1.5 parts, Chinese medicine extract 32 parts, hyaluronic acid 5 parts and 0.02 part, essence.
Preferably, described whitening skin and preserving moisture cosmetic water comprises the raw material of following weight parts: 50 parts, water, glycerol 3 parts, butanediol 3 parts, Margarita powder 2 parts, sorbitol 0.8 part, milk protein 1 part, Chinese medicine extract 24 parts, hyaluronic acid 3 parts and 0.01 part, essence.
Preferably, described whitening skin and preserving moisture cosmetic water also comprises antiseptic 0.1 ~ 1 part.
Preferably, described Chinese medicine extract is obtained by following steps:
S1: take the Cortex Eucommiae, Radix Rhodiolae root, Aloe and Radix Saposhnikoviae respectively by the weight ratio of 3 ~ 8:3 ~ 8:3 ~ 8:3 ~ 8, cleans, for subsequent use;
S2: get the above-mentioned Cortex Eucommiae, Radix Rhodiolae root and Radix Saposhnikoviae, drying and crushing, add the water soaking 45 ~ 60 minutes of medical material gross weight 6 ~ 12 times amount, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filters and retains filtering residue, merging filtrate, obtaining Aqueous extracts;
S3: adding medical material gross weight 5 ~ 10 times amount volume fraction in the filtering residue in S2 is the ethanol of 70 ~ 90%, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filter, merging filtrate, obtains alcohol extract;
S4: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 ~ 24 hours, centrifugal 10 ~ 15 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 25 ~ 40 DEG C, material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.15 ~ 0.25MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 1 ~ 2 time that adds water, merge ultrafiltrate;
S5: by ultrafiltrate vacuum-concentrcted to being the extractum A of 1.15 ~ 1.25 to relative density at 60 DEG C, for subsequent use;
S6: get above-mentioned Aloe, is squeezed with squeezer and is obtained Aloe mixing juice; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract;
S7: merge described extractum A and namely described Aloe extract obtains described Chinese medicine extract.
Milk protein of the present invention contains hydrophilic moisturizing ingredient can protect skin total moisture to prevent from running off; several amino acids composition can promote the quick reparation of injured skin; the content of albumen in skin can be enriched; the intensity of connective tissue can be strengthened simultaneously; can promote that skin generates albumen, make skin plentiful and flexible.
The described Cortex Eucommiae is rich in the unsaturated fatty acid such as linolenic acid, linoleic acid, can safeguard the nutritive equilibrium of cell membrane, resists the infringement of external environment to skin, makes skin present efficient regeneration, moisturizing, the daily life function such as penetrating; Increase cell membrane elasticity and activating cell, improve the quality of epidermal area, reduce the deposition of pigment, skin care, improves coarse, the obscure skin without light quality.
Barbaloin energy regulation of skin contained by described Aloe, has the effect of obvious skin care and Palmitoleic Acid, can promote skin metabolism, be conducive to living again of outer skin tissue, have Promotive union effect to wound.
Described Radix Rhodiolae root can moisten supports moisturizing, maintains the constant humidity elasticity of skin, and has antioxidation and whitening merit
Energy.
Described Radix Saposhnikoviae has antiallergic, antiinflammatory action, effect of Lavender Extract, and gentle pro-skin is safe and non-stimulating.
Described Margarita powder contains abundant multiple proteins, 20 kinds of trace element and vitamin B, can effectively provide skin gloss, improve skin obscure.
Containing milk protein, the Cortex Eucommiae, Aloe, Radix Rhodiolae root, Radix Saposhnikoviae four kinds of natural extracts in whitening skin and preserving moisture cosmetic water of the present invention, skin metabolism is promoted to while skin supply nutrition, whitening skin and preserving moisture stricture of vagina is regenerated, make skin water tender flexible, skin color and luster and brightness is promoted again, strengthening oxidation resistance in conjunction with Margarita powder; Coordinate the basic materials such as glycerol, butanediol, sorbitol, hyaluronic acid and essence, the efficacy exertion of whitening skin and preserving moisture cosmetic water of the present invention is stablized, and stable system safety, gentle hypoallergenic, is easily absorbed by the skin, can life-time service.
Present invention also offers the preparation method of above-mentioned whitening skin and preserving moisture cosmetic water, specifically comprise the following steps:
S1: add in agitated kettle by water, glycerol, butanediol, Margarita powder, sorbitol and hyaluronic acid, homogenizing 3 ~ 8min, be heated to 70 ~ 85 DEG C, be stirred to material dissolution complete;
S2: continue to stir cooling and be down to 35 ~ 60 DEG C, adding milk protein and described Chinese medicine extract, to be stirred to system even;
S3: finally add essence and antiseptic, stir, get final product discharging, obtains whitening skin and preserving moisture cosmetic water.
Preferably, the mixing speed of described stirring is 40 ~ 50r/min.
Preferably, the rotating speed of described homogenizing is 2000 ~ 3000rpm.
Preferably, described Chinese medicine extract is obtained by following steps:
S1: take the Cortex Eucommiae, Radix Rhodiolae root, Aloe and Radix Saposhnikoviae respectively by the weight ratio of 3 ~ 8:3 ~ 8:3 ~ 8:3 ~ 8, cleans, for subsequent use;
S2: get the above-mentioned Cortex Eucommiae, Radix Rhodiolae root and Radix Saposhnikoviae, drying and crushing, add the water soaking 45 ~ 60 minutes of medical material gross weight 6 ~ 12 times amount, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filters and retains filtering residue, merging filtrate, obtaining Aqueous extracts;
S3: adding medical material gross weight 5 ~ 10 times amount volume fraction in the filtering residue in S2 is the ethanol of 70 ~ 90%, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filter, merging filtrate, obtains alcohol extract;
S4: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 ~ 24 hours, centrifugal 10 ~ 15 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 25 ~ 40 DEG C, material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.15 ~ 0.25MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 1 ~ 2 time that adds water, merge ultrafiltrate;
S5: by ultrafiltrate vacuum-concentrcted to being the extractum A of 1.15 ~ 1.25 to relative density at 60 DEG C, for subsequent use;
S6: get above-mentioned Aloe, is squeezed with squeezer and is obtained Aloe mixing juice; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract;
S7: merge described extractum A and namely described Aloe extract obtains described Chinese medicine extract.
Therefore, compared with prior art, advantage of the present invention is:
(1) whitening skin and preserving moisture cosmetic water of the present invention contains milk protein, the Cortex Eucommiae, Aloe, Radix Rhodiolae root, Radix Saposhnikoviae four kinds of natural extracts, can efficiently whitening, moisturizing, to skin supply nutrition, promote skin metabolism, long-acting moisturizing, makes skin beauty water moisten smooth, high resilience.
(2) whitening skin and preserving moisture cosmetic water safety and stability of the present invention, gentle pro-skin, does not stimulate, and skin easily absorbs, and uses rear face salubrious not sticky; And whitening skin and preserving moisture cosmetic water cost of material of the present invention is low, preparation method is simple, and condition is controlled, process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, whitening skin and preserving moisture cosmetic water of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
embodiment 1, whitening skin and preserving moisture cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following parts by weight: 40 parts, water, glycerol 2 parts, butanediol 2 parts, Margarita powder 1 part, sorbitol 0.5 part, milk protein 0.5 part, Chinese medicine extract 12 parts, hyaluronic acid 2 parts, 0.01 part, essence and antiseptic 0.2 part.
preparation method:
S1: get the Cortex Eucommiae 3 parts, Radix Rhodiolae root 3 parts, Aloe 3 parts and Radix Saposhnikoviae 3 parts, cleans, for subsequent use;
S2: get the above-mentioned Cortex Eucommiae, Radix Rhodiolae root and Radix Saposhnikoviae, drying and crushing, add the water soaking 45 minutes of medical material gross weight 6 times amount, reflux, extract, 2 times, each 3 hours, filters and retains filtering residue, merging filtrate, obtaining Aqueous extracts;
S3: adding medical material gross weight 5 times amount volume fraction in the filtering residue in S2 is the ethanol of 75%, reflux, extract, 2 times, each 3 hours, filter, merging filtrate, obtains alcohol extract;
S4: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 hours, centrifugal 10 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 25 DEG C, material liquid pH is 6, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.15MPa, when feed liquid stock solution reduces 1/4, then the ultrafiltration 1 time that adds water, merge ultrafiltrate;
S5: by ultrafiltrate vacuum-concentrcted to being the extractum A of 1.15 to relative density at 60 DEG C, for subsequent use;
S6: get above-mentioned Aloe, is squeezed with squeezer and is obtained Aloe mixing juice; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 time of circulation, obtains Aloe extract;
S7: merge described extractum A and namely described Aloe extract obtains described Chinese medicine extract;
S8: water, glycerol, butanediol, Margarita powder, sorbitol and hyaluronic acid are added in agitated kettle, homogenizing 5min, the rotating speed of homogenizing is 2000rpm, is heated to 75 DEG C, is stirred to material dissolution complete;
S9: continue to stir cooling and be down to 40 DEG C, the mixing speed of stirring is 40r/min, adding milk protein and Chinese medicine extract, to be stirred to system even;
S10: finally add essence and antiseptic, stir, the mixing speed of stirring is 40r/min, gets final product discharging, obtains whitening skin and preserving moisture cosmetic water.
embodiment 2, whitening skin and preserving moisture cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following parts by weight: 60 parts, water, glycerol 5 parts, butanediol 5 parts, Margarita powder 3 parts, sorbitol 1 part, milk protein 1.5 parts, Chinese medicine extract 32 parts, hyaluronic acid 5 parts, 0.02 part, essence, antiseptic 0.5 part.
preparation method:
S1: take the Cortex Eucommiae 8 parts, Radix Rhodiolae root 8 parts, Aloe 8 parts and Radix Saposhnikoviae 8 parts, cleans, for subsequent use;
S2: get the above-mentioned Cortex Eucommiae, Radix Rhodiolae root and Radix Saposhnikoviae, drying and crushing, add the water soaking 60 minutes of medical material gross weight 12 times amount, reflux, extract, 3 times, each 7 hours, filters and retains filtering residue, merging filtrate, obtaining Aqueous extracts;
S3: adding medical material gross weight 10 times amount volume fraction in the filtering residue in S2 is the ethanol of 90%, reflux, extract, 3 times, each 6 hours, filter, merging filtrate, obtains alcohol extract;
S4: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 24 hours, centrifugal 15 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 40 DEG C, material liquid pH is 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.25MPa, when feed liquid stock solution reduces 1/4, then the ultrafiltration 2 times that adds water, merge ultrafiltrate;
S5: by ultrafiltrate vacuum-concentrcted to being the extractum A of 1.25 to relative density at 60 DEG C, for subsequent use;
S6: get above-mentioned Aloe, is squeezed with squeezer and is obtained Aloe mixing juice; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 3 times of circulation, obtains Aloe extract;
S7: merge described extractum A and namely described Aloe extract obtains described Chinese medicine extract;
S8: water, glycerol, butanediol, Margarita powder, sorbitol and hyaluronic acid are added in agitated kettle, homogenizing 6min, the rotating speed of homogenizing is 3000rpm, is heated to 80 DEG C, is stirred to material dissolution complete;
S9: continue to stir cooling and be down to 50 DEG C, the mixing speed of stirring is 50r/min, adding milk protein and Chinese medicine extract, to be stirred to system even;
S10: finally add essence and antiseptic, stir, the mixing speed of stirring is 50r/min, gets final product discharging, obtains whitening skin and preserving moisture cosmetic water.
embodiment 3, whitening skin and preserving moisture cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following parts by weight: 50 parts, water, glycerol 3 parts, butanediol 3 parts, Margarita powder 2 parts, sorbitol 0.8 part, milk protein 1 part, Chinese medicine extract 24 parts, hyaluronic acid 3 parts, 0.01 part, essence and antiseptic 1 part.
preparation method:
S1: take the Cortex Eucommiae 6 parts, Radix Rhodiolae root 6 parts, Aloe 6 parts and Radix Saposhnikoviae 6 parts, cleans, for subsequent use;
S2: get the above-mentioned Cortex Eucommiae, Radix Rhodiolae root and Radix Saposhnikoviae, drying and crushing, add the water soaking 50 minutes of medical material gross weight 9 times amount, reflux, extract, 2 times, each 5 hours, filters and retains filtering residue, merging filtrate, obtaining Aqueous extracts;
S3: adding medical material gross weight 8 times amount volume fraction in the filtering residue in S2 is the ethanol of 80%, reflux, extract, 3 times, each 5 hours, filter, merging filtrate, obtains alcohol extract;
S4: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 hours, centrifugal 10 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 30 DEG C, material liquid pH is 7, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.20MPa, when feed liquid stock solution reduces 1/6, then the ultrafiltration 1 time that adds water, merge ultrafiltrate;
S5: by ultrafiltrate vacuum-concentrcted to being the extractum A of 1.20 to relative density at 60 DEG C, for subsequent use;
S6: get above-mentioned Aloe, is squeezed with squeezer and is obtained Aloe mixing juice; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 2 times of circulation, obtains Aloe extract;
S7: merge described extractum A and namely described Aloe extract obtains described Chinese medicine extract;
S8: water, glycerol, butanediol, Margarita powder, sorbitol and hyaluronic acid are added in agitated kettle, homogenizing 8min, the rotating speed of homogenizing is 3000rpm, is heated to 85 DEG C, is stirred to material dissolution complete;
S9: continue to stir cooling and be down to 60 DEG C, the mixing speed of stirring is 50r/min, adding milk protein and Chinese medicine extract, to be stirred to system even;
S10: finally add essence and antiseptic, stir, the mixing speed of stirring is 50r/min, gets final product discharging, obtains whitening skin and preserving moisture cosmetic water.
Do testing performance index to the whitening skin and preserving moisture cosmetic water of embodiment 1 ~ 3, its test result is as follows:
1, pH value: 5.5 ~ 7.0; 2, viscosity :≤300mpa; 3, heat-resistant stability investigates (45 DEG C × 24h): qualified;
4, cold-resistant study on the stability (~ 15 DEG C × 24h): qualified.
comparative example 1,
formula:be made up of the raw material of following parts by weight: 40 parts, water, butanediol 2 parts, Margarita powder 1 part, sorbitol 0.5 part, milk protein 0.5 part, Chinese medicine extract 12 parts, hyaluronic acid 2 parts, 0.01 part, essence and antiseptic 0.2 part.
Preparation method is with reference to embodiment 1.
comparative example 2,
formula:be made up of the raw material of following parts by weight: 40 parts, water, glycerol 2 parts, butanediol 2 parts, Margarita powder 1 part, sorbitol 0.5 part, milk protein 0.5 part, Chinese medicine extract 9 parts, hyaluronic acid 2 parts, 0.01 part, essence and antiseptic 0.2 part.
Preparation method is with reference to embodiment 1.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the whitening skin and preserving moisture cosmetic water that embodiment 1 ~ 3, comparative example 1 ~ 2 prepare.
Tested crowd's number: 100 people, women.
Age: between 25 ~ 55 years old.
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: 5 groups, often organize 20 people, 26 ± 2 years old mean age.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.025mL ~ 0.035mL drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Three, experimental result: human skin patch result shows: each group experimenter is by the patch test of the whitening skin and preserving moisture cosmetic water of embodiment 1 ~ 3, comparative example 1 ~ 2, dermoreaction is observed at 0.5,6,12,24,48 hour, wherein there is skin adverse reaction in 0 example, the whitening skin and preserving moisture cosmetic water use safety described in explanation.
test example two, product effect assessment
part I:
One, trial target: the whitening skin and preserving moisture cosmetic water that embodiment 1 ~ 3, comparative example 1 ~ 2 prepare.
Two, tested crowd
Sex number: female, 100 people.
Age: between 22 ~ 45 years old.
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 5 groups, often organize 20 people, 24 ± 2 years old mean age.
Three, method of testing: experimenter uses Fes Kai Er SK ~ I skin moisture detector to test the moisture of forehead, left face, right face and chin skin respectively after using clean water face, and get arithmetic mean of instantaneous value, experimenter re-uses above-mentioned whitening skin and preserving moisture cosmetic water, uniform application is in face, pat gently, by the skin moisture content of skin moisture tester test forehead, left face, right face and the same position of chin after 15min, and get arithmetic mean of instantaneous value, re-use skin moisture tester after 12h and test one time.Often organize 20 experimenters and tested result is got arithmetic mean of instantaneous value.
Four, test result is as following table 1.
Wherein, skin average moisture before skin average moisture ~ use cosmetic water is used after cosmetic water 15min after skin moisture content gradient=use cosmetic water 15min;
To use after cosmetic water 12h after skin moisture content gradient=use cosmetic water 12h skin average moisture before skin average moisture ~ use cosmetic water.
Table 1 skin moisture content table with test results
From upper table 1:
(1) whitening of the embodiment of the present invention 1 ~ 3 whitening skin and preserving moisture cosmetic water, moistening effect are good, can not only skin moisture content be significantly improved after using, also can pin moisture, make skin keep long-acting water to moisten, wherein best with the moistening effect of embodiment 3, therefore embodiment 3 is preferred embodiment.
(2) comparative example 1 lacks some component with comparative example 2 compared with embodiment 1, and its moisturizing guarantor, wet effect, all not as embodiment 1, illustrate that each component of whitening skin and preserving moisture cosmetic water of the present invention is worked in coordination with, play good moisturizing, moistening effect.
part II:
One, trial target: embodiment 1 ~ 3, whitening skin and preserving moisture cosmetic water prepared by comparative example 1 ~ 2.
Two, tested crowd
Sex number: female, 200 people.
Age: between 24 ~ 50 years old.
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 5 groups, often organize 40 people, 26 ± 2 years old mean age.
Three, method of testing: respectively use-case 1 ~ 3, whitening skin and preserving moisture cosmetic water prepared by comparative example 1 ~ 2, observes and experiences result of use.Using method: after experimenter cleans face, by above-mentioned whitening skin and preserving moisture cosmetic water uniform application in face, pat gently to skin and all absorb, the every day of each use sooner or later once, adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Four, testing evaluation result is as follows:
(one month) on probation feedback conclusive table of table 2 embodiment 1 whitening skin and preserving moisture cosmetic water
(one month) on probation feedback conclusive table of table 3 embodiment 2 whitening skin and preserving moisture cosmetic water
(one month) on probation feedback conclusive table of table 4 embodiment 3 whitening skin and preserving moisture cosmetic water
(one month) on probation feedback conclusive table of table 5 comparative example 1 cosmetic water
(one month) on probation feedback conclusive table of table 6 comparative example 2 cosmetic water
(1) from upper table 2 ~ 4, whitening skin and preserving moisture cosmetic water the liking and approving extensively by experimenter of embodiment 1 ~ 3, the gentle pro-skin of whitening skin and preserving moisture cosmetic water of the present invention is described, easily absorbs, use rear face salubrious not sticky, whitening, moistening effect are good, to skin supply nutrition, promote skin metabolism, long-acting moisturizing, skin beauty water is moistened smooth, flexible, wherein the highest with the degree of recognition of embodiment 3.
(2) from upper table 5 ~ 6, the result of use of comparative example 1 and comparative example 2 cosmetic water, all not as embodiment 1 ~ 3, illustrates that whitening skin and preserving moisture cosmetic water formula of the present invention is not obtained by the simple combination of each component.
(3) there is not people to occur allergic phenomena in whole experimenter while, all do not occur the situations such as skin pruritus, twinge, redness yet.Therefore, the gentle safety of whitening skin and preserving moisture cosmetic water of the present invention, can life-time service.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.

Claims (10)

1. a whitening skin and preserving moisture cosmetic water, it is characterized in that, comprise the raw material of following weight parts: 40 ~ 60 parts, water, glycerol 2 ~ 5 parts, butanediol 2 ~ 5 parts, Margarita powder 1 ~ 3 part, sorbitol 0.5 ~ 1 part, milk protein 0.5 ~ 1.5 part, hyaluronic acid 2 ~ 5 parts, 0.01 ~ 0.02 part, essence and Chinese medicine extract 10 ~ 35 parts, the raw materials of described Chinese medicine extract is made up of by the weight ratio of 3 ~ 8:3 ~ 8:3 ~ 8:3 ~ 8 Cortex Eucommiae, Radix Rhodiolae root, Aloe, Radix Saposhnikoviae.
2. whitening skin and preserving moisture cosmetic water as claimed in claim 1, it is characterized in that, comprise the raw material of following weight parts: 40 parts, water, glycerol 2 parts, butanediol 2 parts, Margarita powder 1 part, sorbitol 0.5 part, milk protein 0.5 part, Chinese medicine extract 12 parts, hyaluronic acid 2 parts and 0.01 part, essence.
3. whitening skin and preserving moisture cosmetic water as claimed in claim 1, it is characterized in that, comprise the raw material of following weight parts: 60 parts, water, glycerol 5 parts, butanediol 5 parts, Margarita powder 3 parts, sorbitol 1 part, milk protein 1.5 parts, Chinese medicine extract 32 parts, hyaluronic acid 5 parts and 0.02 part, essence.
4. whitening skin and preserving moisture cosmetic water as claimed in claim 1, it is characterized in that, comprise the raw material of following weight parts: 50 parts, water, glycerol 3 parts, butanediol 3 parts, Margarita powder 2 parts, sorbitol 0.8 part, milk protein 1 part, Chinese medicine extract 24 parts, hyaluronic acid 3 parts and 0.01 part, essence.
5. the whitening skin and preserving moisture cosmetic water as described in any one of claim 1 ~ 4, is characterized in that, described whitening skin and preserving moisture cosmetic water also comprises antiseptic 0.1 ~ 1 part.
6. whitening skin and preserving moisture cosmetic water as claimed in claim 1, it is characterized in that, described Chinese medicine extract is obtained by following steps:
S1: take the Cortex Eucommiae, Radix Rhodiolae root, Aloe and Radix Saposhnikoviae respectively by the weight ratio of 3 ~ 8:3 ~ 8:3 ~ 8:3 ~ 8, cleans, for subsequent use;
S2: get the above-mentioned Cortex Eucommiae, Radix Rhodiolae root and Radix Saposhnikoviae, drying and crushing, add the water soaking 45 ~ 60 minutes of medical material gross weight 6 ~ 12 times amount, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filters and retains filtering residue, merging filtrate, obtaining Aqueous extracts;
S3: adding medical material gross weight 5 ~ 10 times amount volume fraction in the filtering residue in S2 is the ethanol of 70 ~ 90%, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filter, merging filtrate, obtains alcohol extract;
S4: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 ~ 24 hours, centrifugal 10 ~ 15 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 25 ~ 40 DEG C, material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.15 ~ 0.25MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 1 ~ 2 time that adds water, merge ultrafiltrate;
S5: by ultrafiltrate vacuum-concentrcted to being the extractum A of 1.15 ~ 1.25 to relative density at 60 DEG C, for subsequent use;
S6: get above-mentioned Aloe, is squeezed with squeezer and is obtained Aloe mixing juice; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract;
S7: merge described extractum A and namely described Aloe extract obtains described Chinese medicine extract.
