CN104944907A - Glazed tile produced from Suzhou clay - Google Patents
Glazed tile produced from Suzhou clay Download PDFInfo
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- CN104944907A CN104944907A CN201510289465.8A CN201510289465A CN104944907A CN 104944907 A CN104944907 A CN 104944907A CN 201510289465 A CN201510289465 A CN 201510289465A CN 104944907 A CN104944907 A CN 104944907A
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- parts
- cotta
- terra
- suzhou soil
- glaze
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- 239000004927 clay Substances 0.000 title abstract 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 25
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 12
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 11
- 229920002472 Starch Polymers 0.000 claims abstract description 11
- 229910052656 albite Inorganic materials 0.000 claims abstract description 11
- 239000010433 feldspar Substances 0.000 claims abstract description 11
- 239000000835 fiber Substances 0.000 claims abstract description 11
- 239000010903 husk Substances 0.000 claims abstract description 11
- 239000010453 quartz Substances 0.000 claims abstract description 11
- 235000009566 rice Nutrition 0.000 claims abstract description 11
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910010271 silicon carbide Inorganic materials 0.000 claims abstract description 11
- 239000008107 starch Substances 0.000 claims abstract description 11
- 235000019698 starch Nutrition 0.000 claims abstract description 11
- 229920000049 Carbon (fiber) Polymers 0.000 claims abstract description 10
- 239000004917 carbon fiber Substances 0.000 claims abstract description 10
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 8
- 239000002689 soil Substances 0.000 claims description 42
- 238000002360 preparation method Methods 0.000 claims description 29
- 239000000758 substrate Substances 0.000 claims description 27
- 239000011021 lapis lazuli Substances 0.000 claims description 17
- 235000012239 silicon dioxide Nutrition 0.000 claims description 17
- 239000002994 raw material Substances 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 14
- 241000209094 Oryza Species 0.000 claims description 10
- 239000001095 magnesium carbonate Substances 0.000 claims description 10
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 claims description 10
- 229910000021 magnesium carbonate Inorganic materials 0.000 claims description 10
- 235000014380 magnesium carbonate Nutrition 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 10
- 229920003987 resole Polymers 0.000 claims description 10
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims description 10
- 229910052727 yttrium Inorganic materials 0.000 claims description 10
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims description 10
- 229910001928 zirconium oxide Inorganic materials 0.000 claims description 10
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 9
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 7
- 238000001354 calcination Methods 0.000 claims description 7
- 229910052799 carbon Inorganic materials 0.000 claims description 7
- 229910052681 coesite Inorganic materials 0.000 claims description 7
- 229910052906 cristobalite Inorganic materials 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 238000007493 shaping process Methods 0.000 claims description 7
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- 229910052682 stishovite Inorganic materials 0.000 claims description 7
- 229910052905 tridymite Inorganic materials 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 7
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 7
- 230000006835 compression Effects 0.000 abstract description 7
- 238000007906 compression Methods 0.000 abstract description 7
- 239000002253 acid Substances 0.000 abstract description 5
- 230000035699 permeability Effects 0.000 abstract description 4
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 abstract 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 abstract 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 abstract 1
- 240000007594 Oryza sativa Species 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 239000010431 corundum Substances 0.000 abstract 1
- 239000000395 magnesium oxide Substances 0.000 abstract 1
- 239000005011 phenolic resin Substances 0.000 abstract 1
- 229920001568 phenolic resin Polymers 0.000 abstract 1
- -1 polytetrafluoroethylene Polymers 0.000 abstract 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 abstract 1
- 239000004810 polytetrafluoroethylene Substances 0.000 abstract 1
- 229910001233 yttria-stabilized zirconia Inorganic materials 0.000 abstract 1
- 239000011787 zinc oxide Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 4
- 230000009970 fire resistant effect Effects 0.000 description 4
- 239000003973 paint Substances 0.000 description 3
- 238000004040 coloring Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 238000009423 ventilation Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
Landscapes
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Catalysts (AREA)
- Treatment Of Sludge (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
Abstract
The invention relates to a glazed tile produced from Suzhou clay. The blank of the glazed tile is composed of Suzhou clay, corundum powder, albite, quartz, fused magnesia, organic fibers, phenolic resin, starch and rice husk; and the glaze of the glazed tile is composed of iron oxide yellow, yttria-stabilized zirconia, feldspar powder, nanometer zinc oxide, silicon carbide, carbon fibers, tin dioxide, TEOS and polytetrafluoroethylene. The surface of the glazed tile is smooth and clean, and has brilliant and bright color, and the glazed tile has excellent compression, fire, acid and alkali resistance, and also has the advantages of light mass, low water absorption rate, good permeability and low cost.
