[go: up one dir, main page]
More Web Proxy on the site http://driver.im/ Skip to main content
Log in

Formation and characterization of high-density silver nanoparticles embedded in silica thin films by “in situ” self-reduction

  • Articles
  • Published:
Journal of Materials Research Aims and scope Submit manuscript

Abstract

Silver nanoparticles (10–20 nm) embedded into silica thin films have been obtained through the use of a silver organometallic precursor compound dissolved in Spin-On-Glass and subsequently spinned onto suitable substrates. In this paper we present a study of the shape, size, and distribution of silver particles through the use of microscopes, x-ray diffraction, and optical extinction. It has been observed that the obtained films are stable for annealing up to 500 °C with a progressive degradation above this temperature. Furthermore it is possible to obtain high-density silver particles up to 15% in weight without affecting the cluster size and shape.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Subscribe and save

Springer+ Basic
£29.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or eBook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price includes VAT (United Kingdom)

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. L.N. Lewis, Chem. Rev. 93, 2693 (1993).

    Google Scholar 

  2. G.C. Bond, Surf. Sci. 156, 966 (1985).

    Article  CAS  Google Scholar 

  3. H. Gleiter Prog. Mater. Sci. 33, 223 (1989).

    Article  CAS  Google Scholar 

  4. G.D. Stucky and J.E. McDougall, Science 247, 669 (1990).

    Article  CAS  Google Scholar 

  5. E.J. Heolweil and R.M. Hachestrasser, J. Chem. Phys. 82, 4762 (1985).

    Article  CAS  Google Scholar 

  6. A.L. Stepanov, D.E. Hole, and P.D. Townsend, J. Non-Cryst. Solids 260, 5–74 (1999).

    Article  Google Scholar 

  7. D. Ila, E.K. Williams, S. Sarkisov, C.C. Smith, D.B. Poker, and D.K. Hensley, Nucl. Instrum. Methods 141, 289 (1998).

    Article  Google Scholar 

  8. D.P. Peters, C. Strohhoöfer, M.L. Brongersma, J. van Elsken, and A. Polman, Nucl. Instrum. Methods 237–244, 168 (2000).

    Article  CAS  Google Scholar 

  9. M. Dubiel, H. Hofmeister, E. Schurin, E. Wendler, and W. Wesch, Nucl. Instrum. Methods 166–167, 871 (2000).

    Google Scholar 

  10. J.P. Carpenter, C.M. Lukehart, S.B. Milne, D.O. Henderson, R. Mu, and S.R. Stock, Chem. Mater. 9, 3164 (1997).

    Article  Google Scholar 

  11. M.E. Fragalà, G. Compagnini, G. Malandrino, C. Spinella, and O. Puglisi, Eur. Phys. J. D9, 631 (1999).

    Article  CAS  Google Scholar 

  12. M.E. Fragalà, G. Malandrino, O. Puglisi, and C. Benelli, Chem. Mater. 12, 290 (2000).

    Article  Google Scholar 

  13. J.D. Romero, M. Khan, H. Fatemi, and J. Turlo, 6, 1996 (1991).

    Article  Google Scholar 

  14. P.J. Hull, J.L. Hutchison, O.V. Salata, and J. Dobson, Adv. Mater. 9, 413 (1997).

  15. B. Palpant, B. Prevél, J. Lermé, E. Cottancin, M. Pellarin, M. Treilleux, A. Perez, J.L. Vialle, and M. Broyer, 3, 57 (1998).

    Article  CAS  Google Scholar 

  16. Z. Liu, H. Li, X. Feng, S. Ren, and H. Wang, 84, 1913 (1998).

  17. W. Cai, L. Zhang, H. Zhong, and G. He, J. Mater. Res. 13, 2888 (1998).

  18. See for instance: I. Tanahashi, M. Yoshida, Y. Manabe, and T. Tohda, J. Mater. Res. 10, 362 (1995).

    Article  CAS  Google Scholar 

  19. H.G. Jiang, M. Ruhle, and E.J. Lavernia, J. Mater. Res. 14, 549 (1999).

    Article  CAS  Google Scholar 

  20. N. Rohrer, C. Akrout, M. Canada, D. Cawthron, B. Davari, R. Floyd, S. Geissler, R. Goldblatt, R. Houle, and P. Kartschoke, Digest of Technical Papers—IEEE International Solid-State Cir-cuits Conference Proceedings of the 1998 IEEE 45th Interna-tional Solid-State Circuits Conference (IEEE, Piscataway, NJ, 1998), pp. 240–241.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to G. Compagnini.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Compagnini, G., Fragal´, M.M., D’Urso, L. et al. Formation and characterization of high-density silver nanoparticles embedded in silica thin films by “in situ” self-reduction. Journal of Materials Research 16, 2934–2938 (2001). https://doi.org/10.1557/JMR.2001.0403

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/JMR.2001.0403

Navigation