CN104560128B - Vertical electrostatic coalescer sledge dressization testing apparatus and method - Google Patents
Vertical electrostatic coalescer sledge dressization testing apparatus and method Download PDFInfo
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- 238000012360 testing method Methods 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title claims abstract description 23
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- 230000005684 electric field Effects 0.000 claims abstract description 33
- 238000000926 separation method Methods 0.000 claims abstract description 30
- 238000012545 processing Methods 0.000 claims abstract description 23
- 239000007762 w/o emulsion Substances 0.000 claims abstract description 23
- 230000000694 effects Effects 0.000 claims abstract description 22
- 238000004821 distillation Methods 0.000 claims abstract description 4
- 238000009434 installation Methods 0.000 claims abstract description 3
- 230000005484 gravity Effects 0.000 claims description 42
- 230000008569 process Effects 0.000 claims description 13
- 238000013461 design Methods 0.000 claims description 10
- 239000002569 water oil cream Substances 0.000 claims description 9
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- 235000013336 milk Nutrition 0.000 claims 2
- 238000012544 monitoring process Methods 0.000 claims 1
- 239000010935 stainless steel Substances 0.000 claims 1
- 238000004581 coalescence Methods 0.000 abstract description 15
- 238000005457 optimization Methods 0.000 abstract description 3
- 239000003921 oil Substances 0.000 description 58
- 238000005070 sampling Methods 0.000 description 28
- 239000000839 emulsion Substances 0.000 description 16
- 230000018044 dehydration Effects 0.000 description 8
- 238000006297 dehydration reaction Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- 229910000831 Steel Inorganic materials 0.000 description 6
- 239000010959 steel Substances 0.000 description 6
- 239000010779 crude oil Substances 0.000 description 4
- 230000005611 electricity Effects 0.000 description 4
- 238000010008 shearing Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 238000000429 assembly Methods 0.000 description 2
- 230000000712 assembly Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000013528 artificial neural network Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 230000005686 electrostatic field Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
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- 238000011160 research Methods 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G33/00—Dewatering or demulsification of hydrocarbon oils
- C10G33/02—Dewatering or demulsification of hydrocarbon oils with electrical or magnetic means
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/06—Separation of liquids from each other by electricity
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- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
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Abstract
立式静电聚结器橇装化试验装置及方法,可以在油田现场进行试验,能够对立式静电聚结器的工作性能进行评价,对设备处理量和电场参数进行优选。所有设备均固定于方便运输的橇装底盘上,主要包括供电设备,聚结设备和分离设备等。供电设备为控制柜和变压器,能够为立式静电聚结器提供高电压,促使油包水乳状液中的水滴发生聚结;利用旁通闸阀和管道泵等调节立式静电聚结器和油水分离器的处理量,通过蒸馏法测量聚结器入口、出口和分离器油出口处的含水率以对比分析试验系统的分离效果,并据此优选设备处理量和电场参数。采用本发明的橇装化设备,具有运输方便,安装快捷的优点,能够测试立式静电聚结器的工作性能,有助于设备的选型和运行参数优化。
The skid-mounted test device and method of the vertical electrostatic coalescer can be tested in the oil field, can evaluate the working performance of the vertical electrostatic coalescer, and optimize the equipment processing capacity and electric field parameters. All equipment is fixed on a skid-mounted chassis for easy transportation, mainly including power supply equipment, coalescing equipment and separation equipment. The power supply equipment is a control cabinet and a transformer, which can provide high voltage for the vertical electrostatic coalescer to promote the coalescence of water droplets in the water-in-oil emulsion; use bypass gate valves and pipeline pumps to adjust the vertical electrostatic coalescer and oil-water For the capacity of the separator, measure the water content at the inlet and outlet of the coalescer and the oil outlet of the separator by distillation to compare and analyze the separation effect of the test system, and optimize the capacity and electric field parameters of the equipment accordingly. The skid-mounted equipment of the present invention has the advantages of convenient transportation and quick installation, can test the working performance of the vertical electrostatic coalescer, and is helpful for equipment selection and operation parameter optimization.
Description
技术领域technical field
本发明涉及一种立式静电聚结器橇装化试验装置及方法,用于模拟立式静电聚结器强化脱水的工艺流程,属于于油气集输系统油田采出液脱水工艺。The invention relates to a skid-mounted test device and method for a vertical electrostatic coalescer, which is used for simulating the process flow of the enhanced dehydration of the vertical electrostatic coalescer, and belongs to the dehydration process of oilfield produced fluid in an oil and gas gathering and transportation system.
背景技术Background technique
油包水乳状液广泛存在于石油、化工等工业生产过程中,通常采用化学和物理方法加速水滴界面膜的薄化和破裂从而提高聚结效率。静电聚结技术是原油脱水过程中常用的方法之一,其基本原理是对乳状液施加高强电场,增加分散水滴的碰撞和聚集,促进水滴聚结,加速油水分离。Water-in-oil emulsions widely exist in industrial production processes such as petroleum and chemical industry. Chemical and physical methods are usually used to accelerate the thinning and rupture of the interfacial film of water droplets to improve the coalescence efficiency. Electrostatic coalescence technology is one of the commonly used methods in the crude oil dehydration process. Its basic principle is to apply a high-strength electric field to the emulsion to increase the collision and aggregation of dispersed water droplets, promote the coalescence of water droplets, and accelerate the separation of oil and water.
