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30 pages, 12252 KiB  
Article
A Novel Strutless Double-Row Structure for Deep Excavation: Working Mechanism Study and Analysis
by Jinqing Jia and Xuegang Pan
Appl. Sci. 2025, 15(4), 2173; https://doi.org/10.3390/app15042173 - 18 Feb 2025
Abstract
This paper presents a novel strut-free earth retaining wall system for excavation, referred to as the asymmetric double-row pile wall (ARPW) retaining system. This system comprises three key elements: front-row reinforced concrete piles, back-row walls, and connecting crossbeams at the top of the [...] Read more.
This paper presents a novel strut-free earth retaining wall system for excavation, referred to as the asymmetric double-row pile wall (ARPW) retaining system. This system comprises three key elements: front-row reinforced concrete piles, back-row walls, and connecting crossbeams at the top of the piles. This paper aims to analyze the deformation characteristics and mechanical behavior of the ARPW retaining system, double-row pile wall (DRPW) retaining system, and single-row pile wall (SPW) retaining system using both physical model tests and numerical simulations. The study reveals that, with reasonable row spacing, double-row structures exhibit substantially lower earth pressure and bending moments compared to SPW. Additionally, all double-row structures display reverse bending points. The optimal row spacing for DRPW and ARPW is within the ranges of 2D to 6D and 4D to 8D, respectively. ARPW outperforms DRPW by efficiently utilizing active zone friction force and soil weight force (Gs) to resist overturning moments, thereby resulting in improved anti-overturning capabilities, reduced deformations, lower internal forces, and enhanced stability. The study also presents a case study from the Jinzhonghe Avenue South Side Plot in Tianjin, demonstrating the practical application and effectiveness of the ARPW system in meeting stringent deformation requirements for deep foundation pits. These research findings provide valuable insights for practical engineering applications. Full article
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Figure 1
<p>Model box.</p>
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<p>Definition of model soil properties based on a steady-state line.</p>
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<p>Particle size distribution curve.</p>
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<p>Steady-state line.</p>
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<p>Model pile.</p>
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<p>Sketch of crossbeam. (<b>a</b>) SPW; (<b>b</b>) DRPW; (<b>c</b>) ARPW.</p>
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<p>Layout of retaining structure.</p>
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<p>Layout of the detection device.</p>
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<p>Filling process.</p>
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<p>Test process (<b>a</b>) diagram; (<b>b</b>) excavation process. Note: RS represents the length of row spacing.</p>
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<p>Numerical simulation model.</p>
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<p>Horizontal displacement of pile top during excavation.</p>
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<p>Pile top horizontal displacement (H = 500 mm).</p>
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<p>Horizontal displacement of the pile (H = 500 mm).</p>
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<p>Horizontal displacement contour diagram (H = 500 mm). (<b>a</b>) SPW; (<b>b</b>) DRPW (4D); (<b>c</b>) ARPW (4D).</p>
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<p>Horizontal displacement contour diagram (H = 500 mm). (<b>a</b>) SPW; (<b>b</b>) DRPW (4D); (<b>c</b>) ARPW (4D).</p>
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<p>Ground settlement outside the excavation pit (H = 500 mm).</p>
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<p>Pit bottom uplift (H = 500 mm).</p>
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<p>Earth pressure diagram.</p>
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<p>E<sub>ff</sub> (H = 500 mm).</p>
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<p>E<sub>rr</sub> (H = 500 mm).</p>
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<p>E<sub>fr</sub> (H = 500 mm) (<b>a</b>) model test results and (<b>b</b>) numerical simulation results.</p>
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<p>E<sub>rf</sub> (H = 500 mm) (<b>a</b>) model test results and (<b>b</b>) numerical simulation results.</p>
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<p>Bending moment of SPW.</p>
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<p>Comparison of 2D bending moment with excavation.</p>
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<p>Comparison of 4D bending moment with excavation.</p>
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<p>Comparison of 6D bending moment with excavation.</p>
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<p>Comparison of bending moment (H = 500 mm).</p>
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<p>Foundation pit plan.</p>
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<p>Horizontal displacement of the front pile.</p>
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<p>Layout of ARPW.</p>
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<p>Bending moment of the front pile.</p>
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<p>Schematic diagram of overall stress analysis of soil between piles.</p>
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20 pages, 7217 KiB  
Article
The Field Monitoring and Numerical Simulation of Spatiotemporal Effects During Deep Excavation in Mucky Soft Soil: A Case Study
by Qiang Wu, Jianxiu Wang, Yanxia Long, Xuezeng Liu, Guanhong Long, Shuang Ding, Li Zhou, Huboqiang Li and Muhammad Akmal Hakim bin Hishammuddin
Appl. Sci. 2025, 15(4), 1992; https://doi.org/10.3390/app15041992 - 14 Feb 2025
Abstract
The issue of geotechnical hazards induced by excavation in soft soil areas has become increasingly prominent. However, the retaining structure and surface settlement deformation induced by the creep of soft soil and spatial effect of the excavation sequence are not fully considered where [...] Read more.
The issue of geotechnical hazards induced by excavation in soft soil areas has become increasingly prominent. However, the retaining structure and surface settlement deformation induced by the creep of soft soil and spatial effect of the excavation sequence are not fully considered where only elastic–plastic deformation is used in design. To understand the spatiotemporal effects of excavation-induced deformation in soft soil pits, a case study was performed with the Huaxi Park Station of the Suzhou Metro Line S1, Jiangsu Province, China, as an example. Field monitoring was conducted, and a three-dimensional numerical model was developed, taking into account the creep characteristics of mucky clay and spatiotemporal response of retaining structures induced by excavations. The spatiotemporal effects in retaining structures and ground settlement during excavation processes were analyzed. The results show that as the excavation depth increased, the horizontal displacement of the diaphragm walls increased linearly and tended to exhibit abrupt changes when approaching the bottom of the pit. The maximum horizontal displacement of the wall at the west end well was close to 70 mm, and the maximum displacement of the wall at the standard section reached approximately 80 mm. The ground settlement on both pit sides showed a “trough” distribution pattern, peaking at about 12 m from the pit edge, with a settlement rate of −1.9 mm/m per meter of excavation depth. The excavation process directly led to the lateral deformation of the diaphragm walls, resulting in ground settlement, which prominently reflected the time-dependent deformation characteristics of mucky soft soil during the excavation process. These findings provide critical insights for similar deep excavation projects in mucky soft soil, particularly regarding excavation-induced deformations, by providing guidance on design standards and monitoring strategies for similar geological conditions. Full article
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<p>Soil profile along the standard section of Huaxi Park Station.</p>
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<p>Layout of monitoring points of Huaxi Park Station foundation pit. (CX is the monitoring point number of diaphragm wall horizontal displacement; DB is the monitoring point number of surface subsidence).</p>
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<p>A 3D numerical model of the Huaxi Park Station foundation pit.</p>
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<p>Structure of CVISC model.</p>
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<p>Variation rule of maximum horizontal displacement of enclosure wall: (<b>a</b>) maximum horizontal displacement of west end well wall; (<b>b</b>) maximum horizontal displacement of standard section wall. RW means retaining wall.</p>
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<p>Surface settlement outside the pit: (<b>a</b>) surface settlement outside the west end head pit; (<b>b</b>) surface settlement outside the standard section pit. D is the distance from the pit. Notes−excavation step sequence: 1−arrangement of the first steel support; 2−arrangement of the second steel support; 3−arrangement of the third steel support; 4−arrangement of the fourth steel support; 5−excavation completed.</p>
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<p>The relationship between the surface settlement outside the pit and the maximum horizontal displacement of the retaining wall: (<b>a</b>) the west end well; (<b>b</b>) the standard section.</p>
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<p>Pore water pressure contour with different construction steps: (<b>a</b>) before excavation; (<b>b</b>) excavation of third floors; (<b>c</b>) final excavation.</p>
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<p>Pore water pressure contour with different construction steps: (<b>a</b>) before excavation; (<b>b</b>) excavation of third floors; (<b>c</b>) final excavation.</p>
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<p>Horizontal displacement of diaphragm wall of Huaxi Park Station foundation pit.</p>
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<p>Horizontal displacement of diaphragm wall (CX5): (<b>a</b>) horizontal displacement versus depth curve; (<b>b</b>) variation curve of maximum horizontal displacement with construction sequence. (Construction sequence: 1—arrangement of the first steel support; 2—arrangement of the second steel support; 3—arrangement of the third steel support; 4—arrangement of the fourth steel support; 5—arrangement of the fifth steel support; 6—completion of the footing pouring.)</p>
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<p>Vertical displacement after the completion of excavation: (<b>a</b>) surface settlement outside the pit; (<b>b</b>) vertical displacement.</p>
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<p>Surface settlement outside the pit after the completion of excavation: (<b>a</b>) DB4; (<b>b</b>) DB6; (<b>c</b>) DB1.</p>
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<p>Change in the axial force of the first concrete support.</p>
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<p>Change in the axial force of the second to fifth supports.</p>
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27 pages, 5081 KiB  
Article
Application of Parameter Inversion of HSS Model Based on BP Neural Network Optimized by Genetic Algorithm in Foundation Pit Engineering
by Xiaosheng Pu, Jin Huang, Tao Peng, Wenzhe Wang, Bin Li and Haitang Zhao
Buildings 2025, 15(4), 531; https://doi.org/10.3390/buildings15040531 - 9 Feb 2025
Abstract
The hardening soil model with small-strain stiffness (HSS model) is widely applied in deep foundation pit engineering in coastal soft-soil areas, yet it is characterized by a multitude of parameters that are relatively cumbersome to acquire. In this study, we incorporate a genetic [...] Read more.
