A kind of antistatic, radiation proof hair cream and preparation method thereof
Technical field
The present invention relates to a kind of hair cream and preparation method thereof, more particularly to a kind of antistatic, radiation proof hair cream and its
Preparation method, belong to household chemicals field.
Background technology
With pursuit of the development and people of society to U.S., people also begin to increasingly focus on the nursing of hair, therefore right
The demand of hair nursing is also increasing.Expanding economy in recent years, wash hair care product market and do not only have rapid progress, but also
There is huge potential market capacity.In addition for increasingly strong ultraviolet, it is also to need that people, which are also gradually recognized for hair,
Carry out sun-proof.In the market various products are too plenty for the eye to take it all in, and many producers, businessman are under the driving of interests, in order to allow product energy
Best effect is played, starts the chemical synthesis substance that the addition in hair products are washed is harmful to hair, does not play hair care
Meanwhile it may can also injure hair.And hair is under the environment such as high temperature, high and cold, dry, high wind, intensive ultraviolet radiation, easily
Dry out, breakage, fracture, bifurcated, withered and yellow occurs.
The content of the invention
For above-mentioned the deficiencies in the prior art, the present invention provides a kind of antistatic, radiation proof hair cream and preparation method thereof,
Hair is overcome to be tanned severely, cannot taken care of hair, occurring breakage, fracture, bifurcated, withered and yellow problem, and also have it is antibacterial, go
Bits, anticreep, antistatic, radiation proof effect.
To achieve the above object, the present invention provides a kind of antistatic, radiation proof hair cream, states and contains following thing in shampoo paste
Matter and its content:
As a further improvement, golden yellow SIMMONDSIA CHINENSIS SEED OIL 1-5g, Eclipta prostrata extract solution 1- are also contained in the hair cream
3ml.This hair cream can not only further hair conditioning, the also effect with black hair.
Here essence can be added according to different demands, described essence is green cucumber essence, flavoring rose essence, fragrance of osmanthus
One or more in essence, peach flavor, lemon extract, flavoring pineapple essence, cream jasmin france.
Antistatic, the radiation proof hair washing ointment preparation, comprises the following steps:
Step 1:0.1-1g ice crystal forming agent AVC are weighed, is dissolved in 30-100ml water, stirs, stand 2-3h,
Treat that it is swelled dissolving naturally, obtain gel A;
Step 2:Cation guar gum 1-2g is weighed, is dissolved in 30-100ml water, is stirred, in 70-90 DEG C of water-bath
In continue stirring to dissolving, cool down 30min under normal temperature, obtain conditioner B;
Step 3:Weigh wheat-germ oil 2-10g, shea butter 1-5g, coconut oil 1-5g, stearic acid 0.1-1g, liquid crystal
Type is placed in beaker from thickener/emulsifier Lipomulse LUXE 2-3g, and 70-90 DEG C of heating of water-bath, is oil phase;
Step 4:Distilled water 10-25g is weighed, 70-90 DEG C of heating of water-bath, is aqueous phase;
Step 5:It is in thread shape by aqueous phase in the case that aqueous phase, oil phase reach mutually synthermal Deng oil phase clear
Add in oil phase, it is stirring while adding, form emulsion bases C;
Step 6:Distilled water 10-30g is weighed, adds sodium sulfate of polyethenoxy ether of fatty alcohol 1-5g, Dutch sodium lactate 2-
It is 10g, cocamidopropyl betaine CAB 1-5g, APG APG 1-5g, sodium lauroyl sarcosine LS301-5g, water-soluble
Property Ve 0.1-1g, trehalose 1-2g, polyquaternium 1-5g, biological polyoses glue FUCOGEL 1.5P 1-5g, dodecyl sulphate
Sodium 0.1-3g, sodium chloride 0.1-3g, stirring and dissolving, obtain solution D;
Step 7:Soapberry extract 1-5g, peppermint extract solution 1-5g are added into emulsion bases C, is uniformly mixed,
Gel A, conditioner B, solution D are added, is uniformly mixed;
Step 8:Weigh disodium ethylene diamine tetraacetate 0.01-0.05g, ethylparaben or sorbic acid 0.1-0.3g, add
Distilled water 5-18ml, heating make its dissolving, add in step 7 system, essence 0.05-0.3ml are added, with 20% citric acid
Solution 0.1-3ml, after regulation pH value is 6.5-7.5,10-15min is stirred, is well mixed, produce antistatic, radiation proof hair washing
Cream.
Described soapberry extract is prepared by the following method:The soapberry for peelling off kernel is taken, 0.15-1h is soaked, adds
Heat decocts extraction 3 times to 90-100 DEG C, and the 1st time plus 6-12 times measure water, extracts 0.5-2h, measures water the 2nd time plus 4-10 times, extracts
0.5-1.5h, the 3rd time plus 3-8 times measure water, extract 0.5-1.5h, every time filtration, and merging filtrate, the volume concentration of filtrate is to without trouble
3-6 times of g/ml of sub- weight, filters and produces.
Described peppermint extract solution is prepared by the following method:Take peppermint soak 0.5-1h, refluxing extraction 3 times, the 1st time plus
10-15 times is measured water, extracts 0.5-2h, measures water the 2nd time plus 8-12 times, extracts 0.5-1.5h, measures water the 3rd time plus 6-10 times, is extracted
0.5-1.5h, every time filtration, merging filtrate, the volume concentration of filtrate to 4-7 times of g/ml of peppermint weight, liquid feeding body weight 1%-
5% activated carbon, 60-100 DEG C of heating water bath stirring, filters, takes filtrate.
The golden yellow SIMMONDSIA CHINENSIS SEED OIL of 1-5 parts by weight is additionally added in the step step 3.
The Eclipta prostrata extract solution of 1-5 parts by weight is additionally added in the step 7.Described Eclipta prostrata extract solution by with
It is prepared by lower section method:Take Eclipta prostrata, refluxing extraction 2 times, the 1st time plus 10-18 times of water, extract 0.5-1.5h, use 10-12 the 2nd time
Times water, 0.5-1.5h is extracted, is filtered every time with 3 layers of gauze, merging filtrate, heats 2-10 times of g/ for being concentrated into Eclipta prostrata weight
Ml, filter and produce.
Various composition in the present invention is as follows:
Soapberry is also fruit of washing one's hands.Containing triterpenoid saponins such as sapindosides in its pericarp.《Compendium of Materia Medica》Described in:Without trouble
Sub- fruit contains natural net rhzomorph.It is that the natural of Chinese traditional washes the precious fruit of shield since ancient times.It has body of not hurting sb.'s feelings, not dirty
Contaminate the characteristic at water source.Soapberry also has the function that antibacterial, anti-dandruff, anticreep.
Eclipta prostrata has the effect of nourishing liver and kidney, crow palpus permanent tooth, cooling blood and hemostasis.Smash juice and apply eyebrow hair, hair growth can be promoted, it is interior
Clothes have black hair, dark hair effect.《The southern regions of the Yunnan Province book on Chinese herbal medicine》Carry, eclipta " permanent tooth, black hair, washes nine kinds of hemorrhoid ".《Compendium of Materia Medica》Point out, ink
Non-irrigated lotus " black beard and hair, kidney-nourishing are cloudy ".Eclipta prostrata controls poliosis, eyebrow moustache comes off.
Peppermint contains the materials such as volatile oil, peppermint essence and tannin, helps to smooth the negative emotions such as angry, dejected, is
Dispelling fatigue, alleviate pressure, dispassionate soul tonic.Peppermint has refrigerant sensation, can antibacterial, antibacterial, it is antipruritic.
Wheat-germ oil is rich in various nutrition, is easily absorbed by the body, and has and suppresses free radical, anti-oxidant, delay body to decline
Always, protect cell membrane, promote skin metabolism, improve body immunity, enhancing anti-cancer, anticancer and the work that stimulates circulation
With, also moisturizing, skin is moistened, improve looks, retain youth, making women skin become soft and moist and high resilience etc. acting on.
It is extremely helpful to moistening dry hair quality, maintenance scalp, it is adapted to various skin quality, has certain effect to chronic eczema, eczema, also with sun-proof
Function, available for body, hair it is sun-proof.
Golden yellow SIMMONDSIA CHINENSIS SEED OIL has good permeability, and molecules align is very similar with the grease of people, is that stability is high, prolongs
The particularly good base oil of malleability, can improve coarse hair quality, be the optimal selection of Hair grooming oil, can prevent hair sunburn, softness
Hair, contribute to hair it is pitch-black, prevention bifurcated.Another characteristic of SIMMONDSIA CHINENSIS SEED OIL is its hydrophily, there is regulation moisture to skin
Function, it is a kind of very perfect skin care and the natural keep-fit composition of hair care.
Cation guar gum can provide hair products excellent conditioning performance, there is good foaming, foam stabilizing, antistatic work
With, dry, the wet comb resistance of hair is reduced, improves the wet comb of hair and dry comb property, hair is kept gloss, softness for a long time, it is rich
It is flexible.It can be adsorbed in a mao bar, form monomolecular adsorbed film, make hair soft, rich in gloss and elasticity, and prevent to produce quiet
Electricity, combing is very convenient, is a kind of preferable conditioner for producing transparent daily chemical products.
Trehalose has the characteristic of excellent, safe moisture-retaining capacity and large biological molecule activity.Hair high temperature, it is high and cold,
Under the environment such as drying, high wind, intensive ultraviolet radiation, easily dry out, breakage, fracture, bifurcated, withered and yellow occurs.Trehalose exists
In this case one layer of special diaphragm can be formed on hair top layer, keeps the original nutrition of scalp and moisture, protect hair
Fiber and hair scale piece exempt from the injury of dehydration, help healthy hair to keep natural structure, therefore it is a kind of efficient NMF, and
And provide the protective effect of the not potential injury of climate.Trehalose also has the function of radiateing external heat, so as to
Protection hair will not be damaged.Trehalose can suppress the generation of the volatile aldehyde caused by Fatty acid degradation, can suppress by
Peculiar smell caused by this.Trehalose has good radiation proof, antistatic effect.
Beneficial effect:Hair cream made by the present invention have the effect of good radiation proof, antistatic, hair care hair care,
Clearly, comfortably, fragrance, while also there is antibacterial bacteriostatic, also there is anti-dandruff, antipruritic, anticreep.Cation Guar
Glue has good foaming foam stabilizing effect, antistatic property, improves the wet comb of hair and dry comb property, hair is kept light for a long time
Pool, soft, high resilience.Composition complements each other in prescription so that the shampoo paste has preferable moistening effect, can nourish head comprehensively
Hair, damaged hair is repaired, supplement nutrition needed for hair follicle, promoted hair follicle cell metabolism, hair is obtained from inside to outside comprehensively
Conditioning, makes hair one comb on earth, smooth soft bright such as silk, high resilience.
Embodiment
With reference to embodiment, the present invention will be further described.
Golden yellow SIMMONDSIA CHINENSIS SEED OIL, wheat-germ oil, the coconut oil of the present invention is commercially available.
Embodiment 1
The present embodiment is antistatic, radiation proof hair cream is made as follows:
Step 1:0.5g ice crystal forming agent AVC are weighed, is dissolved in 100ml water, stirs, 2h is stood, treats its nature
Swelling dissolving, obtains gel A;
Step 2:Cation guar gum 2g is weighed, is dissolved in 100ml water, is stirred, continues to stir in 80 DEG C of water-baths
Mix to dissolving, cool down 30min under normal temperature, obtain conditioner B;
Step 3:Wheat-germ oil 2g, shea butter 1.5g, coconut oil 1g, stearic acid 0.5g, liquid crystal type is weighed to thicken certainly
Emulsifying agent Lipomulse LUXE 2g are placed in beaker, and 80 DEG C of heating of water-bath, are oil phase;
Step 4:Distilled water 15g is weighed, 85 DEG C of heating of water-bath, are aqueous phase;
Step 5:It is in thread shape by aqueous phase in the case that aqueous phase, oil phase reach mutually synthermal Deng oil phase clear
Add in oil phase, it is stirring while adding, form emulsion bases C;
Step 6:Distilled water 10g is weighed, adds sodium sulfate of polyethenoxy ether of fatty alcohol 3g, Dutch sodium lactate 3g, cocounut oil acyl
Aminocarbonyl propyl glycine betaine CAB 2g, APG APG 3g, sodium lauroyl sarcosine LS30 2g, water-soluble Ve 0.8g, marine alga
Sugared 1.5g, polyquaternium 2g, biological polyoses glue FUCOGEL 1.5P 1.5gg, lauryl sodium sulfate 0.3g, sodium chloride 0.5g,
Stirring and dissolving, obtain solution D;
Step 7:Soapberry extract 2g, peppermint extract solution 1.5g are added into emulsion bases C, is uniformly mixed, then
Gel A, conditioner B, solution D are added, is uniformly mixed;
Step 8:Weigh disodium ethylene diamine tetraacetate 0.02g, ethylparaben or sorbic acid 0.1g, add distilled water
8ml, heating make its dissolving, add in step 7 system, add essence 0.05ml, with 20% citric acid solution 1ml, adjust pH
It is worth after 6.8, to stir 10-15min, is well mixed, produces antistatic, radiation proof hair cream.Here can be according to different need
Addition essence is sought, described essence is green cucumber essence, flavoring rose essence, osmanthus flower fragrance, peach flavor, lemon extract, pineapple perfume
One or more in essence, cream jasmin france.
The wherein preparation of soapberry extract:Soapberry peels off kernel, weighs 40g, then soaks 1h, is heated to 100 DEG C, decocts
3 times, the 1st time plus 9 times amount water of extraction are boiled, 1.5h is extracted, the 2nd time plus 9 times amount water, extracts 1h, the 3rd time plus 7 times amount water, extraction
1h, filtration, merging filtrate, the volume concentration of filtrate are filtered and produced to 4 times (g/ml) of soapberry weight every time.
The wherein preparation of peppermint extract solution:Weigh peppermint 30g, soak 1h, refluxing extraction 3 times, the 1st time plus 15 times amount water,
1.5h is extracted, the 2nd time plus 12 times amount water, 1h is extracted, the 3rd time plus 9 times amount water, extracts 1h, every time filtration, merging filtrate, filtrate
Volume concentration to 6 times (g/ml) of peppermint weight, the activated carbon of liquid feeding body weight 3%, 80 DEG C of heating water baths stirrings, filter, i.e.,
Can.
Embodiment 2
The present embodiment is being additionally added 1.5g golden yellow Jojoba with the difference of embodiment 1 in the step step 3
Oil, 2g Eclipta prostrata extract solution is additionally added in the step 7.Described Eclipta prostrata extract solution is prepared by the following method:Claim
Eclipta prostrata 30g is taken, extracts 2 times, the 1st time plus 15 times of waters, 1h is extracted, 10 times of waters of the 2nd use, 1h is extracted, every time with 3 layers of yarn
Cloth filters, merging filtrate, and heating is concentrated into 5 times (g/ml) of Eclipta prostrata weight, filters and produces.
Embodiment 3
The present embodiment is antistatic, radiation proof hair cream is made as follows:
Step 1:0.8 ice crystal forming agent AVC is weighed, is dissolved in 80ml water, stirs, 2h is stood and treats that it is swelled naturally
Dissolving;
Step 2:Cation guar gum 1g is weighed, is dissolved in 80ml water, stirs, with continuing stirring in 80 DEG C of water extremely
Dissolve, cool down 30min under normal temperature, obtain conditioner B;
Step 3:Weigh wheat-germ oil 4g, shea butter 3g, coconut oil 3g, golden yellow SIMMONDSIA CHINENSIS SEED OIL 1.5g, stearic acid
0.5g, liquid crystal type are placed in beaker from thickener/emulsifier Lipomulse LUXE 3g, and 80 DEG C of heating of water-bath, are oil phase;
Step 4:Distilled water 20g is weighed, 80 DEG C of heating of water-bath, are aqueous phase;
Step 5:It is in thread shape by aqueous phase in the case that aqueous phase, oil phase reach mutually synthermal Deng oil phase clear
Add in oil phase, it is stirring while adding, form emulsion bases C;
Step 6:Distilled water 15g is weighed, adds sodium sulfate of polyethenoxy ether of fatty alcohol 2g, Dutch sodium lactate 4g, cocounut oil acyl
Aminocarbonyl propyl glycine betaine CAB 3g, APG APG 2g, sodium lauroyl sarcosine LS30 3g, water-soluble Ve 0.5g, marine alga
Sugared 1g, polyquaternium 3g, biological polyoses glue FUCOGEL 1.5P 3g, lauryl sodium sulfate 0.8g, sodium chloride 0.5g, stirring
Dissolving, obtains solution D;
Step 7:Soapberry extract 3g, Eclipta prostrata extract solution 3g, peppermint extract solution 3g are added into emulsion bases C, is stirred
Mix well mixed, add gel A, conditioner B, solution D, be uniformly mixed;
Step 8:Weigh disodium ethylene diamine tetraacetate 0.04g, ethylparaben or sorbic acid 0.3g, add distilled water
15ml, heating make its dissolving, add in g) system, add essence 0.09ml, with 20% citric acid solution 0.7ml, adjust pH
It is worth after 7, to stir 15min, is well mixed, produces antistatic, radiation proof hair cream.Here can be added according to different demands
Essence, described essence are green cucumber essence, flavoring rose essence, osmanthus flower fragrance, peach flavor, lemon extract, flavoring pineapple essence, jasmine
One or more in essence.
The wherein preparation of soapberry extract:Soapberry peels off kernel, weighs 40g, then soaks 1h, is heated to 100 DEG C, decocts
3 times, the 1st time plus 9 times amount water of extraction are boiled, 1.5h is extracted, the 2nd time plus 9 times amount water, extracts 1h, the 3rd time plus 7 times amount water, extraction
1h, filtration, merging filtrate, the volume concentration of filtrate are filtered and produced to 4 times (g/ml) of soapberry weight every time.
