The content of the invention
For above-mentioned prior art, the invention provides a kind of black fungus super-micro instant electuary with blood fat reducing function,
Its adsorptivity is strong, water imbibition strong, good water solubility, and rapidly dissolvable, good mouthfeel with hypoglycemic, reducing blood lipid, radioresistance, is carried
The effects such as high immunity, antithrombotic, anticancer, fat-reducing, benefit iron;Present invention also offers its preparation method.
The present invention is achieved by the following technical solutions:
A kind of black fungus super-micro instant electuary with blood fat reducing function, is made up of the component of following parts by weight:It is black
4.5~5.5 parts of agaric ultra-fine powder, 2.5~3.5 parts of degreasing black bean powder, 2.5~3.5 parts of rock sugar.It is preferred that, can also include with
The component of lower parts by weight:0.02~0.03 part of jasmine pollen, 0.02~0.03 part of lilium pollen, 0.04~0.06 part of tangerine peel powder
(jasmine pollen, lilium pollen, the addition of tangerine peel powder, with regulation mouthfeel and deliquescent effect, while having collaboration reducing blood lipid
Effect).It is further preferred that be made up of the component of following parts by weight:5 parts of black fungus Ultramicro-powder, 3 parts of degreasing black bean powder,
3 parts of rock sugar.Still further preferably, it is made up of the component of following parts by weight:5 parts of black fungus Ultramicro-powder, degreasing black bean powder 3
Part, 3 parts of rock sugar, 0.025 part of jasmine pollen, 0.025 part of lilium pollen, 0.05 part of tangerine peel powder.
Wherein, the black fungus Ultramicro-powder, which is prepared by the following method, obtains:Take black fungus, remove surface impurity and
After hard root portion, cleaning-drying, carries out preliminary crushing with whirlwind type crushing machine, 100 mesh sieves of mistake obtain coarse powder, then by coarse powder gas
Streaming pulverizer carries out air-flow ultramicro grinding, is dried in vacuum drying chamber to constant weight, obtains black fungus Ultramicro-powder, and its particle diameter is 10
~50 μm, 25 μm of average grain diameter, sealing preserve prevents the moisture absorption.
The degreasing black bean powder, which is prepared by the following method, to be obtained:(degreasing black soya bean is that grease factory will to extracting degreasing black soya bean
Accessory substance after the oil expression of black soya bean raw material, is directly obtained from grease factory, is existing conventional products in the prior art), fry, with rotation
Wind formula pulverizer is crushed, and is crossed 100 mesh sieves, is obtained degreasing black bean powder, sealing preserve.
The jasmine pollen, which is prepared by the following method, to be obtained:Jasmine raw material → cleaning impurity elimination → cleaning → drying
→ coarse crushing → ultramicro grinding (coarse crushing, ultramicro grinding mode with above-mentioned black fungus Ultramicro-powder preparation method).
The lilium pollen, which is prepared by the following method, to be obtained:Lily raw material → cleaning impurity elimination → cleaning → drying
→ coarse crushing → ultramicro grinding.
The tangerine peel powder, which is prepared by the following method, to be obtained:Dried orange peel raw material → cleaning impurity elimination → cleaning → drying → thick
Crushing → ultramicro grinding.
The preparation method of the black fungus super-micro instant electuary with blood fat reducing function is:By each component, (black fungus surpasses
Micro mist, rock sugar, or and:Degreasing black bean powder, jasmine pollen, lilium pollen, tangerine peel powder) mixing mixing, aseptic packaging after sterilizing, i.e.,
.Technological process is as follows:
Black fungus raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding;
Degreasing black soya bean → coarse crushing;
Above two material mixes → sterilizing → packaging with rock sugar.
When edible, warm water Instant Drinks stir, one time 1 bag (1 10 grams of bag).
The black fungus super-micro instant electuary with blood fat reducing function of the present invention, not only solves the absorption of black fungus Ultramicro-powder
The problem of rate is low, also solves the problem of ultrafine powder is instant, also, addition black bean powder is carried out with rock sugar to black fungus powder nutrition
Balance, makes the product preferably serviced by human health.The black fungus ultra micro with blood fat reducing function of the present invention
Instant, blood fat reducing function is significantly better than black fungus raw material, coarse powder, and dissolubility is good, in good taste, with lipid-loweringing, antithrombotic, resists
The physiological functions such as radiation, anti-oxidant, antitumor, hypoglycemic, fat-reducing, beauty, clearing lung-heat, it is adaptable to crowd's food of each age level
With with good economic benefit.
