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CN104511268B - A kind of reactor - Google Patents

A kind of reactor Download PDF

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Publication number
CN104511268B
CN104511268B CN201410694137.1A CN201410694137A CN104511268B CN 104511268 B CN104511268 B CN 104511268B CN 201410694137 A CN201410694137 A CN 201410694137A CN 104511268 B CN104511268 B CN 104511268B
Authority
CN
China
Prior art keywords
reactor
pump
piston cylinder
piston
line
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201410694137.1A
Other languages
Chinese (zh)
Other versions
CN104511268A (en
Inventor
王淑英
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang sunrise Pharmaceutical Co., Ltd
Original Assignee
NINGBO YUANOU FINE CHEMICAL Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NINGBO YUANOU FINE CHEMICAL Co Ltd filed Critical NINGBO YUANOU FINE CHEMICAL Co Ltd
Priority to CN201410694137.1A priority Critical patent/CN104511268B/en
Publication of CN104511268A publication Critical patent/CN104511268A/en
Application granted granted Critical
Publication of CN104511268B publication Critical patent/CN104511268B/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/006Processes utilising sub-atmospheric pressure; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0073Sealings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/04Pressure vessels, e.g. autoclaves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00279Features relating to reactor vessels
    • B01J2219/00281Individual reactor vessels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00479Means for mixing reactants or products in the reaction vessels
    • B01J2219/00481Means for mixing reactants or products in the reaction vessels by the use of moving stirrers within the reaction vessels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)

Abstract

The invention discloses a kind of reactor, including reactor housing, agitating device it is provided with in reactor, connect on housing and have pump-line and some input duct, agitating device includes the piston cylinder that the rotating shaft that the motor being arranged on case top is connected is connected with rotating shaft and the paddle being arranged on piston cylinder circumference with motor output shaft, piston it is provided with in piston cylinder, passage it is provided with in rotating shaft, passage connects piston cylinder and hull outside, pump-line is arranged at the top of reactor, and pump-line is provided with valve.The reactor using this structure makes the energy of air pump consumption be substantially reduced.

Description

A kind of reactor
Technical field
The present invention relates to chemical industry equipment, particularly to a kind of reactor.
Background technology
Reactor is combined reaction container, according to reaction condition to reactor structure function and the design of configuration adnexa.All can complete pre-set reactions steps with higher automaticity from the charging-reaction-discharging started, the temperature in course of reaction, pressure, mechanics are controlled the important parameters such as (stirring, air blast etc.), reactant/product concentration and carry out strict regulation and control.Its structure is typically made up of kettle, actuating device, agitating device, heater, chiller, sealing device.The most supporting auxiliary equipment: dephlegmator, condenser, water knockout drum, collecting tank, filter etc..
Reactor usually needs the space evacuation within reactor when using, this is the highest to the sealing of reactor and the performance requirement of air pump, and needing all to be not readily accessible to chemical reagent not all in the course of reaction of reactor evacuation air, thus substantial amounts of energy is wasted in the operation of whole reactor evacuation.
Summary of the invention
The present invention is directed to prior art not enough, it is provided that a kind of reactor, this reactor is convenient by the cavity evacuation within reactor, and saves big energy.
In order to solve above-mentioned technical problem, the present invention is addressed by following technical proposals: a kind of reactor, including reactor housing, it is provided with agitating device in described reactor, connect on described housing and have pump-line and some input duct, described agitating device includes the motor being arranged on described case top, the rotating shaft being connected with described motor output shaft, the piston cylinder being connected with described rotating shaft and the paddle being arranged on described piston cylinder circumference, it is provided with piston in described piston cylinder, it is provided with passage in described rotating shaft, described passage connects described piston cylinder and described hull outside, described pump-line is arranged at the top of described reactor, it is provided with valve on described pump-line.During the work of this reactor, first will be able to be passed in reactor with the reagent of air contact, bleeding by air pump the most again, make the piston slide outside to piston cylinder, so that the liquid level within reactor raises, until closing valve when having liquid to ooze out in pump-line, so that reach vacuum in reactor, to be able to not be passed in reactor with the reagent of air contact the most again, now piston slide make reactor content cavity increase for be passed through these can not be with the reagent of air contact, the reactor using this structure makes the energy of air pump consumption be substantially reduced.
In technique scheme, it is preferred that be provided with elastic component between described piston and described piston cylinder medial surface.Elastic component is set between piston and piston cylinder so that piston cylinder is provided that suction when not being passed through with the reagent of air contact, it is not necessary to input duct provides pressure.
In technique scheme, it is preferred that be provided with transparent observation panel on described pump-line, be provided with liquid storage cylinder at described observation panel.The opportunity that observation panel convenient observation liquid is drawn out of is set, thus closes air pump and valve timely, liquid storage cylinder is set and prevents chemical reagent from entering in air pump.
In technique scheme, it is preferred that be provided with tap hole below described liquid storage cylinder, tap hole is set for the chemical reagent that is drawn out of of releasing, prevents its entrance air pump.
The present invention is compared with prior art, have the advantages that when this reactor works, first will be able to be passed in reactor with the reagent of air contact, bleeding by air pump the most again, make the piston slide outside to piston cylinder, so that the liquid level within reactor raises, until closing valve when having liquid to ooze out in pump-line, so that reach vacuum in reactor, to be able to not be passed in reactor with the reagent of air contact the most again, now piston slide make reactor content cavity increase for be passed through these can not be with the reagent of air contact, the reactor using this structure makes the energy of air pump consumption be substantially reduced.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention.
Detailed description of the invention
With detailed description of the invention, the present invention is described in further detail below in conjunction with the accompanying drawings: see Fig. 1, a kind of reactor, including reactor housing 1, agitating device 2 it is provided with in described reactor, connect on described housing 1 and have pump-line 3 and some input duct 4, described agitating device 2 includes the motor 5 being arranged on described housing 1 top, the rotating shaft 6 being connected with described motor 5 output shaft, the piston cylinder 7 being connected with described rotating shaft 6 and the paddle 8 being arranged on described piston cylinder 7 circumference, it is provided with piston 9 in described piston cylinder 7, it is provided with passage 61 in described rotating shaft 6, it is outside with described housing 1 that described passage 61 connects described piston cylinder 7, described pump-line 3 is arranged at the top of described reactor, it is provided with valve 10 on described pump-line 3.During the work of this reactor, first will be able to be passed in reactor with the reagent of air contact, bleeding by air pump the most again, make the piston slide outside to piston cylinder, so that the liquid level within reactor raises, until closing valve when having liquid to ooze out in pump-line, so that reach vacuum in reactor, to be able to not be passed in reactor with the reagent of air contact the most again, now piston slide make reactor content cavity increase for be passed through these can not be with the reagent of air contact, the reactor using this structure makes the energy of air pump consumption be substantially reduced.
It is provided with elastic component 11 between described piston 9 and described piston cylinder 7 medial surface.Elastic component is set between piston and piston cylinder so that piston cylinder is provided that suction when not being passed through with the reagent of air contact, it is not necessary to input duct provides pressure.
It is provided with transparent observation panel 31 on described pump-line 3, at described observation panel 31, is provided with liquid storage cylinder 32.The opportunity that observation panel convenient observation liquid is drawn out of is set, thus closes air pump and valve timely, liquid storage cylinder is set and prevents chemical reagent from entering in air pump.
It is provided with tap hole 33 below described liquid storage cylinder 32.Tap hole is set for the chemical reagent that is drawn out of of releasing, prevents its entrance air pump.

Claims (4)

  1. null1. a reactor,Including reactor housing (1),Agitating device (2) it is provided with in described reactor,The upper connection of described housing (1) has pump-line (3) and some input duct (4),It is characterized in that: described agitating device (2) includes being arranged on the motor (5) at described housing (1) top、The rotating shaft (6) being connected with described motor (5) output shaft、The piston cylinder (7) being connected with described rotating shaft (6) and the paddle (8) being arranged on described piston cylinder (7) circumference,Piston (9) it is provided with in described piston cylinder (7),Passage (61) it is provided with in described rotating shaft (6),It is outside with described housing (1) that described passage (61) connects described piston cylinder (7),Described pump-line (3) is arranged at the top of described reactor,Valve (10) it is provided with on described pump-line (3),During work,First will be able to be passed in reactor with the reagent of air contact,Bleeding by air pump the most again,Make the piston slide outside to piston cylinder,So that the liquid level within reactor raises,Until closing valve when having liquid to ooze out in pump-line,So that reach vacuum in reactor,To be able to not be passed in reactor with the reagent of air contact the most again,Now piston slide make reactor content cavity increase for be passed through these can not be with the reagent of air contact.
  2. 2. a kind of reactor as claimed in claim 1, it is characterised in that: it is provided with elastic component (11) between described piston (9) and described piston cylinder (7) medial surface.
  3. 3. a kind of reactor as claimed in claim 1, it is characterised in that: being provided with transparent observation panel (31) on described pump-line (3), described observation panel (31) place is provided with liquid storage cylinder (32).
  4. 4. a kind of reactor as claimed in claim 3, it is characterised in that: described liquid storage cylinder (32) lower section is provided with tap hole (33).
CN201410694137.1A 2014-11-27 2014-11-27 A kind of reactor Active CN104511268B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410694137.1A CN104511268B (en) 2014-11-27 2014-11-27 A kind of reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410694137.1A CN104511268B (en) 2014-11-27 2014-11-27 A kind of reactor

Publications (2)

Publication Number Publication Date
CN104511268A CN104511268A (en) 2015-04-15
CN104511268B true CN104511268B (en) 2016-10-05

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410694137.1A Active CN104511268B (en) 2014-11-27 2014-11-27 A kind of reactor

Country Status (1)

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CN (1) CN104511268B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107913657A (en) * 2017-11-27 2018-04-17 朱新福 Oscillating agitator and the reaction kettle using the blender

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202028353U (en) * 2011-04-06 2011-11-09 江苏德峰药业有限公司 Stirred tank
CN203264623U (en) * 2013-06-11 2013-11-06 贾慧灵 Crystal stirring kettle
CN203486906U (en) * 2013-07-17 2014-03-19 多氟多化工股份有限公司 Device for synthesizing lithium hexafluorophosphate
CN203842576U (en) * 2014-04-01 2014-09-24 江苏玺鑫维生素有限公司 Enamel reaction kettle suitable for producing vitamin E

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202028353U (en) * 2011-04-06 2011-11-09 江苏德峰药业有限公司 Stirred tank
CN203264623U (en) * 2013-06-11 2013-11-06 贾慧灵 Crystal stirring kettle
CN203486906U (en) * 2013-07-17 2014-03-19 多氟多化工股份有限公司 Device for synthesizing lithium hexafluorophosphate
CN203842576U (en) * 2014-04-01 2014-09-24 江苏玺鑫维生素有限公司 Enamel reaction kettle suitable for producing vitamin E

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Publication number Publication date
CN104511268A (en) 2015-04-15

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Address after: No. 388, Beihai Road, Ningbo Petrochemical Economic and Technological Development Zone, Zhenhai District, Ningbo City, Zhejiang Province

Patentee after: Zhejiang sunrise Pharmaceutical Co., Ltd

Address before: 315203, Zhejiang, Ningbo province Crab Industry Development Zone

Patentee before: NINGBO YUANOU FINE CHEMICAL CO., LTD.

CP03 Change of name, title or address