我国绝大部分陆上油田的联合站目前使用的是传统卧式电脱水器,但随着大量三采助剂的使用,形成稳定的油包水乳状液,导致含水率增加,破乳困难,聚合物容易在电脱水器内积聚,并有可能引起电场强度降低、脱水电流过大或者“垮电场”现象,对油田生产造成了极大影响。立式静电聚结器是为应对目前这种情况而开发出来的一种新型高效的乳状液聚结设备,具有在保证油水高效分离的前提下大幅缩减设备体积的优点,节省成本,降低能耗,提高安全性能,适应当今油田生产开发的需要。美国专利US6136174公开了一种原油脱水用静电聚结器(CEC),其电极部分是由绝缘电极和金属电极以立式同轴圆筒的形式交替排列。中国专利200710015911.1(授权专利公告号CN101173182A)公开了一种原油乳状液静电脱水器,其聚结段安装在电脱水器上部,电极部分也是由绝缘电极和金属电极以立式同轴圆筒的形式交替排列。这种形式的电极充分利用了空间,具有结构紧凑,占地面积小等优点。目前,立式静电聚结器大多在使用现场安装,之后再进行调试以确定工作参数。但是由于不同区块所形成的油包水乳状液物化性质有所不同,能够对水滴实现有效电聚结的电场强度、电场频率和电场波形等也有所不同,立式静电聚结器是否适应现场处理环境也未知,有可能造成设备选型不合理或者无法正常工作,浪费投资。因此在安装立式静电聚结器之前评价油包水乳状液通电后的聚结效果,优选电场参数,对于静电聚结器的设计和变压设备的购置具有重要意义。中国专利201320477801.8(授权专利公告号CN203474723U)公开了一种两级自动电脱试验装置,通过剪切油水混合装置将试验原油剪切成符合试验要求的油水乳状液然后注入脱水脱盐罐进行加电脱水试验,但是油包水乳状液的性质除了与剪切强度还与处理环境,管路系统等有关,所以室内电脱试验无法真实还原现场的处理环境,所得到的试验结果也会受到影响。上述设备或因工业产品,体积较大,加工成本较高,运输安装不方便,不能方便的到现场进行试验,或因属于室内实验的,难以完全模拟现场的处理条件,得到的结果也不具有代表性。Most of the combined stations of onshore oilfields in my country currently use traditional horizontal electric dehydrators, but with the use of a large number of tertiary production aids, a stable water-in-oil emulsion is formed, resulting in an increase in water content and difficulty in demulsification. Polymers are easy to accumulate in the electric dehydrator, which may cause a decrease in electric field strength, excessive dehydration current or "collapse electric field", which has a great impact on oil field production. The vertical electrostatic coalescer is a new type of high-efficiency emulsion coalescing equipment developed to cope with the current situation. It has the advantages of greatly reducing the volume of the equipment on the premise of ensuring efficient separation of oil and water, saving costs and reducing energy consumption. , improve safety performance, and adapt to the needs of today's oilfield production and development. US Patent No. 6,136,174 discloses an electrostatic coalescer (CEC) for crude oil dehydration. The electrode part is alternately arranged in the form of vertical coaxial cylinders with insulating electrodes and metal electrodes. Chinese patent 200710015911.1 (authorized patent announcement number CN101173182A) discloses a crude oil emulsion electrostatic dehydrator, the coalescing section is installed on the upper part of the electric dehydrator, and the electrode part is also composed of an insulating electrode and a metal electrode in the form of a vertical coaxial cylinder Alternately. This form of electrode makes full use of the space and has the advantages of compact structure and small footprint. At present, most of the vertical electrostatic coalescers are installed on site, and then debugged to determine the working parameters. However, since the physical and chemical properties of water-in-oil emulsions formed in different blocks are different, the electric field strength, electric field frequency and electric field waveform that can achieve effective electric coalescence of water droplets are also different. Whether the vertical electrostatic coalescer can adapt to the field The processing environment is also unknown, which may result in unreasonable equipment selection or failure to work normally, wasting investment. Therefore, before installing the vertical electrostatic coalescer, it is of great significance to evaluate the coalescence effect of the water-in-oil emulsion after electrification and optimize the electric field parameters for the design of the electrostatic coalescer and the purchase of transformer equipment. Chinese patent 201320477801.8 (authorized patent announcement number CN203474723U) discloses a two-stage automatic electric dehydration test device, which cuts the test crude oil into an oil-water emulsion that meets the test requirements through a shearing oil-water mixing device, and then injects it into a dehydration and desalination tank for dehydration with electricity However, the properties of the water-in-oil emulsion are not only related to the shear strength but also related to the processing environment and piping system, so the indoor electrolysis test cannot truly restore the on-site processing environment, and the obtained test results will also be affected. The above-mentioned equipment may be industrial products with large volume, high processing cost, inconvenient transportation and installation, and cannot be conveniently carried out on-site for testing, or because it is an indoor experiment, it is difficult to completely simulate the processing conditions on site, and the results obtained are also inconsequential. representative.
因此有必要在现场利用立式静电聚结器进行试验,以确定设备的适用性并优选工艺参数,使聚结器的设计和设备的选型更具有针对性。鉴于以上原因,有必要发明一套可以在油田现场使用,能够模拟实际生产工艺流程,对立式静电聚结器聚结效果进行评价,对设备工作参数进行优选的橇装化试验系统,为立式静电聚结器的设计和运行提供依据,使得设备设计更合理,使用更高效。Therefore, it is necessary to use the vertical electrostatic coalescer to conduct tests on site to determine the applicability of the equipment and optimize the process parameters, so that the design of the coalescer and the selection of equipment are more targeted. In view of the above reasons, it is necessary to invent a skid-mounted test system that can be used in the oil field, can simulate the actual production process, evaluate the coalescence effect of the vertical electrostatic coalescer, and optimize the operating parameters of the equipment. It provides a basis for the design and operation of the type electrostatic coalescer, making the equipment design more reasonable and the use more efficient.