Description
Technical field
The invention belongs to terra-cotta field, particularly a kind of terra-cotta utilizing Suzhou soil preparation.
Background technology
Terra-cotta are ancient, the traditional stupaliths of one, China.Along with the development of tourism, people are also more and more for the demand of terra-cotta, are also more and more higher to its requirement.
Terra-cotta, material is firm, bright in luster, glaze colours is smooth, and always as the building object of Chinese tradition, it developed through the successive dynasties, the improvement of quality, owing to having multiple excellent function, and is widely used in modern architecture.
Existing terra-cotta are all adopt multiple pug mixed sintering to form usually, and its glaze layer is general thicker and produce stress, quality weight, easily cause product glaze paint to occur be full of cracks, collapse the defect of stripping.Smooth not, and pug easily produces pollution in process of production, cost and energy consumption high, the quality of product is stable not, and its glaze paint glossiness is inadequate, and colour generation is abundant not, stable, easily fades under solar radiation in climate variability area or for a long time.
The technical problem that the present invention mainly solves is: for the deficiencies in the prior art, a kind of terra-cotta utilizing Suzhou soil preparation are provided, this terra-cotta smooth surface is clean and tidy, bright in colour beautiful, there is the performance of excellent resistance to compression, fire-resistant and acid and alkali-resistance, and quality is light, water-intake rate is low, good permeability, and cost is low.
Summary of the invention
The object of the invention is for the problems referred to above, develop a kind of terra-cotta utilizing Suzhou soil preparation, by optimizing the composition of terra-cotta base substrate and glaze, improve the colouring effect of terra-cotta, resistance to compression, the performance of fire-resistant and acid and alkali-resistance and the physical and chemical performance such as water-intake rate and ventilation property.
Utilize terra-cotta for Suzhou soil preparation, this terra-cotta base substrate weight part is composed as follows:
Suzhou soil 90-140 part; Lapis amiridis 20-30 part; Albite 8-10 part; Quartz 1-6 part; Electrosmelted magnesite clinker 1-6 part; Organic fibre 1-6 part; Resol 1-6 part; Starch 1-6 part; Rice husk 1-6 part;
This terra-cotta glaze weight part is composed as follows:
Iron oxide yellow 40-50 part; Yttrium stable zirconium oxide 1-6 part part; Feldspar Powder 1-6 part part; Nano zine oxide 1-6 part part; Silicon carbide 1-6 part part; Carbon fiber 1-6 part part; Tindioxide 1-6 part part; TEOS 1-6 part part; Tetrafluoroethylene 1-6 part part;
Its preparation method is as follows:
(1) batch mixing: terra-cotta blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 2 days;
(2) pressed compact is shaping, makes type at 50Mpa pressure, is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, during kiln discharge, base substrate water-content is less than 1.2wt%;
(4) glazing: glaze raw material is added water and prepares glaze, and glazing, glaze thickness is 0.2mm; Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, temperature rise rate 60 DEG C/h, after being warming up to 1450 DEG C, be incubated 2 hours, utilize Suzhou soil preparation terra-cotta.
As preferably, the chemical constitution of Suzhou soil is: SiO2 48wt%, Al2O3 39wt%, CaO 7%, other compositions 6wt%.
As preferably, the particle diameter of lapis amiridis is less than 1 μm.
As preferably, this terra-cotta base substrate weight part is composed as follows:
110 parts, Suzhou soil; Lapis amiridis 25 parts; Albite 9 parts; 5 parts, quartz; Electrosmelted magnesite clinker 5 parts; Organic fibre 5 parts; 5 parts, resol; Starch 5 parts; 5 parts, rice husk.
As preferably, this terra-cotta glaze weight part is composed as follows:
Iron oxide yellow 45 parts; Yttrium stable zirconium oxide 5 parts; Feldspar Powder 5 parts; Nano zine oxide 5 parts; 5 parts, silicon carbide; 5 parts, carbon fiber; Tindioxide 5 parts; TEOS 5 parts; Tetrafluoroethylene 5 parts.
Beneficial effect of the present invention:
(1) generally speaking, by optimizing the composition of terra-cotta base substrate and glaze, the colouring effect of terra-cotta, resistance to compression, the performance of fire-resistant and acid and alkali-resistance and the physical and chemical performance such as water-intake rate and ventilation property is improved; This terra-cotta smooth surface is clean and tidy, bright in colour beautiful, and have the performance of excellent resistance to compression, fire-resistant and acid and alkali-resistance, and quality is light, water-intake rate is low, good permeability, and cost is low.The water-intake rate of these terra-cotta is less than 4.6%, and ultimate compression strength is greater than 70Mpa.
(2) in base substrate batching, be the first main raw material with Suzhou soil, lapis amiridis is the second main raw material, and auxiliary albite, quartz, electrosmelted magnesite clinker, organic fibre, resol, starch and rice husk, and the weight part composition by optimizing each component, the resistance to compression of customer service Suzhou soil is strong, the imperfect deficiency of stability, and optimizes water suction and the permeability of base substrate.And there is good viscosity due to Suzhou soil, better with the keying action of glaze layer, therefore, glaze layer can be very thin, thus can prevent glaze paint from occurring be full of cracks, collapse the defect of stripping.Meanwhile, Suzhou soil carries color (pure white), also can produce material impact to the colour brightness of terra-cotta entirety.
(3) by with the addition of yttrium stable zirconium oxide and silicon carbide in glaze, the toughness of upper layer can be improved, and nano zine oxide, the automatically cleaning effect of terra-cotta can be played; And Feldspar Powder can play the effect of sintering aid; And the interpolation of TEOS and tetrafluoroethylene, effective surface protection can be carried out for terra-cotta, improve the smooth degree on surface.Terra-cotta smooth surface out prepared by the application is clean and tidy, bright in colour beautiful, and has good stability.
Embodiment
Below in conjunction with specific embodiment, and comparable data describes in further detail the present invention.Should be understood that these embodiments just in order to demonstrate the invention, but not limit the scope of the invention by any way.
Embodiment 1:
Utilize terra-cotta for Suzhou soil preparation,
This terra-cotta base substrate weight part is composed as follows:
110 parts, Suzhou soil; Lapis amiridis 25 parts; Albite 9 parts; 5 parts, quartz; Electrosmelted magnesite clinker 5 parts; Organic fibre 5 parts; 5 parts, resol; Starch 5 parts; 5 parts, rice husk;
This terra-cotta glaze weight part is composed as follows,
Iron oxide yellow 45 parts; Yttrium stable zirconium oxide 5 parts; Feldspar Powder 5 parts; Nano zine oxide 5 parts; 5 parts, silicon carbide; 5 parts, carbon fiber; Tindioxide 5 parts; TEOS 5 parts; Tetrafluoroethylene 5 parts;
The chemical constitution of Suzhou soil is: SiO2 48wt%, Al2O3 39wt%, CaO 7%, other compositions 6wt%.
The particle diameter of lapis amiridis is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: terra-cotta blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 2 days;
(2) pressed compact is shaping, makes type at 50Mpa pressure, is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, during kiln discharge, base substrate water-content is less than 1.2wt%;
(4) glazing: glaze raw material is added water and prepares glaze, and glazing, glaze thickness is 0.2mm; Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, temperature rise rate 60 DEG C/h, after being warming up to 1450 DEG C, be incubated 2 hours, utilize Suzhou soil preparation terra-cotta.
Embodiment 2:
Utilize terra-cotta for Suzhou soil preparation,
This terra-cotta base substrate weight part is composed as follows:
112 parts, Suzhou soil; Lapis amiridis 26 parts; Albite 8 parts; 5 parts, quartz; Electrosmelted magnesite clinker 4 parts; Organic fibre 5 parts; 4 parts, resol; Starch 5 parts; 5 parts, rice husk;
This terra-cotta glaze weight part is composed as follows,
Iron oxide yellow 46 parts; Yttrium stable zirconium oxide 5 parts; Feldspar Powder 2 parts; Nano zine oxide 2 parts; 5 parts, silicon carbide; 5 parts, carbon fiber; Tindioxide 2 parts; TEOS 5 parts; Tetrafluoroethylene 5 parts;
The chemical constitution of Suzhou soil is: SiO2 48wt%, Al2O3 39wt%, CaO 7%, other compositions 6wt%.
The particle diameter of lapis amiridis is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: terra-cotta blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 2 days;
(2) pressed compact is shaping, makes type at 50Mpa pressure, is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, during kiln discharge, base substrate water-content is less than 1.2wt%;
(4) glazing: glaze raw material is added water and prepares glaze, and glazing, glaze thickness is 0.2mm; Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, temperature rise rate 60 DEG C/h, after being warming up to 1450 DEG C, be incubated 2 hours, utilize Suzhou soil preparation terra-cotta.
Embodiment 3:
Utilize terra-cotta for Suzhou soil preparation,
This terra-cotta base substrate weight part is composed as follows:
109 parts, Suzhou soil; Lapis amiridis 22 parts; Albite 9 parts; 5 parts, quartz; Electrosmelted magnesite clinker 5 parts; Organic fibre 5 parts; 5 parts, resol; Starch 5 parts; 5 parts, rice husk;
This terra-cotta glaze weight part is composed as follows,
Iron oxide yellow 42 parts; Yttrium stable zirconium oxide 5 parts; Feldspar Powder 2 parts; Nano zine oxide 2 parts; 2 parts, silicon carbide; 5 parts, carbon fiber; Tindioxide 5 parts; TEOS2 part; Tetrafluoroethylene 2 parts;
The chemical constitution of Suzhou soil is: SiO2 48wt%, Al2O3 39wt%, CaO 7%, other compositions 6wt%.
The particle diameter of lapis amiridis is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: terra-cotta blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 2 days;
(2) pressed compact is shaping, makes type at 50Mpa pressure, is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, during kiln discharge, base substrate water-content is less than 1.2wt%;
(4) glazing: glaze raw material is added water and prepares glaze, and glazing, glaze thickness is 0.2mm; Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, temperature rise rate 60 DEG C/h, after being warming up to 1450 DEG C, be incubated 2 hours, utilize Suzhou soil preparation terra-cotta.
Embodiment 4:
Utilize terra-cotta for Suzhou soil preparation,
This terra-cotta base substrate weight part is composed as follows:
119 parts, Suzhou soil; Lapis amiridis 27 parts; Albite 9 parts; 2 parts, quartz; Electrosmelted magnesite clinker 5 parts; Organic fibre 2 parts; 2 parts, resol; Starch 2 parts; 5 parts, rice husk;
This terra-cotta glaze weight part is composed as follows,
Iron oxide yellow 47 parts; Yttrium stable zirconium oxide 5 parts; Feldspar Powder 2 parts; Nano zine oxide 2 parts; 2 parts, silicon carbide; 2 parts, carbon fiber; Tindioxide 2 parts; TEOS2 part; Tetrafluoroethylene 2 parts;
The chemical constitution of Suzhou soil is: SiO2 48wt%, Al2O3 39wt%, CaO 7%, other compositions 6wt%.
The particle diameter of lapis amiridis is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: terra-cotta blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 2 days;
(2) pressed compact is shaping, makes type at 50Mpa pressure, is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, during kiln discharge, base substrate water-content is less than 1.2wt%;
(4) glazing: glaze raw material is added water and prepares glaze, and glazing, glaze thickness is 0.2mm; Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, temperature rise rate 60 DEG C/h, after being warming up to 1450 DEG C, be incubated 2 hours, utilize Suzhou soil preparation terra-cotta.
Embodiment 5:
Utilize terra-cotta for Suzhou soil preparation,
This terra-cotta base substrate weight part is composed as follows:
100 parts, Suzhou soil; Lapis amiridis 20 parts; Albite 9 parts; 4 parts, quartz; Electrosmelted magnesite clinker 5 parts; Organic fibre 4 parts; 5 parts, resol; Starch 4 parts; 5 parts, rice husk;
This terra-cotta glaze weight part is composed as follows,
Iron oxide yellow 50 parts; Yttrium stable zirconium oxide 5 parts; Feldspar Powder 2 parts; Nano zine oxide 2 parts; 2 parts, silicon carbide; 2 parts, carbon fiber; Tindioxide 5 parts; TEOS2 part; Tetrafluoroethylene 2 parts;
The chemical constitution of Suzhou soil is: SiO2 48wt%, Al2O3 39wt%, CaO 7%, other compositions 6wt%.
The particle diameter of lapis amiridis is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: terra-cotta blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 2 days;
(2) pressed compact is shaping, makes type at 50Mpa pressure, is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, during kiln discharge, base substrate water-content is less than 1.2wt%;
(4) glazing: glaze raw material is added water and prepares glaze, and glazing, glaze thickness is 0.2mm; Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, temperature rise rate 60 DEG C/h, after being warming up to 1450 DEG C, be incubated 2 hours, utilize Suzhou soil preparation terra-cotta.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (5)
1. utilize terra-cotta for Suzhou soil preparation, it is characterized in that:
This terra-cotta base substrate weight part is composed as follows:
Suzhou soil 90-140 part; Lapis amiridis 20-30 part; Albite 8-10 part; Quartz 1-6 part; Electrosmelted magnesite clinker 1-6 part; Organic fibre 1-6 part; Resol 1-6 part; Starch 1-6 part; Rice husk 1-6 part;
This terra-cotta glaze weight part is composed as follows:
Iron oxide yellow 40-50 part; Yttrium stable zirconium oxide 1-6 part part; Feldspar Powder 1-6 part part; Nano zine oxide 1-6 part part; Silicon carbide 1-6 part part; Carbon fiber 1-6 part part; Tindioxide 1-6 part part; TEOS 1-6 part part; Tetrafluoroethylene 1-6 part part;
Its preparation method is as follows:
(1) batch mixing: terra-cotta blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 2 days;
(2) pressed compact is shaping, makes type at 50Mpa pressure, is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, during kiln discharge, base substrate water-content is less than 1.2wt%;
(4) glazing: glaze raw material is added water and prepares glaze, and glazing, glaze thickness is 0.2mm; Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, temperature rise rate 60 DEG C/h, after being warming up to 1450 DEG C, be incubated 2 hours, utilize Suzhou soil preparation terra-cotta.
2. utilize terra-cotta for Suzhou soil preparation as claimed in claim 1, it is characterized in that, the chemical constitution of Suzhou soil is: SiO2 48wt%, Al2O3 39wt%, CaO 7%, other compositions 6wt%.
3. utilize terra-cotta for Suzhou soil preparation as claimed in claim 1 or 2, it is characterized in that, the particle diameter of lapis amiridis is less than 1 μm.
4. utilize terra-cotta for Suzhou soil preparation as claimed in claim 1, it is characterized in that, this terra-cotta base substrate weight part is composed as follows:
110 parts, Suzhou soil; Lapis amiridis 25 parts; Albite 9 parts; 5 parts, quartz; Electrosmelted magnesite clinker 5 parts; Organic fibre 5 parts; 5 parts, resol; Starch 5 parts; 5 parts, rice husk.
5. the terra-cotta utilizing Suzhou soil preparation as described in claim 1 or 5, it is characterized in that, this terra-cotta glaze weight part is composed as follows:
Iron oxide yellow 45 parts; Yttrium stable zirconium oxide 5 parts; Feldspar Powder 5 parts; Nano zine oxide 5 parts; 5 parts, silicon carbide; 5 parts, carbon fiber; Tindioxide 5 parts; TEOS 5 parts; Tetrafluoroethylene 5 parts.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510289465.8A CN104944907B (en) | 2015-06-01 | 2015-06-01 | A kind of glazed tiles utilizing Suzhou soil to prepare |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510289465.8A CN104944907B (en) | 2015-06-01 | 2015-06-01 | A kind of glazed tiles utilizing Suzhou soil to prepare |
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| Publication Number | Publication Date |
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| CN104944907A true CN104944907A (en) | 2015-09-30 |
| CN104944907B CN104944907B (en) | 2017-01-04 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106082961A (en) * | 2016-06-22 | 2016-11-09 | 徐晓 | A kind of method utilizing Suzhou soil to prepare low grade fever's glazed tiles |
| CN106219974A (en) * | 2016-08-08 | 2016-12-14 | 太仓市科教新城琉璃艺术策划中心 | High-cleanness, high coloured glaze |
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| CN1121496A (en) * | 1994-10-26 | 1996-05-01 | 佘爱华 | Baking-free imitation of ancient art and craft glazed tile and making method |
| CN1143058A (en) * | 1996-07-01 | 1997-02-19 | 张成华 | Preparing method for new type glass tile |
| CN101851119A (en) * | 2009-04-02 | 2010-10-06 | 故宫博物院 | Glazing resintering technology of unglazed ancient colored glaze components |
| CN102276149A (en) * | 2010-06-09 | 2011-12-14 | 故宫博物院 | Method for preparing fritted glaze for ancient glazed members |
| CN104311152A (en) * | 2014-09-30 | 2015-01-28 | 句容金猴机械研究所有限公司 | Glazed tile glaze and preparation method and application thereof |
| CN104418585A (en) * | 2013-08-29 | 2015-03-18 | 孙即杰 | High-temperature molding process for ceramic and colored glaze |
-
2015
- 2015-06-01 CN CN201510289465.8A patent/CN104944907B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1101025A (en) * | 1993-03-01 | 1995-04-05 | 成江 | Glazed porcelain |
| CN1121496A (en) * | 1994-10-26 | 1996-05-01 | 佘爱华 | Baking-free imitation of ancient art and craft glazed tile and making method |
| CN1143058A (en) * | 1996-07-01 | 1997-02-19 | 张成华 | Preparing method for new type glass tile |
| CN101851119A (en) * | 2009-04-02 | 2010-10-06 | 故宫博物院 | Glazing resintering technology of unglazed ancient colored glaze components |
| CN102276149A (en) * | 2010-06-09 | 2011-12-14 | 故宫博物院 | Method for preparing fritted glaze for ancient glazed members |
| CN104418585A (en) * | 2013-08-29 | 2015-03-18 | 孙即杰 | High-temperature molding process for ceramic and colored glaze |
| CN104311152A (en) * | 2014-09-30 | 2015-01-28 | 句容金猴机械研究所有限公司 | Glazed tile glaze and preparation method and application thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106082961A (en) * | 2016-06-22 | 2016-11-09 | 徐晓 | A kind of method utilizing Suzhou soil to prepare low grade fever's glazed tiles |
| CN106082961B (en) * | 2016-06-22 | 2018-11-13 | 嵊州市森汇知识产权运营有限公司 | A method of preparing low fever's glazed tiles using Suzhou soil |
| CN106219974A (en) * | 2016-08-08 | 2016-12-14 | 太仓市科教新城琉璃艺术策划中心 | High-cleanness, high coloured glaze |
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| Publication number | Publication date |
|---|---|
| CN104944907B (en) | 2017-01-04 |
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