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34 pages, 10110 KiB  
Review
Recent Developments in Electrospun Nanofiber-Based Triboelectric Nanogenerators: Materials, Structure, and Applications
by Qinglong Wei, Yuying Cao, Xiao Yang, Guosong Jiao, Xiaowen Qi and Guilin Wen
Membranes 2024, 14(12), 271; https://doi.org/10.3390/membranes14120271 - 16 Dec 2024
Viewed by 414
Abstract
Triboelectric nanogenerators (TENGs) have garnered significant attention due to their high energy conversion efficiency and extensive application potential in energy harvesting and self-powered devices. Recent advancements in electrospun nanofibers, attributed to their outstanding mechanical properties and tailored surface characteristics, have meant that they [...] Read more.
Triboelectric nanogenerators (TENGs) have garnered significant attention due to their high energy conversion efficiency and extensive application potential in energy harvesting and self-powered devices. Recent advancements in electrospun nanofibers, attributed to their outstanding mechanical properties and tailored surface characteristics, have meant that they can be used as a critical material for enhancing TENGs performance. This review provides a comprehensive overview of the developments in electrospun nanofiber-based TENGs. It begins with an exploration of the fundamental principles behind electrospinning and triboelectricity, followed by a detailed examination of the application and performance of various polymer materials, including poly (vinylidene fluoride) (PVDF), polyamide (PA), thermoplastic polyurethane (TPU), polyacrylonitrile (PAN), and other significant polymers. Furthermore, this review analyzes the influence of diverse structural designs—such as fiber architectures, bionic configurations, and multilayer structures—on the performance of TENGs. Applications across self-powered devices, environmental energy harvesting, and wearable technologies are discussed. The review concludes by highlighting current challenges and outlining future research directions, offering valuable insights for researchers and engineers in the field. Full article
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Figure 1
<p>Principle of electrospun nanofibers. (<b>a</b>) Schematic diagram of a basic electrospinning setup [<a href="#B34-membranes-14-00271" class="html-bibr">34</a>]. (<b>b</b>) Schematic diagram showing the path of an electrospun jet [<a href="#B35-membranes-14-00271" class="html-bibr">35</a>]. All essential copyrights and permissions received.</p>
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<p>Working modes of TENGs (the red arrows indicate the direction of triboelectric layers movement; +: positive charge; −: negative charge) [<a href="#B24-membranes-14-00271" class="html-bibr">24</a>]. All essential copyrights and permissions received.</p>
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<p>Fiber structure. (<b>a</b>) Surface roughness curves and fiber diameter histograms of electrospun fiber membranes at different humidity levels [<a href="#B122-membranes-14-00271" class="html-bibr">122</a>]. (<b>b</b>) Schematic diagram of the grating TENG, including top view, side view, and cross-sectional view, as well as a fiber cross-sectional view of PVDF (red dash lines denote the top view, side view, cross-sectional view and SEM images of the same sample position) [<a href="#B123-membranes-14-00271" class="html-bibr">123</a>]. (<b>c</b>) Wave-shaped TENG [<a href="#B127-membranes-14-00271" class="html-bibr">127</a>]. (<b>d</b>) Wrinkle-type TENG (yellow arrow indicates the distance between the upper and lower layers) [<a href="#B128-membranes-14-00271" class="html-bibr">128</a>]. (<b>e</b>) Stack configuration of electrospun PVDF with different dipole orientation and direction [<a href="#B130-membranes-14-00271" class="html-bibr">130</a>]. All essential copyrights and permissions received.</p>