Embodiment
With reference to embodiment, the present invention is further illustrated.
Involved instrument, reagent, material etc. in following embodiments, are existing in the prior art unless otherwise noted
Conventional instrument, reagent, material etc., can be obtained by regular commercial sources.Involved experimental method in following embodiments, inspection
Survey method etc., is existing normal experiment method in the prior art, detection method etc. unless otherwise noted.
Test 1 black fungus Ultramicro-powder, the contrast of the blood fat reducing function of black fungus coarse powder
Test method:40 mouse are divided into 4 groups, i.e. Basal control group (A groups), high fat using arbitrary sampling method to compare
Group (B groups), coarse powder dosage group (C groups) and Ultramicro-powder dosage group (D groups), every group 10.A group basal feeds are given, B, C, D group are
High lipid food (basal feed: lard: cholesterol is 80: 19: 1) is given, every morning, feeding once, freely took food drinking-water, 12h
Periodicity of illumination, temperature is 22 ± 1 DEG C, and humidity is 65%.After 10 days, Basal control group and high lipid food group respectively randomly select 3
Mouse, plucks eyeball and takes eyeground blood, detect serum total cholesterol (TC) level, determine the foundation of hyperlipemia model.
The basal feed is standard mouse grain, and the formula of the high lipid food is:Basal feed: lard: cholesterol=80:
19: 1, mass ratio.
Set up after hyperlipemia model, A groups give basal feed daily;B groups give high lipid food;C groups are removed and give high fat
The black fungus coarse powder of mouse 100mg/kg.d dosage is given outside feed daily;D groups are given small daily while giving high lipid food
The black fungus Ultramicro-powder of mouse 100mg/kg.d dosage.The mouse weight of measurement in one week.A, B, C, D4 group free water.Feed 35
After it, eyeground blood is taken to be put into test tube after fasting 24h, after detection T-CHOL (TC), triglycerides (TG), height after dissolution serum
Density lipoprotein (HDL-C) level.Judge whether black fungus powder has functions that reducing blood lipid by These parameters.Each index is usedRepresent.Compared using t inspections with whether hyperlipemia model control group has conspicuousness.
The black fungus coarse powder, which is prepared by the following method, to be obtained:Black fungus is taken, surface impurity and hard root is removed
Point, preliminary crushing is carried out after cleaning-drying with whirlwind type crushing machine, 100 mesh sieves is crossed, obtains coarse powder.
The black fungus Ultramicro-powder, which is prepared by the following method, to be obtained:Black fungus is taken, surface impurity and hard root is removed
After part, cleaning-drying, preliminary crushing is carried out with whirlwind type crushing machine, cross 100 mesh sieves, obtain coarse powder, then by coarse powder air-flowing type
Pulverizer carries out air-flow ultramicro grinding, is dried in vacuum drying chamber to constant weight, obtains black fungus Ultramicro-powder, and its particle diameter is 10~50
μm, 25 μm of average grain diameter, sealing preserve prevents the moisture absorption.
Result of the test:
(1) 4 group of mouse high lipid food is fed after 10d, and Basal control group and each 3 mouse of high lipid food group are taken at random, is plucked
Eyeball takes blood, measures mice serum total cholesterol level, and results contrast is as shown in table 1.
Mouse TC compares before and after table 1 sets up hyperlipemia model
Note:Compared with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reach the pole level of signifiance (P
< 0.01)
Mouse is after feeding 10 days as can be seen from Table 1, and serum total cholesterol content is significantly raised, with Basal control group phase
Than high lipid food group serum TC content reaches significant difference (P < 0.05).Illustrate that high fat diet can result in mice serum TC
Rise, hyperlipemia model is successfully prepared.
(2) black fungus powder is shown in Table 2 to mouse to serum total cholesterol (TC) TC contents.
The serum total cholesterol of table 2 (TC) content
Note:Compared with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reach the pole level of signifiance (P
< 0.01)
The result of table 2 shows:Compared with high fat control group, black fungus coarse powder plays the role of to reduce TC, but is not reaching to significantly
Effect, Ultramicro-powder reduction hyperlipidemic mice TC reaches significant difference (P < 0.05), and 7.56% and 12.04% are reduced respectively, is surpassed
Micro mist group TC levels drop to Basal control group phase same level substantially.
(3) to Triglycerides in Serum (TG) influence:
After giving mouse polysaccharide 35 days, TG contents are shown in Table 3 in serum.
The serum triglyceride of table 3 (TG) content
Note:Compared with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reach the pole level of signifiance (P
< 0.01)
Result of study shows:Relative to high fat control group, black fungus coarse powder reaches in terms of mice serum TG contents are reduced
Significant difference (P < 0.05), and Ultramicro-powder reaches pole significant difference (P < 0.01), and 12.00% and 22% are reduced respectively.Say
Bright black fungus powder plays the role of to reduce mice serum TG, and the effect of Ultramicro-powder reduction serum TG is more notable compared with coarse powder.
(4) to the influence of serum middle-high density lipoprotein (HDL-C):
After giving mouse black fungus powder 35 days, HDL-C contents are shown in Table 4 in serum.
The serum high-density LP of table 4 (HDL-C) content
Note:Compared with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reach the pole level of signifiance (P
< 0.01)
As a result show:Black fungus coarse powder and Ultramicro-powder have all reached in terms of serum high-density LP content is improved extremely to be shown
The effect for writing HDL-C in difference, but Ultramicro-powder group raising serum is more obvious compared with coarse powder group.Coarse powder group and ultra micro powder component be you can well imagine
It is high by 58.73% and 73.02%.
Found after above-mentioned animal experiment study, the lipid-lowering effect of black fungus Ultramicro-powder is obviously improved.Reducing blood lipid work(
Can test proves black fungus Ultramicro-powder group than coarse powder group reduction blood fat effect more preferably, and black fungus Ultramicro-powder group tool is significantly reduced
T-CHOL (P < 0.05), extremely significant reduction triglycerides (P < 0.01) and pole significantly improve HDL (P <
0.01) act on.
Experiment 2 has the research that the black fungus super-micro instant granule best of blood fat reducing function is matched
1. material and equipment
Material:Black fungus, degreasing black soya bean.
Equipment:Pulverizer, jet mill, electric heating constant-temperature blowing drying box, glutinous analyzer, electronic analytical balance, from
Scheming, constant temperature blender with magnetic force.
2. experimental method
2.1 black fungus Ultramicro-powders, the preparation of degreasing black bean powder
Black fungus Ultramicro-powder:Black fungus is taken, surface impurity and hard root portion is removed, preliminary powder is carried out with whirlwind type crushing machine
It is broken, 100 mesh sieves are crossed, coarse powder is obtained, then coarse powder with jet mill is subjected to air-flow ultramicro grinding, the drying in vacuum drying chamber
To constant weight, black fungus Ultramicro-powder is obtained, its, 150 μm of average grain diameter, sealing preserve prevents the moisture absorption.
Black bean powder:Extracting degreasing black soya bean, is fried, and is crushed with whirlwind type crushing machine, is crossed 100 mesh sieves, is obtained black bean powder, is sealed
Preserve.
Instant:Take black fungus Ultramicro-powder, black bean powder and rock sugar (rock sugar is crushed with whirlwind type crushing machine in advance,
Cross 100 mesh sieves), mixing is mixed, and is produced.
The measure of 2.2 viscositys
Calculation formula:A=k × a
In formula, A is viscosity, mPas;K is the coefficient under different rotor, different rotating speeds;A is the reading of viscosity analyzer.
2.3 sensory evaluation
Using descriptive analysis test method, 10 colleagues are selected to be evaluated.Rice paste is supplied to evaluation by random sequence
Member, each index, which is given a mark, and corresponding sense organ is made describes.Standards of grading are shown in Table 5.
The measure of the instant index of 2.4 electuaries
(1) measure of wetability:The deionized water 200ml of 25 DEG C of addition, weighs 0.5g samples uniform in 250ml beakers
It is laid on the water surface, determines the time (s) added from sample to sample required for settling completely.
(2) dispersed measure:Weigh 5g samples to be put in 100ml beakers, add 25 DEG C of deionization 50ml, with
800r/min rotating speed is stirred in constant temperature blender with magnetic force, is recorded since stirring to the powder agglomates whole scattered required time
(s)。
(3) measure of solubility:Accurate weighing sample 5.00g samples, are placed in 50ml small beakers, add deionized water
With magnetic stirrer 30min under 30ml, room temperature condition, instant is set fully to dissolve.Solution is transferred to 50ml completely
In volumetric flask, deionized water constant volume is used, is fully shaken up.15ml is taken, is put into centrifuge tube, 3000r/min centrifugation 10min take
Clear liquid, is transferred in weighing disk, and 20min is heated in a water bath, is then placed in 105 DEG C of drying boxes and is dried to constant mass.Calculate
Formula is as follows:
In formula, X is sample solubility, g/100g;M is sample quality, g;M1For weighing disk quality, g;M2For weighing disk and
Quality, g after insoluble matter is dried;B is sample moisture.
The sensory evaluation scores standard of table 5
3. result and analysis
3.1 black fungus Ultramicro-powders are most adapted to ratio with degreasing black bean powder
Selected black fungus Ultramicro-powder is respectively 0: 5,5: 5,5: 4,5: 3,5: 2,5: 1,5: 0, ice with degreasing black bean powder proportioning
Sugared mass fraction is 40%, takes sample 5g in 100ml beakers, adds 50ml water (90 DEG C) and reconstitutes, is cooled to after being sufficiently stirred for
Room temperature.
As seen from Figure 1, with the reduction of degreasing black bean powder addition, the viscosity of electuary is in obvious ascendant trend.This be by
Hydrogen bond is broken between starch molecule after gelatinization, and hydrone enters starch crystallite binding structure, the increase of molecule randomness, starch-water body
The viscosity of system is of a relatively high.The presence of degreasing black bean powder have impact on hydrone entrance, make the viscosity of starch-aqueous systems by broken
Bad, the content of starch of black fungus powder is higher than black soya bean, easily gelatinization, therefore the viscosity that black fungus powder matches high nourishing medicinal granule is higher than
Black fungus powder matches low viscosity.From table 6, degreasing black bean powder has an impact to the subjective appreciation of nourishing medicinal granule, with degreasing
The increase of black bean powder addition, it is 5 that the preferable sample of instant sensory evaluation scores, which concentrates on black fungus powder and the ratio of black bean powder:
2nd, (most preferably 5: 3) in the range of 5: 3,5: 4.Reason is that black fungus powder is taupe, and degreasing black bean powder is faint yellow, its content
Then color and luster is shallower for increase, but its content increases so that the viscosity of nourishing medicinal granule has declined, and taste bad, fragrance is thin out.
The sensory evaluation scores of electuary under the different ratios of raw materials of table 6
3.2 reconstitute influence of the water temperature to electuary
Choose black fungus Ultramicro-powder and degreasing black bean powder proportioning 5: 3, rock sugar mass fraction be 40%, take sample 5g in
In 100ml beakers, it is separately added into DEG C water of 50ml60,70,80,90,100 and reconstitutes, room temperature is cooled to after being sufficiently stirred for.
From Figure 2 it can be seen that with the increase for reconstituting water temperature, the viscosity of nourishing medicinal granule is improved.Water temperature is at 60 DEG C, and viscosity is
271.6mPas, viscosity is 1939.5mPas at 80 DEG C, is changed greatly.After 80 DEG C, viscosity 1900~
2500mPas, change is little.This is due to the gelatinization point that nourishing medicinal granule is not up to when temperature is relatively low, the viscosity of nourishing medicinal granule
It is relatively low, and when temperature is more than 80 DEG C, instant gelatinization is more abundant, viscosity is higher.Therefore 80 DEG C or so water temperatures of selection are appropriate.
The difference of table 7 reconstitutes the sensory evaluation scores of electuary under water temperature
As can be seen from Table 7, electuary is sufficiently gelatinized after temperature reaches 80 DEG C, and this is more than 70 with starch in temperature
The theoretical consistent of gelatinization DEG C is begun to, and temperature is higher, the more early gelatinization of starch.Under the conditions of 85~90 DEG C, in 5~6s
There is the phenomenon that jumps of viscosity, and about 20 under the conditions of 70~80 DEG C after viscosity just begin to ramp up.Under this is due to higher temperature
The avalanche of starch crystal is accelerated.The instant being fully gelatinized produces the viscosity of special fragrance and flavour, now nourishing medicinal granule
Higher, the index such as mouthfeel reaches preferable level.
Influence of the 3.3 rock sugar additions to electuary
Black fungus Ultramicro-powder and degreasing black bean powder proportioning 5: 3 are chosen, rock sugar mass fraction is 30,35,40,45,50%, is taken
Sample 5g is separately added into 50ml90 DEG C of water and reconstituted, room temperature is cooled to after being sufficiently stirred in 100ml beakers.
As seen from Figure 3, with the increase of rock sugar addition, the viscosity of nourishing medicinal granule has declined.Reason is rock sugar conduct
Small molecule plays the role of similar hydrone, there is certain diluting effect to starch molecular chain, has delayed the migration of starch molecular chain
Rate, or with sugar infiltration and enter during starch gelatinization inside starch granules, multiple hydroxyls with starch molecule are mutual
Effect, hinders the water swelling of starch, so that viscosity during gelatinization declines [8].The viscosity that control group is not added with rock sugar is
3200mPas, when rock sugar mass fraction is 50%, viscosity is 1367mPas.As can be seen here, with charge ratio and reconstituting water temperature
Compare, rock sugar addition there are some influences to nourishing medicinal granule viscosity.
The sensory evaluation scores of electuary under the different rock sugar additions of table 8
As a kind of sweetener, increasing the addition of rock sugar within the specific limits will necessarily make the taste of nourishing medicinal granule become suitable
Mouthful.As seen from Table 8, rock sugar addition is mainly manifested on the flavour and mouthfeel of nourishing medicinal granule, is influenceed also little to color and luster, is selected ice
Sugared mass fraction is 35%, 40%, 45% appropriate.
The orthogonal experiment of 3.4 mixing formulas
According to single factor experiment result, the orthogonal test of the level of 3 factor 3 is carried out, using subjective appreciation and viscosity measurement to comment
Valency index, determines the optimum formula of instant.As shown in table 9, result of the test is as shown in table 10 for orthogonal test water-glass.By table
10 understand, each factor influences the order of conspicuousness to be B > A > C on instant.It is that influence instant is fully pasted to reconstitute water temperature
The key factor of change, and the local flavor of product can be improved;The addition of degreasing black bean powder mainly influences the color and luster of instant;Addition
Rock sugar is primarily to the sugariness of increase instant, little to viscosity.Viscosity mainly influences the flavour of nourishing medicinal granule, enters
And organoleptic quality is affected.Viscosity is not that the higher the better, and when viscosity is 2178mPas, sensory evaluation scores are most
Up to 90 points.By the synthesis result of subjective appreciation and viscosity measurement, the best of breed for determining instant is A2B3C3, i.e., black wood
The proportioning of ear powder and black bean powder is 5: 3, and it is 90 DEG C to reconstitute water temperature, and the addition mass fraction of rock sugar is 40%.By this combination production
Product carry out subjective appreciation again, and total score is 90.5 points.
The orthogonal array of table 9
The orthogonal experiments of table 10
The measure of the instant index of 3.5 electuaries
By instant (proportioning of best of breed, i.e. black fungus powder and degreasing black bean powder is 5: 3, reconstitutes water temperature for 90 DEG C,
The addition mass fraction of rock sugar is 40%) to do comparative analysis, the instant capacity index determining result such as institute of table 11 with commercially available black sesame powder
Show.
The black fungus super-micro instant instant of table 11 and commercially available black sesame powder instant capacity Indexes Comparison
The solubility of instant is 94.31g/ (100g), and black sesame powder is 95.78 (g/100g), and the two is very close;It is instant
The wetability of electuary is 120.0s, and black sesame powder is 95.5s, and the two is more or less the same;The dispersiveness of instant is 240.0s, sesame
Powder is 112.5s, and the two has the difference of jitter time, it may be possible to which the granularity of finished product instant is not small caused enough.It is molten by each index
Xie Du accounts for 40%, wettability and accounts for the weight analysis that 30%, dispersiveness accounts for 30%, and synthesis thinks, the instant capacity of finished product instant
Overall target does not have significant difference with commercially available black sesame powder, therefore can be edible as a kind of convenient instant electuary.