The hardening soil model with small-strain stiffness (HSS model) is widely applied in deep foundation pit engineering in coastal soft-soil areas, yet it is characterized by a multitude of parameters that are relatively cumbersome to acquire. In this study, we incorporate a genetic algorithm and a back-propagation neural network (BPNN) model into an inversion analysis for HSS model parameters, with the objective of facilitating a more streamlined and accurate determination of these parameters in practical engineering. Utilizing horizontal displacement monitoring data from retaining structures, combined with local engineering, both a BPNN model and a BPNN optimized by a genetic algorithm (GA-BPNN) model were established to invert the stiffness modulus parameters of the HSS model for typical strata. Subsequently, numerical simulations were conducted based on the inverted parameters to analyze the deformation characteristics of the retaining structures. The performances of the BPNN and GA-BPNN models were evaluated using statistical metrics, including R2, MAE, MSE, WI, VAF, RAE, RRSE, and MAPE. The results demonstrate that the GA-BPNN model achieves significantly lower prediction errors, higher fitting accuracy, and predictive performance compared to the BPNN model. Based on the parameters inverted by the GA-BPNN model, the average compression modulus Es12, the reference tangent stiffness modulus Eoedref, the reference secant stiffness modulus E50ref, and the reference unloading–reloading stiffness modulus  Eurref for gravelly cohesive soil were determined as Eoedref=0.83Es12 and Eurref=8.14E50ref; for fully weathered granite, Eoedref=1.54Es12 and Eurref=5.51E50ref. Numerical simulations conducted with these stiffness modulus parameters show excellent agreement with monitoring data, effectively describing the deformation characteristics of the retaining structures. In situations where relevant mechanical tests are unavailable, the application of the GA-BPNN model for the inversion analysis of HSS model parameters is both rational and effective, offering a reference for similar engineering projects. Full article
(This article belongs to the Special Issue Application of Experiment and Simulation Techniques in Engineering)
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<p>Aerial view of the foundation pit.</p>
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<p>Typical cross-section of the foundation pit.</p>
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<p>Topology of the BP neural network.</p>
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<p>Algorithmic flow of the BP neural network optimized by the genetic algorithm.</p>
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<p>Diagram of mean squared error variation with the number of hidden layer nodes in the training set.</p>
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<p>Implementation time (<math display="inline"><semantics> <mrow> <mi>s</mi> </mrow> </semantics></math>) corresponding to different GA parameter settings: (<b>a</b>) population size; (<b>b</b>) crossover probability; (<b>c</b>) mutation probability.</p>
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<p>Mean R<sup>2</sup> values corresponding to different GA parameter settings: (<b>a</b>) population size; (<b>b</b>) crossover probability; (<b>c</b>) mutation probability.</p>
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<p>Comparison diagram of prediction errors for each stiffness modulus in the validation set: (<b>a</b>) prediction error A; (<b>b</b>) prediction error B; (<b>c</b>) prediction error C; (<b>d</b>) prediction error D.</p>
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<p>Comparison diagram of predicted values and expected values for each stiffness: (<b>a</b>) predicted and expected value A; (<b>b</b>) predicted and expected value B; (<b>c</b>) predicted and expected value C; (<b>d</b>) predicted and expected value D.</p>
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<p>Comparison diagram of predicted values and expected values for each stiffness: (<b>a</b>) predicted and expected value A; (<b>b</b>) predicted and expected value B; (<b>c</b>) predicted and expected value C; (<b>d</b>) predicted and expected value D.</p>
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<p>Diagram of three-dimensional numerical model.</p>
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<p>Deformation diagram of the diaphragm wall at typical excavation stages, including both numerical simulation and engineering monitoring results.</p>
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18 pages, 12870 KiB  
Article
Numerical Simulation on an Ultra-Large Seven-Ring Internal Support System Considering the Effects of Soil–Structure Interaction and Temperature
by Hexiang Hu, Yu Tian, Neimeng Zheng, Xiuli Du, Haishan Guo and Zhonghua Xu
Buildings 2025, 15(3), 463; https://doi.org/10.3390/buildings15030463 - 2 Feb 2025
Abstract
The foundation pit area of Kunming International Comprehensive Transportation Hub is 56,800 m2, and the excavation depth ranges from 18 m to 25 m. Because the surrounding environment is very complex, the foundation pit is supported by an underground continuous wall [...] Read more.
The foundation pit area of Kunming International Comprehensive Transportation Hub is 56,800 m2, and the excavation depth ranges from 18 m to 25 m. Because the surrounding environment is very complex, the foundation pit is supported by an underground continuous wall and three layers of internal support system with seven rings. The force of this internal support system is coupled integrally, and the number of rings is the highest in the world at present. In this work, a finite element model considering the interaction between soil and the retaining structure is established. The Hardening Soil model with small strain stiffness is used to simulate and analyze the whole excavation process of the foundation pit. Considering the ultra-large plane size of the foundation pit, we cannot ignore the temperature effect, so the deformation of the underground continuous wall and the force of the internal support system under seasonal temperature variation are investigated. By comparing numerical simulation results with field measurements, the deformation of the ultra-large seven-ring internal support system, the deformation of the surrounding soil, and the axial force of the supports are analyzed. The results show that the finite element simulation agrees well with the measured data. This work provides a reliable method for analyzing ultra-large deep foundation pits. Full article
(This article belongs to the Special Issue Advances in Soil-Structure Interaction for Building Structures)
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<p>Site plan of the foundation pit and surrounding environment of Kunming International Comprehensive Transportation Hub.</p>
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<p>Vertical profile of the internal support system and the corresponding soil layers.</p>
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<p>Layout plan of the internal support system.</p>
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<p>Finite element model for typical cross-section.</p>
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<p>Horizontal ground deformation when the foundation pit is excavated completely.</p>
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<p>Vertical ground deformation when the foundation pit is excavated completely.</p>
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<p>Comparison between the measured and calculated horizontal deformation of the underground continuous wall. (<b>a</b>) Measured and calculated results. (<b>b</b>) Location of the monitoring point.</p>
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<p>Three-dimensional analysis model considering the interaction between the retaining structure and internal support system.</p>
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<p>Three-dimensional finite element model of the retaining structure.</p>
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<p>Overall deformation of the internal support system.</p>
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<p>Spatial deformation of the retaining structure.</p>
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<p>Influence of temperature on the horizontal deformation of the retaining structure. (<b>a</b>) Ignoring the temperature effect. (<b>b</b>) Considering temperature effect.</p>
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<p>Influence of temperature on the horizontal deformation of the retaining structure. (<b>a</b>) Ignoring the temperature effect. (<b>b</b>) Considering temperature effect.</p>
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12 pages, 7576 KiB  
Article
Microstructure Evolution of Extruded TiAl Alloy During Vacuum Isothermal Superplastic Forging Process
by Jintao Li, Xiaopeng Wang, Minyu Gong, Zhenyu Guo and Fantao Kong
Metals 2025, 15(2), 123; https://doi.org/10.3390/met15020123 - 26 Jan 2025
Abstract
Vacuum isothermal forging is an ideal method for preparing high-performance TiAl alloy forgings, as it is carried out under the conditions of a uniform temperature field and oxygen isolation. The mechanical properties of TiAl alloys strongly depend on their microstructure, so it is [...] Read more.
Vacuum isothermal forging is an ideal method for preparing high-performance TiAl alloy forgings, as it is carried out under the conditions of a uniform temperature field and oxygen isolation. The mechanical properties of TiAl alloys strongly depend on their microstructure, so it is important to study their microstructure evolution during the forging process to improve their properties. In this study, TiAl alloy forgings with different deformations were produced from the extruded billets by vacuum isothermal superplastic forging under lower temperatures and extremely low strain rate conditions. The results indicate that the streamlined structure in the extruded alloy was destroyed during the forging process. As the deformation increased, the dynamic recrystallization was more fully carried out, leading to a substantial decrease in remnant lamellar colonies and a significant increase in the γ phase, and the microstructure was transformed from nearly lamellar (NL) to near gamma (NG) structure. The proportion of high-angle grain boundaries (HAGB) increased with increasing deformation, while the grain size reduced from 20 μm to 4.6 μm. In addition, the streamlined features and textures exhibited a weakening trend with increasing deformation, leading to a decrease in the ultimate strength from 891 MPa to 722 MPa. To maintain the streamlined characteristics and retain strengthening effects, the forging deformation should not exceed 56.7%. Full article
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<p>(<b>a</b>) Vacuum isothermal forging machine; (<b>b</b>) extruded rod; (<b>c</b>) extruded square billets; (<b>d</b>) schematic diagram of the direction of the samples; TiAl alloy forgings with reduction of (<b>e</b>) 45%, (<b>f</b>) 62.5%, and (<b>g</b>) 80%, respectively.</p>
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<p>XRD patterns of as-extruded TiAl alloy and as-forged TiAl alloys with different deformations.</p>
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<p>The microstructures of (<b>a</b>,<b>b</b>) as-extruded alloy and as-forged alloys with (<b>c</b>,<b>d</b>) 45% reduction, (<b>e</b>,<b>f</b>) 62.5% reduction, and (<b>g</b>,<b>h</b>) 80% reduction, respectively: (<b>a</b>,<b>c</b>,<b>e</b>,<b>g</b>) OM images; (<b>b</b>,<b>d</b>,<b>f</b>,<b>h</b>) SEM images in BSE mode.</p>
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<p>The EBSD analysis of (<b>a1</b>–<b>a4</b>) as-extruded alloy and as-forged alloys with (<b>b1</b>–<b>b4</b>) 45% reduction, (<b>c1</b>–<b>c4</b>) 62.5% reduction, and (<b>d1</b>–<b>d4</b>) 80% reduction, respectively: (<b>a1</b>,<b>b1</b>,<b>c1</b>,<b>d1</b>) IPF maps; (<b>a2</b>,<b>b2</b>,<b>c2</b>,<b>d2</b>) phase maps; (<b>a3</b>,<b>b3</b>,<b>c3</b>,<b>d3</b>) misorientation angle maps; (<b>a4</b>,<b>b4</b>,<b>c4</b>,<b>d4</b>) grain size maps.</p>
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<p>(<b>a</b>) Pole figures and (<b>b</b>) inverse pole figures of as-extruded alloy and as-forged alloys with different reductions.</p>
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<p>The fitted curve of the room-temperature strength variation tendency of extruded and forged samples.</p>
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12 pages, 4037 KiB  
Article
A Deformation Prediction Model for Concrete Dams Based on RSA-VMD-AttLSTM
by Pei Liu, Hao Gu, Chongshi Gu and Yanbo Wang
Buildings 2025, 15(3), 357; https://doi.org/10.3390/buildings15030357 - 24 Jan 2025
Viewed by 228
Abstract
This paper presents a deformation prediction model for concrete dams that integrates a reptile search algorithm (RSA), a Variational Mode Decomposition (VMD) algorithm, and a long short-term memory network model with attention mechanism (AttLSTM). This model utilizes the RSA to optimize the parameters [...] Read more.
This paper presents a deformation prediction model for concrete dams that integrates a reptile search algorithm (RSA), a Variational Mode Decomposition (VMD) algorithm, and a long short-term memory network model with attention mechanism (AttLSTM). This model utilizes the RSA to optimize the parameters K and α of the VMD algorithm. It combines the variance of the modified mode with the sample entropy of these data as the objective function, effectively converting monitoring data into a stable signal while retaining essential characteristic variation. Data are reformatted into a three-dimensional structure and partitioned into training and testing sets. The AttLSTM network was applied to forecast deformation, and results were validated using practical engineering cases. The performance of the proposed model was compared against that of four other models: LSTM, VMD-LSTM, attention LSTM, and VMD-AttLSTM models. Analysis of the five evaluation criteria revealed that the RSA can better optimize the parameters of the VMD algorithm. Consequently, the proposed model demonstrates superior noise reduction capabilities and improved prediction accuracy. Full article
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<p>Schematic diagram of encircling prey.</p>
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<p>Schematic diagram of hunting prey.</p>
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<p>Schematic diagram of AttLSTM structure.</p>
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<p>Flow chart of RSA-VMD-AttLSTM model.</p>
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<p>Distribution map of concrete dam measurement points.</p>
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<p>Measured displacement values of PL5-3, PL13-3, and PL19-4.</p>
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<p>PL13-3 measurement point RSA-optimized VMD decomposition.</p>
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<p>Comparison of prediction results of each model at each measurement point.</p>
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18 pages, 4006 KiB  
Article
Biochar Amendment as a Mitigation Against Freezing–Thawing Effects on Soil Hydraulic Properties
by Zhongkui Chen, Chitipat Intraravimonmata, Viroon Kamchoom, Rui Chen and Natdanai Sinsamutpadung
Agronomy 2025, 15(1), 137; https://doi.org/10.3390/agronomy15010137 - 8 Jan 2025
Viewed by 596
Abstract
Seasonal freeze–thaw cycles compromise soil structure, thereby increasing hydraulic conductivity but diminishing water retention capacity—both of which are essential for sustaining crop health and nutrient retention in agricultural soils. Prior research has suggested that biochar may alleviate these detrimental effects; however; further investigation [...] Read more.
Seasonal freeze–thaw cycles compromise soil structure, thereby increasing hydraulic conductivity but diminishing water retention capacity—both of which are essential for sustaining crop health and nutrient retention in agricultural soils. Prior research has suggested that biochar may alleviate these detrimental effects; however; further investigation into its influence on soil hydraulic properties through freeze–thaw cycles is essential. This study explores the impact of freeze–thaw cycles on the soil water retention and hydraulic conductivity and evaluates the potential of peanut shell biochar to mitigate these effects. Peanut shell biochar was used, and its effects on soil water retention and unsaturated hydraulic conductivity were evaluated through evaporation tests. The findings indicate that freeze–thaw cycles predominantly affect clay’s ability to retain water and control hydraulic conductivity by generating macropores and fissures; with a notable increase in conductivity at high matric potentials. The impact lessens as matric potential decreases below −30 kPa, resulting in smaller differences in conductivity. Introducing biochar helps mitigate these effects by converting large pores into smaller micro- or meso-pores, effectively increasing water retention, especially at higher content of biochar. While biochar’s impact is more pronounced at higher matric potentials, it also significantly reduces conductivity at lower potentials. The total porosity of the soil increased under low biochar application rates (0% and 1%) but declined at higher application rates (2% and 3%) as the number of freeze–thaw cycles increased. Furthermore, the characteristics of soil deformation during freeze–thaw cycles shifted from frost heaving to thaw settlement with increasing biochar application rates. Notably, an optimal biochar application rate was observed to mitigate soil deformation induced by freeze–thaw processes. These findings contribute to the scientific understanding necessary for the development and management of sustainable agricultural soil systems. Full article
(This article belongs to the Section Water Use and Irrigation)
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<p>Schematic representation of compacted clay amended with biochar, depicting different biochar contents (B0, B2, B4, B8 denote 0%, 2%, 4%, and 8% biochar content, respectively), unit: mm.</p>
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<p>Variation in soil saturated hydraulic conductivity in response to freezing–thawing cycles and soil densities (1.105 g cm<sup>−3</sup>, 1.170 g cm<sup>−3</sup>, 1.235 g cm<sup>−3</sup>) at different biochar contents: (<b>a</b>) 0%, (<b>b</b>) 2%, (<b>c</b>) 4%, and (<b>d</b>) 8%.</p>
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<p>Variation in soil saturated hydraulic conductivity in response to freezing–thawing cycles and soil densities (1.105 g cm<sup>−3</sup>, 1.170 g cm<sup>−3</sup>, 1.235 g cm<sup>−3</sup>) at different biochar contents: (<b>a</b>) 0%, (<b>b</b>) 2%, (<b>c</b>) 4%, and (<b>d</b>) 8%.</p>
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<p>Variation in soil saturated hydraulic conductivity in response to freezing–thawing cycles and soil densities (1.105 g cm<sup>−3</sup>, 1.170 g cm<sup>−3</sup>, 1.235 g cm<sup>−3</sup>) at different biochar contents: (<b>a</b>) 0%, (<b>b</b>) 2%, (<b>c</b>) 4%, and (<b>d</b>) 8%.</p>
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<p>Effect of biochar addition on soil microstructure changes caused by freezing–thawing cycles.</p>
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<p>SEM image (2000×) of BAC specimens after freezing–thawing cycles: (<b>a</b>) B0N0; (<b>b</b>) B8N0; (<b>c</b>) B0N12; (<b>d</b>) B8N12.</p>
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<p>Effects of freezing–thawing on the SWRC of BAC with and without biochar treatment.</p>
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<p>The influence of biochar treatment on the water retention properties of compacted BAC at varying compaction water contents and a soil density of 1.235 g cm<sup>−3</sup>.</p>
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<p>The effects of freezing–thawing on the unsaturated hydraulic conductivity of BAC with and without biochar treatment.</p>
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24 pages, 9657 KiB  
Article
Study on the Stability and Control of Gob-Side Entry Retaining in Paste Backfill Working Face
by Changtao Xu, Xiangyu Wang, Dingchao Chen, Guanghui Wang, Zhenpeng Niu and Huixing Lu
Appl. Sci. 2025, 15(2), 528; https://doi.org/10.3390/app15020528 - 8 Jan 2025
Viewed by 393
Abstract
Due to the poor stability of the roof and floor of the roadway in the 3-1 coal seam of Chahasu Coal Mine, traditional gob-side entry retaining (GER) methods fail to meet the production safety requirements. To address this, a GER technology using paste [...] Read more.
Due to the poor stability of the roof and floor of the roadway in the 3-1 coal seam of Chahasu Coal Mine, traditional gob-side entry retaining (GER) methods fail to meet the production safety requirements. To address this, a GER technology using paste backfill was proposed. This study reveals the stability mechanism of the surrounding rock in GER with paste backfill through theoretical analysis, numerical simulation, and industrial experiments. First, theoretical analysis was conducted to determine the overburden movement characteristics under varying backfill ratios. Uniaxial compressive tests on the paste material demonstrated that its bearing capacity reaches a relatively stable state after 14–28 days of curing. Second, numerical simulations were performed to study the deformation patterns of the surrounding rock and mine pressure characteristics under backfill ratios of 65%, 75%, 85%, and 95%. The Strain-Softening model was used to calibrate the backfill material parameters. The results showed that as the backfill ratio increased, the support provided by the backfill material improved, leading to enhanced bearing capacity of the overlying strata, reduced mine pressure intensity, significantly decreased deformation of the roadway, and substantially improved stability of the surrounding rock. Third, under a backfill ratio of 95%, the evolution of the abutment stress during face advancement was investigated. It was found that as the working face advanced, the backfill material and the overlying strata gradually formed a stable composite structure, with the abutment stress in the mining area stabilizing over time. Finally, to address the issue of insufficient initial strength and limited support capacity of the paste backfill material, a comprehensive control system for surrounding rock stability was proposed. This system integrates a basic bolt-mesh-cable support structure with localized reinforcement using portal hydraulic supports. Field industrial practices demonstrated that after applying this comprehensive control technology, the convergence of roof and floor was approximately 190 mm and the convergence of two ribs was about 140 mm, effectively ensuring the stability of surrounding rock in GER with paste backfill working face. Full article
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<p>Differences in environmental damage between the caving method and the filling method: (<b>a</b>) caving method; (<b>b</b>) filling method.</p>
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<p>Stratigraphic column.</p>
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<p>Layout of working face.</p>
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<p>Characteristics of overburden rock movement in slopes with different backfill ratios: (<b>a</b>) low backfill ratio; (<b>b</b>) Medium backfill ratio; (<b>c</b>) high backfill ratio.</p>
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<p>Characteristics of overburden rock movement in slopes with different backfill ratios: (<b>a</b>) low backfill ratio; (<b>b</b>) Medium backfill ratio; (<b>c</b>) high backfill ratio.</p>
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<p>Age strength of filling materials at different ratios: (<b>a</b>) mass concentration; (<b>b</b>) fly ash proportion; (<b>c</b>) cementitious material proportion.</p>
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<p>Numerical model.</p>
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<p>Strain softening model calibration results.</p>
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<p>Deformation of roadway surrounding rock with different backfill ratios: (<b>a</b>) roof; (<b>b</b>) floor; (<b>c</b>) solid coal rib; (<b>d</b>) backfill rib.</p>
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<p>Vertical stress curve of immediate roof with different backfill ratios.</p>
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<p>Direct displacement curve of different backfill ratios.</p>
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<p>Evolution law of abutment stress in different advancing distances of the mining site: (<b>a</b>) advance 30 m; (<b>b</b>) advance 45 m; (<b>c</b>) advance 60 m; (<b>d</b>) advance 75 m; (<b>e</b>) advance 90 m; (<b>f</b>) advance 105 m; (<b>g</b>) advance 120 m; (<b>h</b>) advance 135 m; (<b>i</b>) advance 150 m; (<b>j</b>) advance 165 m.</p>
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<p>Evolution law of abutment stress in different advancing distances of the mining site: (<b>a</b>) advance 30 m; (<b>b</b>) advance 45 m; (<b>c</b>) advance 60 m; (<b>d</b>) advance 75 m; (<b>e</b>) advance 90 m; (<b>f</b>) advance 105 m; (<b>g</b>) advance 120 m; (<b>h</b>) advance 135 m; (<b>i</b>) advance 150 m; (<b>j</b>) advance 165 m.</p>
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<p>Distribution law of vertical stress in the filling area with different pushing distances.</p>
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<p>Construction process.</p>
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<p>Control concept of GER.</p>
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<p>Basic support of GER.</p>
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<p>Schematic diagram of portal hydraulic support.</p>
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<p>Strengthen support for GER.</p>
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<p>Deformation monitoring of roadway.</p>
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24 pages, 5273 KiB  
Article
Design Optimization of an Innovative Instrumental Single-Sided Formwork Supporting System for Retaining Walls Using Physics-Constrained Generative Adversarial Network
by Wei Liu, Lin He, Jikai Liu, Xiangyang Xie, Ning Hao, Cheng Shen and Junyong Zhou
Buildings 2025, 15(1), 132; https://doi.org/10.3390/buildings15010132 - 4 Jan 2025
Viewed by 634
Abstract
Single-sided formwork supporting systems (SFSSs) play a crucial role in the urban construction of retaining walls using cast-in-place concrete. By supporting the formwork from one side, an SFSS can minimize its spatial footprint, enabling its closer placement to boundary lines without compromising structural [...] Read more.
Single-sided formwork supporting systems (SFSSs) play a crucial role in the urban construction of retaining walls using cast-in-place concrete. By supporting the formwork from one side, an SFSS can minimize its spatial footprint, enabling its closer placement to boundary lines without compromising structural integrity. However, existing SFSS designs struggle to achieve a balance between mechanical performance and lightweight construction. To address these limitations, an innovative instrumented SFSS was proposed. It is composed of a panel structure made of a panel, vertical braces, and cross braces and a supporting structure comprising an L-shaped frame, steel tubes, and anchor bolts. These components are conducive to modular manufacturing, lightweight installation, and convenient connections. To facilitate the optimal design of this instrumented SFSS, a physics-constrained generative adversarial network (PC-GAN) approach was proposed. This approach incorporates three objective functions: minimizing material usage, adhering to deformation criteria, and ensuring structural safety. An example application is presented to demonstrate the superiority of the instrumented SFSS and validate the proposed PC-GAN approach. The instrumented SFSS enables individual components to be easily and rapidly prefabricated, assembled, and disassembled, requiring only two workers for installation or removal without the need for additional hoisting equipment. The optimized instrumented SFSS, designed using the PC-GAN approach, achieves comparable deformation performance (from 2.49 mm to 2.48 mm in maxima) and slightly improved component stress levels (from 97 MPa to 115 MPa in maxima) while reducing the total weight by 20.85%, through optimizing panel thickness, the dimensions and spacings of vertical and lateral braces, and the spacings of steel tubes. This optimized design of the instrumented SFSS using PC-GAN shows better performance than the current scheme, combining significant weight reduction with enhanced mechanical efficiency. Full article
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<p>Arrangement and construction diagram of the tie rod SFSS.</p>
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<p>Typical structural forms of triangular truss SFSS.</p>
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<p>Typical design scheme of steel pipe SFSS.</p>
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<p>Structural layout and constituent parts of the instrumental SFSS.</p>
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<p>Mechanical schematic diagram of the overall structure of the instrumental SFSS.</p>
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<p>Mechanical schematic diagram of the panel structure.</p>
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<p>Mechanical schematic diagram of the triangular supporting structure.</p>
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<p>Flowchart of the PC-GAN approach for design optimization of the SFSS.</p>
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<p>Photos of SFSS assembly construction and completion of concrete wall construction.</p>
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<p>Deformation of the instrumental SFSS of the initial design.</p>
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<p>Stress distribution of the instrumental SFSS of the initial design. (<b>a</b>) The laminated timber panel structure; (<b>b</b>) the steel supporting structure.</p>
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<p>Iterations of the PC-GAN approach and distributions of generated parameter values.</p>
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<p>Deformation of the instrumental SFSS after optimized design.</p>
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<p>Stress distribution of the instrumental SFSS after optimized design. (<b>a</b>) The laminated timber panel structure; (<b>b</b>) the steel supporting structure.</p>
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16 pages, 5520 KiB  
Article
Stability Control of Multilayer Roof Strata in the Large Mining Height Gob-Side Entry: A Case Study
by Yong Chen, Yingpeng Wang, Zhengyuan Qin, Feng Yang and Vivek Agarwal
Appl. Sci. 2025, 15(1), 86; https://doi.org/10.3390/app15010086 - 26 Dec 2024
Viewed by 425
Abstract
Roof separation, destabilization and collapse of multilayer roof structures are difficult to control in large mining height gob-side entries due to severe mining pressure. In the 22301 working face in Tunlan Mine, a mining height of 4.75 m posed great challenges to gob-side [...] Read more.
Roof separation, destabilization and collapse of multilayer roof structures are difficult to control in large mining height gob-side entries due to severe mining pressure. In the 22301 working face in Tunlan Mine, a mining height of 4.75 m posed great challenges to gob-side entry retaining techniques. Through mechanical analysis, the strata movement of a multilayer roof structure was investigated, and numerical analysis was conducted to identify key aspects of the supporting scheme, e.g., ensuring the stability of immediate roof above the filling area, transferring the resistance from the cemented backfill to the roof structure and maintaining self-supporting capacity. A new support strategy was proposed and applied in industrial settings, with entry stability evaluated by monitoring the deformation characteristics, roof separation values and overall support performance. The results showed that the gob-side entry retaining technique was successful in Tunlan Mine, providing valuable insights for similar techniques in large mining height gob-side entries. Full article
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<p>Layout of mining and excavation operations in the 22301 working face.</p>
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<p>Support diagram of 22301 head entry.</p>
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<p>Fracture distribution for monitoring station #5.</p>
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<p>Crack characteristics in the roof rock layers measured by five monitoring stations.</p>
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<p>Fracture distribution characteristics in the roof rock layer along the strike of 22301 head entry.</p>
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<p>Movement of compound roof structure in the large mining height gob-side entry.</p>
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<p>Numerical simulation model.</p>
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<p>Vertical stress distribution in the backfill area.</p>
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<p>The distribution of plastic zone in the 22301 large mining height gob-side entry.</p>
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<p>The distribution of plastic zone in the 22301 large mining height gob-side entry.</p>
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<p>Reinforcement support diagram within the 22301 head entry.</p>
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<p>Reinforcement support diagram of roof above the 22301 head entry.</p>
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<p>Roof delamination for different monitoring stations in the 22301 gob-side entry.</p>
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<p>On-site supporting results of the 22301 gob-side entry.</p>
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23 pages, 8899 KiB  
Article
Loading Frequency Classification in Shape Memory Alloys: A Machine Learning Approach
by Dmytro Tymoshchuk, Oleh Yasniy, Pavlo Maruschak, Volodymyr Iasnii and Iryna Didych
Computers 2024, 13(12), 339; https://doi.org/10.3390/computers13120339 - 14 Dec 2024
Cited by 1 | Viewed by 652
Abstract
This paper investigates the use of machine learning methods to predict the loading frequency of shape memory alloys (SMAs) based on experimental data. SMAs, in particular nickel-titanium (NiTi) alloys, have unique properties that restore the original shape after significant deformation. The frequency of [...] Read more.
This paper investigates the use of machine learning methods to predict the loading frequency of shape memory alloys (SMAs) based on experimental data. SMAs, in particular nickel-titanium (NiTi) alloys, have unique properties that restore the original shape after significant deformation. The frequency of loading significantly affects the functional characteristics of SMAs. Experimental data were obtained from cyclic tensile tests of a 1.5 mm diameter Ni55.8Ti44.2 wire at different loading frequencies (0.1, 0.5, 1.0, and 5.0 Hz). Various machine learning methods were used to predict the loading frequency f (Hz) based on input parameters such as stress σ (MPa), number of cycles N, strain ε (%), and loading–unloading stage: boosted trees, random forest, support vector machines, k-nearest neighbors, and artificial neural networks of the MLP type. Experimental data of 100–140 load–unload cycles for four load frequencies were used for training. The dataset contained 13,365 elements. The results showed that the MLP neural network model demonstrated the highest accuracy in load frequency classification. The boosted trees and random forest models also performed well, although slightly below MLP. The SVM method also performed quite well. The KNN method showed the worst results among all models. Additional testing of the MLP model on cycles that were not included in the training data (200th, 300th, and 1035th cycles) showed that the model retains high efficiency in predicting load frequency, although the accuracy gradually decreases on later cycles due to the accumulation of structural changes in the material. Full article
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<p>The machine for the experiment: (<b>a</b>) general view of the SMT-100 machine; (<b>b</b>) Bi-02-313 sensor; (<b>c</b>) test sample fixed in the grippers.</p>
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<p>The window of the Test Builder software during the experiment.</p>
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<p>Hysteresis loops of 100–120th SMA loading and unloading cycles for a frequency of 0.1 Hz.</p>
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<p>Schematic representation of the Boosted Tree model.</p>
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<p>Schematic representation of the Random Forest model.</p>
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<p>MLP architecture with one hidden layer.</p>
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<p>Model of a neuron.</p>
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<p>Average multinomial deviance change graph depending on the number of trees in the model.</p>
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<p>Confusion matrix of the Boosted Trees model of the test data set.</p>
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<p>Misclassification rate change graph for training and test samples in the process of model training.</p>
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<p>Confusion matrix of the Random Forest model of the test data set.</p>
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<p>Confusion matrix of the SVM model of the test data set.</p>
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<p>Confusion matrix of the KNN model of the test data set.</p>
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<p>Confusion matrix of the 4-51-4 neural network of the test data set.</p>
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<p>Confusion matrix of the 4-51-4 neural network for the 200th cycle.</p>
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<p>Charts of cumulative gain in frequency classification for the 200th cycle.</p>
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<p>Performance indicators of the MLP 4-51-4 neural network for the 200th cycle.</p>
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<p>Confusion matrix of the 4-51-4 neural network for the 300th cycle.</p>
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<p>Charts of cumulative gain in frequency classification for the 300th cycle.</p>
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<p>Performance indicators of the MLP 4-51-4 neural network for the 300th cycle.</p>
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<p>Confusion matrix of the 4-51-4 neural network for the 1035th cycle.</p>
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<p>Performance indicators of the MLP 4-51-4 neural network for the 1035th cycle.</p>
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<p>Charts of cumulative gain in frequency classification for the 1035th cycle.</p>
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<p>Confidence level histograms for the test dataset (<b>a</b>), 200th cycle (<b>b</b>), 300th cycle (<b>c</b>), 1035th cycle (<b>d</b>).</p>
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33 pages, 60830 KiB  
Article
Assessment of the Accuracy of Terrestrial Laser Scanners in Detecting Local Surface Anomaly
by Ali Algadhi, Panos Psimoulis, Athina Grizi and Luis Neves
Remote Sens. 2024, 16(24), 4647; https://doi.org/10.3390/rs16244647 - 11 Dec 2024
Viewed by 668
Abstract
The surface anomaly is a common defect for structures that resist lateral stresses, such as retaining walls. The accurate detection of an anomaly using contactless techniques, such as the Terrestrial Laser Scanner (TLS), is significant for the reliable structural assessment. The influence of [...] Read more.
The surface anomaly is a common defect for structures that resist lateral stresses, such as retaining walls. The accurate detection of an anomaly using contactless techniques, such as the Terrestrial Laser Scanner (TLS), is significant for the reliable structural assessment. The influence of the scanning geometry on the accuracy of the TLS point-clouds was investigated in previous studies; however, a deeper analysis is needed to investigate their impact in the context of structural health monitoring. This paper aims to empirically assess the performance of the TLS in detecting surface anomalies, with respect to the scanning distance and angle of incidence in two cases: (i) when both the reference and deformed clouds are taken from the same scanning position, and (ii) the scans are from different positions. Furthermore, the paper examines the accuracy of estimating the depth of the anomaly using three cloud comparison techniques (i.e., C2C, C2M, and M3C2 methods). The results show that the TLS is capable of detecting the surface anomaly for distances between 2 and 30 m and angles of incidence between 90° and 30°, with a tolerance of within a few millimeters. This is achieved even for the case where scans from different locations (i.e., angles and distances) are applied. Full article
(This article belongs to the Section Environmental Remote Sensing)
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<p>Design of the experimental device (i.e., papier-mâché sheet): (<b>a</b>) front view showing the papier-mâché sheet and the anomaly, (<b>b</b>) side view showing the introduced tilt, (<b>c</b>) rear view for the scenario with no tilt; showing the bolt that was used for attaching the anomaly.</p>
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<p>Scan setup for the papier-mâché experiment: (<b>a</b>) overview of the experiment setup, and (<b>b</b>) plan view of the experiment site showing (i) the thirteen scanning positions, (ii) the papier-mâché sheet, (iii) the three sphere targets, and (iv) the final coordinate system (<span class="html-italic">x</span>- and <span class="html-italic">y</span>-axes) that were aligned to the transverse and lateral axes of the papier-mâché sheet.</p>
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<p>Flowchart of the measurements, processing, and analysis methods.</p>
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<p>Front and side views showing a sample of the point-clouds at the scanning position of 10 m for the papier-mâché sheet at the three deformation scenarios; (i) the initial undeformed state, (ii) the state where no tilt was introduced but only an anomaly at the center of the sheet, and (iii) the state where both the anomaly and global tilt were introduced to the scanned surface.</p>
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<p>The M3C2 distance for the scanning position of 10 m, compared to the initial undeformed state.</p>
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<p>The change in intensity for the scanning position of 10 m, compared to the initial undeformed state.</p>
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<p>The change in the direction of the normal vector along the <span class="html-italic">x</span>-, <span class="html-italic">y</span>-, and <span class="html-italic">z</span>-axes for the scanning position of 10 m, compared to the initial undeformed state.</p>
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<p>The accuracy of estimating the maximum depth of the anomaly using three cloud-comparison techniques: (<b>a</b>) C2C distance, (<b>b</b>) C2M distance, and (<b>c</b>) M3C2 distance.</p>
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<p>Overview of the monitored case study, showing the area of interest.</p>
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<p>The change in the intensity values for the scans that were taken in November 2020, compared to the reference clouds (i.e., orthogonal and oblique).</p>
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<p>The change in the intensity values for each orthogonal scan that was acquired in the morning of each scanning day, compared to the reference cloud that was taken on 4 November 2020.</p>
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<p>The change in direction of the normal vector along the <span class="html-italic">x</span>-axis for each orthogonal scan that was acquired in the morning of each scanning day, compared to the reference cloud that was taken on the 4 November 2020.</p>
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<p>The change in direction of the normal vector along the <span class="html-italic">y</span>-axis for each orthogonal scan that was acquired on the morning of each scanning day, compared to the reference cloud that was taken on 4 November 2020.</p>
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<p>The change in direction of the normal vector along the <span class="html-italic">z</span>-axis for each orthogonal scan that was acquired on the morning of each scanning day, compared to the reference cloud that was taken on 4 November 2020.</p>
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<p>M3C2 distance for the papier-mâché sheet, compared to the initial scan (at the same scanning position) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>M3C2 distance for the papier-mâché sheet, compared to the initial scan (at 10 m) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>Change in intensity of the papier-mâché sheet, compared to the initial scan (at the same scanning position) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>Change in intensity of the papier-mâché sheet, compared to the initial scan (at 10 m) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>The intensity of the reflected signal on each orthogonal scan that was acquired on the morning of each scanning day.</p>
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<p>Change in the normal vector along the <span class="html-italic">x</span>-axis, compared to the initial scan (at the same scanning position) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>Change in the normal vector along the <span class="html-italic">x</span>-axis, compared to the initial scan (at 10 m) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>Change in the normal vector along the <span class="html-italic">y</span>-axis, compared to the initial scan (at the same scanning position) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>Change in the normal vector along the <span class="html-italic">y</span>-axis, compared to the initial scan (at 10 m) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>Change in the normal vector along the <span class="html-italic">z</span>-axis, compared to the initial scan (at the same scanning position) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>Change in the normal vector along the <span class="html-italic">z</span>-axis, compared to the initial scan (at 10 m) with no anomaly: (<b>a</b>) with no tilt, and (<b>b</b>) with tilt.</p>
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<p>The change in the direction of the normal vector along the <span class="html-italic">x</span>-axis for the scans that were taken in November 2020, compared to the reference clouds (i.e., orthogonal and oblique).</p>
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<p>The change in the direction of the normal vector along the <span class="html-italic">y</span>-axis for the scans that were taken in November 2020, compared to the reference clouds (i.e., orthogonal and oblique).</p>
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<p>The change in the direction of the normal vector along the <span class="html-italic">z</span>-axis for the scans that were taken in November 2020, compared to the reference clouds (i.e., orthogonal and oblique).</p>
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15 pages, 10459 KiB  
Article
Identification of Structural Constituents in Advanced Multiphase High-Strength Steels Using Electron Back-Scattered Diffraction
by Aleksandra Kozłowska, Krzysztof Radwański and Adam Grajcar
Symmetry 2024, 16(12), 1630; https://doi.org/10.3390/sym16121630 - 9 Dec 2024
Viewed by 668
Abstract
This study addresses the characterization of the particular microstructural constituents of multiphase transformation-induced plasticity (TRIP)-aided steels belonging to the first and third generations of Advanced High Strength Steels (AHSS) to explore the possibilities of the EBSD method. Complex microstructures composed of ferrite, bainite, [...] Read more.
This study addresses the characterization of the particular microstructural constituents of multiphase transformation-induced plasticity (TRIP)-aided steels belonging to the first and third generations of Advanced High Strength Steels (AHSS) to explore the possibilities of the EBSD method. Complex microstructures composed of ferrite, bainite, retained austenite and martensite were qualitatively and quantitatively assessed. Microstructural constituents with the same crystal structure were distinguished using characteristic EBSD parameters like confidence index (CI), image quality (IQ), kernel average misorientation (KAM) and specific crystallographic orientation relationships. A detailed linear analysis of the IQ parameter and misorientation angles was also performed. These tools are very helpful in linking different symmetric or asymmetric features of metallic alloys with a type of their structure and morphology details. Two types of samples were investigated: thermomechanically processed and subjected to 10% tensile strain to study the microstructural changes caused by plastic deformation. Full article
(This article belongs to the Special Issue Feature Papers in Section "Engineering and Materials" 2024)
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<p>Processing schedules of investigated low-Mn and medium-Mn steels.</p>
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<p>SEM images of low-Mn steel: after thermomechanical processing (<b>a</b>), deformed in a static tensile test up to 10% (<b>b</b>).</p>
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<p>SEM image of medium-Mn steel.</p>
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<p>Kikuchi diffraction bands in a low-Mn steel: ferrite (<b>a</b>), austenite (<b>b</b>), bainite (<b>c</b>) and martensite (<b>d</b>).</p>
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<p>EBSD maps of the thermomechanically processed low-Mn steel: IQ map (<b>a</b>); phase distribution map, where BBC phases are marked in red and FCC phase is marked in green (<b>b</b>); IQ map in reference to the distribution presented in Figure (<b>d</b>) (<b>c</b>); a histogram showing the distribution of IQ parameter (<b>d</b>). F—ferrite, B+RA—bainitic-austenitic areas, M+RA—martensitic-austenitic areas.</p>
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<p>EBSD maps of the thermomechanically processed low-Mn steel: a map displaying the K-S (blue) and N-W (red) orientation relationships between the bainite or martensite and RA (<b>a</b>); phase distribution map with marked misorientation angles corresponding to K-S (blue) and N-W (red) (<b>b</b>); a map showing an average equivalent diameter of RA grains (<b>c</b>) and a corresponding histogram of average equivalent RA diameter distribution (<b>d</b>) a KAM map (<b>e</b>) and a histogram showing the distribution of KAM parameters (<b>f</b>). F—ferrite, B+RA—bainitic-austenitic areas, M+RA—martensitic-austenitic areas, RG—partially recrystallized grains.</p>
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<p>EBSD maps of the low-Mn steel deformed in the tensile test up to 10%: IQ map (<b>a</b>); phase distribution map, where BBC phases are marked in red and FCC phase is marked in green (<b>b</b>); IQ map in reference to the distribution presented in Figure (<b>d</b>) (<b>c</b>); a histogram showing the distribution of IQ parameters (<b>d</b>).</p>
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<p>EBSD maps of the low-Mn steel deformed in the tensile test up to 10%: a map displaying the K-S (blue) and N-W (red) relationships between bainite or martensite and RA (<b>a</b>); a phase distribution map with marked misorientation angles corresponding to K-S (blue) and N-W (red) (<b>b</b>); a map showing an average equivalent diameter of RA grains (<b>c</b>) and a corresponding histogram of average equivalent RA diameter distribution (<b>d</b>), a KAM map (<b>e</b>) and a histogram showing the distribution of KAM parameter (<b>f</b>).</p>
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<p>The IQ map of medium-Mn steel combined with the phase distribution map (RA marked in green) (<b>a</b>) and a linear analysis of IQ parameter (<b>b</b>) and a linear analysis of misorientation angles (<b>c</b>) along the line in Figure (<b>a</b>). TM—tempered martensite, RA—retained austenite, B—bainite formed during the partitioning step.</p>
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14 pages, 9261 KiB  
Article
Stretchable and Shape-Transformable Organohydrogel with Gallium Mesh Frame
by Mincheol Lee, Youngjin Choi, Young Min Bae, Seonghyeon Nam and Kiyoung Shin
Gels 2024, 10(12), 769; https://doi.org/10.3390/gels10120769 - 26 Nov 2024
Viewed by 699
Abstract
Shape-memory materials are widely utilized in biomedical devices and tissue engineering, particularly for their ability to undergo predefined shape changes in response to external stimuli. In this study, a shape-transformable organohydrogel was developed by incorporating a gallium mesh into a polyacrylamide/alginate/glycerol matrix. The [...] Read more.
Shape-memory materials are widely utilized in biomedical devices and tissue engineering, particularly for their ability to undergo predefined shape changes in response to external stimuli. In this study, a shape-transformable organohydrogel was developed by incorporating a gallium mesh into a polyacrylamide/alginate/glycerol matrix. The gallium mesh, which transitions between solid and liquid states at moderate temperatures (~29.8 °C), enhanced the hydrogel’s mechanical properties and enabled shape-memory functionality. The composite organohydrogel exhibited a high elastic modulus of ~900 kPa in the solid gallium state and ~30 kPa in the liquid gallium state, enabling reversible deformation and structural stability. Glycerol improved the hydrogel’s moisture retention, maintaining stretchability and repeated heating and cooling cycles. After multiple cycles of the shape-changing process, the organohydrogel retained its mechanical integrity, achieving shape-fixation and recovery ratios of ~96% and 95%, respectively. This combination of shape-memory functionality, stretchability, and mechanical stability makes this organohydrogel highly suitable for applications in flexible electronics, soft robotics, and biomedical devices, where adaptability and shape retention are essential. Full article
(This article belongs to the Section Gel Processing and Engineering)
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Graphical abstract

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<p>Overall schematic of the shape-transformable organohydrogel. (<b>a</b>) The structure of the shape-transformable organohydrogel. (<b>b</b>) The shape transformation cycle of the organohydrogel illustrating the transition between the original and deformed states.</p>
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<p>Effect of glycerol concentration on the anti-drying properties of organohydrogels. (<b>a</b>) Visual comparison of organohydrogel samples with varying glycerol concentrations (0–50 wt% of aqueous solution) before and after a drying process. The top row shows the original organohydrogel samples, while the bottom row shows the samples after drying. (<b>b</b>) Normalized weight loss of organohydrogels over time in a 60 °C convection oven.</p>
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<p>Mechanical properties of organohydrogels with varying glycerol concentrations after a drying process. (<b>a</b>) Stress–strain curves of organohydrogels with varying glycerol concentration before drying. Stress–strain curves of the organohydrogel (<b>b</b>) without glycerol and (<b>c</b>) with glycerol after the drying period. (<b>d</b>) Stress relaxation tests under 100% elongation of the organohydrogels.</p>
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<p>Fabrication process of the shape-transformable organohydrogel.</p>
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<p>Mechanical properties of the shape-transformable organohydrogel in different states. (<b>a</b>) Microscopic images showing the gallium-reinforced organohydrogel: top view (left) and cross section (right). Red dotted box indicates the layer of the gallium mesh frame. (<b>b</b>) Stress–strain curves comparing the modulus of the organohydrogel in its initial state (black), heated state (red), and transformed state after stretching (blue) and the organohydrogel without gallium frame (green). (<b>c</b>) Elastic modulus of the shape-transformable organohydrogel in different states.</p>
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<p>Shape transformation and fixation process of the shape-transformable organohydrogel. (<b>a</b>) Organohydrogel without (top) and with gallium mesh frame (bottom). (<b>b</b>) Top view of the organohydrogel with gallium mesh frame (<b>c</b>) Overlay image of sequential deformation of the organohydrogel with gallium mesh frame under heating. Red arrow indicates the moving direction. (<b>d</b>) Image showing the organohydrogel in its fixed state after cooling, with the shape retained from the previous deformation.</p>
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<p>Bending angle fixation and recovery of the shape-transformable organohydrogel. (<b>a</b>) Schematic representation of the bending angle measurement for shape fixation and recovery. Maximum bending angle, including the maximum bending angle (<math display="inline"><semantics> <mrow> <msub> <mrow> <mi>θ</mi> </mrow> <mrow> <mi>m</mi> <mi>a</mi> <mi>x</mi> <mtext> </mtext> </mrow> </msub> </mrow> </semantics></math> = 180°) and the recovered angle after reheating (<math display="inline"><semantics> <mrow> <msub> <mrow> <mi>θ</mi> </mrow> <mrow> <mi>i</mi> </mrow> </msub> </mrow> </semantics></math>). (<b>b</b>) Organohydrogel bent to a maximum angle and cooled in the mold to retain the fixed shape. (<b>c</b>) Organohydrogel returned to its original shape after reheating (<math display="inline"><semantics> <mrow> <msub> <mrow> <mi>θ</mi> </mrow> <mrow> <mi>i</mi> </mrow> </msub> </mrow> </semantics></math> = 0°).</p>
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<p>Fixed shapes of the shape-transformable organohydrogel at various bending angles. (<b>a</b>) Organohydrogel sample positioned in an acrylic mold for shape fixation (<b>b</b>–<b>f</b>) Organohydrogel fixed at bending angles of approximately 30°, 60°, 90°, 120° and 150°, respectively, demonstrating the organohydrogel’s ability to retain a range of deformed angles.</p>
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<p>Step-by-step process for the stretching fixation test of the shape-transformable organohydrogel. (<b>a</b>) Initial length (<span class="html-italic">L<sub>i</sub></span>) measurement of the organohydrogel sample before stretching. (<b>b</b>) Positioning of the heated sample in the stretching device. (<b>c</b>) Sample stretched to the deformed length (<span class="html-italic">L<sub>d</sub></span>) under 100% stretching. (<b>d</b>) Fixed length (<span class="html-italic">L<sub>f</sub></span>) measurement after cooling to maintain the deformed shape. (<b>e</b>) Recovered length (<span class="html-italic">L<sub>r</sub></span>) measurement after reheating, illustrating the organohydrogel’s shape recovery capability.</p>
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<p>Multiple-cycle stretching fixation and recovery test results for the shape-transformable organohydrogel. (<b>a</b>) Graph showing the shape fixation and recovery ratios over multiple cycles. (<b>b,c</b>) Microscopic images of the gallium frame within the organohydrogel after multiple cycles.</p>
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<p>Shape transformation and fixation process of the shape-transformable organohydrogel. (<b>a</b>–<b>d</b>) folding and recovery process of the shape-transformable organohydrogel. (<b>e</b>–<b>g</b>) One-dimensional stretching and shape fixation of the shape-transformable organohydrogel. (<b>h</b>) Thermal imaging of the shape recovery process. (<b>i</b>–<b>l</b>) Two-dimensional stretching and shape recovery of the shape-transformable organohydrogel.</p>
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20 pages, 4539 KiB  
Article
Development of Soft Wrinkled Micropatterns on the Surface of 3D-Printed Hydrogel-Based Scaffolds via High-Resolution Digital Light Processing
by Mauricio A. Sarabia-Vallejos, Scarleth Romero De la Fuente, Nicolás A. Cohn-Inostroza, Claudio A. Terraza, Juan Rodríguez-Hernández and Carmen M. González-Henríquez
Gels 2024, 10(12), 761; https://doi.org/10.3390/gels10120761 - 23 Nov 2024
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Abstract
The preparation of sophisticated hierarchically structured and cytocompatible hydrogel scaffolds is presented. For this purpose, a photosensitive resin was developed, printability was evaluated, and the optimal conditions for 3D printing were investigated. The design and fabrication by additive manufacturing of tailor-made porous scaffolds [...] Read more.
The preparation of sophisticated hierarchically structured and cytocompatible hydrogel scaffolds is presented. For this purpose, a photosensitive resin was developed, printability was evaluated, and the optimal conditions for 3D printing were investigated. The design and fabrication by additive manufacturing of tailor-made porous scaffolds were combined with the formation of surface wrinkled micropatterns. This enabled the combination of micrometer-sized channels (100–200 microns) with microstructured wrinkled surfaces (1–3 μm wavelength). The internal pore structure was found to play a critical role in the mechanical properties. More precisely, the TPMS structure with a zero local curvature appears to be an excellent candidate for maintaining its mechanical resistance to compression stress, thus retaining its structural integrity upon large uniaxial deformations up to 70%. Finally, the washing conditions selected enabled us to produce noncytotoxic materials, as evidenced by experiments using AlamarBlue to follow the metabolic activity of the cells. Full article
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<p>Schematical description of the process followed to obtain the wrinkled scaffolds.</p>
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<p>(<b>a</b>) FT-IR spectra of liquid and polymerized resin for sample 300:50:150, and (<b>b</b>) magnification of vinyl bands (C=C, 1619–1635 cm<sup>−1</sup>, red dashed box) where Gaussian fitting (green line) of the peaks is depicted.</p>
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<p>STL representation of the CAD models used for test 3D-printed scaffolds: gyroid-TPMS (<b>left</b>), solid (<b>center</b>), and straight cylindrical channels (<b>right</b>).</p>
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<p>Stress–strain curves from the compressive mechanical tests of the three different structures studied.</p>
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<p>OM images of the surface wrinkled micropatterns obtained at different vacuum exposure times from 30 min to 180 min.</p>
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<p>(<b>a</b>) AFM micrographs and FFT image; (<b>b</b>) wavelength (black line) and amplitude (red line) of the wrinkled patterns and roughness of the samples using different times and speed rotations via spin coating, according to Table 6 for sample 300:50:150.</p>
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<p>FE-SEM micrographs of wrinkled surfaces with different compositions: (<b>a</b>) 500:0:0, (<b>b</b>) 400:100:0, (<b>c</b>) 400:0:100, (<b>d</b>) 300:100:100, (<b>e</b>) 300:50:150 of PEGDA:DMAEMA:AAm.</p>
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<p>Cell viability results based on the AlamarBlue assay for various resin compositions at 1, 3, and 7 days of culture. Data are expressed as mean ± standard deviation (<span class="html-italic">n</span> = 3). * <span class="html-italic">p</span> &lt; 0.05; ** <span class="html-italic">p</span> &lt; 0.01; *** <span class="html-italic">p</span> &lt; 0.001; n.s., nonsignificant differences.</p>
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<p>Adhesion of MC3T3-E1 cells on resin surfaces at 24 h of incubation. Bar: 50 µM, magnification: 20×, 40×, and 63×.</p>
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