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MD332C2 - Method of obtaining cis-2-(1H-1,2,4-triazole-1-yl-methyl)-2-(halogenphenyl)-3-(halogenphenyl)-oxirane - Google Patents

Method of obtaining cis-2-(1H-1,2,4-triazole-1-yl-methyl)-2-(halogenphenyl)-3-(halogenphenyl)-oxirane

Info

Publication number
MD332C2
MD332C2 MD95-0016A MD950016A MD332C2 MD 332 C2 MD332 C2 MD 332C2 MD 950016 A MD950016 A MD 950016A MD 332 C2 MD332 C2 MD 332C2
Authority
MD
Moldova
Prior art keywords
halogenphenyl
triazole
oxirane
methyl
restorer
Prior art date
Application number
MD95-0016A
Other languages
Romanian (ro)
Russian (ru)
Other versions
MD332B1 (en
Inventor
Hickmann Eckhard
Rainer Seele
Kober Reiner
Heinz Isak
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of MD332B1 publication Critical patent/MD332B1/en
Publication of MD332C2 publication Critical patent/MD332C2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D405/00—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom
    • C07D405/02—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom containing two hetero rings
    • C07D405/06—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom containing two hetero rings linked by a carbon chain containing only aliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
    • C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/12—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/56—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention relates to the method of obtaining cis-2-(1H-1,2,4-triazole-1-yl-methyl)-2-(halogenphenyl)-3-(halogenphenyl)-oxirane with the following formula:The purpose of the invention is to increase the going out of the product with a special purpose and to diminish the cleaning expenses.The method if put into practice by the epoxidation of Z-3-(1H-1,2,4-triazole-1-yl)-2-(halogenphenyl)-1-(halogenphenyl)-propene with Permalloy acid with a further renewal. As a restorer may be used sodium hydrosulfite, sodium dithion or sodium thiosulfate or hydrogen in the presence of rhenium nickel. the restorer is added to the reaction composition in a quantity exceeding the quantity which is necessary for the dissociation of probably existing Permalloy acid.Claims:2
MD95-0016A 1989-11-04 1994-12-13 Method of obtaining cis-2-(1H-1,2,4-triazole-1-yl-methyl)-2-(halogenphenyl)-3-(halogenphenyl)-oxirane MD332C2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3936821A DE3936821A1 (en) 1989-11-04 1989-11-04 METHOD FOR PRODUCING CIS-2- (1H-1,2,4-TRIAZOL-1-YLMETHYL) -2- (HALOGENPHENYL) -3- (HALOGENPHENYL) -OXIRAN
SU904831490A RU2071473C1 (en) 1989-11-04 1990-11-02 Process for preparing cis-2-(1h-triazol-1-yl-methyl)-2- (halogenphenyl)-3-(halogenphenyl)oxirane

Publications (2)

Publication Number Publication Date
MD332B1 MD332B1 (en) 1995-11-30
MD332C2 true MD332C2 (en) 1996-03-31

Family

ID=6392916

Family Applications (1)

Application Number Title Priority Date Filing Date
MD95-0016A MD332C2 (en) 1989-11-04 1994-12-13 Method of obtaining cis-2-(1H-1,2,4-triazole-1-yl-methyl)-2-(halogenphenyl)-3-(halogenphenyl)-oxirane

Country Status (10)

Country Link
EP (1) EP0427061B1 (en)
JP (1) JP2983054B2 (en)
KR (1) KR0157314B1 (en)
AT (1) ATE116315T1 (en)
CA (1) CA2028650C (en)
DE (2) DE3936821A1 (en)
DK (1) DK0427061T3 (en)
ES (1) ES2066089T3 (en)
MD (1) MD332C2 (en)
RU (1) RU2071473C1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NZ272586A (en) * 1995-07-17 1996-10-28 Apotex Inc Process for preparing fluconazole and triazolylepoxypropane precursors
EP1517906B1 (en) * 2002-06-24 2007-03-28 Basf Aktiengesellschaft Method for the production of 1,2,4-triazolylmethyl-oxiranes
EP2746275A1 (en) 2012-12-19 2014-06-25 Basf Se New substituted triazoles and imidazoles and their use as fungicides
CN103936723B (en) * 2013-01-23 2016-06-29 沈阳中化农药化工研发有限公司 A kind of method that catalysis triazole alkene epoxidation prepares epoxiconazole
CN111848504A (en) * 2019-04-29 2020-10-30 沈阳中化农药化工研发有限公司 Manganese catalyst and application thereof in catalyzing epoxidation of triazolene to prepare epoxiconazole

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2952755A1 (en) * 1979-12-29 1981-07-02 Bayer Ag, 5090 Leverkusen METHOD FOR PRODUCING OXIRANES
CA1271764A (en) * 1985-03-29 1990-07-17 Stefan Karbach Azolylmethyloxiranes, their preparation and their use as crop protection agents

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Cererea nr. 3218129, DE, Int. Cl. C 07 D 405 /06, 1983. *

Also Published As

Publication number Publication date
RU2071473C1 (en) 1997-01-10
ATE116315T1 (en) 1995-01-15
KR910009695A (en) 1991-06-28
ES2066089T3 (en) 1995-03-01
EP0427061B1 (en) 1994-12-28
JPH03153682A (en) 1991-07-01
EP0427061A3 (en) 1992-01-02
DK0427061T3 (en) 1995-02-27
DE59008135D1 (en) 1995-02-09
JP2983054B2 (en) 1999-11-29
KR0157314B1 (en) 1998-11-16
EP0427061A2 (en) 1991-05-15
MD332B1 (en) 1995-11-30
CA2028650A1 (en) 1991-05-05
DE3936821A1 (en) 1991-05-08
CA2028650C (en) 2003-09-30

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Legal Events

Date Code Title Description
FG4A Patent for invention issued
IF99 Valid patent on 19990615

Free format text: EXPIRES: 20101102

KA4A Patent for invention lapsed due to non-payment of fees (with right of restoration)
MM4A Patent for invention definitely lapsed due to non-payment of fees