CA1313453C - Apparatus and method for hydroenhancing fabric - Google Patents
Apparatus and method for hydroenhancing fabricInfo
- Publication number
- CA1313453C CA1313453C CA 597326 CA597326A CA1313453C CA 1313453 C CA1313453 C CA 1313453C CA 597326 CA597326 CA 597326 CA 597326 A CA597326 A CA 597326A CA 1313453 C CA1313453 C CA 1313453C
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- Prior art keywords
- fabric
- fluid
- approximately
- yarn
- spun
- Prior art date
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C29/00—Finishing or dressing, of textile fabrics, not provided for in the preceding groups
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/492—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres by fluid jet
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H18/00—Needling machines
- D04H18/04—Needling machines with water jets
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Woven Fabrics (AREA)
- Treatment Of Fiber Materials (AREA)
- Physical Water Treatments (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Abstract APPARATUS AND METHOD FOR HYDROENHANCING FABRIC
An apparatus 10 and related process for enhancement of woven and knit fabrics through use of dynamic fluids which entangle and bloom fabric yarns. A two stage enhancement process is employed in which top and bottom sides of the fabric are respectively supported on members 22, 34 and impacted with a fluid curtain including high pressure jet streams. Controlled process energies and use of support members 22, 34 having open areas 26, 36 which are aligned in offset relation to the process line produces fabrics having a uniform finish and improved characteristics including, edge fray, drape, stability, abrasion resistance, fabric weight and thickness.
An apparatus 10 and related process for enhancement of woven and knit fabrics through use of dynamic fluids which entangle and bloom fabric yarns. A two stage enhancement process is employed in which top and bottom sides of the fabric are respectively supported on members 22, 34 and impacted with a fluid curtain including high pressure jet streams. Controlled process energies and use of support members 22, 34 having open areas 26, 36 which are aligned in offset relation to the process line produces fabrics having a uniform finish and improved characteristics including, edge fray, drape, stability, abrasion resistance, fabric weight and thickness.
Description
~3~.~3 Description APPARATUS AND METHOD FOR HYDROENHANCING FABRIC PROPERTIES
Field of Invention This invention generally relates to a textile finishing process for upgrading the quality of woven and knit fabrics.
' More particularly, it is concerned with a hydroentangling process whieh enhanees woven and knit ~abries through use of dynamic fluid jets to entangle and eause fabric yarns to bloom.
Fabrics produced by the method of the invention have enhaneed surfaee finish and improved eharacteristics sueh as eover, abrasion resistanee, drape, stability as well as redueed air permeability, wrinkle reeovery, seam slippage, and edge fray.
Baekaround Art The quality of a woven or knit fabric can be measured by various properties, such as, the yarn count, thread eount, abrasion resistanee, cover, weight, yarn bulk, yarn bloom, torque resistance, wrinkle recovery, drape and hand.
Yarn eount is the numerical designation given to indieate yarn size and is the relationship of length to weight.
; Thread count in woven or knit fabrics, respeeti~ely, defines the nu~.~her e~lds and picks, and wales and courses per inch vf fabric. For example, the count of cloth is indicated by enumerating first the number of warp ends per inch, then the number of filling picks per inch. Thus, 6~ x 72 defines a fabric 5 having 68 warp ends and 72 filling picks per inch.
Abrasion resistance is the ability of a fabric to withstand loss of appearance, utility, pile or surface through destructive action of surface wear and rubbing.
50ver is the degree to which underlying structure in a 10 fabric is concealed by surface material. A measure of cover is provided by fabric air permeability, that is, the ease with which air passes through the fabric. Permeability measures fundamelltal fabric qualities and characteristics such as filtration and cover.
Yarn bloom is a measure of the opening and spread of f ibers in yarn.
Fabric weight is measured in weight per unit area, for example, the number of ounces per square yard.
Torque of fabric refers to that characteristic which tends 20 to make it turn on itself as a result of twisting. It is desirable to remove or diminish torque in fabrics. For example, fabrics used in vertical blinds should have no torque, since such torque will make the fabric twist when hanging in a strip.
Wrinkle recovery is the property of a fabric which enables 25 it to recover from folding deformations.
Hand refers to tactile fabric properties such as softness and drapability.
~L3~3~53 It is known in the prior art to employ hydroentangling processes in the production of nonwoven materials. In conventional hydroentangling proceises, webs of nonwoven fibers are treated T~rith high pressure fluids while supported on 5 apertured patterning screens. Typically, the patterning screen is provided on a drum or continuous planar conveyor which traverses pressurized fluid jets to entangle the web into cohesive ordered fiber groups and configurations corresponding to open areas in the screen. Entanglement is efrected by 10 action of the fluid jets ~Ihich cause fibers in the web to migrate to open areas in the screen, entangle and intertwine.
Prior art hydroentangling processes for produclng patterned nonwoven fabrics are represented by U.S. Patent Nos.
3,485,706 and 3,498,874, respectively, to Evans and Evans et 15 al., and U.S. Patent Nos. 3,873,255 and 3,917,785 to Kalwaites.
Hydroentangling technology has also been employed by the art to enhance woven and knit fabrics. In such applications warp and pick fibers in fabrics are hydroentangled at cross-over points to effect enhancement in fabric cover. However, 20 conventional processes have not proved entirely satisfactory in yielding uniform fabric enhancement. The art has also failed to develop apparatus and process line technolog~ which achieves production line efficiencies.
Australian Patent Specification 287821 to Bunting et al.
25 is representative of the state of the art. Bunting impacts high speed columnar fluid streams on fabrics supported on course porous members. Preferred parameters employed in the Bunting _4_ ~3~34~3 process, described in the Specification Example Nos. XV - XVII, include 20 and 30 mesh support screens, fluid pressure of 1500 psi, and jet orifices having 0.007 inch diameters on 0.050 inch centers. Fabrics are processed employing multiple 5 hydroentangling passes in which the fabric is reoriented on a bias direction with respect to the process direction in order to effect uniform entanglement. Data set forth in the Examples evidences a modest enhancement in fabric cover and stability.
Another approach of art is repr~sented by European Patent 10 Application 0 177 277 to Willb ~ s et al which is d~rec-ted to hydro-patterning technology. Willbanks impinges high velocity fluids onto woven, knitted and bonded fabrics for decorative effects.
Patterning is effected by redistributing yarn tension within the fabric - yarns are selectively compacted, loosened and opened -~5 to impart relief structure to the fabric.
Fabric enhancement of limited extent is obtained in Willbanks as a secondary product of the patterning process.
However, Willbanks fails to suggest or teach a hydroentangling ; process that can be employed to uniformly enhance fabric 20 characteristics. See Willbanks, Example 4, page 40.
There is a need in the art for an improved woven textilehydroenhancing process which is commercially viable. It will be appreciated that fabric enhancement offers aesthetic and functional advantages which have application in a wide diversity 25 of fabrics. Hydroenhancement improves fabric cover through dynamic fluid entanglement and bulking of fabric yarns for improved fabric stability. These results are advantageously ,.
... .; .. .. .. ..
~" R~' ~ `3 ~ ~j 3 _F~_ obtained without requirement of conventional fabric finishing processes.
The art also requires apparatus of uncomplex design for hydroenhancing textile materials. Co}nmercial production 5 requires apparatus for continuous fabric hydroenhancing and in-line drying of such fabrics under controlled conditions to yield fabrics of uniform specifications.
Accordingly, it is a broad object of the inv~ntion to provide an improved textile hydroenhancing process and related 10 apparatus for production of a variety of novel woven and knit fabrics having improved characteristics which advance the art.
A more specific object of the invention is to provide a hydroenhancing process for enhancement of fabrics made of spun and spun/filament yarn.
Another object of the invention is to provide a hydroenhancing process having application for the fabrication of ; novel composite and layered fabrics.
A further object of the invention is to provide a hydroenhancing production line apparatus which is less comple~
20 and improved over the prior art.
Disclosure of the Inventlon In the present invention, these purposes, as well as others which will be apparent, are achieved generally by providing an apparatus and a related method for hydroenhancing 25 woven and knit fabrics through dynamic fluid action. A
hydroenhancing module is employed in the invention in which the fabric is supported on a member and impacted with a ~luid , :.. ::
-6- ~3~345~
curtain under con~rolled process energies. Enhancement of the fabric is effected by entanglement and intertwinin~ of yarn fibers at cross-over points in the fabric weave or knit. ~abrics enhance~ in accor~ance with the invention have a uniform finish 5 and improved characteristics, such as, edge fray, drape, stabllity, wrinkle recovery, abrasion resistance, fabric weight and thickness.
According to the preferred method of the invention, the woven or knit fabric is advanced on a process line through a weft 10 straightener to two in-line fluid modules for first and second stage fabric enhancement. Top and bottom sides of the fabric are respectively supported on members in the modules and impacted by fluid curtains to impart a uniform finish to the fabric.
Preferred support members are fluid pervious, include open areas 15 of approximately 25%, and have fine mesh patterns which permit fluid passage without imparting a patterned effect to the fabric.
It is a feature of the invention to employ support members in the modules which include fine mesh patterned screens which are arranged in offset relation with respect to the process line.
20 This offset orientation limits fluid streaks and eliminates reed marking in processed fabrics.
First and second stage enhancement is preferably effected by columnar fluid jets which impact the fabric at pressures within the range of 200 to 3000 p5i and impart a total 25 energy to the fabric of approximately .10 to 2.0 hp-hr/lb.
Following enhancement, the fabric is advanced to a tenter frame which dries the fabric to a specified width under tension . . .~.~. .
.. . . . . ..
~ . ~ s~ " .. .....
~3~L3~3 to produce a uniform fabric finish.
Advanta~e in the invention apparatus is obtained by provision of a continuous process llne of uncomplex design. The first and second enhancement stations include a plurality of 5 cross-directionally ("C~") aligned and spaced manifolds.
Columnar jet no~zles having orifice diameters of approximately 0.005 inches with center-to-center spacings of approximately .017 inches are mounted approximately .5 inches from the screens. At the process energies of the invention, this spacing arrangement 10 provides a curtain of fluid which yields a uniform fabric enhancement. Use of fluid pervious support members which are oriented in offset relation, preferably 45~, efl`ectively limits jet streaks and eliminates reed markings in processed fabrics.
Optimum fabric enhancement results are obtain~d in fabrics 15 woven or knit of yarns including fibers with deniers and staple lengths in the range of 0.5 to 6.0, and 0.5 to 5 inches, respectively, and yarn counts in the range of .5s to 50s.
Preferred yarn spinning systems of the invention fabrics include cotton spun, wrap spun, wool spun and friction spun.
Other objects, features and advantages of the present invention will be apparent when the detailed description of the preferred embodiments of the invention are considered in conjunction with the drawings which should be construed in an illustrative and not limiting sense as follows:
25 Brief Descri~tion of the Drawinqs Fig. 1 is a schematic view of a production line including a weft straightener, flat and drum hydroenhancing modules, and 3~3 tenter frame, for the hydroenhancement of woven and knit fabrics in accordance with the inventi,on;
Figs. 2A and B are photographs at lOX magnification of 36x29 90 and 40~40 45 mesh plain weave support members, 5 respectively, employed in the flat and drum enhancing modules of Fig. l;
Figs. 3A and B are photomicrographs at lOX magnification of a fine polyester woven fabric before and after hydroenhancement in accordance with the invention;
Figs. 4A and B are photomicrographs at 16X magnification of the control and processed fabric of Figs. 3A and B;
Figs. 5A and B are photomicrographs at lOX magni~ication of a control and hydroenhanced woven acrylic fabric;
Figs. 6A and B are photomicrographs at lOX magnification of 15 a control and hydroenhanced acrylic fabric woven of wrap spun yarn;
Figs. 7A and B are photomicrographs at lOX magnification of a control and hydroenhanced acrylic fabric woven of wrap spun yarn;
Figs. 8A and B are photomicrographs at lOX magnification of a control and hydroenhanced acrylic fabric including open end wool spun yarn;
Figs. 9A and B are photomicro~raphs at 16X magnification of a control and hydroenhanced wool nylon (80/20~) fabric;
Figs. lOA and B are photomicrographs at 16X magnification of a control and hydroenhanced spun/filament polyester/cotton twill fabric;
~L3~3~
g Figs. llA and B are photomicrographs at 16X magnification of a control and hydroenhanced doubleknit fabric;
Figs. 12A and B are front and back side photomicrographs at 16X magnification of a c~ntrol wall covering fabric;
Figs. 13A and B are front and back side photomicrographs at 16X magnification of the wall covering fabric of Figs. 12A
and B hydroenhanced in accordance with the invention;
Flgs. 14A and B are photomacrographs a~ O.O9X magnification of a control and hydroenhanced acrylic fabric strips, the fabric of 10 Figs. 7A and B, showing the reduction in fabric torque achieved in the invention process;
Figs. 15 A-C are photomacrographs at 0.23X magnification, respectively, of the woven acrylic fabrics of Figs. 5, 7 and 8 comprised of wrap spun and open end wool spun yarns, showing 15 washability and wrinkle characteristics of control and processed fabrics;
Fig. 16 is a schematic view of an alternative production line apparatus for the hydroenhancement of woven and knit fabrics in accordance with the invention; and Fig. 17 illustrates a composite fabric including nappe~
fabric components which are bonded into an integral structure employing the hydroenhancing process of the invention.
Best Mode of Carryinq out The Invention ~ith further reference to the drawings, Fig. l illustrates a preferred embodiment of a productlon line of the invention, generally designated lO, for hydroenhancement of a fabric 12 :3L3~3~i3 including spun and/or spun/filament yarns. The line includes a conv~ntional weft straightener 1~, fla-t and drum enhancing modules 16, 18, and a tenter frame 20.
Modules 16, 18 effect two sided enhancement of the fabric 5 through fluid entanglement and bulking of fabric yarns. Such entanglement is imparted to the fabric in areas of yarn cross-over or intersection. Control of process energies and provision of a uniform curtain of fluid produces fabrics having a uniform finish and improved characteristics including, edge fray, torque, lo wrinkle recovery, cupping, drape, stability, abrasion resistance, fabric weight and thickness.
Method and ~echanism o~ the Enhancln~ Modules Fabric is advanced through the weft straightener 14 which aligns the fabric weft prior to processing in enhancement 15 modules 16, 18. Following hydroenhancement, the fabric is advanced to the tenter frame 20, which is of conventional design, where it is dried under tension to produce a uniform fabric of specified width.
Module 16 includes a first support member 22 which is 20 supported on an endless conveyor means including rollers 24 and drive means (not shown) for rotation of the rollers. Preferred line speeds for the conveyor are in the range of 10 to 500 ft/min. Line speeds are adjusted in accordance with process energy requirements which vary as a function of fabric type and 25 weight.
Support member 22, which preferably has a flat configuration, includes closely spaced fluid pervious open areas ~3~
26. A preferred support member 22, shown in Fig. 2A, ls a 36x29 90~ mesh plain weave having a 23.7% open area, fabricatecl of polyester warp and shute round wire. Support member 22 i.s a tight seamless weave which is not subject to angular 5 displacement or snag. Specifications for the screen, which is manufactured by Albany International, Appleton Wire Division, P.o. Box 1939, Appleton, Wisconsin 54913 are set forth in Table I.
TABLE I
Support Screen Specifications _ .
Property 36x29 90 flat mesh 40x40 45 drum mesh 15 Wire polyester stainless steel Warp wire .0157 0.010 Shute w.ire .0157 0.010 Weave type plain plain Open area 23.7% 36%
Module 16 also includes an arrangement of parallel and spaced manifolds 30 oriented in a cross-direction ("CD") relative 30 to movement of the fabric 12. The manifolds which are spaced approximately 8 inches apart each include a plurality of closely aligned and spaced columnar jet orifices 32 which are spaced approximately .5 inches from the support member 22.
I'he jet orifices have diameters and center-to-center 35 spacin~s in the range of .005 to .010 inches and .017 to .034 inches, respectively, and are designed to i.mpact the fabric with -12~ 3 fluid pressures in the range of 200 to 3000 psi. Preferred orifices have diameters of approximately .005 inches with center~to-center spacings of approximately .017 inches~
This arrangement of fluid jets provides a curtain of fluid 5 entangling streams which yield optimum enhancement in the fabric.
Energy input to the fabric is cumulative along the line and preferably set at approximately the same level in modules 16, 18 (two stage system) to impart uniform enhancement to top and bottom surfaces of the fabric. Effective first stage enhancement 10 of fabric yarn is achieved at an energy output of at least .05 hp-hr/lb and preferably in the range of .1 to 2.0 hp-hr/lb.
Following the Pirst stage enhancement, the fabric is advanced to module 18 which enhances the other side of the fabric. Module 18 includes a second support member 34 of 15 cylindrical configuration which is supported on a drum. The member 34 includes closely spaced fluid pervious open areas 36 which comprise approximately 36% of the screen area. A
preferred support member 34, shown in Fig. 2B, is a 40x40 45 mesh stainless steel screen, manufactured by Appleton Wire, ~0 havlng the specifications set forth in Table I.
Module 18 functions in the same manner as the planar module 16. Manifolds 30 and jet orifices 32 are provided which ha~e substantially the same specifications as in the first stage enhancement module. Fluid energy to the fabric of at least 0.5 25 hp-hr/lb and preferably in the range of .1 to 2.0 hp-hr/lb effects second stage enhancement.
Conventional weaving processes impart reed marks to ~3~ 3 fabrics. Illustrations of such markings are shown in Figs. 3A
and 4A which are photomicrographs at lOX and 16X magnification of a polyester LIBBEY brand fabric style no. S/x-A805 (see Tab~e-II). Reed marks in Yigs. 3A and 4A are designated by the let'~er 5 "~".
The invention overcomes this defect in conventional weaving processes through use of a single and preferably two stage hydroenhancement process. Advantage is obtained in the invention process by orienting the drum support member 3~ in lO offset relation, preferably 45, relative to machine direction ("MD") of the hydroenhancing line. See Figs. 2~ and B.
Support members 22 and 3~ are preferably provided with fine mesh open areas which are dimensioned to effect fluid passage through the members without imparting a patterned effect to the 15 fabric. The preferred members have an effective open area for fluid passage in the range of 17 - ~0%.
Comparison of the control and processed polyester fabric of Figs. 3A, B and ~A, B illustrates the advantages obtained through use of the enhancement process. Reed marks R in control 20 polyester fabric are essentially eliminated through enhancement of the fabric. The offset screen arrangement is also effective in diminishing linear jet streak markings associated with the enhancement process.
Exam~lesI-XIII
Figs. 3 - 15 illustrate representative woven and knit fabrics enhanced in accordance with the method of the invention, i3 employing test conditions which simulate the line of Fig. 1.
Table II sets forth specifications for the fabri~s illustrated in the drawings.
As ln the Fig. l line, the -test manifolds 30 were spaced 5 approximately 8 inches apart in modules 16, 18, and provided with densely packed columnar jet orifices 32 of approximately 60/inch.
Orifices 32 each had a diameter of 0.005 inches and were spaced approximately .5 inches from the first and second support members 22, 3~.
The process line of Fig. 1 includes enhancement modules 16, 18 which, respectively, are provided with six manifolds. In the Examples, modules 16, 18 were each fitted with two manifolds 34.
To simulate line conditions, the fabrics were advanced through multiple runs on the line. Three processing runs in each two 15 manifold module was deemed to be equivalent to a SlX manifold module.
Fabrics were hydroenhanced at process pressures of approximately 1500 psi. Line speed and cumulative energy output to the modules were respectively maintained at approximately 30 20 fpm and 0.~6 hp-hr/lb. Adjustments in the line speed and fluid pressure were made to accommodate differences in fabric weight for uniform processing and to maintain the preferred energy level.
Fabrics processed in the Examples exhibited marked 25 enhancement in aesthetic appearance and quality including, characteristics such as cover, bloom, ~brasion resistance, drape, stability, and reduction in seam slippage, and edge fray.
. ., , ~
3~;3 Tables III - XI set forth data for fabrics enhanced in accordance with invention on the test process line. Standard testing procedures of The American Society for Testing and Materials (ASTM) were employed to test control and processed 5 characteristics of fabrics. Data set forth in the Tables was generated in accordance with the following ASTM standards:
Fabric Characteristic STM Standard Weight D3776-79 Thickness Dl777-64 (Ames Tester) Tensile Load D1682-6~ (1975) (Cut strip/grab) Elongation D1682-64 (1975) Air Permeability D737-75 (1980) (Frazier) Thread Count D3775-79 Ball Burst D3787-80A
Seam Slippage D4159-82 Tongue Tear D2261-71 Wrinkle Recovery D1295-67 (1972) Abrasion Resistance D3884-80 Pilling D3514-81 Washability tests were conducted in accordance with the following procedure. Weight measurements ("before wash") were 25 taken of control and processed fabric samples each having a dimension of 8.5"xll" (8.5" fill direction and 11" warp direction). The samples were then washed and dried in conventional washer and dryers three consecutive times and "after wash" measurements were taken. The percent weight loss -~3~3~53 of the pre and post wash samples was determined in accordance the following formula:
% weight loss = D/B x 100 where, B = before wash sample weight; A = after wash sample 5 weight; and D = B-A.
Photomicrographs of the fabrics, Figs. 4-15, illustrate the enhancement in fabric cover obtained in the invention.
Attention is directed to open areas in the unprocessed fabrics, photographs designated A, these areas are of reduced size in the 10 processed fabrics in the photographs designated B.
Hydroenhancement caused fabric yarns to bloom and entangle at cross-over points, filling in open areas to improve cover and reduce air permeability in the fabrics.
Figs. 12 and 13 are photomicrographs of a HYTEX brand wall 15 covering fabric, manufactured by Hytex, Inc, Randolph, Massachuset~. A multi-textured surface appearance of the fabric is provided by yarns which are woven through discrete areas of the front fabric surface. Free floating weave stitches, designated by the letter "S" in Figs. 12B and 13B~ are formed on 20 the backside of the fabric.
Hydroenhancement of HYTEX wall covering fabric secured the free-floating stitches S to the fabric backside enhancing fabric stability and cover. See Figs. 12B, 13B. In wall covering applications, fabric enhance~ent and associated stabilizing 25 effects reduces or eliminates the need for adhesive backcoatings.
Enhancement of the fabric also limits wicking of wall cover application adhesives through the fabric. Further advantage is :~3:~L3~3 ob-tained when enhanced fabrics are used in acoustic applications; elimination of backcoating reduces sound reflection and furthers efficient transmission of sound through the fabric.
TABLE II
.
Fabric Specifications Fiber Brand and Styl~ Desiqnation Fiqure(s) NOMEX S/x-A805* 3A,B, 4A,B
Fiber : 2 denier-1.9 inch Yarn : Open end cotton spun 17s LIBBEY SJ022** 5A,B
Warp:
Fiber: 3 denier - 1.5 inch acrylic Yarn : Open end cotton spun 9s 28 ends per inch Fill:
Fiber: 3 denier ~ 3 inch acrylic Yarn : Open end wool spun . 4s 14, 16 or 18 picks per inch 30 LIBBEy S/x-1160 6A,B
Fiber: 3 denier-3 inch acrylic Yarn : Wrap spun w/100 den textured polyester ~s 14 ends x 16 picks per inch LIBBEY S/406 7A,B, 14A,B
~iO
Warp:
Fiber: 3 denier - 1.5 inch acrylic Yarn : Open end cotton spun 9s 2~ ends per inch Fill:
Fiber: 3 denier - 3.inch acrylic Yarn : Hollow spun 6 twists/inch 4s 14, 16 or 18 picks per inch , . . . . . .
. ~ .
~.
~33L3~53 Table II, continued 5 LIBBEY S/152 8A, B
Warp:
Fiber: 3 denier - 2.5 inch acrylic Yarn : Open end cotton spun 4s 14 ends per inch Fill:
Fiber: 3 denier - 3 inch acrylic Yarn : Open end wool spun 2.6s . 14, 16 or 18 picks per inch Guilford Wool/Nylon 9A,B
80% wool/20~ nylon ., .