The wherein preparation of Eclipta prostrata extract solution:Eclipta prostrata 50g is weighed, extracts 2 times, the 1st time plus 15 times of waters, extracts 1h,
2nd use, 12 times of waters, 1h is extracted, is filtered every time with 3 layers of gauze, merging filtrate, heating is concentrated into 5 times of Eclipta prostrata weight
(g/ml), filter and produce.
The wherein preparation of peppermint extract solution:Weigh peppermint 30g, soak 1h, refluxing extraction 3 times, the 1st time plus 15 times amount water,
1.5h is extracted, the 2nd time plus 12 times amount water, 1h is extracted, the 3rd time plus 9 times amount water, extracts 1h, every time filtration, merging filtrate, filtrate
Volume concentration to 6 times (g/ml) of peppermint weight, the activated carbon of liquid feeding body weight 3%, 80 DEG C of heating water baths stirrings, filter, i.e.,
Can.
The physical and chemical index and result of embodiment 1,2,3 are as follows:
Character:Each embodiment is that viscosity is suitable, and foaming abundancy, cool and comfortable, stability is good, fragrant, fine and smooth
Uniform milky hair cream.
Hair cream obtained by taking each embodiment, is determined with pH meter, measures pH value between 6.0-7.0.
Each hair cream is packaged in transparence cosmetic bottle, in 4 DEG C of refrigerator cold-storage observations in one month without lamination.In
24h in 55 DEG C of insulating box, hair cream without layering, it is spoiled phenomena such as.
Each hair cream is packaged in 3000r/min in tool plug test tube, centrifuges 20min, no lamination.
1,2,3 made hair cream of embodiment is placed in bottle for cosmetics, is stored at room temperature and investigates 6 months, no lamination,
Feel unchanged after, smell is unchanged.
Irritation test, anaphylaxis experiment
Small white mouse back cuts off hair, smears respectively by hair cream prepared by embodiment 1,2,3 in cutting plucked position, with less
Amount water rubs foam, is then cleaned with clear water, and does not apply position and be compared, as a result without excitant and allergic reaction.
(15-65 year, 150 people) hair cream prepared with embodiment 1,2,3 of volunteer is washed hair, and is observed after spending 30 minutes, head
There is not rubescent, dermexanthesis, foaming phenomena in Pi Jun, and hair is also without dry and astringent, the uninteresting phenomenon of appearance, and find in use
The hair cream is homogeneous, easily goes out foam, and foam is fine and smooth, easily cleans, fragrant, feels that hair is submissive, glossy after washing, rich
It is flexible.
Hair cream resultant effect is investigated
Following with probation the effect of feeling to evaluate hair cream that embodiment 1,2,3 produces.Commented using opinion poll
Point-score, the people of 150 25-65 year age brackets is chosen as object on probation, three groups are arbitrarily divided into, respectively with embodiment 1,2,3
The hair cream cleaning hair of preparation.Wash hair weekly twice, usage time is two months.Every using effect total score is 5 points:5 points
For best result, represent preferable, it is very satisfied;4 points are fine;3 points are to receive;Less than 3 points are bad, it is impossible to are received.With
It is down every average, the results are shown in Table 1:
The resultant effect of table 1 is investigated
In summary, the hair cream exquisiteness is soft and smooth, there is fine an alimentary, moisture retention and antistatic effect, feels during use
It is very salubrious comfortable, it is easy to clean, and foam is fine and smooth stable.Embodiment 2 is more preferably embodiment of the invention.
To embodiment 2,3 black hair measure of merit
Choosing the hair of 100 25-40 year age brackets has the people of sallow situation as object on probation, is arbitrarily divided into two
Group, before experiment, first pass through take pictures and each cut a small amount of hair do contrast use.Then washed respectively with prepared by embodiment 2,3
Hair cream cleans hair.Wash hair 3 times weekly, usage time is 3 months, during which respectively asks for a small amount of hair contrast every other month and sees
Examine.After off-test, by observation, record experimental result can be seen that the sallow situation of the hair of two groups of people makes moderate progress, and
With the lengthening of usage time, pitch-black phenomenon is more obvious.Thus experiment is it can be seen that this hair cream has preferable pitch-black hair
Effect, long-term use of hair is pitch-black shinny, elegant submissive.
The invention is not limited in above-described embodiment, in the case where not departing from spirit and its real situation of the invention, this area
Those of ordinary skill can be made according to the present invention it is various it is corresponding change and deformation, these modifications that the present invention should be mutually carried out or
Equivalent substitution, it all should cover among the protective scope of the claims of the present invention.