CN104312271A - Quick-drying alcohol-based printing ink and preparation method thereof - Google Patents
Quick-drying alcohol-based printing ink and preparation method thereof Download PDFInfo
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- CN104312271A CN104312271A CN201410627081.8A CN201410627081A CN104312271A CN 104312271 A CN104312271 A CN 104312271A CN 201410627081 A CN201410627081 A CN 201410627081A CN 104312271 A CN104312271 A CN 104312271A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses quick-drying alcohol-based printing ink. The quick-drying alcohol-based printing ink is characterized by being prepared from the following raw materials in part by weight: 3-5 parts of cellulose nitrate, 20-25 parts of polyamide resin, 3-6 parts of carboxymethyl chitosan, 15-18 parts of amyl acetate, 18-24 parts of butyl acrylate, 27-35 parts of ethanol, 25-30 parts of 1, 2-propylene glycol, 2-4 parts of hydrogenated castor oil, 0.4-0.7 part of aloe oil, 1-2 parts of graphite powder, 12-15 parts of iron oxide red pigment, 2-4 parts of wormwood, 3-5 parts of dandelion, 4-8 parts of metakaolin, 0.6-0.9 part of a silane coupling agent KH-550 and 4-8 parts of an auxiliary agent. The quick-drying alcohol-based printing ink prepared by taking modified iron oxide red pigment and the polyamide resin as bonding materials, and adding the wormwood and the dandelion into the raw materials is small in odor, good in drying balance, high in drying speed, bright in color, good in gloss and excellent in adhesion and composite strength, and when being applied to plastic flexible packaging gravure printing, has the advantages of low process requirements, high production efficiency, stable product quality and the like.
Description
Technical field
The present invention relates to printing material technical field, be specifically related to a kind of fast-drying type alcohol based printing ink and preparation method thereof.
Background technology
Ink is the material for the formation of graph text information in printing process, by chromoplastid (as pigment, dyestuff etc.), low-melting ink vehicle, fill out the uniform mixture with the pulpous state adherent of certain degree of mobilization that the materials such as (filling) expects, additional material form, can print, and dry in printed body.Therefore ink should have chromatic colour, good printing adaptability, suitable rate of drying.In addition, the application indexes of the aspects such as certain solvent resistant, acid, alkali, water, light, heat, wear-resisting, fungus and mildew resistance should also be had.Along with printing, paper and other requirement etc. are more and more higher, the printing-ink that prior art is produced cannot meet the demand of Printing industry and goods completely.
For overcoming the deficiencies in the prior art, be necessary to be improved existing printing-ink production technology, thus produce the printing-ink with functions such as cost is low, function diversification, high temperature resistant, hardness is high, wear-resisting, chemically burn into rate of drying is fast, printing adaptability is good.
Summary of the invention
Object of the present invention is just to provide a kind of fast-drying type alcohol based printing ink and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of fast-drying type alcohol based printing ink, it is characterized in that, be made up of the raw material of following weight part: Nitrocellulose 3-5, polyamide resin 20-25, cm-chitosan 3-6, pentyl acetate 15-18, butyl acrylate 18-24, ethanol 27-35,1,2-PD 25-30, hydrogenated castor oil 2-4, Aloe oil 0.4-0.7, Graphite Powder 99 1-2, ferric oxide red colorant 12-15, wormwood 2-4, taraxacum 3-5, metakaolin 4-8, silane resin acceptor kh-550 0.6-0.9, auxiliary agent 4-8.
Described auxiliary agent is made up of following raw materials in part by weight: tree ash 5-8, irgasfos 168 0.3-0.6, permeate agent SF-102 0.2-0.5, Magnesium Stearate 0.4-0.7, isocaprylic acid zinc 0.6-0.9, lauryl alcohol phosphoric acid ester potassium 1.1-2.1, tributyl phosphate 6-9, N-BUTYL ACETATE 7-10, benzylideneacetone 1-2, paraffin 3-4, paste dryer 2-3, peanut oil 2.3-3.5, propyl methocel 0.03-0.06, polybutene 2.1-3.6, propylene glycol 4-7, its preparation method first the hydrochloric acid soln of tree ash 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly tributyl phosphate is added in tree ash after the treatment, propylene glycol, paraffin, paste dryer, Magnesium Stearate, lauryl alcohol phosphoric acid ester potassium heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
The preparation method of described a kind of fast-drying type alcohol based printing ink, is characterized in that comprising the following steps:
(1) obtained the concentrated liquid of tradition Chinese medicine is filtered in wormwood, taraxacum boiling, add ferric oxide red colorant, Graphite Powder 99, cm-chitosan agitation grinding 1-2 hour, spraying dry;
(2) metakaolin is put into calcining furnace and process 40-50 minute at 760-870 DEG C, cooling adds hydrogenated castor oil grinding 30-60 minute;
(3) by ethanol, 1,2-propylene glycol stirring and evenly mixing, add pentyl acetate, butyl acrylate be heated to 70-90 DEG C stir 1-2 hour, add Nitrocellulose again, polyamide resin stirs 30 minutes, add step (1), 30-40 minute is stirred in (2) continuation, add hydrogenated castor oil, silane resin acceptor kh-550 and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
The present invention has following beneficial effect: the present invention adopts the ferric oxide red colorant of modification and urethane resin as binder, add ink obtained in wormwood and taraxacum to raw material simultaneously, smell is little, desiccated balance and rate of drying good, lovely luster, glossiness is good, sticking power and combined strength bination excellent, has processing requirement low as plastic flexible package intaglio printing, the advantages such as production efficiency is high, constant product quality.
Embodiment
Described a kind of fast-drying type alcohol based printing ink, it is characterized in that, be made up of the raw material of following weight part: Nitrocellulose 4, polyamide resin 23, cm-chitosan 6, pentyl acetate 17, butyl acrylate 19, ethanol 29,1,2-PD 28, hydrogenated castor oil 2, Aloe oil 0.6, Graphite Powder 99 1, ferric oxide red colorant 12, wormwood 2, taraxacum 5, metakaolin 8, silane resin acceptor kh-550 0.6, auxiliary agent 6.
Described auxiliary agent is made up of following raw materials in part by weight: tree ash 7, irgasfos 168 0.5, permeate agent SF-102 0.4, Magnesium Stearate 0.6, isocaprylic acid zinc 0.8, lauryl alcohol phosphoric acid ester potassium 1.8, tributyl phosphate 6, N-BUTYL ACETATE 7, benzylideneacetone 1, paraffin 3, paste dryer 3, peanut oil 2.9, propyl methocel 0.03, polybutene 2.6, propylene glycol 4, its preparation method first the hydrochloric acid soln of tree ash 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly tributyl phosphate is added in tree ash after the treatment, propylene glycol, paraffin, paste dryer, Magnesium Stearate, lauryl alcohol phosphoric acid ester potassium heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
Making method comprises the following steps:
(1) obtained the concentrated liquid of tradition Chinese medicine is filtered in wormwood, taraxacum boiling, add ferric oxide red colorant, Graphite Powder 99, cm-chitosan agitation grinding 1-2 hour, spraying dry;
(2) metakaolin is put into calcining furnace and process 40-50 minute at 760-870 DEG C, cooling adds hydrogenated castor oil grinding 30-60 minute;
(3) by ethanol, 1,2-propylene glycol stirring and evenly mixing, add pentyl acetate, butyl acrylate be heated to 70-90 DEG C stir 1-2 hour, add Nitrocellulose again, polyamide resin stirs 30 minutes, add step (1), 30-40 minute is stirred in (2) continuation, add hydrogenated castor oil, silane resin acceptor kh-550 and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
The technical parameter index of the printing-ink using the present invention to produce is as follows:
(1) quality is homogeneous, uses cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, 100% attachment;
(2) tinting strength (%): 98;
(3) viscosity (S): 45;
(4) first dryness (mm): 32.
Claims (2)
1. a fast-drying type alcohol based printing ink, it is characterized in that, be made up of the raw material of following weight part: Nitrocellulose 3-5, polyamide resin 20-25, cm-chitosan 3-6, pentyl acetate 15-18, butyl acrylate 18-24, ethanol 27-35,1,2-PD 25-30, hydrogenated castor oil 2-4, Aloe oil 0.4-0.7, Graphite Powder 99 1-2, ferric oxide red colorant 12-15, wormwood 2-4, taraxacum 3-5, metakaolin 4-8, silane resin acceptor kh-550 0.6-0.9, auxiliary agent 4-8, described auxiliary agent is made up of following raw materials in part by weight: tree ash 5-8, irgasfos 168 0.3-0.6, permeate agent SF-102 0.2-0.5, Magnesium Stearate 0.4-0.7, isocaprylic acid zinc 0.6-0.9, lauryl alcohol phosphoric acid ester potassium 1.1-2.1, tributyl phosphate 6-9, N-BUTYL ACETATE 7-10, benzylideneacetone 1-2, paraffin 3-4, paste dryer 2-3, peanut oil 2.3-3.5, propyl methocel 0.03-0.06, polybutene 2.1-3.6, propylene glycol 4-7, its preparation method first the hydrochloric acid soln of tree ash 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly tributyl phosphate is added in tree ash after the treatment, propylene glycol, paraffin, paste dryer, Magnesium Stearate, lauryl alcohol phosphoric acid ester potassium heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
2. the making method of a kind of fast-drying type alcohol based printing ink according to claim 1, is characterized in that comprising the following steps:
(1) obtained the concentrated liquid of tradition Chinese medicine is filtered in wormwood, taraxacum boiling, add ferric oxide red colorant, Graphite Powder 99, cm-chitosan agitation grinding 1-2 hour, spraying dry;
(2) metakaolin is put into calcining furnace and process 40-50 minute at 760-870 DEG C, cooling adds hydrogenated castor oil grinding 30-60 minute;
(3) by ethanol, 1,2-propylene glycol stirring and evenly mixing, add pentyl acetate, butyl acrylate be heated to 70-90 DEG C stir 1-2 hour, add Nitrocellulose again, polyamide resin stirs 30 minutes, add step (1), 30-40 minute is stirred in (2) continuation, add hydrogenated castor oil, silane resin acceptor kh-550 and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410627081.8A CN104312271A (en) | 2014-11-10 | 2014-11-10 | Quick-drying alcohol-based printing ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410627081.8A CN104312271A (en) | 2014-11-10 | 2014-11-10 | Quick-drying alcohol-based printing ink and preparation method thereof |
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| CN104312271A true CN104312271A (en) | 2015-01-28 |
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| CN201410627081.8A Pending CN104312271A (en) | 2014-11-10 | 2014-11-10 | Quick-drying alcohol-based printing ink and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105504966A (en) * | 2016-02-19 | 2016-04-20 | 魏本武 | Novel lithographic plate offset printing ink |
| CN106280692A (en) * | 2016-08-15 | 2017-01-04 | 安徽明诚塑业有限公司 | A kind of Environmental-protection water-based ink and preparation method thereof |
| CN107556424A (en) * | 2017-08-31 | 2018-01-09 | 广东立得新材料科技有限公司 | A kind of water-based 3D printing ink acrylic resin and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102321405A (en) * | 2011-07-28 | 2012-01-18 | 黄山新力油墨科技有限公司 | Environmentally-friendly surface printing plastic white ink and preparation method thereof |
| JP2012107131A (en) * | 2010-11-18 | 2012-06-07 | Toyo Ink Sc Holdings Co Ltd | Gravure printing ink composition for front printing |
| CN103627249A (en) * | 2013-11-29 | 2014-03-12 | 洋紫荆油墨（浙江）有限公司 | Ester-soluble polyurethane compound printing ink with high composite strength and preparation method thereof |
| CN103725085A (en) * | 2013-12-26 | 2014-04-16 | 中山大学 | Stereoscopic offset printing ink prepared by using waste vegetable oil foots as well as preparation method and application of stereoscopic offset printing ink |
-
2014
- 2014-11-10 CN CN201410627081.8A patent/CN104312271A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2012107131A (en) * | 2010-11-18 | 2012-06-07 | Toyo Ink Sc Holdings Co Ltd | Gravure printing ink composition for front printing |
| CN102321405A (en) * | 2011-07-28 | 2012-01-18 | 黄山新力油墨科技有限公司 | Environmentally-friendly surface printing plastic white ink and preparation method thereof |
| CN103627249A (en) * | 2013-11-29 | 2014-03-12 | 洋紫荆油墨（浙江）有限公司 | Ester-soluble polyurethane compound printing ink with high composite strength and preparation method thereof |
| CN103725085A (en) * | 2013-12-26 | 2014-04-16 | 中山大学 | Stereoscopic offset printing ink prepared by using waste vegetable oil foots as well as preparation method and application of stereoscopic offset printing ink |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105504966A (en) * | 2016-02-19 | 2016-04-20 | 魏本武 | Novel lithographic plate offset printing ink |
| CN106280692A (en) * | 2016-08-15 | 2017-01-04 | 安徽明诚塑业有限公司 | A kind of Environmental-protection water-based ink and preparation method thereof |
| CN107556424A (en) * | 2017-08-31 | 2018-01-09 | 广东立得新材料科技有限公司 | A kind of water-based 3D printing ink acrylic resin and preparation method thereof |
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Application publication date: 20150128 |
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