Polyester/cotton (53/47) 10A,B
Weight: 10 ounces/yd2 Yarn : Spun Filament Weave : 3xl Twill Thread Count: 120x38 30 50% Polyester/50% cotton Doubleknit llA,B
Yarn: wrap spun with 100 : denier polyester wrap 35 HYTEX Wall covering*** 12, 13 ~LIBBEY is a trademark of W. S. Libbey Co., One Mill Street, Lewiston, ME 04 2 4 0 .
40 **NOMEX is a trademark of E.I. Du Pont de Nemours and Company, Wilminqton, Del.
HYTEX is a trademark of Hytex , Inc., Randolph, MA.
f ~' ~
, ,., , , , 1 ' ~ i TABLæ III
Nomex A805 - Fiq. 4 ControlProcessed % Chance 20 Wei~ht (gsy) 195 197 +1.0 Thickness (mils) 42 42 0 Air Perm. (ft3/ft2/ 331 156 -52.9 min) Strip Tensile (lbs/in) warp 115 132 +14.8 ~ill 59 47 -20.3 Elonqatlon (%) warp 48 50 +4.2 fill 62 71 +14.5 -20- ~3~3~3 TABLE IV
022/6075 (16 ppi) - Fi~. 5 Control Processed % Chanqe 15 Wei~ht (gsy)158 165 + 4.4 Thickness (mils) 48 49 ~ 2.1 Air Perm. (ft3/ft2 406 259 -36.2 min) ~I{L~ _ ile (lbs/in) warp 34 36 + 5.9 fill 37 31 -16.2 Elon~ation (%) warp 33 27 -18.2 fill 27 28 + 3.7 30 Seam Slippaqe (lbs/in) warp 5 60 +1100.0 ~ fill 7 55 + 685.7 `~ Tonaue Tear (lbs) warp 18 10 ~-44.4 ~ill 21 8 -~1.9 , Wt. Loss In Wash (%) 37 5 -86.5 40 Wrinkle Recoverv* 123 138 +12.2 (recovery angle) * Under ASTM test standards (Dl295-67) improvements in the 45 wrinkle recovery of a fabric are indicated by an increase in the recovery angle.
.~
,,, '. ..
~3~3453 TABLE V
Libbey S/x-1160 - Fi.g. 6 Control Processed % Chanqe : 15 Weiqht (gsy)146.8 160.2 9.1 Thickness (mils) 38.1 52.7 38.3 ~0 Ai ~ rm_ (ft3/ft2. 457.2 188.5 .-58.8 min) 25 Grab Tensile (lbs/in) warp80.2 89.3 11.4 ill105.0 111.4 6.1 : Elonqation (%) ; 30 ~ warp 30.0 34~0 13.3 ~ ~ill32.0 46.0 43.8 ; Ball Burst (lbs) 190 157 -17.4 .
.
.~ , .
:. , . ~j -22- 1~3~3 ~ABLE VI
406/6075 (16 ppi) - Fig. 7 Control Processed % Chanqe Weiqht (gsy)159 166 + 4.4 Thickness (mils) 48 50 -~ 4.2 20 Air Perm. (ft3/~t2 351 184 -47.6 mln) nsile (lbs~in) warp 42 36 -14.3 ~ill 66 58 -12.1 Elonaation (%) warp 23 31 +34.8 . fill 49 33 -32.7 Se~ S1iPDag~ (lbs) warp 29 36 +89.5 fill 21 76 + 261.9 35 Tonque Tear (lbs) warp 23 18 -21.7 ~ill 19 . 15 - 1.1 Wt. Loss In Wash (%) 28 4 -85.7 Wrinkle Recovery 140 148 n + 5.7 (recovery angle) :
~a3~3~;3 TABLE VII
__ 152~6076 (16 ppi) - Fia. 8 ControlProcessed % Chanae 10 Weiqht (gsy) 231 257 +11.3 Thickness (mils) 259 238 - 8.1 Air Perm. (ft3/ft2/ 204 106 -48.0 ~in) Strip Tensile (lbs/in) warp 48 58 +20.8 fill 56 72 +28.6 Elonaation (%) warp 33 33 f.ill 34 39 +14.7 25 _am Slippaae (lbs) warp 6~ 81 +26.6 fill 78 112 +43.6 Tonaue Tear (lbs) warp 21 18 -14.3 fill 17 15 -11.8 Wt. Loss In Wash (%) -- -- ----35 Wrinkle Recovery 117 136 ~16.2 (recovery angle) TABLE VIII
_ Guilford Wool (80% wool/20% nylon) - Fiq. 9 Control Process % Chanae Air Perm. 243 147 -39.5 ~
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Field of Invention This invention generally relates to a textile finishing process for upgrading the quality of woven and knit fabrics.
' More particularly, it is concerned with a hydroentangling process whieh enhanees woven and knit ~abries through use of dynamic fluid jets to entangle and eause fabric yarns to bloom.
Fabrics produced by the method of the invention have enhaneed surfaee finish and improved eharacteristics sueh as eover, abrasion resistanee, drape, stability as well as redueed air permeability, wrinkle reeovery, seam slippage, and edge fray.
Baekaround Art The quality of a woven or knit fabric can be measured by various properties, such as, the yarn count, thread eount, abrasion resistanee, cover, weight, yarn bulk, yarn bloom, torque resistance, wrinkle recovery, drape and hand.
Yarn eount is the numerical designation given to indieate yarn size and is the relationship of length to weight.
; Thread count in woven or knit fabrics, respeeti~ely, defines the nu~.~her e~lds and picks, and wales and courses per inch vf fabric. For example, the count of cloth is indicated by enumerating first the number of warp ends per inch, then the number of filling picks per inch. Thus, 6~ x 72 defines a fabric 5 having 68 warp ends and 72 filling picks per inch.
Abrasion resistance is the ability of a fabric to withstand loss of appearance, utility, pile or surface through destructive action of surface wear and rubbing.
50ver is the degree to which underlying structure in a 10 fabric is concealed by surface material. A measure of cover is provided by fabric air permeability, that is, the ease with which air passes through the fabric. Permeability measures fundamelltal fabric qualities and characteristics such as filtration and cover.
Yarn bloom is a measure of the opening and spread of f ibers in yarn.
Fabric weight is measured in weight per unit area, for example, the number of ounces per square yard.
Torque of fabric refers to that characteristic which tends 20 to make it turn on itself as a result of twisting. It is desirable to remove or diminish torque in fabrics. For example, fabrics used in vertical blinds should have no torque, since such torque will make the fabric twist when hanging in a strip.
Wrinkle recovery is the property of a fabric which enables 25 it to recover from folding deformations.
Hand refers to tactile fabric properties such as softness and drapability.
~L3~3~53 It is known in the prior art to employ hydroentangling processes in the production of nonwoven materials. In conventional hydroentangling proceises, webs of nonwoven fibers are treated T~rith high pressure fluids while supported on 5 apertured patterning screens. Typically, the patterning screen is provided on a drum or continuous planar conveyor which traverses pressurized fluid jets to entangle the web into cohesive ordered fiber groups and configurations corresponding to open areas in the screen. Entanglement is efrected by 10 action of the fluid jets ~Ihich cause fibers in the web to migrate to open areas in the screen, entangle and intertwine.
Prior art hydroentangling processes for produclng patterned nonwoven fabrics are represented by U.S. Patent Nos.
3,485,706 and 3,498,874, respectively, to Evans and Evans et 15 al., and U.S. Patent Nos. 3,873,255 and 3,917,785 to Kalwaites.
Hydroentangling technology has also been employed by the art to enhance woven and knit fabrics. In such applications warp and pick fibers in fabrics are hydroentangled at cross-over points to effect enhancement in fabric cover. However, 20 conventional processes have not proved entirely satisfactory in yielding uniform fabric enhancement. The art has also failed to develop apparatus and process line technolog~ which achieves production line efficiencies.
Australian Patent Specification 287821 to Bunting et al.
25 is representative of the state of the art. Bunting impacts high speed columnar fluid streams on fabrics supported on course porous members. Preferred parameters employed in the Bunting _4_ ~3~34~3 process, described in the Specification Example Nos. XV - XVII, include 20 and 30 mesh support screens, fluid pressure of 1500 psi, and jet orifices having 0.007 inch diameters on 0.050 inch centers. Fabrics are processed employing multiple 5 hydroentangling passes in which the fabric is reoriented on a bias direction with respect to the process direction in order to effect uniform entanglement. Data set forth in the Examples evidences a modest enhancement in fabric cover and stability.
Another approach of art is repr~sented by European Patent 10 Application 0 177 277 to Willb ~ s et al which is d~rec-ted to hydro-patterning technology. Willbanks impinges high velocity fluids onto woven, knitted and bonded fabrics for decorative effects.
Patterning is effected by redistributing yarn tension within the fabric - yarns are selectively compacted, loosened and opened -~5 to impart relief structure to the fabric.
Fabric enhancement of limited extent is obtained in Willbanks as a secondary product of the patterning process.
However, Willbanks fails to suggest or teach a hydroentangling ; process that can be employed to uniformly enhance fabric 20 characteristics. See Willbanks, Example 4, page 40.
There is a need in the art for an improved woven textilehydroenhancing process which is commercially viable. It will be appreciated that fabric enhancement offers aesthetic and functional advantages which have application in a wide diversity 25 of fabrics. Hydroenhancement improves fabric cover through dynamic fluid entanglement and bulking of fabric yarns for improved fabric stability. These results are advantageously ,.
... .; .. .. .. ..
~" R~' ~ `3 ~ ~j 3 _F~_ obtained without requirement of conventional fabric finishing processes.
The art also requires apparatus of uncomplex design for hydroenhancing textile materials. Co}nmercial production 5 requires apparatus for continuous fabric hydroenhancing and in-line drying of such fabrics under controlled conditions to yield fabrics of uniform specifications.
Accordingly, it is a broad object of the inv~ntion to provide an improved textile hydroenhancing process and related 10 apparatus for production of a variety of novel woven and knit fabrics having improved characteristics which advance the art.
A more specific object of the invention is to provide a hydroenhancing process for enhancement of fabrics made of spun and spun/filament yarn.
Another object of the invention is to provide a hydroenhancing process having application for the fabrication of ; novel composite and layered fabrics.
A further object of the invention is to provide a hydroenhancing production line apparatus which is less comple~
20 and improved over the prior art.
Disclosure of the Inventlon In the present invention, these purposes, as well as others which will be apparent, are achieved generally by providing an apparatus and a related method for hydroenhancing 25 woven and knit fabrics through dynamic fluid action. A
hydroenhancing module is employed in the invention in which the fabric is supported on a member and impacted with a ~luid , :.. ::
-6- ~3~345~
curtain under con~rolled process energies. Enhancement of the fabric is effected by entanglement and intertwinin~ of yarn fibers at cross-over points in the fabric weave or knit. ~abrics enhance~ in accor~ance with the invention have a uniform finish 5 and improved characteristics, such as, edge fray, drape, stabllity, wrinkle recovery, abrasion resistance, fabric weight and thickness.
According to the preferred method of the invention, the woven or knit fabric is advanced on a process line through a weft 10 straightener to two in-line fluid modules for first and second stage fabric enhancement. Top and bottom sides of the fabric are respectively supported on members in the modules and impacted by fluid curtains to impart a uniform finish to the fabric.
Preferred support members are fluid pervious, include open areas 15 of approximately 25%, and have fine mesh patterns which permit fluid passage without imparting a patterned effect to the fabric.
It is a feature of the invention to employ support members in the modules which include fine mesh patterned screens which are arranged in offset relation with respect to the process line.
20 This offset orientation limits fluid streaks and eliminates reed marking in processed fabrics.
First and second stage enhancement is preferably effected by columnar fluid jets which impact the fabric at pressures within the range of 200 to 3000 p5i and impart a total 25 energy to the fabric of approximately .10 to 2.0 hp-hr/lb.
Following enhancement, the fabric is advanced to a tenter frame which dries the fabric to a specified width under tension . . .~.~. .
.. . . . . ..
~ . ~ s~ " .. .....
~3~L3~3 to produce a uniform fabric finish.
Advanta~e in the invention apparatus is obtained by provision of a continuous process llne of uncomplex design. The first and second enhancement stations include a plurality of 5 cross-directionally ("C~") aligned and spaced manifolds.
Columnar jet no~zles having orifice diameters of approximately 0.005 inches with center-to-center spacings of approximately .017 inches are mounted approximately .5 inches from the screens. At the process energies of the invention, this spacing arrangement 10 provides a curtain of fluid which yields a uniform fabric enhancement. Use of fluid pervious support members which are oriented in offset relation, preferably 45~, efl`ectively limits jet streaks and eliminates reed markings in processed fabrics.
Optimum fabric enhancement results are obtain~d in fabrics 15 woven or knit of yarns including fibers with deniers and staple lengths in the range of 0.5 to 6.0, and 0.5 to 5 inches, respectively, and yarn counts in the range of .5s to 50s.
Preferred yarn spinning systems of the invention fabrics include cotton spun, wrap spun, wool spun and friction spun.
Other objects, features and advantages of the present invention will be apparent when the detailed description of the preferred embodiments of the invention are considered in conjunction with the drawings which should be construed in an illustrative and not limiting sense as follows:
25 Brief Descri~tion of the Drawinqs Fig. 1 is a schematic view of a production line including a weft straightener, flat and drum hydroenhancing modules, and 3~3 tenter frame, for the hydroenhancement of woven and knit fabrics in accordance with the inventi,on;
Figs. 2A and B are photographs at lOX magnification of 36x29 90 and 40~40 45 mesh plain weave support members, 5 respectively, employed in the flat and drum enhancing modules of Fig. l;
Figs. 3A and B are photomicrographs at lOX magnification of a fine polyester woven fabric before and after hydroenhancement in accordance with the invention;
Figs. 4A and B are photomicrographs at 16X magnification of the control and processed fabric of Figs. 3A and B;
Figs. 5A and B are photomicrographs at lOX magni~ication of a control and hydroenhanced woven acrylic fabric;
Figs. 6A and B are photomicrographs at lOX magnification of 15 a control and hydroenhanced acrylic fabric woven of wrap spun yarn;
Figs. 7A and B are photomicrographs at lOX magnification of a control and hydroenhanced acrylic fabric woven of wrap spun yarn;
Figs. 8A and B are photomicrographs at lOX magnification of a control and hydroenhanced acrylic fabric including open end wool spun yarn;
Figs. 9A and B are photomicro~raphs at 16X magnification of a control and hydroenhanced wool nylon (80/20~) fabric;
Figs. lOA and B are photomicrographs at 16X magnification of a control and hydroenhanced spun/filament polyester/cotton twill fabric;
~L3~3~
g Figs. llA and B are photomicrographs at 16X magnification of a control and hydroenhanced doubleknit fabric;
Figs. 12A and B are front and back side photomicrographs at 16X magnification of a c~ntrol wall covering fabric;
Figs. 13A and B are front and back side photomicrographs at 16X magnification of the wall covering fabric of Figs. 12A
and B hydroenhanced in accordance with the invention;
Flgs. 14A and B are photomacrographs a~ O.O9X magnification of a control and hydroenhanced acrylic fabric strips, the fabric of 10 Figs. 7A and B, showing the reduction in fabric torque achieved in the invention process;
Figs. 15 A-C are photomacrographs at 0.23X magnification, respectively, of the woven acrylic fabrics of Figs. 5, 7 and 8 comprised of wrap spun and open end wool spun yarns, showing 15 washability and wrinkle characteristics of control and processed fabrics;
Fig. 16 is a schematic view of an alternative production line apparatus for the hydroenhancement of woven and knit fabrics in accordance with the invention; and Fig. 17 illustrates a composite fabric including nappe~
fabric components which are bonded into an integral structure employing the hydroenhancing process of the invention.
Best Mode of Carryinq out The Invention ~ith further reference to the drawings, Fig. l illustrates a preferred embodiment of a productlon line of the invention, generally designated lO, for hydroenhancement of a fabric 12 :3L3~3~i3 including spun and/or spun/filament yarns. The line includes a conv~ntional weft straightener 1~, fla-t and drum enhancing modules 16, 18, and a tenter frame 20.
Modules 16, 18 effect two sided enhancement of the fabric 5 through fluid entanglement and bulking of fabric yarns. Such entanglement is imparted to the fabric in areas of yarn cross-over or intersection. Control of process energies and provision of a uniform curtain of fluid produces fabrics having a uniform finish and improved characteristics including, edge fray, torque, lo wrinkle recovery, cupping, drape, stability, abrasion resistance, fabric weight and thickness.
Method and ~echanism o~ the Enhancln~ Modules Fabric is advanced through the weft straightener 14 which aligns the fabric weft prior to processing in enhancement 15 modules 16, 18. Following hydroenhancement, the fabric is advanced to the tenter frame 20, which is of conventional design, where it is dried under tension to produce a uniform fabric of specified width.
Module 16 includes a first support member 22 which is 20 supported on an endless conveyor means including rollers 24 and drive means (not shown) for rotation of the rollers. Preferred line speeds for the conveyor are in the range of 10 to 500 ft/min. Line speeds are adjusted in accordance with process energy requirements which vary as a function of fabric type and 25 weight.
Support member 22, which preferably has a flat configuration, includes closely spaced fluid pervious open areas ~3~
26. A preferred support member 22, shown in Fig. 2A, ls a 36x29 90~ mesh plain weave having a 23.7% open area, fabricatecl of polyester warp and shute round wire. Support member 22 i.s a tight seamless weave which is not subject to angular 5 displacement or snag. Specifications for the screen, which is manufactured by Albany International, Appleton Wire Division, P.o. Box 1939, Appleton, Wisconsin 54913 are set forth in Table I.
TABLE I
Support Screen Specifications _ .
Property 36x29 90 flat mesh 40x40 45 drum mesh 15 Wire polyester stainless steel Warp wire .0157 0.010 Shute w.ire .0157 0.010 Weave type plain plain Open area 23.7% 36%
Module 16 also includes an arrangement of parallel and spaced manifolds 30 oriented in a cross-direction ("CD") relative 30 to movement of the fabric 12. The manifolds which are spaced approximately 8 inches apart each include a plurality of closely aligned and spaced columnar jet orifices 32 which are spaced approximately .5 inches from the support member 22.
I'he jet orifices have diameters and center-to-center 35 spacin~s in the range of .005 to .010 inches and .017 to .034 inches, respectively, and are designed to i.mpact the fabric with -12~ 3 fluid pressures in the range of 200 to 3000 psi. Preferred orifices have diameters of approximately .005 inches with center~to-center spacings of approximately .017 inches~
This arrangement of fluid jets provides a curtain of fluid 5 entangling streams which yield optimum enhancement in the fabric.
Energy input to the fabric is cumulative along the line and preferably set at approximately the same level in modules 16, 18 (two stage system) to impart uniform enhancement to top and bottom surfaces of the fabric. Effective first stage enhancement 10 of fabric yarn is achieved at an energy output of at least .05 hp-hr/lb and preferably in the range of .1 to 2.0 hp-hr/lb.
Following the Pirst stage enhancement, the fabric is advanced to module 18 which enhances the other side of the fabric. Module 18 includes a second support member 34 of 15 cylindrical configuration which is supported on a drum. The member 34 includes closely spaced fluid pervious open areas 36 which comprise approximately 36% of the screen area. A
preferred support member 34, shown in Fig. 2B, is a 40x40 45 mesh stainless steel screen, manufactured by Appleton Wire, ~0 havlng the specifications set forth in Table I.
Module 18 functions in the same manner as the planar module 16. Manifolds 30 and jet orifices 32 are provided which ha~e substantially the same specifications as in the first stage enhancement module. Fluid energy to the fabric of at least 0.5 25 hp-hr/lb and preferably in the range of .1 to 2.0 hp-hr/lb effects second stage enhancement.
Conventional weaving processes impart reed marks to ~3~ 3 fabrics. Illustrations of such markings are shown in Figs. 3A
and 4A which are photomicrographs at lOX and 16X magnification of a polyester LIBBEY brand fabric style no. S/x-A805 (see Tab~e-II). Reed marks in Yigs. 3A and 4A are designated by the let'~er 5 "~".
The invention overcomes this defect in conventional weaving processes through use of a single and preferably two stage hydroenhancement process. Advantage is obtained in the invention process by orienting the drum support member 3~ in lO offset relation, preferably 45, relative to machine direction ("MD") of the hydroenhancing line. See Figs. 2~ and B.
Support members 22 and 3~ are preferably provided with fine mesh open areas which are dimensioned to effect fluid passage through the members without imparting a patterned effect to the 15 fabric. The preferred members have an effective open area for fluid passage in the range of 17 - ~0%.
Comparison of the control and processed polyester fabric of Figs. 3A, B and ~A, B illustrates the advantages obtained through use of the enhancement process. Reed marks R in control 20 polyester fabric are essentially eliminated through enhancement of the fabric. The offset screen arrangement is also effective in diminishing linear jet streak markings associated with the enhancement process.
Exam~lesI-XIII
Figs. 3 - 15 illustrate representative woven and knit fabrics enhanced in accordance with the method of the invention, i3 employing test conditions which simulate the line of Fig. 1.
Table II sets forth specifications for the fabri~s illustrated in the drawings.
As ln the Fig. l line, the -test manifolds 30 were spaced 5 approximately 8 inches apart in modules 16, 18, and provided with densely packed columnar jet orifices 32 of approximately 60/inch.
Orifices 32 each had a diameter of 0.005 inches and were spaced approximately .5 inches from the first and second support members 22, 3~.
The process line of Fig. 1 includes enhancement modules 16, 18 which, respectively, are provided with six manifolds. In the Examples, modules 16, 18 were each fitted with two manifolds 34.
To simulate line conditions, the fabrics were advanced through multiple runs on the line. Three processing runs in each two 15 manifold module was deemed to be equivalent to a SlX manifold module.
Fabrics were hydroenhanced at process pressures of approximately 1500 psi. Line speed and cumulative energy output to the modules were respectively maintained at approximately 30 20 fpm and 0.~6 hp-hr/lb. Adjustments in the line speed and fluid pressure were made to accommodate differences in fabric weight for uniform processing and to maintain the preferred energy level.
Fabrics processed in the Examples exhibited marked 25 enhancement in aesthetic appearance and quality including, characteristics such as cover, bloom, ~brasion resistance, drape, stability, and reduction in seam slippage, and edge fray.
. ., , ~
3~;3 Tables III - XI set forth data for fabrics enhanced in accordance with invention on the test process line. Standard testing procedures of The American Society for Testing and Materials (ASTM) were employed to test control and processed 5 characteristics of fabrics. Data set forth in the Tables was generated in accordance with the following ASTM standards:
Fabric Characteristic STM Standard Weight D3776-79 Thickness Dl777-64 (Ames Tester) Tensile Load D1682-6~ (1975) (Cut strip/grab) Elongation D1682-64 (1975) Air Permeability D737-75 (1980) (Frazier) Thread Count D3775-79 Ball Burst D3787-80A
Seam Slippage D4159-82 Tongue Tear D2261-71 Wrinkle Recovery D1295-67 (1972) Abrasion Resistance D3884-80 Pilling D3514-81 Washability tests were conducted in accordance with the following procedure. Weight measurements ("before wash") were 25 taken of control and processed fabric samples each having a dimension of 8.5"xll" (8.5" fill direction and 11" warp direction). The samples were then washed and dried in conventional washer and dryers three consecutive times and "after wash" measurements were taken. The percent weight loss -~3~3~53 of the pre and post wash samples was determined in accordance the following formula:
% weight loss = D/B x 100 where, B = before wash sample weight; A = after wash sample 5 weight; and D = B-A.
Photomicrographs of the fabrics, Figs. 4-15, illustrate the enhancement in fabric cover obtained in the invention.
Attention is directed to open areas in the unprocessed fabrics, photographs designated A, these areas are of reduced size in the 10 processed fabrics in the photographs designated B.
Hydroenhancement caused fabric yarns to bloom and entangle at cross-over points, filling in open areas to improve cover and reduce air permeability in the fabrics.
Figs. 12 and 13 are photomicrographs of a HYTEX brand wall 15 covering fabric, manufactured by Hytex, Inc, Randolph, Massachuset~. A multi-textured surface appearance of the fabric is provided by yarns which are woven through discrete areas of the front fabric surface. Free floating weave stitches, designated by the letter "S" in Figs. 12B and 13B~ are formed on 20 the backside of the fabric.
Hydroenhancement of HYTEX wall covering fabric secured the free-floating stitches S to the fabric backside enhancing fabric stability and cover. See Figs. 12B, 13B. In wall covering applications, fabric enhance~ent and associated stabilizing 25 effects reduces or eliminates the need for adhesive backcoatings.
Enhancement of the fabric also limits wicking of wall cover application adhesives through the fabric. Further advantage is :~3:~L3~3 ob-tained when enhanced fabrics are used in acoustic applications; elimination of backcoating reduces sound reflection and furthers efficient transmission of sound through the fabric.
TABLE II
.
Fabric Specifications Fiber Brand and Styl~ Desiqnation Fiqure(s) NOMEX S/x-A805* 3A,B, 4A,B
Fiber : 2 denier-1.9 inch Yarn : Open end cotton spun 17s LIBBEY SJ022** 5A,B
Warp:
Fiber: 3 denier - 1.5 inch acrylic Yarn : Open end cotton spun 9s 28 ends per inch Fill:
Fiber: 3 denier ~ 3 inch acrylic Yarn : Open end wool spun . 4s 14, 16 or 18 picks per inch 30 LIBBEy S/x-1160 6A,B
Fiber: 3 denier-3 inch acrylic Yarn : Wrap spun w/100 den textured polyester ~s 14 ends x 16 picks per inch LIBBEY S/406 7A,B, 14A,B
~iO
Warp:
Fiber: 3 denier - 1.5 inch acrylic Yarn : Open end cotton spun 9s 2~ ends per inch Fill:
Fiber: 3 denier - 3.inch acrylic Yarn : Hollow spun 6 twists/inch 4s 14, 16 or 18 picks per inch , . . . . . .
. ~ .
~.
~33L3~53 Table II, continued 5 LIBBEY S/152 8A, B
Warp:
Fiber: 3 denier - 2.5 inch acrylic Yarn : Open end cotton spun 4s 14 ends per inch Fill:
Fiber: 3 denier - 3 inch acrylic Yarn : Open end wool spun 2.6s . 14, 16 or 18 picks per inch Guilford Wool/Nylon 9A,B
80% wool/20~ nylon ., .
Polyester/cotton (53/47) 10A,B
Weight: 10 ounces/yd2 Yarn : Spun Filament Weave : 3xl Twill Thread Count: 120x38 30 50% Polyester/50% cotton Doubleknit llA,B
Yarn: wrap spun with 100 : denier polyester wrap 35 HYTEX Wall covering*** 12, 13 ~LIBBEY is a trademark of W. S. Libbey Co., One Mill Street, Lewiston, ME 04 2 4 0 .
40 **NOMEX is a trademark of E.I. Du Pont de Nemours and Company, Wilminqton, Del.
HYTEX is a trademark of Hytex , Inc., Randolph, MA.
f ~' ~
, ,., , , , 1 ' ~ i TABLæ III
Nomex A805 - Fiq. 4 ControlProcessed % Chance 20 Wei~ht (gsy) 195 197 +1.0 Thickness (mils) 42 42 0 Air Perm. (ft3/ft2/ 331 156 -52.9 min) Strip Tensile (lbs/in) warp 115 132 +14.8 ~ill 59 47 -20.3 Elonqatlon (%) warp 48 50 +4.2 fill 62 71 +14.5 -20- ~3~3~3 TABLE IV
022/6075 (16 ppi) - Fi~. 5 Control Processed % Chanqe 15 Wei~ht (gsy)158 165 + 4.4 Thickness (mils) 48 49 ~ 2.1 Air Perm. (ft3/ft2 406 259 -36.2 min) ~I{L~ _ ile (lbs/in) warp 34 36 + 5.9 fill 37 31 -16.2 Elon~ation (%) warp 33 27 -18.2 fill 27 28 + 3.7 30 Seam Slippaqe (lbs/in) warp 5 60 +1100.0 ~ fill 7 55 + 685.7 `~ Tonaue Tear (lbs) warp 18 10 ~-44.4 ~ill 21 8 -~1.9 , Wt. Loss In Wash (%) 37 5 -86.5 40 Wrinkle Recoverv* 123 138 +12.2 (recovery angle) * Under ASTM test standards (Dl295-67) improvements in the 45 wrinkle recovery of a fabric are indicated by an increase in the recovery angle.
.~
,,, '. ..
~3~3453 TABLE V
Libbey S/x-1160 - Fi.g. 6 Control Processed % Chanqe : 15 Weiqht (gsy)146.8 160.2 9.1 Thickness (mils) 38.1 52.7 38.3 ~0 Ai ~ rm_ (ft3/ft2. 457.2 188.5 .-58.8 min) 25 Grab Tensile (lbs/in) warp80.2 89.3 11.4 ill105.0 111.4 6.1 : Elonqation (%) ; 30 ~ warp 30.0 34~0 13.3 ~ ~ill32.0 46.0 43.8 ; Ball Burst (lbs) 190 157 -17.4 .
.
.~ , .
:. , . ~j -22- 1~3~3 ~ABLE VI
406/6075 (16 ppi) - Fig. 7 Control Processed % Chanqe Weiqht (gsy)159 166 + 4.4 Thickness (mils) 48 50 -~ 4.2 20 Air Perm. (ft3/~t2 351 184 -47.6 mln) nsile (lbs~in) warp 42 36 -14.3 ~ill 66 58 -12.1 Elonaation (%) warp 23 31 +34.8 . fill 49 33 -32.7 Se~ S1iPDag~ (lbs) warp 29 36 +89.5 fill 21 76 + 261.9 35 Tonque Tear (lbs) warp 23 18 -21.7 ~ill 19 . 15 - 1.1 Wt. Loss In Wash (%) 28 4 -85.7 Wrinkle Recovery 140 148 n + 5.7 (recovery angle) :
~a3~3~;3 TABLE VII
__ 152~6076 (16 ppi) - Fia. 8 ControlProcessed % Chanae 10 Weiqht (gsy) 231 257 +11.3 Thickness (mils) 259 238 - 8.1 Air Perm. (ft3/ft2/ 204 106 -48.0 ~in) Strip Tensile (lbs/in) warp 48 58 +20.8 fill 56 72 +28.6 Elonaation (%) warp 33 33 f.ill 34 39 +14.7 25 _am Slippaae (lbs) warp 6~ 81 +26.6 fill 78 112 +43.6 Tonaue Tear (lbs) warp 21 18 -14.3 fill 17 15 -11.8 Wt. Loss In Wash (%) -- -- ----35 Wrinkle Recovery 117 136 ~16.2 (recovery angle) TABLE VIII
_ Guilford Wool (80% wool/20% nylon) - Fiq. 9 Control Process % Chanae Air Perm. 243 147 -39.5 ~
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TABLE IXB
A sion -- S~un Filam~nt~Bottom Weiqhts - _~ lo ASTM Standard - Twill side up; 500 cycles; 500 g weight; H-18 wheels Weight Weight Weight % Improve-10 Sam~le Before(q) After(q) Loss(~)% I,oss ment lC 3.32 3.020.30 9.0 lP 3.36 3.130.23 6.9 23%
2C 4.64 4.160.48 10.4 15 2P 4.83 4.570.26 5.4 48%
3C 4.73 4.470.26 5.5 3P 4.91 5.130.22 4.5 18%
20 4C 4.47 4.180.29 6.5 4P 4.71 4.530.18 3.8 41%
TABLE X
oubleknit - Fiq. 11 ; Control Processed ~O Chan~e Air Perm. (Ft3/ft2113.1 95.1 -15.9 min) Abrasion 1.0 0.6 -40.0 40 ASTM (D-3884-80): 250 Cycles, H-18 wheel ~ (1-5 rating) 4.3 4.3 0 ASTM (D-3914-81): 300 cycles Figs. 14A, B are photomacrographs of control and processed 50 acrylic vertical blind fabric, manufactured by W.S. Llbbey, style designation S/406. Enhancement of the fabric reduces fabric .
~3~3~
torque which is particularly advantageous in vertical blind applications. The torque reduction test of Figs. 14A, B employed fabric strips 84" long and 3.5" wide, which were suspended vertically without restraint. Torque was measured with 5 reference to the angle of fabric twist from a flat support surface. As can be seen in the photographs, a torque of 90 in the unprocessed fabric, Fig. 14A, was eliminated in the enhancement process.
Figs. 15A-C are macrophotographs of control and processed 10 acrylic fabrics, LIBBEY style nos. 022, 406 and 152, respectively, which were tested for washability. Unprocessed fabrics exhibited excessive fraying and destruction, in contrast to the enhanced fabrics which exhibit limited fraying and yarn (weight) loss. Table XI sets forth washability test weight loss 15 data.
TABLE XI
022. 406 152 - Fi~s. 15A-C
Percent Wei~ht Loss (3 wash~dry cycles) am~le Control Processed 022 36.5 5.0 406 28.0 4.0 30152 28.1 7.2 Fig. 16 illustrates an alternative embodiment of the invention apparatus, generally designated 40. The apparatus -27- ~3~3~3 includes a plurality of drums 42a-d over which a fabric 44 is advanced for enhancement processing. Speci~ically, the fabric 44 traverses the line in a sinuous path under and over the drums 42 in succession. Rollers 46a and b are provided at opposite 5 ends of the line adjacent drums 42a and d to support the fabric.
Any or all of the drums can be rotated by a suitable motor drive (not shown) to advance the fabric on the line.
A plurality of manifolds 48 are provided in groups, Fig. 16 illustrates groups of four, which are respectively spaced from 10 each of the drums 42a-d. An arrangement of manifold groups at 90 inter~als on the slnuous fabric path successively positions the manifolds in spaced relation with respect to opposing surfaces of the fabric. Each manifold 48 impinges columnar fluid jets 50, such as water, against the fabric. Fluid supply 15 52 supplies fluid to the manifolds 4~ which is collected in liquid sump 54 during processing for recirculation via line 56 to the manifolds.
The support drums 42 may be porous or non-porous. It will be recognized that advantage is obtained through use of drums 20 which include perforated suppor-t surfaces. Open areas in the support surfaces facilitate recirculation of the fluid employed in the enhancement process.
Further advantage is obtained, as previously set forth in discussion of the first embodiment, through use of support 25 surfaces having a fine mesh open area pattern which facilitates flu.id passage. Offset arrangement of the support member orientations, ~or example at 45~ offset orientation as shown in "~ ;
:~3:~3~3 Fig. 2, limits process water streak and weave reed marks in the enhanced fabric.
Enhancement is a function of energy which is imparted to the fabric. Preferred energy levels for enhancement in 5 accordance with the invention are in the range of .1 to 2.0 hp-hr/lb. Variables which determine process energy levels include line speed, the amount and velocity of liquid which impinges on the fabric, and fabric weight and characteristics.
Fluid velocity and pressure are determined in part by the 10 characteristics of the fluid orifices, for example, columnar versus fan jet configuration, and arrangement and spacing from the process line~ It is a feature of the invention to impinge a curtain of fluid on a process line to impart an energy flux of approximately 0.46 hp-hr/lb to the fabric. Preferred 15 specifications for orifice type and arrangement are set forth in description of the embodiment of Fig. 1. Briefly, orifices 16 are closely spaced with center-to-center spacings of approximately 0.017 inches and are spaced 0.5 lnches from the support members. Orifice diameters of .005 inches and densities 20 of 60 per manifold inch eject columnar fluid jets which form a uniform fluid curtain.
The following Examples are representative of the results obtained on the process line illustrated in Fig. 17.
Exam~le XIV
A plain woven 100~ polyester fabxic comprised of friction spun yarns having the following specifications was processed in accor~ance with the inventionO count of 16 x 10 yarns/in2, -` ~3~3'~
weight of 8 ounces/yd2, an abrasion resistance of 500 grams (measured by 50 cycles of a CS17 abrasion test wheel) and an air permeability of 465 ft3/ft2/min.
The fabric was processed on a test line to simulate a speed 5 of 300 ft/min. on process apparatus including four drums 42 and eighteen nozzles 16 at a pressure of approximately 1500 psi.
Energy output to fabric at these process parameters was approximately .46 hp-hr/lb. Table XII sets forth control and processed characteristics of the fabric.
TABLE XII
100% Polyester Friction Spun Fabric :
15 Fabric Characteristic ControlProcessed Count (yarns/in.2) 16xlO 17xlO
Weight (ounces/yd.2) 8 8.2 Abrasion resistance (cycles) 50 85 Air permeability (ft3ft2/min.) 4~5 181 __ Examples XV and XVI
The process conditions of Example XIV were employed to process a plain woven cotton osnaburg and plain woven polyester 25 ring spun fabrics yielding the results set forth in Tables XIV
and XV.
~3~3~i3 TABLE XV
.. ..
~`
Plain Woven Cotton Osnabur~
5 Fabric Characteristic Control Processed Count (yarns/in.2) 32x26 32x32 Abrasion resistance (cycles) 140 344 Air permeability (ft3ft2/min.) 710 120 _ TABLE XIV
Plain Woven PolYester Rinq Spun Yarn 15 Fabric Characteristic Control Processed Count (yarns/in.2) 44x28 48x32 Abrasion resistance (cycles) 100 225 Air permeability (ft.3/ft2/min.) 252 63 Fabrics processed in Examplss XIV-XVI are characterized by a substantial reduction in air permeability and increase in abrasion resistance. Process energy levels in these Examples were apprcximately .46 hp-hr/lb. It has been discovered that 25 there is a correlation between process energy and enhancement.
Increased energy levels yield optimum enhancement effects.
The foregoing Examples illustrate applications of the ~3~L3~
hydroenhancing process of the invention for upgrading the quality of single ply woven and knit fabrics.
In an alternative application of the hydroenhancing process of the invention, fabric strata are hydrobonded into integral 5 composite fabric. Fig. 17 illustrates a composite flannel fabric 60 including fabric layers 62, 64. ~Iydrobonding of the layers is effected by first nappin~ opposing surfaces 62a, 64a of each of the layers to raise surface fibers. The opposing surfaces 62a, 44a are then arranged in overlying relation and processed on the 10 production line of the invention. See Figs. 1 and 16.
Enhancement of the layers 62, 6~ effects entanglement of fibers in the napped surfaces and bonding of the layers to form a integral composite Pabria 60. Exterior surfaces 62b, 6~b are also enhanced in the process yielding improvements in cover and 15 quality in ~he composite fabric.
Napped surfaces 62a, 62b are provided by use of conventional mechanical napping apparatus. Such apparatus include cylinders covered with metal points or teasel burrs which abrade fabric surfaces.
Advantageously, composite fabric 60 is manufactured without re~uirement of conventional laminating adhesives. As a result, the composite fabric breaths and has improved tactile characteristics than obtained in prior art laminated composites.
It will be recognized that such composite fabrics have diverse 25 applications in fields such as apparel and footwear.
Optimum enhancement (in single and multi-ply fabrics) is a function of energy. Preferred results are obtained at energy , ~L3~L3~3 levels of approximately .46 hp-hr/lb. Energy requirements will of course vary for different fab~ics as will process conditions required to achieve optimum energy levels. In general, process speeds, nozzle configuration and spacing may be varied to obtain 5 preferred process energy levels.
Enhanced fabrics of the invention are preferably fabricated of yarns including fibers having deniers and lengths, respectively, in the ranges of 0.3 to 10.0 and 0.5 to 6.0 inches, and yarn counts of .5s to 80s. Optimum enhancement is obtained 10 in fabrics having fiber deniers in the range of .5 to 6, staple fibers of .5 to 6.0 inches, and yarn counts in the range of .5s to 50s. Preferred yarn spinning systems employed in the invention fabrics include cotton spun, wrap spun and wool spun.
Experimentation indicates that preferred enhancement results are 15 obtained in fabrics including low denier, short lengths fibers, and loosely twisted yarns.
The invention advances the art by recognizing that superior fabric enhancement can be obtained under controlled process conditions and energy levels. Heretofore, the art has not 20 recognized the advantages and the extent to which hydroenhancement can be employed to upgrade fabric quality. It is submitted that the results achieved in the invention reflect a substantial and surprising contribution to the art.
Numerous modifications are possible in light of the above 25 disclosure. For example, although the preferred process and apparatus employ fluid pervious support members, non-porous support members are within the scope of the invention.
!~ .
~3~L3~3 Similarly, Figs. 1 and 16 respectively illustrate two and four stage enhancement process lines. System configurations which include one or more modules having flat, drum or othex support member configuration may be employed in the invention.
It will be recognized that the process of the invention has wide application for the production of a diversity of enhanced fabrics. Thus, the Examples are not inkended to limit the invention.
Finally, although the disclosed enhancement process employs 10 columnar jet orifices to provide a fluid curtain, other apparatus may be employed for this purpose. Attention is directed to U.S.
Patent No. 4,995,151, en-titled "~pparatus and Me-thod for Mydro-patterning Fabric", dated February 26, 1991, assigned to Inter- ;
national Paper Company, the assignee of the present case, which 15 discloses a divergent jet fluid entangling apparatus for use in hydropatterning woven and nonwoven textile fabrics.
Therefore, although the invention has been described with reference to certain preferred e~bodiments, it will be appreciated that other hydroentangling apparatus and processes 20 may be devised, which are nevertheless within the scope and spirit of the invention as defined in the claims appended hereto.
; l
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TABLE IXB
A sion -- S~un Filam~nt~Bottom Weiqhts - _~ lo ASTM Standard - Twill side up; 500 cycles; 500 g weight; H-18 wheels Weight Weight Weight % Improve-10 Sam~le Before(q) After(q) Loss(~)% I,oss ment lC 3.32 3.020.30 9.0 lP 3.36 3.130.23 6.9 23%
2C 4.64 4.160.48 10.4 15 2P 4.83 4.570.26 5.4 48%
3C 4.73 4.470.26 5.5 3P 4.91 5.130.22 4.5 18%
20 4C 4.47 4.180.29 6.5 4P 4.71 4.530.18 3.8 41%
TABLE X
oubleknit - Fiq. 11 ; Control Processed ~O Chan~e Air Perm. (Ft3/ft2113.1 95.1 -15.9 min) Abrasion 1.0 0.6 -40.0 40 ASTM (D-3884-80): 250 Cycles, H-18 wheel ~ (1-5 rating) 4.3 4.3 0 ASTM (D-3914-81): 300 cycles Figs. 14A, B are photomacrographs of control and processed 50 acrylic vertical blind fabric, manufactured by W.S. Llbbey, style designation S/406. Enhancement of the fabric reduces fabric .
~3~3~
torque which is particularly advantageous in vertical blind applications. The torque reduction test of Figs. 14A, B employed fabric strips 84" long and 3.5" wide, which were suspended vertically without restraint. Torque was measured with 5 reference to the angle of fabric twist from a flat support surface. As can be seen in the photographs, a torque of 90 in the unprocessed fabric, Fig. 14A, was eliminated in the enhancement process.
Figs. 15A-C are macrophotographs of control and processed 10 acrylic fabrics, LIBBEY style nos. 022, 406 and 152, respectively, which were tested for washability. Unprocessed fabrics exhibited excessive fraying and destruction, in contrast to the enhanced fabrics which exhibit limited fraying and yarn (weight) loss. Table XI sets forth washability test weight loss 15 data.
TABLE XI
022. 406 152 - Fi~s. 15A-C
Percent Wei~ht Loss (3 wash~dry cycles) am~le Control Processed 022 36.5 5.0 406 28.0 4.0 30152 28.1 7.2 Fig. 16 illustrates an alternative embodiment of the invention apparatus, generally designated 40. The apparatus -27- ~3~3~3 includes a plurality of drums 42a-d over which a fabric 44 is advanced for enhancement processing. Speci~ically, the fabric 44 traverses the line in a sinuous path under and over the drums 42 in succession. Rollers 46a and b are provided at opposite 5 ends of the line adjacent drums 42a and d to support the fabric.
Any or all of the drums can be rotated by a suitable motor drive (not shown) to advance the fabric on the line.
A plurality of manifolds 48 are provided in groups, Fig. 16 illustrates groups of four, which are respectively spaced from 10 each of the drums 42a-d. An arrangement of manifold groups at 90 inter~als on the slnuous fabric path successively positions the manifolds in spaced relation with respect to opposing surfaces of the fabric. Each manifold 48 impinges columnar fluid jets 50, such as water, against the fabric. Fluid supply 15 52 supplies fluid to the manifolds 4~ which is collected in liquid sump 54 during processing for recirculation via line 56 to the manifolds.
The support drums 42 may be porous or non-porous. It will be recognized that advantage is obtained through use of drums 20 which include perforated suppor-t surfaces. Open areas in the support surfaces facilitate recirculation of the fluid employed in the enhancement process.
Further advantage is obtained, as previously set forth in discussion of the first embodiment, through use of support 25 surfaces having a fine mesh open area pattern which facilitates flu.id passage. Offset arrangement of the support member orientations, ~or example at 45~ offset orientation as shown in "~ ;
:~3:~3~3 Fig. 2, limits process water streak and weave reed marks in the enhanced fabric.
Enhancement is a function of energy which is imparted to the fabric. Preferred energy levels for enhancement in 5 accordance with the invention are in the range of .1 to 2.0 hp-hr/lb. Variables which determine process energy levels include line speed, the amount and velocity of liquid which impinges on the fabric, and fabric weight and characteristics.
Fluid velocity and pressure are determined in part by the 10 characteristics of the fluid orifices, for example, columnar versus fan jet configuration, and arrangement and spacing from the process line~ It is a feature of the invention to impinge a curtain of fluid on a process line to impart an energy flux of approximately 0.46 hp-hr/lb to the fabric. Preferred 15 specifications for orifice type and arrangement are set forth in description of the embodiment of Fig. 1. Briefly, orifices 16 are closely spaced with center-to-center spacings of approximately 0.017 inches and are spaced 0.5 lnches from the support members. Orifice diameters of .005 inches and densities 20 of 60 per manifold inch eject columnar fluid jets which form a uniform fluid curtain.
The following Examples are representative of the results obtained on the process line illustrated in Fig. 17.
Exam~le XIV
A plain woven 100~ polyester fabxic comprised of friction spun yarns having the following specifications was processed in accor~ance with the inventionO count of 16 x 10 yarns/in2, -` ~3~3'~
weight of 8 ounces/yd2, an abrasion resistance of 500 grams (measured by 50 cycles of a CS17 abrasion test wheel) and an air permeability of 465 ft3/ft2/min.
The fabric was processed on a test line to simulate a speed 5 of 300 ft/min. on process apparatus including four drums 42 and eighteen nozzles 16 at a pressure of approximately 1500 psi.
Energy output to fabric at these process parameters was approximately .46 hp-hr/lb. Table XII sets forth control and processed characteristics of the fabric.
TABLE XII
100% Polyester Friction Spun Fabric :
15 Fabric Characteristic ControlProcessed Count (yarns/in.2) 16xlO 17xlO
Weight (ounces/yd.2) 8 8.2 Abrasion resistance (cycles) 50 85 Air permeability (ft3ft2/min.) 4~5 181 __ Examples XV and XVI
The process conditions of Example XIV were employed to process a plain woven cotton osnaburg and plain woven polyester 25 ring spun fabrics yielding the results set forth in Tables XIV
and XV.
~3~3~i3 TABLE XV
.. ..
~`
Plain Woven Cotton Osnabur~
5 Fabric Characteristic Control Processed Count (yarns/in.2) 32x26 32x32 Abrasion resistance (cycles) 140 344 Air permeability (ft3ft2/min.) 710 120 _ TABLE XIV
Plain Woven PolYester Rinq Spun Yarn 15 Fabric Characteristic Control Processed Count (yarns/in.2) 44x28 48x32 Abrasion resistance (cycles) 100 225 Air permeability (ft.3/ft2/min.) 252 63 Fabrics processed in Examplss XIV-XVI are characterized by a substantial reduction in air permeability and increase in abrasion resistance. Process energy levels in these Examples were apprcximately .46 hp-hr/lb. It has been discovered that 25 there is a correlation between process energy and enhancement.
Increased energy levels yield optimum enhancement effects.
The foregoing Examples illustrate applications of the ~3~L3~
hydroenhancing process of the invention for upgrading the quality of single ply woven and knit fabrics.
In an alternative application of the hydroenhancing process of the invention, fabric strata are hydrobonded into integral 5 composite fabric. Fig. 17 illustrates a composite flannel fabric 60 including fabric layers 62, 64. ~Iydrobonding of the layers is effected by first nappin~ opposing surfaces 62a, 64a of each of the layers to raise surface fibers. The opposing surfaces 62a, 44a are then arranged in overlying relation and processed on the 10 production line of the invention. See Figs. 1 and 16.
Enhancement of the layers 62, 6~ effects entanglement of fibers in the napped surfaces and bonding of the layers to form a integral composite Pabria 60. Exterior surfaces 62b, 6~b are also enhanced in the process yielding improvements in cover and 15 quality in ~he composite fabric.
Napped surfaces 62a, 62b are provided by use of conventional mechanical napping apparatus. Such apparatus include cylinders covered with metal points or teasel burrs which abrade fabric surfaces.
Advantageously, composite fabric 60 is manufactured without re~uirement of conventional laminating adhesives. As a result, the composite fabric breaths and has improved tactile characteristics than obtained in prior art laminated composites.
It will be recognized that such composite fabrics have diverse 25 applications in fields such as apparel and footwear.
Optimum enhancement (in single and multi-ply fabrics) is a function of energy. Preferred results are obtained at energy , ~L3~L3~3 levels of approximately .46 hp-hr/lb. Energy requirements will of course vary for different fab~ics as will process conditions required to achieve optimum energy levels. In general, process speeds, nozzle configuration and spacing may be varied to obtain 5 preferred process energy levels.
Enhanced fabrics of the invention are preferably fabricated of yarns including fibers having deniers and lengths, respectively, in the ranges of 0.3 to 10.0 and 0.5 to 6.0 inches, and yarn counts of .5s to 80s. Optimum enhancement is obtained 10 in fabrics having fiber deniers in the range of .5 to 6, staple fibers of .5 to 6.0 inches, and yarn counts in the range of .5s to 50s. Preferred yarn spinning systems employed in the invention fabrics include cotton spun, wrap spun and wool spun.
Experimentation indicates that preferred enhancement results are 15 obtained in fabrics including low denier, short lengths fibers, and loosely twisted yarns.
The invention advances the art by recognizing that superior fabric enhancement can be obtained under controlled process conditions and energy levels. Heretofore, the art has not 20 recognized the advantages and the extent to which hydroenhancement can be employed to upgrade fabric quality. It is submitted that the results achieved in the invention reflect a substantial and surprising contribution to the art.
Numerous modifications are possible in light of the above 25 disclosure. For example, although the preferred process and apparatus employ fluid pervious support members, non-porous support members are within the scope of the invention.
!~ .
~3~L3~3 Similarly, Figs. 1 and 16 respectively illustrate two and four stage enhancement process lines. System configurations which include one or more modules having flat, drum or othex support member configuration may be employed in the invention.
It will be recognized that the process of the invention has wide application for the production of a diversity of enhanced fabrics. Thus, the Examples are not inkended to limit the invention.
Finally, although the disclosed enhancement process employs 10 columnar jet orifices to provide a fluid curtain, other apparatus may be employed for this purpose. Attention is directed to U.S.
Patent No. 4,995,151, en-titled "~pparatus and Me-thod for Mydro-patterning Fabric", dated February 26, 1991, assigned to Inter- ;
national Paper Company, the assignee of the present case, which 15 discloses a divergent jet fluid entangling apparatus for use in hydropatterning woven and nonwoven textile fabrics.
Therefore, although the invention has been described with reference to certain preferred e~bodiments, it will be appreciated that other hydroentangling apparatus and processes 20 may be devised, which are nevertheless within the scope and spirit of the invention as defined in the claims appended hereto.
; l
Claims (41)
1. A method for enhancing and finishing textile fabrics including spun and/or spun filament yarns which intersect at cross-over points, and first and second sides, the fabric including yarn fibers having deniers and lengths in the range of 0.3 to 16.0 and .5 to 8 inches, respectively, and yarn counts in the range of .5s to 80s, the method comprising the steps of:
supporting the fabric on a first support member, and traversing the first side of said fabric with a first continuous curtain of fluid for sufficient duration to effect entanglement of said yarns at the cross-over points, thereby enhancing fabric cover and quality, said curtain of fluid impacting the fabric with an energy in the range .1 and 2.0 hp-hr/lb.
supporting the fabric on a first support member, and traversing the first side of said fabric with a first continuous curtain of fluid for sufficient duration to effect entanglement of said yarns at the cross-over points, thereby enhancing fabric cover and quality, said curtain of fluid impacting the fabric with an energy in the range .1 and 2.0 hp-hr/lb.
2. The method of Claim 1, wherein said fluid curtain is provided by columnar fluid jet orifices having a diameter of approximately 0.005 inches, center-to-center spacing of approximately .017 inches, and spacing from said first support member of approximately .5 inches, said fluid jets impinging the fabric with fluids at pressure of approximately 1500 psi.
3. The method of Claim 2, wherein said support member includes a pattern of closely spaced fluid pervious open areas aligned in a first direction to effect fluid passage through said support member.
4. The method of Claim 3, wherein said open areas occupy approximately 17 to 40% of said support member.
5. The method of Claim 1, comprising the further steps of:
supporting said enhanced fabric on a second support member, and traversing the second side of said enhanced fabric in a second enhancement stage with a second continuous fluid curtain for sufficient duration to further enhance fabric cover and provide a uniform fabric finish, said second enhancement stage impacting the fabric with an energy in the range 0.1 and 2.0 hp-hr/lb.
supporting said enhanced fabric on a second support member, and traversing the second side of said enhanced fabric in a second enhancement stage with a second continuous fluid curtain for sufficient duration to further enhance fabric cover and provide a uniform fabric finish, said second enhancement stage impacting the fabric with an energy in the range 0.1 and 2.0 hp-hr/lb.
6. The method of Claim 5, wherein:
said first and second fluid curtains are provided by columnar fluid jets each having a diameter of approximately 0.005 inches and center-to-center spacing of approximately .017 inches, said fluid curtains are spaced approximately .5 inches from said first and second members, and said fluid jets impinge the fabric with fluids at a pressure of approximately 1500 psi, said first and second support members each include a pattern of closely spaced fluid pervious open areas, respectively aligned in first and second directions, said open areas being dimensioned to effect fluid passage through said support members without imparting a patterned effect to the fabric.
said first and second fluid curtains are provided by columnar fluid jets each having a diameter of approximately 0.005 inches and center-to-center spacing of approximately .017 inches, said fluid curtains are spaced approximately .5 inches from said first and second members, and said fluid jets impinge the fabric with fluids at a pressure of approximately 1500 psi, said first and second support members each include a pattern of closely spaced fluid pervious open areas, respectively aligned in first and second directions, said open areas being dimensioned to effect fluid passage through said support members without imparting a patterned effect to the fabric.
7. The method of Claim 6, wherein said open areas occupy approximately 17 to 40% of each of said first and second support members.
8. The method of Claim 7, wherein said first and second support members respectively have flat and drum configurations.
9. The method of Claim 7, wherein said first and second support members have drum configurations.
10. The method of Claim 8, wherein said first and second directions are offset approximately 45°.
11. The method of Claim 9, wherein said first and second directions are offset approximately 45°.
12. The method of Claim 6, comprising the further step, following said second stage enhancement, of drying the enhanced fabric to a specified width under tension.
13. An enhanced textile fabric made by the method of Claim 6, the fabric including yarn fibers having deniers and lengths in the range of 0.3 to 16 and 0.5 to 8 inches, respectively, and thread counts in the range of 0.5s to 80s, the yarn cross-over points in the fabric weave define interstitial open areas, wherein the process effects enhancement of the yarns in the interstitial open areas, thereby enhancing fabric cover.
14. An enhanced textile fabric made by the method of Claim 6, the fabric including yarn fibers having deniers and lengths in the range of 0.5 to 6 and 0.5 to 8 inches, respectively, and thread counts in the range of 0.5s to 50s, the yarn cross-over points in the fabric weave define interstitial open areas, wherein the process effects enhancement of the yarns in the interstitial open areas, thereby enhancing fabric cover, and yields a reduction in fabric air permeability in the range of 10 to 90%.
15. An enhanced woven polyester fabric made by the method of Claim 6, wherein the fabric includes 2 denier, 1.9 inch polyester fiber, open-end cotton spun yarn having a yarn number of 17s and count of 49x23 per inch, and the process yields an approximate 48% reduction in air permeability in the fabric.
16. An enhanced woven acrylic fabric made by the method of Claim 6, wherein the fabric includes 3 denier, 1.5 inch fiber, open-end cotton warp yarn having a yarn number of 9s, 28 ends per inch, and a 3 denier, 3 inch acrylic fiber, open-end wool spun fill yarn having a number of 4s, 16 picks per inch, and the process yields an approximate 36% reduction in air permeability in the fabric.
17. An enhanced acrylic wrap spun fabric made by the method of Claim 6, wherein the fabric includes 3 denier, 3.0 inch acrylic fiber, wrap spun with 100 denier textured polyester yarn having a yarn number of 4s and count of 14 x 16 per inch, and the process yields an approximate 65% reduction in air permeability in the fabric.
18. An enhanced woven acrylic fabric made by the method of Claim 6, wherein the fabric includes 3 denier, 1.5 inch acrylic fiber, open-end cotton spun warp yarn having a yarn number of 9s, 28 ends per inch, and a 3 denier, 3 inch acrylic fiber, hollow wrap spun fill yarn, 6 twists per inch having a number of 4s, 16 picks per inch, and the process yields an approximate 48%
reduction in air permeability in the fabric.
reduction in air permeability in the fabric.
19. An enhanced woven acrylic fabric made by the method of Claim 6, wherein the fabric includes 3 denier, 1.5 inch acrylic fiber, open-end wool spun warp yarn having a yarn number of 4s, 14 ends per inch, and a 3 denier, 3 inch acrylic fiber, open-end wool spun fill yarn having a yarn number of 2.6s, 16 picks per inch, and the process yields an approximate 48% reduction in air permeability in the fabric.
20. An enhanced woven fabric made by the method of Claim 6, wherein the fabric includes 80% wool/20% nylon in a 2x1 twill weave, and the process yields an approximate 49.5% reduction in air permeability in the fabric.
21. An enhanced 53% polyester/47% cotton fabric made by the method of Claim 6, wherein the fabric includes a 3x1 twill weave, a thread count of 120 ends x 38 picks, and the process yields an approximate 50.6% reduction in air permeability in the fabric.
22. An enhanced 50% polyester/50% cotton doubleknit fabric made by the method of Claim 6, wherein the fabric includes wrap spun yarn with 100 denier polyester wrap, and the process yields an approximate 16% reduction in air permeability in the fabric.
23. An enhanced woven or knit textile fabric which comprises: spun and/or spun filament yarns which intersect at cross-over points to define interstitial open areas, said yarns including fibers having deniers and lengths in the range of 0.3 to 16 and 0.5 to 8 inches respectively, wherein said yarns are fluid entangled in said interstitial open areas by application of fluid energy in the range of .1 to 2.0 hp-hr/lb.
24. An enhanced woven or knit textile fabric according to Claim 23, wherein the yarn is cotton spun.
25. An enhanced woven or knit textile fabric according to Claim 23, wherein the yarn is wrap spun.
26. An enhanced woven or knit textile fabric according to Claim 23, wherein the yarn is wool spun.
27. A method for hydrobonding woven or knit fabric materials to form a composite textile fabric, the fabric including spun and/or spun filament yarns in a structured pattern including yarns which intersect at cross-over points, the method comprising the steps of:
napping first and second surfaces of the fabric to raise surface fibers thereof, arranging said first and second surfaces in opposing and overlying layered relation, supporting the layered fabric on a support member, and traversing one side of said layered fabric with a first continuous curtain of fluid for sufficient duration to effect entanglement of said raised surface fibers in said first and second surfaces, said curtain of fluid impacting the fabric with an energy in the range .1 and 2.0 hp-hr/lb.
napping first and second surfaces of the fabric to raise surface fibers thereof, arranging said first and second surfaces in opposing and overlying layered relation, supporting the layered fabric on a support member, and traversing one side of said layered fabric with a first continuous curtain of fluid for sufficient duration to effect entanglement of said raised surface fibers in said first and second surfaces, said curtain of fluid impacting the fabric with an energy in the range .1 and 2.0 hp-hr/lb.
28. The method of Claim 27, wherein said fluid curtain is provided by columnar fluid jet orifices having a diameter of approximately 0.005 inches and center-to-center spacing of approximately .017 inches, said fluid curtain impinging the fabric with fluids at pressure of approximately 1500 psi.
29. The method of Claim 28, wherein said support member includes a pattern of closely spaced fluid pervious open areas aligned in a first direction to effect fluid passage through said support member.
30. The method of Claim 29, wherein said open areas occupy approximately 17 to 40% of said support member.
31. The method of Claim 27, comprising the further steps of:
supporting said layered fabric on a second support member, and traversing the other side of said layered fabric in a second entanglement stage with a second continuous fluid curtain to effect a uniform composite fabric bond and finish, said second entanglement stage impacting the layered fabric with an energy in the range 0.1 and 2.0 hp-hr/1b.
supporting said layered fabric on a second support member, and traversing the other side of said layered fabric in a second entanglement stage with a second continuous fluid curtain to effect a uniform composite fabric bond and finish, said second entanglement stage impacting the layered fabric with an energy in the range 0.1 and 2.0 hp-hr/1b.
32. The method of Claim 31, wherein:
said first and second fluid curtains are provided by columnar fluid jets having a diameter of approximately 0.005 inches and center-to-center spacing of approximately .017 inches, said fluid jets impinging the fabric with fluids at pressure of approximately 1500 psi, said first and second support members each include a pattern of closely spaced fluid pervious open areas, respectively aligned in first and second directions, said open areas being dimensioned to effect fluid passage through said support members without imparting a patterned effect to the fabric.
said first and second fluid curtains are provided by columnar fluid jets having a diameter of approximately 0.005 inches and center-to-center spacing of approximately .017 inches, said fluid jets impinging the fabric with fluids at pressure of approximately 1500 psi, said first and second support members each include a pattern of closely spaced fluid pervious open areas, respectively aligned in first and second directions, said open areas being dimensioned to effect fluid passage through said support members without imparting a patterned effect to the fabric.
33. An enhanced composite woven or knit textile fabric which comprises:
at least two fabric layers which each include spun and/or spun filament yarns in a structured pattern of yarns which intersect at cross-over points, said fabric layers including first and second napped surfaces which have raised surface fibers, said napped surfaces being arranged in overlying and opposed relation and bonded together by dynamic fluid energy through entanglement of said raised surface fibers in said first and second surfaces.
at least two fabric layers which each include spun and/or spun filament yarns in a structured pattern of yarns which intersect at cross-over points, said fabric layers including first and second napped surfaces which have raised surface fibers, said napped surfaces being arranged in overlying and opposed relation and bonded together by dynamic fluid energy through entanglement of said raised surface fibers in said first and second surfaces.
34. An apparatus for enhancing and finishing woven and knit fabric including spun and/or spun filament yarn by impacting the fabric with pressurized fluid jets, the fabric including yarns which intersect at cross-over points, and first and second sides, the apparatus comprising:
conveyor means for conveying the fabric in a machine direction ("MD") through a production line including a first enhancing station, said conveying means supporting a first support member which underlies the fabric in said enhancing station;
curtain means spaced from said first support member for directing a curtain of fluid onto the first side of the fabric, said curtain means including a plurality of densely spaced orifices which eject high pressure fluid jets;
said curtain means coacting with said first support member to entangle fabr?c yarns at the cross-over points, enhancing fabric cover and imparting a uniform finish to the fabric.
conveyor means for conveying the fabric in a machine direction ("MD") through a production line including a first enhancing station, said conveying means supporting a first support member which underlies the fabric in said enhancing station;
curtain means spaced from said first support member for directing a curtain of fluid onto the first side of the fabric, said curtain means including a plurality of densely spaced orifices which eject high pressure fluid jets;
said curtain means coacting with said first support member to entangle fabr?c yarns at the cross-over points, enhancing fabric cover and imparting a uniform finish to the fabric.
35. An apparatus as set forth in Claim 34, wherein said fluid orifices have a columnar configuration, a diameter of approximately 0.005 inches and center-to-center spacing of approximately 0.17 inches, and impart energy to the fabric of approximately 0.1 to 2.0 hp-hr/lb.
36. An apparatus as set forth in Claim 35, wherein said fluid jets have a spray pressure of approximately 1500 psi.
37. An apparatus as set forth in Claim 34, further comprising a second enhancing station, a second support member which underlies the fabric and is supported for movement on the production line by said conveyor means, and a second curtain means spaced from said second support member for directing a curtain of fluid onto the second side of the fabric, said second curtain means including a second plurality of densely spaced orifices which eject high pressure fluid jets, thereby further enhancing the fabric.
38. An apparatus as set forth in Claim 37, wherein said first and second fluid curtains respectively impart energy to the fabric of approximately 0.1 to 2.0 hp-hr/lb.
39. An apparatus as set forth in Claim 38, wherein said second support member is fluid pervious and has open areas aligned on a bias relative to the machine direction of the line.
40. An apparatus as set forth in Claim 39, wherein said first and second curtain means are spaced approximately .5 inches from said first and second support members, said fluid jets have a spray pressure of approximately 1500 psi, and conveyor means speed is approximately 100 fpm.
41. An apparatus as set forth in Claim 40, wherein said first and second support members respectively have generally flat and cylindrical configurations.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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US18435088A | 1988-04-21 | 1988-04-21 | |
US184,350 | 1988-04-21 |
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CA1313453C true CA1313453C (en) | 1993-02-09 |
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Application Number | Title | Priority Date | Filing Date |
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CA 597326 Expired - Fee Related CA1313453C (en) | 1988-04-21 | 1989-04-20 | Apparatus and method for hydroenhancing fabric |
Country Status (11)
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EP (1) | EP0412099B1 (en) |
JP (1) | JP3212595B2 (en) |
KR (1) | KR940002697B1 (en) |
CN (1) | CN1031079C (en) |
AT (1) | ATE142290T1 (en) |
AU (1) | AU3544189A (en) |
CA (1) | CA1313453C (en) |
DE (1) | DE68927102T2 (en) |
ES (1) | ES2010941A6 (en) |
RU (1) | RU2043434C1 (en) |
WO (1) | WO1989010441A1 (en) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5235733A (en) * | 1984-09-28 | 1993-08-17 | Milliken Research Corporation | Method and apparatus for patterning fabrics and products |
US5080952A (en) * | 1984-09-28 | 1992-01-14 | Milliken Research Corporation | Hydraulic napping process and product |
US5136761A (en) * | 1987-04-23 | 1992-08-11 | International Paper Company | Apparatus and method for hydroenhancing fabric |
US5066535A (en) * | 1987-05-01 | 1991-11-19 | Milliken Research Corporation | Fabric patterning process and product |
US5142752A (en) * | 1990-03-16 | 1992-09-01 | International Paper Company | Method for producing textured nonwoven fabric |
CA2140915A1 (en) * | 1992-07-27 | 1994-02-03 | Richard M. Girardot | Laminated dual textured treatment pads |
GB9602313D0 (en) * | 1996-02-06 | 1996-04-03 | Courtaulds Eng Ltd | Nonwoven fabric manufacture |
GB2313851B (en) * | 1996-02-06 | 1998-12-02 | Courtaulds Eng Ltd | Nonwoven fabric manufacture |
BR0006924A (en) * | 1999-06-25 | 2001-07-31 | Milliken & Co | Carded fabric and process |
JP2002235263A (en) * | 2001-02-08 | 2002-08-23 | Unitica Fibers Ltd | Knitted fabric having excellent windproof property and soft feeing, and method for producing the same |
DE102005007757A1 (en) * | 2005-02-18 | 2006-08-31 | Fleissner Gmbh | Device for patterning and solidifying a web with exchangeable pattern shell |
JP5520091B2 (en) * | 2010-03-10 | 2014-06-11 | ユニ・チャーム株式会社 | Laminate processing equipment |
CN102701133B (en) * | 2012-06-27 | 2014-10-29 | 际华三五三四制衣有限公司 | Automatic cotton quilt production line |
DE102016119480A1 (en) * | 2016-10-12 | 2018-04-12 | TRüTZSCHLER GMBH & CO. KG | Nozzle bar for processing fibers with water jets |
RU2682810C1 (en) * | 2017-12-08 | 2019-03-21 | Лариса Александровна Соболева | Felted mesh with fabric connection unit, the unit structural elements and its implementation method |
CN113358855B (en) * | 2021-08-11 | 2021-10-22 | 南通永盛汇维仕纤维新材料有限公司 | Low-melting-point polyester filament cohesiveness detection device |
Family Cites Families (9)
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CA739652A (en) * | 1966-08-02 | J. Evans Franklin | Jet stitching of batt | |
US3917785A (en) * | 1971-01-27 | 1975-11-04 | Johnson & Johnson | Method for producing nonwoven fabric |
US3747161A (en) * | 1971-08-20 | 1973-07-24 | Johnson & Johnson | Method for producing a rearranged fabric having improved cross-strength |
JPS5411433A (en) * | 1977-06-28 | 1979-01-27 | Hitachi Maxell | Alkaline cell |
JPS5735051A (en) * | 1980-08-06 | 1982-02-25 | Mitsubishi Rayon Co | Three dimensional nonwoven structure reinforced by base cloth and method |
DK268683A (en) * | 1982-06-11 | 1983-12-12 | Milliken Res Corp | METHOD AND APPARATUS FOR CREATING VISUAL SURFACE EFFECTS |
JPH0673445B2 (en) * | 1984-08-31 | 1994-09-21 | 麒麟麦酒株式会社 | Liquor manufacturing method |
IL76495A (en) * | 1984-09-28 | 1990-09-17 | Milliken Res Corp | Method and apparatus for texturing fabrics |
JPS61252339A (en) * | 1985-04-30 | 1986-11-10 | 東レ株式会社 | Knitted fabric and its production |
-
1989
- 1989-04-14 DE DE68927102T patent/DE68927102T2/en not_active Expired - Fee Related
- 1989-04-14 JP JP50504589A patent/JP3212595B2/en not_active Expired - Fee Related
- 1989-04-14 AU AU35441/89A patent/AU3544189A/en not_active Abandoned
- 1989-04-14 WO PCT/US1989/001593 patent/WO1989010441A1/en active IP Right Grant
- 1989-04-14 KR KR1019890702415A patent/KR940002697B1/en not_active IP Right Cessation
- 1989-04-14 EP EP19890905247 patent/EP0412099B1/en not_active Expired - Lifetime
- 1989-04-14 AT AT89905247T patent/ATE142290T1/en not_active IP Right Cessation
- 1989-04-20 CA CA 597326 patent/CA1313453C/en not_active Expired - Fee Related
- 1989-04-21 ES ES8901405A patent/ES2010941A6/en not_active Expired
- 1989-04-21 CN CN89104407A patent/CN1031079C/en not_active Expired - Fee Related
-
1990
- 1990-10-19 RU SU4831574/12A patent/RU2043434C1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
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WO1989010441A1 (en) | 1989-11-02 |
KR940002697B1 (en) | 1994-03-30 |
RU2043434C1 (en) | 1995-09-10 |
EP0412099A4 (en) | 1991-04-10 |
JPH03504990A (en) | 1991-10-31 |
ATE142290T1 (en) | 1996-09-15 |
DE68927102T2 (en) | 1997-02-13 |
JP3212595B2 (en) | 2001-09-25 |
CN1031079C (en) | 1996-02-21 |
CN1040070A (en) | 1990-02-28 |
EP0412099A1 (en) | 1991-02-13 |
ES2010941A6 (en) | 1989-12-01 |
AU3544189A (en) | 1989-11-24 |
DE68927102D1 (en) | 1996-10-10 |
KR900700675A (en) | 1990-08-16 |
EP0412099B1 (en) | 1996-09-04 |
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