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NO20011920L - Process for the preparation of a MEL type titanium silicalite, the product obtained and its use in catalysis - Google Patents

Process for the preparation of a MEL type titanium silicalite, the product obtained and its use in catalysis

Info

Publication number
NO20011920L
NO20011920L NO20011920A NO20011920A NO20011920L NO 20011920 L NO20011920 L NO 20011920L NO 20011920 A NO20011920 A NO 20011920A NO 20011920 A NO20011920 A NO 20011920A NO 20011920 L NO20011920 L NO 20011920L
Authority
NO
Norway
Prior art keywords
preparation
type titanium
titanium silicalite
catalysis
product obtained
Prior art date
Application number
NO20011920A
Other languages
Norwegian (no)
Other versions
NO20011920D0 (en
Inventor
Jean-Louis Grieneisen
Henri Kessler
Eric Fache
Anne-Marie Le Govic
Michel Costantini
Original Assignee
Rhodia Chimie Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Chimie Sa filed Critical Rhodia Chimie Sa
Publication of NO20011920D0 publication Critical patent/NO20011920D0/en
Publication of NO20011920L publication Critical patent/NO20011920L/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/60—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by oxidation reactions introducing directly hydroxy groups on a =CH-group belonging to a six-membered aromatic ring with the aid of other oxidants than molecular oxygen or their mixtures with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Oppfinnelsen vedrører en ny fremgangsmåte for fremstilling av MEL-type titansilikalitt, det oppnådde produkt og dets forskjellige anvendelser på området katalyse. Fremgangsmåten ifølge oppfinnelsen for fremstilling av MEL-type titan- silikalitt kjennetegnes ved at den består i: impregnering av en amorf xerogel (Ti02-Si02) omfattende minst elementene silisium og titan med en oppløsning omfattende minst ett strukturmiddel og minst ett mobiliseringsmiddel OH", idet impregneringsopplzsningen omfatter minst en effektiv mengde av en forbindelse av typen 3,5-dimetylpiperidinium anvendt som strukturmiddel, oppvarming av reaksjonsblandingen opp til krystalliseringstemperaturen for zeolitten, deretter utvinning og kalsinering av den oppnådde zeolitt. De oppnådde zeolittkrystaller fremviser en morfologi som resulterer fra deres fremstillingsmetode.The invention relates to a novel process for the preparation of MEL-type titanium silicalite, the product obtained and its various applications in the field of catalysis. The process of the invention for the preparation of MEL-type titanium silicalite is characterized in that it consists in: impregnating an amorphous xerogel (TiO2-SiO2) comprising at least the elements silicon and titanium having a solution comprising at least one structural agent and at least one mobilizing agent OH the impregnating solution comprises at least an effective amount of a compound of the type 3,5-dimethylpiperidinium used as a structural agent, heating the reaction mixture up to the crystallization temperature of the zeolite, then recovering and calcining the obtained zeolite.

NO20011920A 1998-10-19 2001-04-18 Process for the preparation of a MEL type titanium silicalite, the product obtained and its use in catalysis NO20011920L (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9813078A FR2784672B1 (en) 1998-10-19 1998-10-19 PROCESS FOR THE PREPARATION OF MEL-TYPE TITANIUM SILICALITY, PRODUCT OBTAINED AND ITS APPLICATIONS IN CATALYSIS
PCT/FR1999/002478 WO2000023377A1 (en) 1998-10-19 1999-10-13 Method for preparing a mel-type titanium silicalite, resulting product and uses in catalysis

Publications (2)

Publication Number Publication Date
NO20011920D0 NO20011920D0 (en) 2001-04-18
NO20011920L true NO20011920L (en) 2001-06-19

Family

ID=9531724

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20011920A NO20011920L (en) 1998-10-19 2001-04-18 Process for the preparation of a MEL type titanium silicalite, the product obtained and its use in catalysis

Country Status (7)

Country Link
EP (1) EP1131264A1 (en)
JP (1) JP2002527347A (en)
CN (1) CN1324325A (en)
AU (1) AU6206799A (en)
FR (1) FR2784672B1 (en)
NO (1) NO20011920L (en)
WO (1) WO2000023377A1 (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6968669B2 (en) 2002-11-06 2005-11-29 Lancer Partnership Ltd. Flexible packaging
FR2869033B1 (en) * 2004-04-20 2006-06-02 Rhodia Chimie Sa PROCESS FOR THE PREPARATION OF METHYLENEDIOXYBENZENE
FR2905374B1 (en) 2006-09-04 2008-11-14 Rhodia Recherches & Tech PROCESS FOR THE PREPARATION OF HIGH PURITY HYDROQUINONE
FR2925489B1 (en) 2007-12-19 2010-02-05 Rhodia Operations PROCESS FOR THE PREPARATION OF PURIFIED PYROCATECHOL
FR2987046B1 (en) * 2012-02-17 2014-03-21 Rhodia Operations HYDROXYLATION PROCESS FOR AROMATIC COMPOUNDS, HYDROXYLATION CATALYST AND PROCESS FOR PREPARING THE SAME
JP5972694B2 (en) * 2012-07-18 2016-08-17 ユニゼオ株式会社 Fe (II) -substituted MEL type zeolite, gas adsorbent containing the same, method for producing the same, and method for removing nitric oxide and hydrocarbon
CN106268927B (en) * 2015-05-27 2021-04-06 中国石油化工股份有限公司 Ti-beta molecular sieve obtained by modifying all-silicon beta molecular sieve and preparation method and application thereof
FR3067348B1 (en) 2017-06-13 2019-06-28 Rhodia Operations COMPOSITIONS COMPRISING HYDROQUINONE AND CATECHOL, PROCESS FOR PREPARING THESE COMPOSITIONS
FR3074177A1 (en) 2017-11-30 2019-05-31 Rhodia Operations COMPOSITIONS COMPRISING 4-ALKOXYPHENOL AND 2-ALKOXYPHENOL, AND PROCESS FOR THEIR PREPARATION
FR3075198B1 (en) * 2017-12-15 2020-04-03 Rhodia Operations PROCESS FOR HYDROXYLATION OF AN AROMATIC COMPOUND
CN111484031B (en) * 2019-01-28 2023-03-10 中国石油化工股份有限公司 Modified titanium-silicon molecular sieve, preparation method and application thereof, and thioether oxidation method

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1222868B (en) * 1987-10-12 1990-09-12 Montedipe Spa METHOD FOR THE PREPARATION OF TITANIUM SILICALITES
AU5485296A (en) * 1995-05-04 1996-11-21 Chevron U.S.A. Inc. Pure phase titanium, containing zeolite having mel structure
DE19623972A1 (en) * 1996-06-15 1997-12-18 Degussa Titanium containing molecular sieves used as oxidation catalysts and for the epoxidation of olefin(s) are prepared simply and reliably
GB9703093D0 (en) * 1997-02-14 1997-04-02 Exxon Chemical Patents Inc Metal molecular sieve catalysts

Also Published As

Publication number Publication date
WO2000023377A1 (en) 2000-04-27
FR2784672B1 (en) 2000-12-29
JP2002527347A (en) 2002-08-27
FR2784672A1 (en) 2000-04-21
EP1131264A1 (en) 2001-09-12
NO20011920D0 (en) 2001-04-18
AU6206799A (en) 2000-05-08
CN1324325A (en) 2001-11-28

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