CN104450014A - Wear-resistant metal cutting oil containing nano-titanium dioxide and having good dispersity and preparation method thereof - Google Patents
Wear-resistant metal cutting oil containing nano-titanium dioxide and having good dispersity and preparation method thereof Download PDFInfo
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- CN104450014A CN104450014A CN201410567666.5A CN201410567666A CN104450014A CN 104450014 A CN104450014 A CN 104450014A CN 201410567666 A CN201410567666 A CN 201410567666A CN 104450014 A CN104450014 A CN 104450014A
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Abstract
The invention discloses wear-resistant metal cutting oil containing nano-titanium dioxide and having good dispersity. The wear-resistant metal cutting oil is characterized by being prepared from the following raw materials in parts by weight: 19-22 parts of polymethylphenyl siloxane fluid, 23-30 parts of vulcanized lard oil, 3-5 parts of polyacrylamide, 3-5 parts of nano-titanium dioxide, 2-3 parts of alundum powder, 4-6 parts of cassava starch, 7-9 parts of water, 11-14 parts of white oil, 1-2 parts of silicon tetrachloride, 2-3 parts of tributyl borate, 1.5-2.5 parts of lead naphthenate, 8-11 parts of polyoxyethylene fatty alcohol ether and 9-11 parts of modified waste engine oil. By adding the nano-titanium dioxide, alundum powder and other abrasive materials, the wear-resistant metal cutting oil is high in hardness, good in dispersity and the sticky status of the wear-resistant metal cutting oil can be improved; the cassava starch and water are added into the wear-resistant metal cutting oil through the special technology, and in cooperation with the addition of the modified waste engine oil, a layer of protective film is formed on the surface of metal so as to protect a metal section, and the cost can be saved due to utilization of wastes; and the processing production efficiency is high, and the wear-resistant metal cutting oil is applicable to cutting processing of various metals.
Description
Technical field
The present invention relates to cutting fluid field, particularly a kind of wear-resisting scattered metal cutting oil adding nano titanium oxide and preparation method thereof.
Background technology
Nano titanium oxide adds in metal cutting oil as abrasive material by the present invention's imagination, is uniformly dispersed, has good wear resistance, can change the character of machining oil thickness, and be watered the rear good fluidity of dilution, cleaning is better.The present invention adopts concentrated type oil in water emulsion formula, uses front thin up to use, the shortcoming solving bad transport and not easily preserve, and the cutting fluid result of use of matching while using is good.The present invention adds the modification used oil of especial manufacture, and utilization of waste material, while energy-conserving and environment-protective, reduces cost, enhances flame retardant resistance, thermal diffusivity, improves antirust passivation effect and film-forming properties, effectively protects metal tangent plane.
Summary of the invention
The object of this invention is to provide a kind of wear-resisting scattered metal cutting oil adding nano titanium oxide and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
Add a wear-resisting scattered metal cutting oil for nano titanium oxide, be made up of the raw material of following weight part: polymethylphenyl siloxane fluid 19-22, sulfurized lard 23-30, polyacrylamide 3-5, nano titanium oxide 3-5, lapis amiridis 2-3, tapioca (flour) 4-6, water 7-9, white oil 11-14, silicon tetrachloride 1-2, tributyl borate 2-3, lead naphthenate 1.5-2.5, polyoxyethylene gather fatty alcohol-ether 8-11, modification used oil 9-11;
Described modification used oil is prepared from by the raw material of following weight part: used oil 40-45, waste coal oil 11-13, atlapulgite 2-3, sulfonated castor oil 2-3, Emulsion acrylic resin 4-5, alcohol ester 12 1-2, Viscoat 295 2-3, sorbester p17 1-2, dodecenylsuccinic acid diglycollic amide 1-2, hexahydroaniline 1-2, glycerine 2-3, antimonous oxide 2-3, aquadag 4-6; Preparation method is first warming up to 120 DEG C-140 DEG C by after used oil, the mixing of waste coal oil, adds atlapulgite, stirs 30-40 minute, leave standstill 9-12 hour, filtered while hot at 110 DEG C-120 DEG C under constant temperature; Add sorbester p17, dodecenylsuccinic acid diglycollic amide, hexahydroaniline, glycerine when being cooled to 50 DEG C-60 DEG C, stir 20-30 minute; Continue to add Emulsion acrylic resin, alcohol ester 12, Viscoat 295, stirring reaction 1-2 hour; Finally add all the other remaining components, stir under the condition of 500-600 rev/min 2-3 hour and get final product.
A kind of wear-resisting scattered metal cutting oil adding nano titanium oxide of the present invention, be made up of following concrete steps:
(1) tapioca (flour) is soluble in water, add nano titanium oxide, lapis amiridis, mix, grinding 1.5-2 hour;
(2) polymethylphenyl siloxane fluid, sulfurized lard, polyacrylamide, white oil, polyoxyethylene are gathered fatty alcohol-ether and mix, be heated to 65 DEG C-70 DEG C and stir 20-30 minute, be then warming up to 100 DEG C-120 DEG C, keep constant temperature and fully stir 30-40 minute;
(3) step (1) is mixed with step (2), add modification used oil, stir 20-30 minute with the speed of 1000-1100 rev/min, continue to add all the other remaining components, stir 1-1.5 hour with the speed of 400-500 rev/min and get final product.
Excellent effect of the present invention is: the present invention adds the abrasive material such as nano titanium oxide, lapis amiridis, and hardness is large, scattered, improves the state of product thickness; Add tapioca (flour) and water, by special process, add in product, coordinate the interpolation of modification used oil, can form layer protecting film in metallic surface, protection metal tangent plane, and utilization of waste material, saved cost; Processing efficiency of the present invention is high, is applicable to various metals machining.
Embodiment
Below by specific examples, the present invention is described in detail.
Add a wear-resisting scattered metal cutting oil for nano titanium oxide, be made up of the raw material of following weight part (kilogram): polymethylphenyl siloxane fluid 19, sulfurized lard 23, polyacrylamide 3, nano titanium oxide 3, lapis amiridis 2, tapioca (flour) 4, water 7, white oil 11, silicon tetrachloride 1, tributyl borate 2, lead naphthenate 1.5, polyoxyethylene gather fatty alcohol-ether 8, modification used oil 9;
Described modification used oil is prepared from by the raw material of following weight part (kilogram): used oil 40, waste coal oil 11, atlapulgite 2, sulfonated castor oil 2, Emulsion acrylic resin 4, alcohol ester 12, Viscoat 295 2, sorbester p17 1, dodecenylsuccinic acid diglycollic amide 1, hexahydroaniline 1, glycerine 2, antimonous oxide 2, aquadag 4; Preparation method is first warming up to 120 DEG C-140 DEG C by after used oil, the mixing of waste coal oil, adds atlapulgite, stirs 30-40 minute, leave standstill 9-12 hour, filtered while hot at 110 DEG C-120 DEG C under constant temperature; Add sorbester p17, dodecenylsuccinic acid diglycollic amide, hexahydroaniline, glycerine when being cooled to 50 DEG C-60 DEG C, stir 20-30 minute; Continue to add Emulsion acrylic resin, alcohol ester 12, Viscoat 295, stirring reaction 1-2 hour; Finally add all the other remaining components, stir under the condition of 500-600 rev/min 2-3 hour and get final product.
A kind of wear-resisting scattered metal cutting oil adding nano titanium oxide of the present invention, be made up of following concrete steps:
(1) tapioca (flour) is soluble in water, add nano titanium oxide, lapis amiridis, mix, grinding 1.5-2 hour;
(2) polymethylphenyl siloxane fluid, sulfurized lard, polyacrylamide, white oil, polyoxyethylene are gathered fatty alcohol-ether and mix, be heated to 65 DEG C-70 DEG C and stir 20-30 minute, be then warming up to 100 DEG C-120 DEG C, keep constant temperature and fully stir 30-40 minute;
(3) step (1) is mixed with step (2), add modification used oil, stir 20-30 minute with the speed of 1000-1100 rev/min, continue to add all the other remaining components, stir 1-1.5 hour with the speed of 400-500 rev/min and get final product.
The machining oil that the present invention obtains uses after being watered dilution, and can dilute 5-20 in proportion doubly, diluent has excellent extreme boundary lubrication and rust-preventing characteristic, and after tested, the diluent of 20 times can reach following technical requirements:
Claims (2)
1. one kind is added the wear-resisting scattered metal cutting oil of nano titanium oxide, it is characterized in that, be made up of the raw material of following weight part: polymethylphenyl siloxane fluid 19-22, sulfurized lard 23-30, polyacrylamide 3-5, nano titanium oxide 3-5, lapis amiridis 2-3, tapioca (flour) 4-6, water 7-9, white oil 11-14, silicon tetrachloride 1-2, tributyl borate 2-3, lead naphthenate 1.5-2.5, polyoxyethylene gather fatty alcohol-ether 8-11, modification used oil 9-11;
Described modification used oil is prepared from by the raw material of following weight part: used oil 40-45, waste coal oil 11-13, atlapulgite 2-3, sulfonated castor oil 2-3, Emulsion acrylic resin 4-5, alcohol ester 12 1-2, Viscoat 295 2-3, sorbester p17 1-2, dodecenylsuccinic acid diglycollic amide 1-2, hexahydroaniline 1-2, glycerine 2-3, antimonous oxide 2-3, aquadag 4-6; Preparation method is first warming up to 120 DEG C-140 DEG C by after used oil, the mixing of waste coal oil, adds atlapulgite, stirs 30-40 minute, leave standstill 9-12 hour, filtered while hot at 110 DEG C-120 DEG C under constant temperature; Add sorbester p17, dodecenylsuccinic acid diglycollic amide, hexahydroaniline, glycerine when being cooled to 50 DEG C-60 DEG C, stir 20-30 minute; Continue to add Emulsion acrylic resin, alcohol ester 12, Viscoat 295, stirring reaction 1-2 hour; Finally add all the other remaining components, stir under the condition of 500-600 rev/min 2-3 hour and get final product.
2. a kind of wear-resisting scattered metal cutting oil adding nano titanium oxide according to claim 1, is characterized in that, be made up of following concrete steps:
(1) tapioca (flour) is soluble in water, add nano titanium oxide, lapis amiridis, mix, grinding 1.5-2 hour;
(2) polymethylphenyl siloxane fluid, sulfurized lard, polyacrylamide, white oil, polyoxyethylene are gathered fatty alcohol-ether and mix, be heated to 65 DEG C-70 DEG C and stir 20-30 minute, be then warming up to 100 DEG C-120 DEG C, keep constant temperature and fully stir 30-40 minute;
(3) step (1) is mixed with step (2), add modification used oil, stir 20-30 minute with the speed of 1000-1100 rev/min, continue to add all the other remaining components, stir 1-1.5 hour with the speed of 400-500 rev/min and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410567666.5A CN104450014A (en) | 2014-10-22 | 2014-10-22 | Wear-resistant metal cutting oil containing nano-titanium dioxide and having good dispersity and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410567666.5A CN104450014A (en) | 2014-10-22 | 2014-10-22 | Wear-resistant metal cutting oil containing nano-titanium dioxide and having good dispersity and preparation method thereof |
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| CN104450014A true CN104450014A (en) | 2015-03-25 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106701292A (en) * | 2016-12-19 | 2017-05-24 | 钦州市科学技术开发中心 | Emulsion for cutting and preparation method thereof |
| CN110218606A (en) * | 2019-06-27 | 2019-09-10 | 合肥工业大学 | The preparation method of metal cutting process highly concentrated nano titanium dioxide water lubrication liquid |
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| CN1122824A (en) * | 1994-11-09 | 1996-05-22 | 化学工业部天津化工研究院 | Colloidal lubricant used for core rod of continuous tube rolling mill |
| CN101560433A (en) * | 2009-05-11 | 2009-10-21 | 启东尤希路化学工业有限公司 | Anti-magnesium hard water anti-magnesium corrosion environmentally-friendly water soluble cutting solution |
| CN102433201A (en) * | 2011-11-05 | 2012-05-02 | 安徽工业大学 | Light-cured dry film lubricant |
| CN103710127A (en) * | 2013-12-05 | 2014-04-09 | 马鞍山市恒毅机械制造有限公司 | Cutting fluid containing waste engine oil and preparation method therefor |
| CN103966009A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Drawing fluid for high-speed drawing of superfine copper wire |
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2014
- 2014-10-22 CN CN201410567666.5A patent/CN104450014A/en not_active Withdrawn
Patent Citations (5)
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| CN1122824A (en) * | 1994-11-09 | 1996-05-22 | 化学工业部天津化工研究院 | Colloidal lubricant used for core rod of continuous tube rolling mill |
| CN101560433A (en) * | 2009-05-11 | 2009-10-21 | 启东尤希路化学工业有限公司 | Anti-magnesium hard water anti-magnesium corrosion environmentally-friendly water soluble cutting solution |
| CN102433201A (en) * | 2011-11-05 | 2012-05-02 | 安徽工业大学 | Light-cured dry film lubricant |
| CN103710127A (en) * | 2013-12-05 | 2014-04-09 | 马鞍山市恒毅机械制造有限公司 | Cutting fluid containing waste engine oil and preparation method therefor |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106701292A (en) * | 2016-12-19 | 2017-05-24 | 钦州市科学技术开发中心 | Emulsion for cutting and preparation method thereof |
| CN110218606A (en) * | 2019-06-27 | 2019-09-10 | 合肥工业大学 | The preparation method of metal cutting process highly concentrated nano titanium dioxide water lubrication liquid |
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Application publication date: 20150325 |