7. the preparation method of whitening skin and preserving moisture cosmetic water as claimed in claim 1, is characterized in that, comprise the following steps:
S1: add in agitated kettle by water, glycerol, butanediol, Margarita powder, sorbitol and hyaluronic acid, homogenizing 3 ~ 8min, be heated to 70 ~ 85 DEG C, be stirred to material dissolution complete;
S2: continue to stir cooling and be down to 35 ~ 60 DEG C, adding milk protein and described Chinese medicine extract, to be stirred to system even;
S3: finally add essence and antiseptic, stir, get final product discharging, obtains whitening skin and preserving moisture cosmetic water.
8. the preparation method of whitening skin and preserving moisture cosmetic water as claimed in claim 7, it is characterized in that, the mixing speed of described stirring is 40 ~ 50r/min.
9. the preparation method of whitening skin and preserving moisture cosmetic water as claimed in claim 7, it is characterized in that, the rotating speed of described homogenizing is 2000 ~ 3000rpm.
10. the preparation method of whitening skin and preserving moisture cosmetic water as claimed in claim 7, it is characterized in that, described Chinese medicine extract is obtained by following steps:
S1: take the Cortex Eucommiae, Radix Rhodiolae root, Aloe and Radix Saposhnikoviae respectively by the weight ratio of 3 ~ 8:3 ~ 8:3 ~ 8:3 ~ 8, cleans, for subsequent use;
S2: get the above-mentioned Cortex Eucommiae, Radix Rhodiolae root and Radix Saposhnikoviae, drying and crushing, add the water soaking 45 ~ 60 minutes of medical material gross weight 6 ~ 12 times amount, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filters and retains filtering residue, merging filtrate, obtaining Aqueous extracts;
S3: adding medical material gross weight 5 ~ 10 times amount volume fraction in the filtering residue in S2 is the ethanol of 70 ~ 90%, reflux, extract, 2 ~ 3 times, each 3 ~ 7 hours, filter, merging filtrate, obtains alcohol extract;
S4: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 ~ 24 hours, centrifugal 10 ~ 15 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 25 ~ 40 DEG C, material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.15 ~ 0.25MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 1 ~ 2 time that adds water, merge ultrafiltrate;
S5: by ultrafiltrate vacuum-concentrcted to being the extractum A of 1.15 ~ 1.25 to relative density at 60 DEG C, for subsequent use;
S6: get above-mentioned Aloe, is squeezed with squeezer and is obtained Aloe mixing juice; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract;
S7: merge described extractum A and namely described Aloe extract obtains described Chinese medicine extract.
CN201510799233.7A 2015-11-18 2015-11-18 Whitening and hydrating toner and method for manufacturing same Withdrawn CN105267123A (en)

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CN106074322A (en) * 2016-06-21 2016-11-09 江苏奇力康皮肤药业有限公司 A kind of whitening skin and preserving moisture aloe ointment
CN106137843A (en) * 2016-08-09 2016-11-23 许备占 Wild Hibisci Mutabilis cosmetic water and preparation method thereof
CN110339116A (en) * 2019-08-15 2019-10-18 宁波灏然生物科技有限公司 A kind of plant quintessence UV white whitening toner cosmetics and its processing method
CN112022784A (en) * 2020-09-28 2020-12-04 南京慧智莲华科技有限公司 Removable fragrant toner and preparation method thereof
CN113908089A (en) * 2021-09-10 2022-01-11 蔡彬弟 Composition with effects of moisturizing and soothing skin and application thereof

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106074322A (en) * 2016-06-21 2016-11-09 江苏奇力康皮肤药业有限公司 A kind of whitening skin and preserving moisture aloe ointment
CN106137843A (en) * 2016-08-09 2016-11-23 许备占 Wild Hibisci Mutabilis cosmetic water and preparation method thereof
CN110339116A (en) * 2019-08-15 2019-10-18 宁波灏然生物科技有限公司 A kind of plant quintessence UV white whitening toner cosmetics and its processing method
CN112022784A (en) * 2020-09-28 2020-12-04 南京慧智莲华科技有限公司 Removable fragrant toner and preparation method thereof
CN113908089A (en) * 2021-09-10 2022-01-11 蔡彬弟 Composition with effects of moisturizing and soothing skin and application thereof

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Application publication date: 20160127