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<p>Bionic structure. (<b>a</b>) TENG based on petiole-shaped fiber mat [<a href="#B136-membranes-14-00271" class="html-bibr">136</a>]. (<b>b</b>) Janus textile inspired by the internal structures of plants (red dot lines mark a small part of the Janus textile that will be attached to the skin and point to the corresponding structure) [<a href="#B137-membranes-14-00271" class="html-bibr">137</a>]. (<b>c</b>) Structural design of the TENG-based e-skin (black dot lines mark the all-nanofiber TENG-based e-skin and point to the corresponding structure.) [<a href="#B141-membranes-14-00271" class="html-bibr">141</a>]. (<b>d</b>) Bio-inspired hydrophobic/cancellous/hydrophilic Trimurti-based TENG [<a href="#B142-membranes-14-00271" class="html-bibr">142</a>]. (<b>e</b>) Silk-inspired nanofibers [<a href="#B143-membranes-14-00271" class="html-bibr">143</a>]. (<b>f</b>) Bioinspired soft TENG fabricated based on animal body structures [<a href="#B144-membranes-14-00271" class="html-bibr">144</a>]. All essential copyrights and permissions received.</p>
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<p>Multilayer structure. (<b>a</b>) Schematic representation of the TENG construction [<a href="#B149-membranes-14-00271" class="html-bibr">149</a>]. (<b>b</b>) Structure of PT-NG [<a href="#B152-membranes-14-00271" class="html-bibr">152</a>]. (<b>c</b>) Schematic diagram of the hybrid generator [<a href="#B155-membranes-14-00271" class="html-bibr">155</a>]. (<b>d</b>) Schematic diagram of the double-layer nanofibrous TENG [<a href="#B156-membranes-14-00271" class="html-bibr">156</a>]. (<b>e</b>) Schematic illustration showing the layer-by-layer structure of the self-charging SPC [<a href="#B157-membranes-14-00271" class="html-bibr">157</a>]. (<b>f</b>) Structural model diagram of the MS-CES [<a href="#B158-membranes-14-00271" class="html-bibr">158</a>]. All essential copyrights and permissions received.</p>
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<p>Self-powered devices based on electrospun nanofiber TENGs. (<b>a</b>) Schematic illustration of CSYF TENG as a self-powered humidity sensor [<a href="#B167-membranes-14-00271" class="html-bibr">167</a>]. (<b>b</b>) Output performance of STENG as visible-blind UV photodetector [<a href="#B169-membranes-14-00271" class="html-bibr">169</a>]. (<b>c</b>) A real-time smart home control system using an MOF/PVDF (MPVDF) NF-based TENG device (red circle marks the MPVDF NF-based TENG) [<a href="#B170-membranes-14-00271" class="html-bibr">170</a>]. (<b>d</b>) Schematic of a natural human breath test [<a href="#B171-membranes-14-00271" class="html-bibr">171</a>]. (<b>e</b>) Illustration of the integration of SUPS for noninvasive multi-indicator cardiovascular monitoring (red circle marks the SUPS) [<a href="#B172-membranes-14-00271" class="html-bibr">172</a>]. (<b>f</b>) Structure diagram of self-powered TENG and its principle diagram in wound healing (large grey arrow points to the position of TENG, indicating its location in the whole system; small grey arrows represent the healing of wounds from both sides, approaching towards the middle, showing the direction and process of wound healing) [<a href="#B173-membranes-14-00271" class="html-bibr">173</a>]. All essential copyrights and permissions received.</p>
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<p>Environmental energy harvesting based on electrospun nanofiber TENGs (<b>a</b>) Acoustic NFM TENG (yellow arrow points to the overall structure of TENG; red arrow indicates a small part of the PLA layer and the MWCNTs within it; red line represents the wire) [<a href="#B191-membranes-14-00271" class="html-bibr">191</a>]. (<b>b</b>) Wind-driven TENG for W/O emulsion separation (red dash line marks the copper electrode and shows the charge distribution within it) [<a href="#B193-membranes-14-00271" class="html-bibr">193</a>]. (<b>c</b>) Water energy harvesting mechanism of the SNF-TENG (purple arrow shows the direction of charge movement) [<a href="#B194-membranes-14-00271" class="html-bibr">194</a>]. (<b>d</b>) When the rain droplets roll down the MWTT, triboelectric electricity is generated [<a href="#B195-membranes-14-00271" class="html-bibr">195</a>]. (<b>e</b>) Schematics of the G-TENG array for harvesting water wave energy [<a href="#B126-membranes-14-00271" class="html-bibr">126</a>]. All essential copyrights and permissions received.</p>
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<p>Wearable devices based on electrospun nanofiber TENGs (<b>a</b>) The TENG integrated into the mask is used to monitor breathing after walking or running at different speeds on a treadmill [<a href="#B218-membranes-14-00271" class="html-bibr">218</a>]. (<b>b</b>) The voltage changes in our device attached on throat muscle movement [<a href="#B219-membranes-14-00271" class="html-bibr">219</a>]. (<b>c</b>) Schematic diagram of the communication system for the real-time monitoring of abdominal respiratory status by the TENG sensor using a wired transmission device [<a href="#B107-membranes-14-00271" class="html-bibr">107</a>]. (<b>d</b>) The applications of ALTFM-based wearable electronics for human motion monitoring (pink arrows serve as pointers) [<a href="#B125-membranes-14-00271" class="html-bibr">125</a>]. (<b>e</b>) Human body movement recognition and detection using PENG and TENG devices based on PAG2-10 NFs fixed on different locations [<a href="#B220-membranes-14-00271" class="html-bibr">220</a>]. All essential copyrights and permissions received.</p>
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10 pages, 5839 KiB  
Communication
Broadband Thermo-Optic Photonic Switch for TE and TM Modes with Adiabatic Design
by Babak Hashemi, Maurizio Casalino, Teresa Crisci, Mohamed Mammeri and Francesco G. Della Corte
Photonics 2024, 11(12), 1177; https://doi.org/10.3390/photonics11121177 - 14 Dec 2024
Viewed by 295
Abstract
Optical power switches are essential components in fiber optic communication systems, requiring minimal losses, a broad operating wavelength range, and high tolerance to fabrication errors for optimal performance. Adiabatic optical power switches inherently meet these criteria and are well suited for manufacturing processes [...] Read more.
Optical power switches are essential components in fiber optic communication systems, requiring minimal losses, a broad operating wavelength range, and high tolerance to fabrication errors for optimal performance. Adiabatic optical power switches inherently meet these criteria and are well suited for manufacturing processes which support large-scale production at low costs. This paper presents the design and simulation of an adiabatic switch with a flat response in the whole 1525–1625 nm wavelength range (C band and L band) for both TE and TM polarizations. The switch is based on the thermo-optic effect induced by local variations in temperature. The impacts of the design parameters, such as the device length and dissipated heat, are analyzed. The simulation results indicate that the switch achieved high efficiency and low insertion losses, highlighting the potential of adiabatic switches for reliable and scalable integration into advanced optical circuits. Full article
(This article belongs to the Special Issue Photonics: 10th Anniversary)
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Figure 1
<p>Geometry of an adiabatic thermo-optic switch with all relevant parameters.</p>
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<p>Electric field propagation at uniform temperature (T = 300 K) for (<b>a</b>) TE mode and (<b>b</b>) TM mode, showing the 50% splitting action at λ = 1.55 µm. The device has L<sub>t</sub> = 100 <math display="inline"><semantics> <mrow> <mi mathvariant="sans-serif">μ</mi> </mrow> </semantics></math>m (<a href="#photonics-11-01177-f001" class="html-fig">Figure 1</a>).</p>
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<p>(<b>a</b>) Temperature distribution at the switch center (A-A’ of <a href="#photonics-11-01177-f001" class="html-fig">Figure 1</a>) with a generated heat of 0.5 mW per unit length (µm) of the right heater. (<b>b</b>) Temperature profile along X-X’ cut line at the three cross sections—A-A’, B-B’, and C-C’—in <a href="#photonics-11-01177-f001" class="html-fig">Figure 1</a> for the same generated heat. (<b>c</b>) Temperature at waveguide center as a function of power.</p>
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<p>Transmission at the switch output ports as a function of power for different lengths of the tapered waveguides (Lt): (<b>a</b>) TE mode at <math display="inline"><semantics> <mrow> <mi>λ</mi> </mrow> </semantics></math> = 1.525 µm; (<b>b</b>) TM mode at <math display="inline"><semantics> <mrow> <mi>λ</mi> </mrow> </semantics></math> = 1.525 µm; (<b>c</b>) TE mode at <math display="inline"><semantics> <mrow> <mi>λ</mi> </mrow> </semantics></math> = 1.625 µm; and (<b>d</b>) TM mode <math display="inline"><semantics> <mrow> <mi>λ</mi> </mrow> </semantics></math> = 1.625 µm.</p>
