BR112017024524A2 - innovative form of sulfentrazone, a process for its preparation and use - Google Patents
innovative form of sulfentrazone, a process for its preparation and useInfo
- Publication number
- BR112017024524A2 BR112017024524A2 BR112017024524A BR112017024524A BR112017024524A2 BR 112017024524 A2 BR112017024524 A2 BR 112017024524A2 BR 112017024524 A BR112017024524 A BR 112017024524A BR 112017024524 A BR112017024524 A BR 112017024524A BR 112017024524 A2 BR112017024524 A2 BR 112017024524A2
- Authority
- BR
- Brazil
- Prior art keywords
- crystal
- preparation
- sulfentrazone
- innovative
- innovative form
- Prior art date
Links
- 238000002360 preparation method Methods 0.000 title abstract 3
- OORLZFUTLGXMEF-UHFFFAOYSA-N sulfentrazone Chemical compound O=C1N(C(F)F)C(C)=NN1C1=CC(NS(C)(=O)=O)=C(Cl)C=C1Cl OORLZFUTLGXMEF-UHFFFAOYSA-N 0.000 title abstract 2
- 239000013078 crystal Substances 0.000 abstract 5
- 238000004458 analytical method Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000003905 agrochemical Substances 0.000 abstract 1
- 238000009472 formulation Methods 0.000 abstract 1
- 230000002363 herbicidal effect Effects 0.000 abstract 1
- 230000008635 plant growth Effects 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
- C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
- C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
- C07D249/10—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D249/12—Oxygen or sulfur atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/647—Triazoles; Hydrogenated triazoles
- A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
trata-se de uma nova forma cristalina de sulfentrazona de fórmula (i), do processo de preparação de cristal, das análises do cristal através de vários métodos analíticos e do uso do cristal para preparar uma formulação agroquímica estável. a invenção também descreve o uso de vários solventes em relação às condições de preparação da forma de cristal. a forma de cristal inovadora é particularmente adequada para uso em composições herbicidas e no controle de crescimento de plantas indesejadas.It is a novel crystalline form of sulfentrazone of formula (I), the crystal preparation process, crystal analysis by various analytical methods and the use of crystal to prepare a stable agrochemical formulation. The invention also describes the use of various solvents with respect to the conditions of preparation of the crystal form. The innovative crystal form is particularly suited for use in herbicidal compositions and in controlling unwanted plant growth.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1608830.4A GB2550399B (en) | 2016-05-19 | 2016-05-19 | A novel form of sulfentrazone, a process for its preparation and use the same |
PCT/CN2017/070458 WO2017197909A1 (en) | 2016-05-19 | 2017-01-06 | Novel form of sulfentrazone, process for its preparation and use thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
BR112017024524A2 true BR112017024524A2 (en) | 2018-07-24 |
Family
ID=56369637
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112017024524A BR112017024524A2 (en) | 2016-05-19 | 2017-01-06 | innovative form of sulfentrazone, a process for its preparation and use |
Country Status (5)
Country | Link |
---|---|
CN (1) | CN109071463B (en) |
BR (1) | BR112017024524A2 (en) |
GB (1) | GB2550399B (en) |
TW (1) | TWI735574B (en) |
WO (1) | WO2017197909A1 (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US11447455B2 (en) | 2016-12-20 | 2022-09-20 | Fmc Corporation | Polymorphs of herbicidal sulfonamides |
UY39134A (en) * | 2020-03-20 | 2021-04-30 | Upl Ltd | AN AGROCHEMICAL COMPOSITION |
CN114644599A (en) * | 2020-12-18 | 2022-06-21 | 南京理工大学 | Micro-reaction method for synthesizing phenyl tetra-substituted triazolinone herbicide intermediate by one-step nitration |
CN114181162B (en) * | 2021-11-08 | 2024-04-16 | 浙大宁波理工学院 | Preparation method of sulfonyl carfentrazone-ethyl |
CN114044758B (en) * | 2021-11-08 | 2024-03-26 | 浙大宁波理工学院 | Synthetic method of intermediate for preparing triazolinone herbicide sulfenamide |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN85106905A (en) * | 1985-08-08 | 1987-02-04 | Fmc公司 | Contain 1-aryl-Δ 2-1,2,4, weedicide of-triazoline-5-ketone and preparation method thereof |
US4909831A (en) * | 1989-02-06 | 1990-03-20 | Fmc Corporation | Safening of crops against a triazolinone herbicide with 1,8-naphthalic anhydride |
IL152702A0 (en) * | 2000-06-05 | 2003-06-24 | Fmc Corp | Process to prepare sulfonamides |
CA2652169C (en) * | 2008-02-14 | 2016-08-23 | Fmc Corporation | Stable dispersions of sulfentrazone in a continuous phase of aqueous glyphosate salt |
CN103951627B (en) * | 2014-05-06 | 2017-04-19 | 泸州东方农化有限公司 | Method for synthesizing sulfentrazone midbody and sulfentrazone |
CN104672157B (en) * | 2015-02-12 | 2017-06-27 | 山东潍坊润丰化工股份有限公司 | A kind of preparation method of aryltriazolinones |
US11447455B2 (en) * | 2016-12-20 | 2022-09-20 | Fmc Corporation | Polymorphs of herbicidal sulfonamides |
-
2016
- 2016-05-19 GB GB1608830.4A patent/GB2550399B/en not_active Expired - Fee Related
-
2017
- 2017-01-06 BR BR112017024524A patent/BR112017024524A2/en not_active Application Discontinuation
- 2017-01-06 CN CN201780021722.7A patent/CN109071463B/en active Active
- 2017-01-06 WO PCT/CN2017/070458 patent/WO2017197909A1/en active Application Filing
- 2017-05-17 TW TW106116243A patent/TWI735574B/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
TWI735574B (en) | 2021-08-11 |
CN109071463A (en) | 2018-12-21 |
GB2550399B (en) | 2022-06-22 |
CN109071463B (en) | 2022-04-29 |
GB201608830D0 (en) | 2016-07-06 |
TW201741289A (en) | 2017-12-01 |
WO2017197909A1 (en) | 2017-11-23 |
GB2550399A (en) | 2017-11-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06W | Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette] | ||
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL.MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |