CN104825361B - A kind of natural shampoo containing Tsubaki-saponin - Google Patents
A kind of natural shampoo containing Tsubaki-saponin Download PDFInfo
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- CN104825361B CN104825361B CN201510231144.2A CN201510231144A CN104825361B CN 104825361 B CN104825361 B CN 104825361B CN 201510231144 A CN201510231144 A CN 201510231144A CN 104825361 B CN104825361 B CN 104825361B
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- tsubaki
- saponin
- solid
- liquid ratio
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Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a kind of natural shampoo containing Tsubaki-saponin and preparation method thereof, with wheat leaf, blue or green tea, rosemary, picric acid mould, ginger, radix pseudostellariae, radix scutellariae, tansy, capsicum, the extracted form natural plant such as headdress flower Japanese Stephania Root composition is used as basic function composition, Tsubaki-saponin, sapindoside, otoginsenoside, alginic acid etc. is used as emulsifying agent and foam improver, wild tea oil, lactic acid, lactylate salt, the security elements such as sodium chloride develop into a kind of natural shampoo, there is good nutrition to scalp, promote blood circulation, conditioning, wetting, antibacterial (including cause the chlosma of scurf）, anti-inflammatory, the reduction effect such as excitant, there is good cleaning, anti-dandruff, antipruritic, Anti-hair loss, sun-proof, nutrition, hair care, dark hair etc. to act on to hair.
Description
Technical field
The invention belongs to bath article field, and in particular to a kind of natural shampoo and its preparation side containing Tsubaki-saponin
Method.
Background technology
Shampoo is the daily chemical product that people are commonly used, but it is original that used shampoo, which is essentially chemical synthesis,
Material, washes away the sebum of its protective effect on scalp, causes dry scalp easily by the infection of dermatophyte so as to produce dandruff, also
Hair is dried up, some even have to scalp and hair-care the generation such as certain stimulation, sensitization, damage allergy, itch, dandruff etc. no
Good influence, the addition such as nipalgins of some chemical synthesis preservatives be it is generally acknowledged have carcinogenesis, allow people to day
Fear is felt in the use of change deeply, and scalp, hair to be made to dry, chap, damage under the radiation of solar ultraviolet etc. bad to cash,
Therefore welcome deeply by enterprise and consumer using the daily chemical products that plant, agricultural byproducts are developed as raw material, therefore the present invention
Also a safe, green, natural shampoo is developed as original intention, not only with good protection, the effect of nutrition scalp also
There are good anti-dandruff, antipruritic, Anti-hair loss, hair care, profit hair etc..
The content of the invention
It is an object of the invention to provide a kind of natural shampoo containing Tsubaki-saponin and preparation method thereof, with wheat leaf
The extracted form natural plant compositions such as son, blue or green tea, rosemary, picric acid mould, ginger, radix pseudostellariae, radix scutellariae, tansy, capsicum, headdress flower Japanese Stephania Root
As basic function composition, Tsubaki-saponin, sapindoside, otoginsenoside, alginic acid etc. are as emulsifying agent and foam improver, wild tea
The security elements such as oil, lactic acid, lactylate salt, sodium chloride develop into a kind of natural shampoo, have good nutrition to scalp, promote blood
Circulation, conditioning, wetting, antibacterial (include the chlosma of cause scurf）, anti-inflammatory, the reduction effect such as excitant, have very well to hair
Clean, anti-dandruff, antipruritic, Anti-hair loss, sun-proof, profit hair, nutrition, hair care, dark hair etc. are acted on.
To achieve the above object, the technical solution adopted by the present invention is：
A kind of natural shampoo containing Tsubaki-saponin, primary raw material is based on following parts by weight：Wild tea oil 5-10 parts, it is small
4-8 parts of wheat leaf, blue or green 4-8 parts of tea, 3-8 parts of Tsubaki-saponin, 3-5 parts of rosemary, 2-5 parts of sapindoside, otoginsenoside 2-5
Part, 1-3 parts of radix pseudostellariae, 1-3 parts of picric acid mould, 1-5 parts of ginger, 1-3 parts of radix scutellariae, 1-3 parts of tansy, 0.1-0.5 parts of headdress flower Japanese Stephania Root,
1-3 parts of lactic acid, 1-3 parts of pesudotsuga taxifolia, 1-3 parts of lactylate salt, 0.5-1 parts of sodium alginate, 0.5-1 parts of capsicum, sodium chloride 1.5-2.5
Part.
Preparation method comprises the following steps：
1）Wheat leaf and tansy are extracted with wild tea oil, leaching liquor 1 is obtained；
2）By radix pseudostellariae boiling distillation flooding, radix pseudostellariae Aqueous extracts are obtained；Filter residue is extracted with wild tea oil, obtains leaching liquor
2；
3）By picric acid mould, radix scutellariae, the Aqueous extracts of radix pseudostellariae, ginger juice, and blue or green tea, rosemary, capsicum, pesudotsuga taxifolia, headdress flower thousand
The alcohol extract mixing of golden rattan, is heated to 75 DEG C, adds leaching liquor 1 and leaching liquor 2, and 70 DEG C of constant temperature adds Tsubaki-saponin, soapberry
Saponin(e and otoginsenoside, stirring and emulsifying 20min are cooled to 60 DEG C, add sodium alginate, lactic acid, and pH=6- is adjusted with lactylate salt
7, adjust viscosity with sodium chloride.
Step 1）By the wheat leaf of drying and crushing and fresh tansy, 5d is extracted in tea oil out of office, is filtered.
Step 2）By the radix pseudostellariae of drying and crushing boiling distillation flooding 1.5h, solid-liquid ratio 1：10, filtering, concentrated by rotary evaporation；
Filter residue carries out normal temperature extraction 5d with wild tea oil, and solid-liquid ratio is 1:6, filtering.
It is prepared by picric acid mould Aqueous extracts：By the picric acid mould of drying and crushing, 30min, solid-liquid ratio 1 are extracted with boiling distilled water:10, subtract
Press suction filtration；
It is prepared by radix scutellariae Aqueous extracts：Radix scutellariae through drying, crush, 60 DEG C of distilled water ultrasonic extraction 1.5h, solid-liquid ratio is 1:10, mistake
Filter, concentrated by rotary evaporation.
It is prepared by ginger juice：First using method of squeezing the juice, then carry out decompression suction filtration.
It is prepared by blue or green tea alcohol extract：80 DEG C of the green grass or young crops tea 40wt.% ethanol solutions of drying for being ground into 20-40 mesh are extracted
30min, solid-liquid ratio is 1:10, it is filtered under diminished pressure, revolving reclaims ethanol；
It is prepared by pesudotsuga taxifolia alcohol extract：Dry star-spangled banner pine needle 80 DEG C of extraction 5h of 45wt.% ethanol solutions, solid-liquid ratio is 1:
6, depressurize suction filtration；
It is prepared by capsicum alcohol extract：Capsicum is through drying, crushing, with 45wt.% alcohol solution dipping 3d, solid-liquid ratio 1:6, decompression
Suction filtration；
It is prepared by rosemary, headdress flower Japanese Stephania Root alcohol extract：It is dried and crushed into rosemary, the headdress flower Japanese Stephania Root 20wt.% of 10 mesh
60 DEG C of extraction 8h of ethanol solution, solid-liquid ratio 1:6, suction filtration is depressurized, revolving reclaims ethanol.
The preparation of Tsubaki-saponin：It will dry after the crushing of camellia cake, 3h is extracted with deionized water, temperature is 100 DEG C, solid-liquid ratio
1:6, filtering, concentrated by rotary evaporation；
The preparation of sapindoside：By the soapberry kind skin of drying and crushing, 2h is extracted with deionized water, temperature is 100 DEG C,
Solid-liquid ratio is 1:10, filtering, concentrated by rotary evaporation；
The preparation of otoginsenoside：Buckeye seed extracts 3.5h through drying, crushing with deionized water, and temperature is 100 DEG C,
Solid-liquid ratio is 1:10, filtering, concentrated by rotary evaporation.
The component such as wild tea oil abundant unsaturated oleic acid, linoleic acid rises in the natural shampoo containing Tsubaki-saponin of the present invention
To moisturizing, anti-irritant, anti-allergic effects, squalene therein can well extract wheat leaf, tansy with anti-inflammatory and antibacterial
In have antibacterial, anti-oxidant, anti-corrosion, Anti-hair loss and stimulate natural on-off cycles of hair growth component, have to its extract on scalp, hair well
Promote the effect of oozing；Tsubaki-saponin is pentacyclic triterpene saponins, and HLB value is 16, has emulsification well, scattered, washability, can strengthen
The immunocompetence of scalp, while have good anti-skin pathomycete, anti-inflammatory, antisepsis, reaches hair washing, anti-dandruff, antipruritic
Effect；Containing compositions such as Tea Polyphenols, free amino acid, theophylline, caffeines in blue or green tea, Tea Polyphenols not only makes anti-oxidant well
Agent, which also has, absorbs ultraviolet, sterilization, the effect of anti-inflammatory suppression Achorion schoenleini, so having good astriction, nutrition hair to scalp
Capsule, hair care（Protect hair follicle）, dark hair effect, have good antioxidation in itself to shampoo；Carnosic acid in rosemary,
Composition the has antibacterial such as carnosol, Rosmarinic acid, ursolic acid, pinane be dilute, anti-inflammatory, anti-corrosion, it is anti-oxidant, absorb ultraviolet sun-proof etc., fan
Repeatedly fragrant fragrance is also used as the fragrance of the body note part of shampoo；Main component picric acid mould in picric acid mould have softening head
Skin, the effect for suppressing sebum secretion, there is extremely strong killing fungi, have to kill well to the fungi for causing scurf and make
With picric acid mould also has good antioxidation in itself to shampoo；The main component of radix pseudostellariae has polysaccharide, triterpenoid saponin, ring
The composition such as peptides, amino acid, fat-soluble, wherein amino acid can play the effect for reaching Anti-hair loss, triterpene soap with nutrition hair follicle
Glycosides has antivirus action that scalp, polysaccharide component can be protected to improve the immunity of scalp, also reaches protection scalp, hair
Effect；Radix scutellariae mainly contains scutelloside, neobaicalein, sitosterol, benzoic acid more composition, have in shampoo good antibacterial,
Anti-inflammatory, anti-inflammatory, antipruritic, absorption ultraviolet etc. reach skin care, can suppress the secretion of sebum, play corrosion-resistant work in itself to shampoo
With；Sapindoside in soapberry has good surface-active, the sebum of smegma can be removed well, with antibacterial
Property, especially dermatophyte has stronger killing action, so as to play a part of antipruritic, anti-dandruff etc.；Have in ginger certain gingerol,
The compositions such as zingiberone, gingerol, its permeability is stronger, has good Anti-hair loss, promoting blood circulation to stimulate hair tonic, anti-dandruff, neutralization super oxygen free
Base, sun-proof etc. are acted on, and have good anti-oxidant, antibacterial action in itself to shampoo；Aescin only do not help well emulsification,
Foam enhancing is acted on, and has good opsonic action to scalp and skin；Sodium alginate can play a part of emulsifying and thicken；Headdress flower thousand
The cepharanthine of golden rattan has the blood circulation of promotion scalp to stimulate hair tonic, also has opsonic action for scalp and hair-care, also there is certain
Antibiotic property；Yew foline in pesudotsuga taxifolia can increase DNA activity, be hair follicle cell propagation, can play growth-promoting hair, improve head
The quality and intensity of hair, anti-alopecia-stopping；Capsicum contains abundant piquancy component, can not only aid in suppressing bacterium in shampoo
Fungi, can be with relieving itching and removing dandruff.
The remarkable advantage of the present invention is：Mainly by the high composition of different botanical extract and natural safety, no
Only there are good nutrition, rush blood circulation, conditioning, wetting, antibacterial (to include causing the chlosma of scurf to scalp）, anti-inflammatory, reduction
Excitant etc. is acted on, and has good cleaning, anti-dandruff, antipruritic, Anti-hair loss, sun-proof, profit hair, nutrition, hair care, dark hair etc. to hair
Effect.
Embodiment
Embodiment 1
Primary raw material：Based on following parts by weight, wild 10 parts of tea oil, 4 parts of wheat leaf, blue or green 8 parts of tea, Tsubaki-saponin 6
Part, 3 parts of rosemary, 3 parts of sapindoside, 3 parts of otoginsenoside, 3 parts of radix pseudostellariae, 1 part of picric acid mould, 3 parts of ginger, 3 parts of radix scutellariae, Chinese mugwort
2 parts of chrysanthemum, 3 parts of pesudotsuga taxifolia, 0.3 part of headdress flower Japanese Stephania Root, 2 parts of lactic acid, 1 part of lactylate salt, 1 part of sodium alginate, 0.5 part of capsicum, chlorine
Change 0.5 part of sodium, essence（Cinnamic acid oil, laurel）In right amount.
Preparation technology：Wild tea oil, wheat leaf, tansy, second of extract of radix pseudostellariae be component 1, blue or green tea, rosemary,
Picric acid mould, radix scutellariae, pesudotsuga taxifolia, capsicum, headdress flower Japanese Stephania Root, radix pseudostellariae first time extract and ginger juice be component 2, Tsubaki-saponin,
Sapindoside, otoginsenoside are component 3, and component 2 is heated into 75 DEG C, component 1 is added in component 2, temperature is maintained at
More than 70 DEG C, component 3 is gradually added into, and is constantly stirred emulsification 20min, treats that temperature drops to 60 DEG C and adds sodium alginate, breast
Acid, adds sodium lactate regulation pH in 6-7.0 or so, sodium chloride regulation viscosity, and be stirred continuously successively addition cinnamic acid oil and the moon
Bay leaves oil.
Embodiment 2
Primary raw material：Based on following parts by weight, wild 5 parts of tea oil, 8 parts of wheat leaf, blue or green 8 parts of tea, Tsubaki-saponin 6
Part, 3 parts of rosemary, 3 parts of sapindoside, 3 parts of otoginsenoside, 3 parts of radix pseudostellariae, 3 parts of picric acid mould, 3 parts of ginger, 3 parts of radix scutellariae, Chinese mugwort
2 parts of chrysanthemum, 3 parts of pesudotsuga taxifolia, 0.3 part of headdress flower Japanese Stephania Root, 2 parts of lactic acid, 1 part of lactylate salt, 1 part of sodium alginate, 0.5 part of capsicum, chlorine
Change 0.5 part of sodium, essence（Cinnamic acid oil, laurel）In right amount.
Preparation technology：Wild tea oil, wheat leaf, tansy, second of extract of radix pseudostellariae be component 1, blue or green tea, rosemary,
Picric acid mould, radix scutellariae, pesudotsuga taxifolia, capsicum, headdress flower Japanese Stephania Root, radix pseudostellariae first time extract and ginger juice be component 2, Tsubaki-saponin,
Sapindoside, otoginsenoside are component 3, and component 2 is heated into 75 DEG C, component 1 is added in component 2, temperature is maintained at
More than 70 DEG C, component 3 is gradually added into, and is constantly stirred emulsification 20min, treats that temperature drops to 60 DEG C and adds sodium alginate, breast
Acid, adds sodium lactate regulation pH in 6-7.0 or so, sodium chloride regulation viscosity, and be stirred continuously successively addition cinnamic acid oil and the moon
Bay leaves oil.
Shampoo physical and chemical index
1st, pH is 6.5, the requirement of shampoo is met between 4.0 ~ 8.5, the structure of shampoo is finer and smoother.
2nd, room temperature is returned in -5 DEG C ~ -15 DEG C 24h, room temperature is returned to after 40 DEG C of 24h without water-oil separating, illustrate tool
There is good stability cold-resistant, heat-resisting.
3rd, the sun-proof ability of shampoo is determined：Method uses SPF vitro assays, i.e., using the instrument of SPF external tests
Equipment is directly determined, and measurement result shows that the spf value of case 1 and case 2 can reach 10,8 respectively, illustrates have necessarily
Anti-sunlight function, has certain effect using the shampoo of the present invention for sun-proof, the reduction hair damage of hair.
4th, application method is, shampoo is put in hair and carries out light smear to having and stops 2 ~ 5 minutes after certain foam, it
It is rinsed afterwards with water.There is more oil phase in case 1, be relatively adapted to the use of dry hair people, while this formula is also relatively adapted to
The people of mixed type hair quality uses；Containing more suppression sebum secretion so being more suited to the use of oily hair in case 2.
5th, spumescence
It is measured, and is compareed with daily Pantene shampoo using Roche foam meter, as a result such as table 1, is as a result represented
There is this product higher foaming capacity and its foam to have higher stability.
The shampoo foamability of table 1 and Stability Determination result
6th, antibacterial experiment in vitro
Assay method, it is that disinfectant acts on mould, Epidermophvton that experimental group, which is that two kinds of natural shampoo are diluted after 10 times,
The experiment bacterium solution of tinea bacterium, samples and inoculation is poured into agar, control group does same after then diluting 10 times with Pantene shampoo
Operation, and 15d is cultivated under the conditions of 37 DEG C together, and observe result.As a result such as table 2, as a result show, natural hair washing of the invention
Dew have well suppress and bactericidal effect, illustrate shampoo can kill well with suppress dermatophyte and play protect skin,
The generation of scurf is reduced, particularly with several natural plants saponin(es, radix scutellariae, rosemary, ginger, tansy etc. for main active component
Play an important role.
The bactericidal effect of the shampoo of table 2
7th, shampoo using effect is investigated
It is continuously on probation one month by 80 volunteers, examine the using effect of shampoo each side.Test event scores
Standard is very satisfied 5 points, is satisfied with 4 points, general 3 points, is unsatisfied with 2 points, very dissatisfied 1 point, the results are shown in Table 3.Tested aspiration
Person represents to feel quite pleased to the shampoo of the present invention.
The shampoo using effect of table 3
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification, should all belong to the covering scope of the present invention.
Claims (7)
1. a kind of natural shampoo containing Tsubaki-saponin, it is characterised in that：Primary raw material is based on following parts by weight：Wild tea oil
5-10 parts, 4-8 parts of wheat leaf, blue or green 4-8 parts of tea, 3-8 parts of Tsubaki-saponin, 3-5 parts of rosemary, sapindoside 2-5
Part, 2-5 parts of otoginsenoside, 1-3 parts of radix pseudostellariae, 1-3 parts of picric acid mould, 1-5 parts of ginger, 1-3 parts of radix scutellariae, 1-3 parts of tansy,
0.1-0.5 parts of headdress flower Japanese Stephania Root, 1-3 parts of lactic acid, 1-3 parts of pesudotsuga taxifolia, 1-3 parts of lactylate salt, 0.5-1 parts of sodium alginate,
0.5-1 parts of capsicum, 1.5-2.5 parts of sodium chloride；
The preparation method of the described natural shampoo containing Tsubaki-saponin, comprises the following steps：
1）Wheat leaf and tansy are extracted with wild tea oil, leaching liquor 1 is obtained；
2）By radix pseudostellariae boiling distillation flooding, radix pseudostellariae Aqueous extracts are obtained；Filter residue is extracted with wild tea oil, obtains leaching liquor 2；
3）By picric acid mould, radix scutellariae, the Aqueous extracts of radix pseudostellariae, ginger juice, and blue or green tea, rosemary, capsicum, pesudotsuga taxifolia, headdress flower Japanese Stephania Root
Alcohol extract mixing, be heated to 75 DEG C, add leaching liquor 1 and leaching liquor 2,70 DEG C of constant temperature adds Tsubaki-saponin, soapberry soap
Glycosides and otoginsenoside, stirring and emulsifying 20min are cooled to 60 DEG C, add sodium alginate, lactic acid, and pH=6-7 is adjusted with lactylate salt,
Viscosity is adjusted with sodium chloride.
2. a kind of natural shampoo containing Tsubaki-saponin according to claim 1, it is characterised in that：Step 1）By drying
5d is extracted in the wheat leaf of crushing and fresh tansy, tea oil out of office, is filtered.
3. a kind of natural shampoo containing Tsubaki-saponin according to claim 1, it is characterised in that：Step 2）By drying
The radix pseudostellariae of crushing boiling distillation flooding 1.5h, solid-liquid ratio 1：10, filtering, concentrated by rotary evaporation；Filter residue carries out normal temperature with wild tea oil
5d is extracted, solid-liquid ratio is 1:6, filtering.
4. a kind of natural shampoo containing Tsubaki-saponin according to claim 1, it is characterised in that：Picric acid mould Aqueous extracts
Prepare：By the picric acid mould of drying and crushing, 30min, solid-liquid ratio 1 are extracted with boiling distilled water:10, depressurize suction filtration；
It is prepared by radix scutellariae Aqueous extracts：Radix scutellariae through drying, crush, 60 DEG C of distilled water ultrasonic extraction 1.5h, solid-liquid ratio is 1:10, filtering,
Concentrated by rotary evaporation.
5. a kind of natural shampoo containing Tsubaki-saponin according to claim 1, it is characterised in that：It is prepared by ginger juice：First adopt
With the method for squeezing the juice, then carry out decompression suction filtration.
6. a kind of natural shampoo containing Tsubaki-saponin according to claim 1, it is characterised in that：Blue or green tea alcohol extract system
It is standby：80 DEG C of the green grass or young crops tea 40wt.% ethanol solutions of drying for being ground into 20-40 mesh are extracted into 30min, solid-liquid ratio is 1:10, decompression
Filtering, revolving reclaims ethanol；
It is prepared by pesudotsuga taxifolia alcohol extract：Dry star-spangled banner pine needle 80 DEG C of extraction 5h of 45wt.% ethanol solutions, solid-liquid ratio is 1:6, subtract
Press suction filtration；
It is prepared by capsicum alcohol extract：Capsicum is through drying, crushing, with 45wt.% alcohol solution dipping 3d, solid-liquid ratio 1:6, decompression is taken out
Filter；
It is prepared by rosemary, headdress flower Japanese Stephania Root alcohol extract：It is dried and crushed into rosemary, the headdress flower Japanese Stephania Root 20wt.% second of 10 mesh
60 DEG C of extraction 8h of alcoholic solution, solid-liquid ratio 1:6, suction filtration is depressurized, revolving reclaims ethanol.
7. a kind of natural shampoo containing Tsubaki-saponin according to claim 1, it is characterised in that：The system of Tsubaki-saponin
It is standby：It will dry after the crushing of camellia cake, 3h is extracted with deionized water, temperature is 100 DEG C, solid-liquid ratio 1:6, filtering, concentrated by rotary evaporation；
The preparation of sapindoside：By the soapberry kind skin of drying and crushing, 2h is extracted with deionized water, temperature is 100 DEG C, feed liquid
Than for 1:10, filtering, concentrated by rotary evaporation；
The preparation of otoginsenoside：Buckeye seed extracts 3.5h through drying, crushing with deionized water, and temperature is 100 DEG C, feed liquid
Than for 1:10, filtering, concentrated by rotary evaporation.
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| JP2017066071A (en) * | 2015-09-29 | 2017-04-06 | 株式会社マンダム | Cosmetic composition |
| CN105534803A (en) * | 2016-01-08 | 2016-05-04 | 张秀丽 | Moistening and dandruff removing shampoo and preparation method thereof |
| CN107259274A (en) * | 2017-07-28 | 2017-10-20 | 张可池 | A kind of Chinese phoenix's eye fruit compound beverage |
| CN107802547A (en) * | 2017-12-06 | 2018-03-16 | 湖南省雅迭香科技有限公司 | A kind of rosemary shampoo |
| US20230201097A1 (en) * | 2020-05-28 | 2023-06-29 | Lg Household & Health Care Ltd. | Composition for inhibiting hair graying, and use thereof |
| CN113181165B (en) * | 2021-05-25 | 2022-11-01 | 浙江大学医学院附属邵逸夫医院 | Application of alpine or its composition in the preparation of medicine or preparation for treating hair loss |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08199190A (en) * | 1995-01-23 | 1996-08-06 | Chuo Aerosol Kagaku Kk | Liquid composition for producing foam-containing lump |
| CN104042461A (en) * | 2013-03-12 | 2014-09-17 | 长沙理工大学 | Natural plant shampoo employing camellia seed products as base-material and preparation method thereof |
| CN103479539B (en) * | 2013-08-16 | 2016-01-27 | 广州环亚化妆品科技有限公司 | A kind of shampoo containing saponin and natural thickener |
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