ATE120742T1 - Verfahren zur herstellung von e-caprolacton. - Google Patents
Verfahren zur herstellung von e-caprolacton.Info
- Publication number
- ATE120742T1 ATE120742T1 AT91303594T AT91303594T ATE120742T1 AT E120742 T1 ATE120742 T1 AT E120742T1 AT 91303594 T AT91303594 T AT 91303594T AT 91303594 T AT91303594 T AT 91303594T AT E120742 T1 ATE120742 T1 AT E120742T1
- Authority
- AT
- Austria
- Prior art keywords
- mole
- caprolactone
- cyclohexanone
- hydrogen peroxide
- less
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D315/00—Heterocyclic compounds containing rings having one oxygen atom as the only ring hetero atom according to more than one of groups C07D303/00 - C07D313/00
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives
- C07C407/006—Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyrane Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2107674A JPH0798816B2 (ja) | 1990-04-25 | 1990-04-25 | ε―カプロラクトンの製造法 |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE120742T1 true ATE120742T1 (de) | 1995-04-15 |
Family
ID=14465118
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT91303594T ATE120742T1 (de) | 1990-04-25 | 1991-04-22 | Verfahren zur herstellung von e-caprolacton. |
Country Status (7)
Country | Link |
---|---|
US (1) | US5250707A (de) |
EP (1) | EP0454397B1 (de) |
JP (1) | JPH0798816B2 (de) |
CN (1) | CN1035379C (de) |
AT (1) | ATE120742T1 (de) |
CA (1) | CA2040270A1 (de) |
DE (1) | DE69108600T2 (de) |
Families Citing this family (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0974581A4 (de) * | 1997-09-16 | 2002-01-02 | Daicel Chem | Verfahren zur herstellung von peroxysäure im gleichgewicht und verfahren zur herstellung von lacton |
JP2004143047A (ja) * | 2002-10-22 | 2004-05-20 | Daicel Chem Ind Ltd | ε−カプロラクトンの製造方法 |
JP2005139110A (ja) * | 2003-11-06 | 2005-06-02 | Ecology Maximum Co Ltd | ε−カプロラクトンの製造方法、並びに、ε−カプロラクトンを用いたポリカプロラクトンの製造方法 |
JP4297152B2 (ja) | 2006-10-06 | 2009-07-15 | トヨタ自動車株式会社 | 車両前部構造 |
US8871807B2 (en) | 2008-03-28 | 2014-10-28 | Ecolab Usa Inc. | Detergents capable of cleaning, bleaching, sanitizing and/or disinfecting textiles including sulfoperoxycarboxylic acids |
US8809392B2 (en) | 2008-03-28 | 2014-08-19 | Ecolab Usa Inc. | Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents |
CN102105443B (zh) | 2008-03-28 | 2014-05-28 | 埃科莱布有限公司 | 磺基过氧羧酸、它们的制备和用作漂白剂和抗微生物剂的方法 |
CN102584776A (zh) * | 2011-01-12 | 2012-07-18 | 中国石油化工集团公司 | 一种制备ε-己内酯的方法 |
CN102584775B (zh) * | 2011-01-12 | 2015-04-22 | 中国石油化工集团公司 | 制备ε-己内酯的方法 |
CN102304117A (zh) * | 2011-09-19 | 2012-01-04 | 武汉理工大学 | 一种合成ε-己内酯的方法 |
US9321664B2 (en) * | 2011-12-20 | 2016-04-26 | Ecolab Usa Inc. | Stable percarboxylic acid compositions and uses thereof |
US9242879B2 (en) | 2012-03-30 | 2016-01-26 | Ecolab Usa Inc. | Use of peracetic acid/hydrogen peroxide and peroxide-reducing agents for treatment of drilling fluids, frac fluids, flowback water and disposal water |
US20140256811A1 (en) | 2013-03-05 | 2014-09-11 | Ecolab Usa Inc. | Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids |
CN104003972A (zh) * | 2014-04-28 | 2014-08-27 | 安徽红太阳新材料有限公司 | 一种制备己内酯的方法 |
CN104130234A (zh) * | 2014-07-25 | 2014-11-05 | 南京红太阳新材料有限公司 | 一种制备己内酯的方法 |
US10172351B2 (en) | 2015-09-04 | 2019-01-08 | Ecolab Usa Inc. | Performic acid on-site generator and formulator |
CN105315442A (zh) * | 2015-12-01 | 2016-02-10 | 仇颖超 | 一种淀粉改性聚己内酯塑料材料的制备方法 |
GB2548137A (en) * | 2016-03-09 | 2017-09-13 | Perstorp Ab | Production equipment (I) for production of a caprolactone |
GB2548138A (en) * | 2016-03-09 | 2017-09-13 | Perstorp Ab | Production equipment (II) for production of a caprolactone |
CN107163018A (zh) * | 2017-06-23 | 2017-09-15 | 中山大学惠州研究院 | 一种分离ε‑己内酯的精馏方法 |
WO2020041545A1 (en) | 2018-08-22 | 2020-02-27 | Ecolab Usa Inc. | Hydrogen peroxide and peracid stabilization with molecules based on a pyridine carboxylic acid at c-3, -4 or -5 |
WO2021026410A1 (en) | 2019-08-07 | 2021-02-11 | Ecolab Usa Inc. | Polymeric and solid-supported chelators for stabilization of peracid-containing compositions |
CN111763192B (zh) * | 2020-07-14 | 2023-09-12 | 湖南瑞源石化股份有限公司 | 一种ε-己内酯的制备方法及其装置 |
CN115490623B (zh) * | 2021-06-18 | 2024-08-30 | 中国石油化工股份有限公司 | 合成无水过氧有机酸的方法和合成ε-己内酯的方法 |
CN114835669A (zh) * | 2022-03-23 | 2022-08-02 | 华东理工大学 | 高纯度ε-己内酯的微流控合成方法 |
CN115812713B (zh) * | 2022-11-29 | 2024-03-29 | 湖南聚仁新材料股份公司 | 消毒剂和己内酯生产过程中联产过氧羧酸消毒剂的方法 |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3064008A (en) * | 1962-11-13 | I i i i i i | ||
US2914556A (en) * | 1956-04-13 | 1959-11-24 | Union Carbide Corp | Preparation of lactone adducts |
US3189619A (en) * | 1962-09-25 | 1965-06-15 | Exxon Research Engineering Co | Synthesis of carpolactone |
US3317563A (en) * | 1963-12-26 | 1967-05-02 | Celanese Corp | Preparation of epsilon-caprolactone |
FR1474098A (fr) * | 1966-01-25 | 1967-03-24 | Electro Chimie Soc D | Procédé de préparation d'epsilon-caprolactone |
FR1474903A (fr) * | 1966-02-12 | 1967-03-31 | Electrochimie Soc | Procédé de préparation d'epsiloncaprolactone |
GB1140184A (en) * | 1967-06-13 | 1969-01-15 | Chisso Corp | Process for manufacturing e-caprolactone |
US3624258A (en) * | 1969-03-22 | 1971-11-30 | Teijin Ltd | Process for the preparation of {68 -caprolactone |
DE2038455A1 (de) * | 1970-08-01 | 1972-02-10 | Bayer Ag | Verfahren zur Herstellung von epsilon-Caprolacton |
US3781350A (en) * | 1971-07-09 | 1973-12-25 | Teijin Ltd | Process for preparation of omega-hydroxy saturated aliphatic monocarboxylic acids |
US3825570A (en) * | 1971-11-02 | 1974-07-23 | Teijin Ltd | Process for the preparation of epsilon-caprolactone |
US4183863A (en) * | 1978-04-18 | 1980-01-15 | Union Carbide Corporation | Conversion of cyclohexanol to ε-caprolactone |
DE2920436A1 (de) * | 1979-05-19 | 1980-12-04 | Bayer Ag | Verfahren zur herstellung von epsilon -caprolacton |
DE2934659A1 (de) * | 1979-08-28 | 1981-03-19 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von sehr reinem epsilon -caprolacton |
FR2500453A1 (fr) * | 1981-02-20 | 1982-08-27 | Ugine Kuhlmann | Procede d'obtention de l'epsilon-caprolactone |
FR2519985A1 (fr) * | 1982-01-15 | 1983-07-22 | Ugine Kuhlmann | Procede perfectionne de fabrication de l'e-caprolactone |
JPH0237919B2 (ja) * | 1983-05-04 | 1990-08-28 | Mitsubishi Chem Ind | Kapurorakutonnoseizohoho |
JPS61200120A (ja) * | 1985-03-01 | 1986-09-04 | Nippon Shokubai Kagaku Kogyo Co Ltd | ラクトン変性化合物の製造方法 |
DE3823213A1 (de) * | 1988-07-08 | 1990-01-11 | Basf Ag | Verfahren zur herstellung von caprolacton |
-
1990
- 1990-04-25 JP JP2107674A patent/JPH0798816B2/ja not_active Expired - Fee Related
-
1991
- 1991-04-22 DE DE69108600T patent/DE69108600T2/de not_active Expired - Fee Related
- 1991-04-22 EP EP91303594A patent/EP0454397B1/de not_active Expired - Lifetime
- 1991-04-22 AT AT91303594T patent/ATE120742T1/de not_active IP Right Cessation
- 1991-04-22 US US07/689,151 patent/US5250707A/en not_active Expired - Fee Related
- 1991-04-24 CA CA002040270A patent/CA2040270A1/en not_active Abandoned
- 1991-10-25 CN CN91109988A patent/CN1035379C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
US5250707A (en) | 1993-10-05 |
EP0454397A1 (de) | 1991-10-30 |
CN1035379C (zh) | 1997-07-09 |
EP0454397B1 (de) | 1995-04-05 |
CA2040270A1 (en) | 1991-10-26 |
DE69108600D1 (de) | 1995-05-11 |
DE69108600T2 (de) | 1996-01-11 |
JPH0798816B2 (ja) | 1995-10-25 |
CN1071923A (zh) | 1993-05-12 |
JPH049378A (ja) | 1992-01-14 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |