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ATE312058T1 - METHOD FOR PRODUCING HYDROGEN Cyanide BY OXIDATION OF NITROGEN-CONTAINING HYDROCARBONS IN A FLAME - Google Patents

METHOD FOR PRODUCING HYDROGEN Cyanide BY OXIDATION OF NITROGEN-CONTAINING HYDROCARBONS IN A FLAME

Info

Publication number
ATE312058T1
ATE312058T1 AT03771088T AT03771088T ATE312058T1 AT E312058 T1 ATE312058 T1 AT E312058T1 AT 03771088 T AT03771088 T AT 03771088T AT 03771088 T AT03771088 T AT 03771088T AT E312058 T1 ATE312058 T1 AT E312058T1
Authority
AT
Austria
Prior art keywords
gas
hydrogen cyanide
flame
nitrogen
oxidation
Prior art date
Application number
AT03771088T
Other languages
German (de)
Inventor
Kai Rainer Ehrhardt
Mayke Mueller-Eversbusch
Dieter Stapf
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Application granted granted Critical
Publication of ATE312058T1 publication Critical patent/ATE312058T1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00Cyanogen; Compounds thereof
    • C01C3/02Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208Preparation in gaseous phase
    • C01C3/0245Preparation in gaseous phase from organic nitriles, e.g. acetonitrile

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Hydrogen, Water And Hydrids (AREA)

Abstract

A process is described for preparing hydrogen cyanide by autothermal noncatalytic oxidation of one or more nitrogenous hydrocarbons or a nitrogenous hydrocarbon mixture in which the nitrogenous hydrocarbons, an oxygen-containing gas, with or without ammonia, with or without water, with or without a gas containing nitrogen oxides and with or without other essentially inert feed gas constituents are introduced into a flame reaction zone, react in the flame reaction zone and a post-reaction zone at a temperature of from 1000 to 1800° C. for a reaction time of 0.03 to 0.3 s to form a cleavage gas which comprises at least the constituents hydrogen cyanide, carbon oxides, hydrogen, water, ammonia, nitrogen, light hydrocarbons with or without other cleavage gas constituents, the atomic C/N ratio in the reaction zones being from 1 to 7 and the atomic air ratio lambda<SUB>ato </SUB>being <0.6, the cleavage gas being cooled and separated.
AT03771088T 2002-07-25 2003-07-24 METHOD FOR PRODUCING HYDROGEN Cyanide BY OXIDATION OF NITROGEN-CONTAINING HYDROCARBONS IN A FLAME ATE312058T1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10233931A DE10233931A1 (en) 2002-07-25 2002-07-25 Process for the production of hydrogen cyanide by oxidation of nitrogenous hydrocarbons in a flame
PCT/EP2003/008128 WO2004011373A2 (en) 2002-07-25 2003-07-24 Method for the production of hydrocyanic acid by oxidation of nitrogen-containing hydrocarbons in a flame

Publications (1)

Publication Number Publication Date
ATE312058T1 true ATE312058T1 (en) 2005-12-15

Family

ID=30010378

Family Applications (1)

Application Number Title Priority Date Filing Date
AT03771088T ATE312058T1 (en) 2002-07-25 2003-07-24 METHOD FOR PRODUCING HYDROGEN Cyanide BY OXIDATION OF NITROGEN-CONTAINING HYDROCARBONS IN A FLAME

Country Status (9)

Country Link
US (1) US7294325B2 (en)
EP (1) EP1527015B1 (en)
JP (1) JP2006501120A (en)
CN (1) CN1323945C (en)
AT (1) ATE312058T1 (en)
AU (1) AU2003266241A1 (en)
DE (2) DE10233931A1 (en)
PL (1) PL201774B1 (en)
WO (1) WO2004011373A2 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070122329A1 (en) * 2005-11-30 2007-05-31 Alain Briglia Purification of raw hydrogen
CN101033412B (en) * 2007-03-29 2010-09-29 河北志诚化工集团有限公司 Circulation utilization method for light oil cracking tail gas
FR2926549B1 (en) * 2008-01-18 2015-05-01 Rhodia Operations PROCESS FOR PRODUCING NITRILIC COMPOUNDS
WO2009100437A1 (en) * 2008-02-10 2009-08-13 Hemisphere Gps Llc Antenna alignment and monitoring system and method using gnss
US20150360965A1 (en) * 2012-12-18 2015-12-17 Invista Technologies S.A.R.L. Apparatus and method for decreasing humidity during an andrussow process
US10563596B2 (en) * 2017-03-31 2020-02-18 Generac Power Systems, Inc. Carbon monoxide detecting system for internal combustion engine-based machines

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2596421A (en) 1948-04-12 1952-05-13 Union Oil Co Flame synthesis of hydrogen cyanide
DE1159409B (en) 1960-10-17 1963-12-19 Toyo Koatsu Ind Inc Process for the production of hydrocyanic acid
US3371990A (en) * 1963-07-19 1968-03-05 Monsanto Co Production of hydrogen cyanide
US3661494A (en) * 1970-04-27 1972-05-09 Degussa Process for carrying out endothermic gas reactions
US4136156A (en) * 1976-08-30 1979-01-23 E. I. Du Pont De Nemours And Company Production of hcn from organic nitriles
US4981670A (en) 1989-12-15 1991-01-01 Bp America Inc. HCN from crude aceto
US5204079A (en) * 1991-02-15 1993-04-20 Standard Oil Company HCN by catalytic ammoxidation of crude acetonitrile
DE19709261A1 (en) * 1997-03-06 1998-09-10 Basf Ag Process for the simultaneous production of acetylene and hydrocyanic acid from acrylonitrile
DE19805481A1 (en) * 1998-02-11 1999-08-12 Degussa Tube furnace for carrying out continuous endothermic gas reactions, its use and processes for the production of gaseous substances
DE19810484A1 (en) * 1998-03-11 1999-09-16 Degussa Process for the production of hydrocyanic acid
US6221327B1 (en) * 1998-05-15 2001-04-24 Rohm And Haas Company Catalyst system using flow-through radiation shielding and a process for producing hydrogen cyanide using the same
DE19954188A1 (en) * 1999-11-11 2001-05-31 Krc Umwelttechnik Gmbh Process and device for recycling organic nitrogen compounds by gasification

Also Published As

Publication number Publication date
EP1527015A2 (en) 2005-05-04
JP2006501120A (en) 2006-01-12
DE10233931A1 (en) 2004-02-05
WO2004011373A3 (en) 2004-04-08
AU2003266241A1 (en) 2004-02-16
PL375402A1 (en) 2005-11-28
CN1323945C (en) 2007-07-04
EP1527015B1 (en) 2005-12-07
CN1671623A (en) 2005-09-21
PL201774B1 (en) 2009-05-29
WO2004011373A2 (en) 2004-02-05
US20050220693A1 (en) 2005-10-06
US7294325B2 (en) 2007-11-13
DE50301881D1 (en) 2006-01-12

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