发明内容Contents of the invention
本发明目的是提供一种立式静电聚结器橇装化试验装置及方法,解决油包水乳状液处理环境不同,室内试验无法完全再现等问题,并且能够方便快捷地应用于油田现场,对立式静电聚结器处理效果和工作参数进行评价及优选。利用立式静电聚结器橇装化试验装置得到的结果能够为工业级设备的设计提供参考依据。The purpose of the present invention is to provide a skid-mounted test device and method for a vertical electrostatic coalescer, which solves the problems of different treatment environments for water-in-oil emulsions and the inability to completely reproduce indoor tests, and can be conveniently and quickly applied to oil field sites. The treatment effect and working parameters of the vertical electrostatic coalescer were evaluated and optimized. The results obtained by using the vertical electrostatic coalescer skid-mounted test device can provide a reference for the design of industrial-grade equipment.
一种立式静电聚结器橇装化试验装置,其特征在于包括入口管路、出口管路、流量计、立式静电聚结器、重力式分离器、水出口流量计,油出口流量计,管道泵,变压器,变压器支架,橇装底盘;A skid-mounted test device for a vertical electrostatic coalescer, characterized in that it includes an inlet pipeline, an outlet pipeline, a flow meter, a vertical electrostatic coalescer, a gravity separator, a water outlet flowmeter, and an oil outlet flowmeter , pipeline pumps, transformers, transformer brackets, skid-mounted chassis;
所述的立式静电聚结器,重力式分离器和变压器均安装在橇装底盘上,所述扶梯是在现场安装到变压器支架上;The vertical electrostatic coalescer, the gravity separator and the transformer are all installed on the skid-mounted chassis, and the escalator is installed on the transformer support on site;
所述的入口管路通过三通分别连接闸阀1和旁通闸阀2,所述的闸阀1和旁通闸阀2组成控制阀组用于控制入口管路的流量;所述的闸阀1前端连接有计量模块;所述计量模块由主管路和带球阀的旁通管路组成,其中主管路依次由球阀、过滤器、压力表、流量计、后端球阀组成;The inlet pipeline is respectively connected to the gate valve 1 and the bypass gate valve 2 through a tee, and the gate valve 1 and the bypass gate valve 2 form a control valve group for controlling the flow of the inlet pipeline; the front end of the gate valve 1 is connected with A metering module; the metering module is composed of a main pipeline and a bypass pipeline with a ball valve, wherein the main pipeline is sequentially composed of a ball valve, a filter, a pressure gauge, a flow meter, and a rear-end ball valve;
在所述计量模块的前端连接立式静电聚结器,所述立式静电聚结器的入口端和出口端分别设有入口取样口和出口取样口,所述的立式静电聚结器与变压器连接,所述的立式静电聚结器的出口端通过三通分别与重力分离管路和旁通管路相连,其中重力分离管路上依次设有闸阀和重力式分离器;所述重力式分离器的出口端分为水出口和油出口,所述水出口和油出口分别设有水出口取样口和油出口取样口。所述水出口和油出口的前端分别连接有计量模块,所述计量模块均由带流量计的主管路和带球阀的旁通管路组成;所述水出口和油出口的计量模块的前端均通过单向阀连接至管道泵模块;A vertical electrostatic coalescer is connected to the front end of the metering module, and the inlet and outlet ports of the vertical electrostatic coalescer are respectively provided with an inlet sampling port and an outlet sampling port, and the vertical electrostatic coalescer is connected to the Transformer connection, the outlet end of the vertical electrostatic coalescer is connected to the gravity separation pipeline and the bypass pipeline through a tee, wherein the gravity separation pipeline is provided with a gate valve and a gravity separator in sequence; The outlet end of the separator is divided into a water outlet and an oil outlet, and the water outlet and the oil outlet are respectively provided with a water outlet sampling port and an oil outlet sampling port. The front ends of the water outlet and the oil outlet are respectively connected with metering modules, and the metering modules are composed of a main pipeline with a flow meter and a bypass pipeline with a ball valve; the front ends of the metering modules of the water outlet and the oil outlet are all Connected to the in-line pump module through a check valve;
所述的立式静电聚结器出口端的旁通管路依次通过闸阀2和单向阀与所述管道泵模块相连,所述的旁通闸阀1和闸阀2组成控制阀组用于控制重力式分离器的流量;The bypass pipeline at the outlet end of the vertical electrostatic coalescer is sequentially connected to the pipeline pump module through the gate valve 2 and the check valve, and the bypass gate valve 1 and the gate valve 2 form a control valve group for controlling the gravity type separator flow;
所述的与入口管路相连的旁通闸阀2另一端也与所述管道泵模块相连;The other end of the bypass gate valve 2 connected to the inlet pipeline is also connected to the pipeline pump module;
所述的管道泵模块由含管道泵的主管路和含调节阀的旁通管路组成,用于为整个系统提供动力,管道泵模块的出口端为出口管路。The pipeline pump module is composed of a main pipeline containing a pipeline pump and a bypass pipeline containing a regulating valve, which are used to provide power for the entire system, and the outlet end of the pipeline pump module is an outlet pipeline.
如果试验系统摩阻较大,乳状液无法正常流动可以通过管道泵提供动力,如果可以正常流动则不需要开泵只需走管道泵的旁通阀即可。If the frictional resistance of the test system is large and the emulsion cannot flow normally, the pipeline pump can be used to provide power. If it can flow normally, there is no need to turn on the pump, just use the bypass valve of the pipeline pump.
所述入口管路和出口管路的端口都带有不锈钢钢丝软管,可以通过法兰和变径与现场处理设备相连接。The ports of the inlet pipeline and the outlet pipeline are all equipped with stainless steel wire hoses, which can be connected with on-site processing equipment through flanges and variable diameters.
所述静电聚结器处理量为0~300m3/d(12.5m3/h),高度为2300mm,筒体外径300mm。所述重力式分离器的处理量为0~24m3/d(1m3/h),直径0.5m,长1600mm。通过旁通闸阀2可以调节立式静电聚结器的处理流量,而通过旁通闸阀1可以调节重力式分离器的处理流量。利用流量计、水出口流量计和油出口流量计可以精确计量立式静电聚结器和重力式分离器的处理流量。The processing capacity of the electrostatic coalescer is 0-300m 3 /d (12.5m 3 /h), the height is 2300mm, and the outer diameter of the cylinder is 300mm. The gravity separator has a processing capacity of 0-24m 3 /d (1m 3 /h), a diameter of 0.5m and a length of 1600mm. The treatment flow of the vertical electrostatic coalescer can be adjusted through the bypass gate valve 2, and the treatment flow of the gravity separator can be adjusted through the bypass gate valve 1. The treatment flow of vertical electrostatic coalescer and gravity separator can be accurately measured by flowmeter, water outlet flowmeter and oil outlet flowmeter.
所述的变压器和立式静电聚结器之间经由防爆钢丝软管和高压接线棒连接;在重力式分离器的周围有变压器支架设置在所述的橇装底盘上,所述的变压器安装在变压器支架上方,在变压器周围设有护栏,在橇装底盘上还安装有通向变压器的扶梯。The transformer and the vertical electrostatic coalescer are connected via an explosion-proof steel wire hose and a high-voltage wiring rod; a transformer bracket is arranged on the skid-mounted chassis around the gravity separator, and the transformer is installed on the Above the transformer support, a guardrail is provided around the transformer, and an escalator leading to the transformer is installed on the skid-mounted chassis.
本发明的工作过程为:通过货车将安装在橇装底盘上的立式静电聚结器试验系统运到油田现场后,利用入口管路和出口管路通过不锈钢钢丝软管,变径和法兰等与现场处理系统相连接,管道泵提供动力,以便乳状液能够通过试验系统。变压器放置在变压器支架上,并加装了护栏,保证安全。通过变压器产生高压电经过防爆钢丝软管和高压接线棒输入到立式静电聚结器中处理油包水乳状液。打开闸阀1和旁通闸阀2调节进入立式静电聚结器的油包水乳状液的流量,并通过流量计进行计量,当流量满足试验要求后即可以进行试验。通过控制柜调节输入电压并经变压器升压后输出至立式静电聚结器中,从而对油水乳状液施加高强电场,促使水滴发生聚结,加速油水分离。受占地面积的限制,重力式分离器的体积较小,当流经立式静电聚结器的油包水乳状液的流量较大超过重力式分离器的处理量时,可以通过控制旁通闸阀1的开度来调节进入重力式分离器的流量,同时通过水出口流量计和油出口流量计的测量值来得到重力式分离器的处理量。没有经过重力式分离器的油包水乳状液直接与水出口和油出口流出的水、油混合并经出口管路流到后续处理设备。由于试验系统流程紧凑,设备较多,摩阻较大,当现场分离系统内的压力无法保证油包水乳状液通过试验系统时,需要启动管道泵为试验系统提供动力。管道泵没有放到入口管路处是为了防止过度剪切油包水乳状液,增加分离的难度。试验过程中通过水出口取样口测量水中含油率,采用蒸馏的方法监测入口取样口,出口取样口和油出口取样口的含水率来分析试验系统的分离效果,并据此确定分离效果最优时立式静电聚结器和重力式分离器的处理量。同时可以通过控制柜调节输入波形,电压和频率等,以对不同电场参数下的分离效果进行评价,进而确定最优的电场参数,为设备设计和选型提供指导。The working process of the present invention is as follows: After the vertical electrostatic coalescer test system installed on the skid-mounted chassis is transported to the oilfield site by truck, the stainless steel wire hose, variable diameter and flange are used to pass through the inlet pipeline and outlet pipeline. etc. are connected to the on-site processing system, and the pipeline pump provides power so that the emulsion can pass through the test system. The transformer is placed on the transformer support, and a guardrail is installed to ensure safety. The high-voltage electricity generated by the transformer is input to the vertical electrostatic coalescer through the explosion-proof steel wire hose and the high-voltage wiring rod to process the water-in-oil emulsion. Open the gate valve 1 and the bypass gate valve 2 to adjust the flow of the water-in-oil emulsion entering the vertical electrostatic coalescer, and measure it through the flow meter. When the flow meets the test requirements, the test can be carried out. The input voltage is adjusted through the control cabinet and output to the vertical electrostatic coalescer after being boosted by the transformer, thereby applying a high-strength electric field to the oil-water emulsion to promote the coalescence of water droplets and accelerate the separation of oil and water. Due to the limitation of the floor area, the volume of the gravity separator is small. When the flow rate of the water-in-oil emulsion flowing through the vertical electrostatic coalescer exceeds the processing capacity of the gravity separator, the bypass can be controlled. The opening of the gate valve 1 is used to adjust the flow into the gravity separator, and at the same time, the processing capacity of the gravity separator is obtained through the measured values of the water outlet flowmeter and the oil outlet flowmeter. The water-in-oil emulsion that has not passed through the gravity separator is directly mixed with the water and oil flowing out of the water outlet and the oil outlet, and flows to the subsequent processing equipment through the outlet pipeline. Due to the compact flow of the test system, a large number of equipment, and high friction, when the pressure in the on-site separation system cannot ensure that the water-in-oil emulsion passes through the test system, it is necessary to start the pipeline pump to provide power for the test system. The pipeline pump is not placed in the inlet pipeline to prevent excessive shearing of the water-in-oil emulsion and increase the difficulty of separation. During the test, the oil content in the water is measured through the water outlet sampling port, and the water content of the inlet sampling port, outlet sampling port and oil outlet sampling port is monitored by distillation to analyze the separation effect of the test system, and the optimal separation effect is determined accordingly. Throughput of vertical electrostatic coalescers and gravity separators. At the same time, the input waveform, voltage and frequency can be adjusted through the control cabinet to evaluate the separation effect under different electric field parameters, and then determine the optimal electric field parameters to provide guidance for equipment design and selection.
本发明的基本原理是将试验装置通过不锈钢钢丝软管连入油田现场的生产系统中,油包水乳状液经过流量计后进入立式静电聚结器,利用可控硅自动调压或恒流源控制柜(与变压器20连接)调节输入电压并经变压器升压后输入到立式静电聚结器中对流经聚结器的油水乳状液施加高强电场,促使水滴发生聚结,加速油水分离。流经立式静电聚结器后的油包水乳状液一部分被分流,一部分进入重力式分离器进行重力沉降,分离出的油相、水相通过油出口和水出口排出,并与未经重力式分离器分离的油水乳状液混合,进入后续分离设备。采用静电聚结器入口、出口、分离器油出口处的含水率的变化来评价静电聚结器的聚结效果。The basic principle of the present invention is to connect the test device into the production system of the oilfield site through a stainless steel wire hose, and the water-in-oil emulsion enters the vertical electrostatic coalescer after passing through the flowmeter, and uses the silicon controlled silicon to automatically adjust the voltage or constant current The source control cabinet (connected to the transformer 20) adjusts the input voltage and after boosted by the transformer, it is input to the vertical electrostatic coalescer to apply a high-strength electric field to the oil-water emulsion flowing through the coalescer to promote the coalescence of water droplets and accelerate the separation of oil and water. Part of the water-in-oil emulsion flowing through the vertical electrostatic coalescer is diverted, and part of it enters the gravity separator for gravity sedimentation. The separated oil phase and water phase are discharged through the oil outlet and water outlet, and are separated from those without gravity. The oil-water emulsion separated by the type separator is mixed and enters the subsequent separation equipment. The coalescence effect of the electrostatic coalescer was evaluated by the change of water content at the inlet, outlet and oil outlet of the electrostatic coalescer.
本发明的有益效果是,所有的设备安装在橇装底盘上,结构紧凑,占地面积小,可以用货运汽车将设备运到油田进行现场试验;试验系统的入口和出口均配有法兰,可以通过不锈钢钢丝软管和变径等与油田现场工艺流程快速连接,不影响正常生产;管路系统包覆有保温层保证乳状液温度保持稳定;用立式静电聚结器入口、出口、分离器油出口处的含水率的变化来评价试验系统的处理效果;通过旁通闸阀可以控制立式静电聚结器和分离器的处理流量,即使聚结器处理量超过分离器处理量,也可通过闸阀分离使设备正常工作,进而可以确定设备最优的处理量,为设备设计和运行提供参数;控制柜和调压器结合可以提供多种波形,调节电压和频率,从而能够评价不同电场参数作用下系统的分离效果,为电场参数优选提供参考;在出口处安装管道泵,既能为试验系统提供动力又避免在入口处对油包水乳状液过度剪切;变压器放置于变压器支架上可以提高空间利用率,并且操作方便;护栏和扶梯能够保证操作时的安全。The beneficial effect of the present invention is that all the equipment is installed on the skid-mounted chassis, the structure is compact, and the occupied area is small, and the equipment can be transported to the oil field for on-site testing by truck; the inlet and outlet of the test system are equipped with flanges, It can be quickly connected to the oilfield on-site process through stainless steel wire hoses and variable diameters, without affecting normal production; the pipeline system is covered with an insulation layer to ensure that the temperature of the emulsion remains stable; the inlet, outlet, and separation of the vertical electrostatic coalescer are used The treatment effect of the test system can be evaluated by the change of water content at the oil outlet of the device; the treatment flow of the vertical electrostatic coalescer and separator can be controlled through the bypass gate valve, even if the treatment capacity of the coalescer exceeds the treatment capacity of the separator, it can The equipment can work normally by separating the gate valve, so that the optimal processing capacity of the equipment can be determined, and parameters can be provided for the design and operation of the equipment; the combination of the control cabinet and the voltage regulator can provide a variety of waveforms, adjust the voltage and frequency, and thus be able to evaluate different electric field parameters The separation effect of the system under the action provides a reference for the optimization of electric field parameters; installing a pipeline pump at the outlet can not only provide power for the test system but also avoid excessive shearing of the water-in-oil emulsion at the inlet; the transformer can be placed on the transformer support Improve space utilization and facilitate operation; guardrails and escalators can ensure safety during operation.
附图说明:Description of drawings:
图1是本发明的流程图;Fig. 1 is a flow chart of the present invention;
其中,1—入口管路2—闸阀13—球阀4—过滤器5—压力表6—流量计7—入口取样口8—立式静电聚结器9—出口取样口10—重力式分离器11—水出口12—油出口13—水出口取样口14—油出口取样口15—水出口流量计16—单向阀17—油出口流量计18—管道泵19—出口管路20—变压器21—旁通闸阀122—旁通闸阀229—闸阀2。Among them, 1—inlet pipeline 2—gate valve 13—ball valve 4—filter 5—pressure gauge 6—flow meter 7—inlet sampling port 8—vertical electrostatic coalescer 9—outlet sampling port 10—gravity separator 11 —Water outlet 12—Oil outlet 13—Water outlet sampling port 14—Oil outlet sampling port 15—Water outlet flowmeter 16—Check valve 17—Oil outlet flowmeter 18—Pipeline pump 19—Outlet pipeline 20—Transformer 21— Bypass gate valve 122—bypass gate valve 229—gate valve 2.
图2是本发明的结构示意图。Fig. 2 is a structural schematic diagram of the present invention.
其中,23—防爆钢丝软管24—护栏25—变压器支架26—橇装底盘27—扶梯28—高压接线棒。Among them, 23—explosion-proof steel wire hose 24—guardrail 25—transformer bracket 26—skid-mounted chassis 27—escalator 28—high voltage wiring rod.
具体实施方式detailed description
参见附图1和附图2,本发明由入口管路(1)、闸阀1(2)、球阀(3)、过滤器(4)、压力表(5)、流量计(6)、入口取样口(7)、立式静电聚结器(8)、出口取样口(9)、重力式分离器(10)、水出口(11),油出口(12),水出口取样口(13),油出口取样口(14),水出口流量计(15),单向阀(16),油出口流量计(17),管道泵(18),出口管路(19),变压器(20),旁通闸阀1(21),旁通闸阀2(22),防爆钢丝软管(23),护栏(24),变压器支架(25),橇装底盘(26),扶梯(27),高压接线棒(28),闸阀2(29)等组成。除了扶梯(27)是到了现场安装到变压器支架(25)上,其它设备都是固定在橇装底盘(26)上。Referring to accompanying drawing 1 and accompanying drawing 2, the present invention is by inlet pipeline (1), gate valve 1 (2), ball valve (3), filter (4), pressure gauge (5), flowmeter (6), inlet sampling Port (7), vertical electrostatic coalescer (8), outlet sampling port (9), gravity separator (10), water outlet (11), oil outlet (12), water outlet sampling port (13), Oil outlet sampling port (14), water outlet flowmeter (15), check valve (16), oil outlet flowmeter (17), pipeline pump (18), outlet pipeline (19), transformer (20), bypass Through gate valve 1 (21), bypass gate valve 2 (22), explosion-proof steel wire hose (23), guardrail (24), transformer support (25), skid-mounted chassis (26), escalator (27), high-voltage wiring rod ( 28), gate valve 2 (29) etc. are formed. Arrived to be installed on the transformer support (25) on the scene except escalator (27), other equipment all is to be fixed on the skid-mounted chassis (26).
如图1、2,本发明提供的装置集聚结和分离设备于一体,能够方便地在油田现场应用,对立式静电聚结器聚结效果进行评价,对电场参数进行优选的橇装化试验系统,包括:入口管路(1)、闸阀1(2)、球阀(3)、过滤器(4)、压力表(5)、流量计(6)、入口取样口(7)、立式静电聚结器(8)、出口取样口(9)、重力式分离器(10)、水出口(11),油出口(12),水出口取样口(13),油出口取样口(14),水出口流量计(15),单向阀(16),油出口流量计(17),管道泵(18),出口管路(19),变压器(20),旁通闸阀1(21),旁通闸阀2(22),防爆钢丝软管(23),护栏(24),变压器支架(25),橇装底盘(26),扶梯(27),高压接线棒(28),闸阀2(29)等。其特征是:所有设备都安装在橇装底盘(26)上,底盘宽2000mm,长6000mm,可以通过货运汽车运抵油田现场进行试验;通过入口管路(1)和出口管路(19)与油田现场油水处理系统相连;变压器(20)通过防爆钢丝软管(23)和高压接线棒(28)将高压电输入到立式静电聚结器(8)中。As shown in Figures 1 and 2, the device provided by the present invention integrates coalescence and separation equipment, and can be conveniently applied in the oil field to evaluate the coalescence effect of the vertical electrostatic coalescer and conduct a skid-mounted test on the electric field parameters. System, including: inlet pipeline (1), gate valve 1 (2), ball valve (3), filter (4), pressure gauge (5), flow meter (6), inlet sampling port (7), vertical electrostatic Coalescer (8), outlet sampling port (9), gravity separator (10), water outlet (11), oil outlet (12), water outlet sampling port (13), oil outlet sampling port (14), Water outlet flowmeter (15), check valve (16), oil outlet flowmeter (17), pipeline pump (18), outlet pipeline (19), transformer (20), bypass gate valve 1 (21), bypass Gate valve 2 (22), explosion-proof steel wire hose (23), guardrail (24), transformer bracket (25), skid-mounted chassis (26), escalator (27), high-voltage wiring rod (28), gate valve 2 (29) Wait. It is characterized in that all equipment is installed on the skid-mounted chassis (26), the chassis is 2000mm wide and 6000mm long, and can be transported to the oilfield site by freight truck for testing; The on-site oil-water treatment system of the oilfield is connected; the transformer (20) inputs high-voltage electricity into the vertical electrostatic coalescer (8) through an explosion-proof steel wire hose (23) and a high-voltage wiring rod (28).
立式静电聚结器(8)利用静电场处理油包水乳状液,设置有入口取样口(7)和出口取样口(9),可以测量油中含水率和乳状液的微观形态。立式静电聚结器(8)的内电极可以方便拆卸,能够根据油品性质更换不同的电极组件,也可以对电极组件的工作特性进行检测。The vertical electrostatic coalescer (8) uses an electrostatic field to process the water-in-oil emulsion, and is provided with an inlet sampling port (7) and an outlet sampling port (9), which can measure the water content in the oil and the microscopic morphology of the emulsion. The inner electrode of the vertical electrostatic coalescer (8) can be easily disassembled, different electrode assemblies can be replaced according to the properties of the oil, and the working characteristics of the electrode assemblies can also be tested.
所述的管道泵安装在出口管路(19)处,以防止安装在入口管路(1)处会对乳状液产生强烈剪切,导致破乳困难,无法保证试验结果准确性。The pipeline pump is installed at the outlet pipeline (19) to prevent strong shearing of the emulsion when it is installed at the inlet pipeline (1), resulting in difficulty in breaking the emulsion and failing to guarantee the accuracy of the test results.
所述的变压器安装于变压器支架(25)上,并有护栏(24)和扶梯(27)保护,方便操作,保障安全。The transformer is installed on the transformer support (25), and is protected by a guardrail (24) and an escalator (27), which is convenient for operation and ensures safety.
所述的重力式分离器安装于立式静电聚结器(8)之后,可以利用重力场全部或部分处理经过立式静电聚结器(8)的油包水乳状液,对水相进行分离。并在水出口(11)和油出口(12)分别安装水出口取样口(13)和油出口取样口(14)以方便对水中含油率和油中含水率进行分析After the gravity separator is installed in the vertical electrostatic coalescer (8), the gravity field can be used to process all or part of the water-in-oil emulsion passing through the vertical electrostatic coalescer (8) to separate the water phase . And water outlet sampling port (13) and oil outlet sampling port (14) are respectively installed at water outlet (11) and oil outlet (12) to facilitate the analysis of oil content in water and water content in oil
所述的旁通闸阀:通过旁通闸阀1(21)可以调节重力式分离器(10)的处理量,即使立式静电聚结器(8)处理量超过重力式分离器(10)的处理量,也可以通过分流的方式保证试验系统正常工作,从而减小了重力式分离器(10)的占地面积和橇装系统的占地面积。The bypass gate valve: the processing capacity of the gravity separator (10) can be adjusted through the bypass gate valve 1 (21), even if the processing capacity of the vertical electrostatic coalescer (8) exceeds the processing capacity of the gravity separator (10) The normal operation of the test system can also be ensured by means of diversion, thereby reducing the footprint of the gravity separator (10) and the footprint of the skid-mounted system.
所述的单向阀安装于水出口流量计(15)和油出口流量计(17)之后,管道泵(18)之前,以防止液体倒流,对设备和生产系统造成破坏。The check valve is installed behind the water outlet flowmeter (15) and the oil outlet flowmeter (17) and before the pipeline pump (18), so as to prevent the liquid from flowing back and causing damage to the equipment and production system.
利用上述立式静电聚结器橇装化试验装置进行设备工作参数优选的方法,其特征在于包括以下步骤:Utilize above-mentioned vertical electrostatic coalescer skid-mounted test device to carry out the method for equipment working parameter optimization, it is characterized in that comprising the following steps:
1)通过货车将上述立式静电聚结器橇装化试验装置运到油田现场,利用入口管路(1)和出口管路(19)与现场处理系统相连接,1) Transport the above-mentioned vertical electrostatic coalescer skid-mounted test device to the oilfield site by truck, and use the inlet pipeline (1) and outlet pipeline (19) to connect with the on-site processing system,
2)以管道泵(18)提供动力,以使乳状液能够通过试验系统;2) Provide power with the pipeline pump (18), so that the emulsion can pass through the test system;
3)通过变压器(20)产生高压电输入到立式静电聚结器(8)中处理油包水乳状液;打开闸阀1(2)和旁通闸阀2(22)调节进入立式静电聚结器(8)的油包水乳状液的流量,并通过流量计(6)进行计量,当流量满足预设的要求后即可以进行试验;3) The high-voltage electricity generated by the transformer (20) is input to the vertical electrostatic coalescer (8) to process the water-in-oil emulsion; the gate valve 1 (2) and the bypass gate valve 2 (22) are opened to adjust and enter the vertical electrostatic coalescer The flow rate of the water-in-oil emulsion of the knotter (8) is measured by the flow meter (6), and the test can be carried out when the flow rate meets the preset requirements;
4)通过调节输入电压并经变压器(20)升压后输出至立式静电聚结器(8)中,从而对油水乳状液施加高强电场,促使水滴发生聚结,加速油水分离;4) By adjusting the input voltage and outputting it to the vertical electrostatic coalescer (8) after being boosted by the transformer (20), a high-strength electric field is applied to the oil-water emulsion to promote the coalescence of water droplets and accelerate the separation of oil and water;
5)当流经立式静电聚结器(8)的油包水乳状液的流量较大超过重力式分离器(10)的处理量时,通过控制旁通闸阀1(21)的开度来调节进入重力式分离器(10)的流量,同时通过水出口流量计(15)和油出口流量计(17)的测量值来得到重力式分离器的处理量;没有经过重力式分离器(10)的油包水乳状液直接与水出口(11)和油出口(12)流出的水、油混合并经出口管路(19)流到后续处理设备;5) When the flow rate of the water-in-oil emulsion flowing through the vertical electrostatic coalescer (8) exceeds the processing capacity of the gravity separator (10), control the opening of the bypass gate valve 1 (21) to Regulate the flow that enters the gravity type separator (10), and obtain the processing capacity of the gravity type separator through the measured values of the water outlet flowmeter (15) and the oil outlet flowmeter (17) simultaneously; not through the gravity type separator (10 ) water-in-oil emulsion directly mixes with the water and oil flowing out from the water outlet (11) and the oil outlet (12) and flows to the follow-up processing equipment through the outlet pipeline (19);
6)试验过程中通过水出口取样口(13)测量水中含油率,采用蒸馏的方法监测入口取样口(7),出口取样口(9)和油出口取样口(14)的含水率来分析试验系统的分离效果,并据此确定当分离效果最优时立式静电聚结器(8)和重力式分离器(10)的处理量;6) During the test, measure the oil content in the water through the water outlet sampling port (13), and use distillation to monitor the water content of the inlet sampling port (7), outlet sampling port (9) and oil outlet sampling port (14) to analyze the test The separation effect of the system, and accordingly determine the processing capacity of the vertical electrostatic coalescer (8) and the gravity separator (10) when the separation effect is optimal;
7)通过控制柜调节输入波形,电压和频率,以对不同电场参数下的分离效果进行评价,进而确定最优的电场参数包括波形,电场强度和频率;7) Adjust the input waveform, voltage and frequency through the control cabinet to evaluate the separation effect under different electric field parameters, and then determine the optimal electric field parameters including waveform, electric field intensity and frequency;
利用静电聚结器中的聚结效果与电场强度E的平方成正比,与频率f成正比,与电场作用时间tE成正比,与油的粘度μo成反比的性质;以及利用重力分离效果与重力分离器中的分离时间ts成正比,与油密度ρo和水密度ρw之差成反比,与油的密度μo成反比,与乳状液厚度H成反比的性质;The coalescence effect in the electrostatic coalescer is proportional to the square of the electric field intensity E, proportional to the frequency f, proportional to the electric field action time t E , and inversely proportional to the viscosity μ o of the oil; and utilizing the gravity separation effect Proportional to the separation time t s in the gravity separator, inversely proportional to the difference between the oil density ρ o and the water density ρ w , inversely proportional to the oil density μ o , and inversely proportional to the emulsion thickness H;
得到两个准则数只要满足试验设备和工业设备的两个准则数相等即可;如果对于同一油水乳状液,并且已经通过实验得到了最优电场强度和频率,那么在设计电脱水器时只要满足tE,ts/H保持一致即可;get two criterion numbers As long as the two criteria of test equipment and industrial equipment are equal; if for the same oil-water emulsion, and the optimal electric field strength and frequency have been obtained through experiments, then it is only necessary to satisfy t E , t s when designing the electric dehydrator /H can be consistent;
其中tE=LEAE/QE,LE为静电聚结器高度,QE为静电聚结器流量,AE为静电聚结器截面积;ts/H=Qs/AsLsH,Ls为分离器长度,Qs为分离器流量,AE为静电聚结器截面积;通过上述公式即可以得到静电聚结器和重力分离器工业产品的设计参数。Where t E = L E A E /Q E , L E is the height of the electrostatic coalescer, Q E is the flow rate of the electrostatic coalescer, A E is the cross-sectional area of the electrostatic coalescer; t s /H=Q s /A s L s H, L s is the length of the separator, Q s is the flow rate of the separator, A E is the cross-sectional area of the electrostatic coalescer; through the above formula, the design parameters of the electrostatic coalescer and gravity separator industrial products can be obtained.
如现场的静电聚结器流量QE是已经知道的参数;LE为静电聚结器高度,AE为静电聚结器截面积,是两个参数可以互相调节的参数,比如如果现场有高度要求那LE已知,可求出AE。如果没有要求那就根据设备的实际情况调整LE和AE满足要求即可,最终目的就是通过已知的流量QE得到LE和AE。同理对于分离器ts/H=Qs/AsLsH,也是Qs已知,根据规范《SY/T0515-2007分离器规范》确定参数As,Ls,H。For example, the on-site electrostatic coalescer flow rate Q E is a known parameter; L E is the height of the electrostatic coalescer, and A E is the cross-sectional area of the electrostatic coalescer. These two parameters can be adjusted to each other. For example, if the site has a height It is required that L E is known, and A E can be obtained. If there is no requirement, adjust LE and A E according to the actual situation of the equipment to meet the requirements. The ultimate goal is to obtain LE and A E through the known flow Q E. Similarly, for the separator t s /H=Q s /A s L s H, Q s is also known, and the parameters A s , L s , and H are determined according to the specification "SY/T0515-2007 Separator Specification".
其原理是根据本发明研究分析,可知静电聚结器中的聚结过程与电场强度E的平方成正比,与频率f成正比,与电场作用时间tE成正比,与油的粘度μo成反比;Its principle is according to the research and analysis of the present invention, it can be known that the coalescence process in the electrostatic coalescer is proportional to the square of the electric field intensity E, proportional to the frequency f, proportional to the action time t E of the electric field, and proportional to the viscosity μ o of the oil. inverse ratio;
重力分离过程与重力分离器中的分离时间ts成正比,与油密度ρo和水密度ρw之差成反比,与油的密度μo成反比,与乳状液厚度H成反比;The gravity separation process is proportional to the separation time t s in the gravity separator, inversely proportional to the difference between the oil density ρ o and the water density ρ w , inversely proportional to the oil density μ o , and inversely proportional to the emulsion thickness H;
因此可以得到两个准则数只要满足试验设备和工业设备的两个准则数相等即可;如果对于同一油水乳状液,并且已经通过实验得到了最优电场强度和频率,那么在设计电脱水器时只要满足tE,ts/H保持一致即可;Therefore, two criterion numbers can be obtained As long as the two criteria of experimental equipment and industrial equipment are equal; if for the same oil-water emulsion, and the optimal electric field strength and frequency have been obtained through experiments, then it is only necessary to satisfy t E , t s when designing the electric dehydrator /H can be consistent;
其中tE=LEAE/QE,LE为静电聚结器高度,QE为静电聚结器流量,AE为静电聚结器截面积;ts=Qs/AsLs,Ls为分离器长度,Qs为分离器流量,AE为静电聚结器截面积;通过上述公式即可以得到静电聚结器和重力分离器工业产品的设计参数。Where t E = L E A E /Q E , L E is the height of the electrostatic coalescer, Q E is the flow rate of the electrostatic coalescer, A E is the cross-sectional area of the electrostatic coalescer; t s = Q s /A s L s , L s is the length of the separator, Q s is the flow rate of the separator, A E is the cross-sectional area of the electrostatic coalescer; the design parameters of the electrostatic coalescer and gravity separator industrial products can be obtained through the above formula.
当然也可通过人工神经网络方法,得到分离效果φ与电场强度E,电场频率f,油水密度差ρw-ρo,油的粘度μo,静电聚结器流量QE,分离器流量Qs间的关系,分离器乳状液层厚度H间的关系,φ=f(E,f,ρw-ρo,μo,QE,Qs,H),可用于制作工业产品的参数。Of course, the separation effect φ and electric field intensity E, electric field frequency f, oil-water density difference ρ w -ρ o , oil viscosity μ o , electrostatic coalescer flow Q E , and separator flow Q s can also be obtained by artificial neural network method. The relationship between the separator emulsion layer thickness H, φ=f(E,f,ρ w -ρ o ,μ o ,Q E ,Q s ,H), can be used to make parameters of industrial products.
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