Lu et al., 2016 - Google Patents
Ionizing aromatic compounds in petroleum by electrospray with HCOONH4 as ionization promoterLu et al., 2016
- Document ID
- 9508563785766381049
- Author
- Lu J
- Zhang Y
- Shi Q
- Publication year
- Publication venue
- Analytical chemistry
External Links
Snippet
Electrospray ionization (ESI) coupled with Fourier ion cyclotron resonance mass spectrometry (FTICR MS) has been successfully used for molecular characterization of petroleum. However, ESI can not ionize nonpolar components which generally are dominant …
- 239000003208 petroleum 0 title abstract description 69
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by the preceding groups
- G01N33/26—Investigating or analysing materials by specific methods not covered by the preceding groups oils; viscous liquids; paints; inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by the preceding groups
- G01N33/48—Investigating or analysing materials by specific methods not covered by the preceding groups biological material, e.g. blood, urine; Haemocytometers
- G01N33/50—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8665—Signal analysis for calibrating the measuring apparatus
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electro-chemical, or magnetic means
- G01N27/02—Investigating or analysing materials by the use of electric, electro-chemical, or magnetic means by investigating the impedance of the material
- G01N27/22—Investigating or analysing materials by the use of electric, electro-chemical, or magnetic means by investigating the impedance of the material by investigating capacitance
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
- G01N30/94—Development
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Shi et al. | Characterization of middle-temperature gasification coal tar. Part 3: Molecular composition of acidic compounds | |
Lu et al. | Ionizing aromatic compounds in petroleum by electrospray with HCOONH4 as ionization promoter | |
Shi et al. | Characterization of basic nitrogen species in coker gas oils by positive-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry | |
Wu et al. | Resolution of 10 000 compositionally distinct components in polar coal extracts by negative-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry | |
Mckenna et al. | Heavy petroleum composition. 1. Exhaustive compositional analysis of Athabasca bitumen HVGO distillates by Fourier transform ion cyclotron resonance mass spectrometry: A definitive test of the Boduszynski model | |
McKenna et al. | Identification of vanadyl porphyrins in a heavy crude oil and raw asphaltene by atmospheric pressure photoionization Fourier transform ion cyclotron resonance (FT-ICR) mass spectrometry | |
Klein et al. | Use of saturates/aromatics/resins/asphaltenes (SARA) fractionation to determine matrix effects in crude oil analysis by electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry | |
Pomerantz et al. | Orbitrap mass spectrometry: a proposal for routine analysis of nonvolatile components of petroleum | |
Qian et al. | Reading chemical fine print: Resolution and identification of 3000 nitrogen-containing aromatic compounds from a single electrospray ionization Fourier transform ion cyclotron resonance mass spectrum of heavy petroleum crude oil | |
Rodgers et al. | Resolution, elemental composition, and simultaneous monitoring by Fourier transform ion cyclotron resonance mass spectrometry of organosulfur species before and after diesel fuel processing | |
Lobodin et al. | Compositional space boundaries for organic compounds | |
McKenna et al. | Heavy petroleum composition. 2. Progression of the Boduszynski model to the limit of distillation by ultrahigh-resolution FT-ICR mass spectrometry | |
Liu et al. | Characterization of sulfide compounds in petroleum: selective oxidation followed by positive-ion electrospray Fourier transform ion cyclotron resonance mass spectrometry | |
Shi et al. | Distribution of acids and neutral nitrogen compounds in a Chinese crude oil and its fractions: characterized by negative-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry | |
Marshall et al. | Petroleomics: the next grand challenge for chemical analysis | |
Zhu et al. | Characterization of nitrogen compounds in coker heavy gas oil and its subfractions by liquid chromatographic separation followed by Fourier transform ion cyclotron resonance mass spectrometry | |
Purcell et al. | Sulfur speciation in petroleum: Atmospheric pressure photoionization or chemical derivatization and electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry | |
Shi et al. | Characterization of heteroatom compounds in a crude oil and its saturates, aromatics, resins, and asphaltenes (SARA) and non-basic nitrogen fractions analyzed by negative-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry | |
Eckert et al. | Chemical characterization of crude petroleum using nanospray desorption electrospray ionization coupled with high-resolution mass spectrometry | |
Zhou et al. | Analysis of saturated hydrocarbons by redox reaction with negative-ion electrospray Fourier transform ion cyclotron resonance mass spectrometry | |
Zhang et al. | Partitioning of crude oil acidic compounds into subfractions by extrography and identification of isoprenoidyl phenols and tocopherols | |
McKenna et al. | Molecular-level characterization of asphaltenes isolated from distillation cuts | |
Qian et al. | Determination of structural building blocks in heavy petroleum systems by collision-induced dissociation Fourier transform ion cyclotron resonance mass spectrometry | |
Gutiérrez Sama et al. | Molecular fingerprints and speciation of crude oils and heavy fractions revealed by molecular and elemental mass spectrometry: keystone between petroleomics, metallopetroleomics, and petrointeractomics | |
Qian et al. | Measurement of total acid number (TAN) and TAN boiling point distribution in petroleum products by electrospray ionization mass spectrometry |