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<p>Electric field profile as a function of distance along X-X’ cut line of <a href="#photonics-11-01177-f003" class="html-fig">Figure 3</a>a for TE and TM modes at λ = 1550 nm and applied heating power of 0 mW/µm.</p>
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<p>Extinction ratio (ER) at different wavelengths for (<b>a</b>) TE mode and (<b>b</b>) TM mode, with taper length L<sub>t</sub> = 250 µm and dissipated power P = 1 mW/µm. The values are provided for a waveguide with the geometry specified in <a href="#photonics-11-01177-t001" class="html-table">Table 1</a>, as well as considering fabrication tolerances for the waveguide width (ΔW = ±10 nm) and Si thickness (<math display="inline"><semantics> <mrow> <mo>Δ</mo> </mrow> </semantics></math>h = ±5 nm).</p>
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9 pages, 13511 KiB  
Communication
Polarization-Independent Focusing Vortex Beam Generation Based on Ultra-Thin Spiral Diffractive Lens on Fiber End-Facet
by Luping Wu, Zhiyong Bai, Rui Liu, Yuji Wang, Jian Yu, Jianjun Ran, Zikai Chen, Zilun Luo, Changrui Liao, Ying Wang, Jun He, George Y. Chen and Yiping Wang
Photonics 2024, 11(12), 1167; https://doi.org/10.3390/photonics11121167 - 11 Dec 2024
Viewed by 427
Abstract
An ultra-thin spiral diffractive lens (SDL) was fabricated by using focused ion beam milling on a fiber end-facet coated with a 100 nm thick Au film. Focusing vortex beams (FVBs) were successfully excited by the SDLs due to the coherent superposition of diffracted [...] Read more.
An ultra-thin spiral diffractive lens (SDL) was fabricated by using focused ion beam milling on a fiber end-facet coated with a 100 nm thick Au film. Focusing vortex beams (FVBs) were successfully excited by the SDLs due to the coherent superposition of diffracted waves and their azimuth dependence of the phase accumulated from the spiral aperture to the beam axis. The polarization and phase characteristics of the FVBs were experimentally investigated. Results show that the input beams with various polarization states were converted to FVBs, whose polarization states were the same as those of the input beams. Furthermore, the focal length of the SDL and the in-tensity and phase distribution at the focus spot of the FVBs were numerically simulated by the FDTD method in the ultra-wide near-infrared waveband from 1300 nm to 1800 nm. The focal length was tuned from 21.8 μm to 14.7 μm, the intensity profiles exhibited a doughnut-like shape, and the vortex phase was converted throughout the broadband range. The devices are expected to be candidates for widespread applications including optical communications, optical imaging, and optical tweezers. Full article
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Figure 1
<p>(<b>a</b>) The schematic diagram of SDL with <span class="html-italic">l</span> = 1; (<b>b</b>) simulated intensity distribution at the focal spot for <span class="html-italic">l</span> = 1; (<b>c</b>) the phase distribution at the focal spot for <span class="html-italic">l</span> = 1; (<b>d</b>) The schematic diagram of SDL with <span class="html-italic">l</span> = 2; (<b>e</b>) simulated intensity distribution at the focal spot for <span class="html-italic">l</span> = 2; (<b>f</b>) the phase distribution at the focal spot for <span class="html-italic">l</span> = 2.</p>
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<p>(<b>a</b>) Schematic diagram of the structure of the SDL fabricated on the multimode fiber end-facet; (<b>b</b>) calculation and experimental measurement of divergence angles <span class="html-italic">θ</span> of output beams from the GIF with different lengths; (<b>c</b>) intensity distribution of outputting beam from the GIF about 400 μm long.</p>
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<p>(<b>a</b>,<b>b</b>) SEM images of SDLs fabricated with <span class="html-italic">l</span> = 1 and 2 on the fiber end-facet, respectively; (<b>c</b>) schematic diagram of the measurement system to characterize the outputting beam; (<b>d</b>) measured intensity distribution at the focal spot for <span class="html-italic">l</span> = 1; (<b>e</b>) measured interference patterns between the focal spot and an extended Gaussian beam for <span class="html-italic">l</span> = 1; (<b>f</b>) measured intensity distribution at the focal spot for <span class="html-italic">l</span> = 2; (<b>g</b>) measured interference patterns between the focal spot and an extended Gaussian beam for <span class="html-italic">l</span> = 2.</p>
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<p>Measured intensity distribution and the interference patterns with different polarization state beams injected into the hybrid fiber. (<b>a</b>) <span class="html-italic">l</span> = 1; (<b>b</b>) <span class="html-italic">l</span> = 2.</p>
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<p>Simulated results for the focusing characteristics of the SDL with <span class="html-italic">l</span> = 2, under different wavelengths: (<b>a</b>) 1300 nm, (<b>b</b>) 1400 nm, (<b>c</b>) 1500 nm, (<b>d</b>) 1600 nm, (<b>e</b>) 1700, and (<b>f</b>) 1800 nm. The panels in the first two rows depict the phase distribution and intensity distribution at the focal spot, respectively; the panels in the bottom row illustrate the intensity distributions in the (<span class="html-italic">x</span>, <span class="html-italic">z</span>) plane.</p>
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7 pages, 2101 KiB  
Article
Palladium Nanocubes as Saturable Absorbers for Mode-Locked Laser Generation at 1.56 μm
by Zhe Kang and Fang Wang
Nanomaterials 2024, 14(23), 1971; https://doi.org/10.3390/nano14231971 - 8 Dec 2024
Viewed by 466
Abstract
Palladium (Pd) nanocubes, a type of metallic nanostructure, have demonstrated remarkable optoelectronic properties, garnering significant attention. However, their nonlinear optical characteristics and related device applications remain underexplored. In this study, we report the fabrication of a novel saturable absorber (SA) by depositing Pd [...] Read more.
Palladium (Pd) nanocubes, a type of metallic nanostructure, have demonstrated remarkable optoelectronic properties, garnering significant attention. However, their nonlinear optical characteristics and related device applications remain underexplored. In this study, we report the fabrication of a novel saturable absorber (SA) by depositing Pd nanocubes onto a D-shaped fiber (DF). The Pd nanocubes, with an average size of 12 nm, were synthesized and integrated with a DF, resulting in a highly robust SA with broadband saturable absorption characteristics. When incorporated into Er3+-doped laser cavities, the Pd-DF SA enabled the generation of ultrafast pulses with a central wavelength of 1560 nm, a corresponding repetition rate of 26.7 MHz, and a temporal width of 1.85 ps. Our findings highlight the strong potential of the Pd-DF device as a versatile SA for constructing high-energy ultrafast fiber lasers. Full article
(This article belongs to the Special Issue Nonlinear Optical Property and Sensing Applications of Nanomaterials)
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Figure 1
<p>(<b>a</b>) Solution and (<b>b</b>) TEM image of the as-synthesized Pd nanocubes.</p>
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<p>Absorption spectrum of the Pd nanocube film.</p>
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<p>(<b>a</b>) DF structure. (<b>b</b>) Fabrication process. (<b>c</b>) Nonlinear transmission response at 1.56 μm.</p>
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<p>Schematic diagram of the mode-locked EDFL.</p>
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<p>(<b>a</b>) Spectrum. (<b>b</b>) Power variation. (<b>c</b>) Pulse width. (<b>d</b>) Pulse sequence. (<b>e</b>) RF property. (<b>f</b>) Stability test.</p>
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<p>(<b>a</b>) Spectral and (<b>b</b>) temporal properties at 410 mW.</p>
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14 pages, 3485 KiB  
Article
Fiber-Based Laser Doppler Vibrometer for Middle Ear Diagnostics
by Adam T. Waz, Marcin Masalski and Krzysztof Morawski
Photonics 2024, 11(12), 1152; https://doi.org/10.3390/photonics11121152 - 6 Dec 2024
Viewed by 543
Abstract
Laser Doppler vibrometry (LDV) is an essential tool in assessing by evaluating ossicle vibrations. It is used in fundamental research to understand hearing physiology better and develop new surgical techniques and implants. It is also helpful for the intraoperative hearing assessment and evaluation [...] Read more.
Laser Doppler vibrometry (LDV) is an essential tool in assessing by evaluating ossicle vibrations. It is used in fundamental research to understand hearing physiology better and develop new surgical techniques and implants. It is also helpful for the intraoperative hearing assessment and evaluation of postoperative treatment results. Traditional volumetric LDVs require access in a straight line to the test object, which is challenging due to the structure of the middle ear and the way the auditory ossicles are accessible. Here, we demonstrate the usage of a fiber-based laser Doppler vibrometer (FLDV) for middle ear diagnostics. Compared to classical vibrometers, the main advantages of this device are the ability to analyze several arbitrarily selected points simultaneously and the flexibility achieved by employing fiber optics to perform analysis in hard-to-reach locations, which are particularly important during endoscopic ear surgery. The device also allows for a simple change in measuring probes depending on the application. In this work, we demonstrate the properties of the designed probe and show that using it together with the FLDV enables recording vibrations of the auditory ossicles of the human ear. The obtained signals enable hearing analysis. Full article
(This article belongs to the Special Issue Optical Fiber Lasers and Laser Technology)
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<p>The concept of a fiber-based vibrometer (AO—acousto-optic, EDFA—Erbium Doped Fiber Amplifier, Fibers—standard single mode fibers).</p>
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<p>The four-channel FLDV that was made at WUST [<a href="#B18-photonics-11-01152" class="html-bibr">18</a>].</p>
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<p>Default (universal) motorized FLDV head: (<b>a</b>) an idea; (<b>b</b>) a real photo.</p>
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<p>Ceramic hand probe tip: (<b>a</b>) the design; (<b>b</b>,<b>c</b>) photos.</p>
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<p>Handheld probe (HP): (<b>a</b>) photo; (<b>b</b>) far-field beam profiles (samples: 3760, target scan rate: 10 Hz, resolution 2.4 μm, 9.68 fps).</p>
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<p>Comparison of the beam’s diameter emitted from a fiber and a collimator.</p>
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<p>Retroreflective sticker with glass beads.</p>
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<p>Measuring the power of scattered light returning to the system: (<b>a</b>) setup with universal head (UH); (<b>b</b>) results.</p>
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<p>Measuring the power of scattered light returning to the system: (<b>a</b>) setup with handheld probe (HP); (<b>b</b>) results.</p>
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<p>Typical access to the middle ear: (<b>a</b>) setup for measuring middle ear vibrations; (<b>b</b>) actual photo with visible ossicles and dimensions; (<b>c</b>) photo of the measurement on the posterior crus of stapes.</p>
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<p>Averaged spectrum for 60 dB HL excitation over noise background [<a href="#B18-photonics-11-01152" class="html-bibr">18</a>].</p>
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<p>The amplitude of vibration of the superstructure of the stapes of an example ear as a function of stimulation intensity.</p>
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14 pages, 3042 KiB  
Article
Enhanced Interfacial Properties of Carbon Fiber/Polymerization of Monomers Reactants Method Polyimide Composite by Polyimide Sizing
by Chengyu Huang, Jinsong Sun, Zhiwei Liu, Bo Li, Mingchen Sun, Hansong Liu, Yan Zhao, Peng Zhang and Jianwen Bao
Materials 2024, 17(23), 5962; https://doi.org/10.3390/ma17235962 - 5 Dec 2024
Viewed by 362
Abstract
Carbon fiber (CF)-reinforced polyimide (PI) resin matrix composites have great application potential in areas such as rail transport, medical devices, and aerospace due to their excellent thermal stability, dielectric properties, solvent resistance, and mechanical properties. However, the epoxy sizing agent used for traditional [...] Read more.
Carbon fiber (CF)-reinforced polyimide (PI) resin matrix composites have great application potential in areas such as rail transport, medical devices, and aerospace due to their excellent thermal stability, dielectric properties, solvent resistance, and mechanical properties. However, the epoxy sizing agent used for traditional carbon fiber cannot withstand the processing temperature of polyimide resin, of up to 350 °C, resulting in the formation of pores or defects at the interface between the fiber and the resin matrix, leading to the degradation of the overall composite properties. To overcome this problem, in this study, a low-molecular-weight thermosetting polyimide sizing agent was prepared and the processability of the sized carbon fiber was optimized by a thermoplastic polyimide. Compared with the unsized carbon fiber polyimide composites, the interfacial properties of the composites after the polyimide sizing treatment were significantly improved, with the interfacial shear strength (IFSS) increasing from 82.08 MPa to 136.27 MPa, the interlaminar shear strength (ILSS) increasing from 103.7 to 124.9 MPa, and the bending strength increasing from 2262.2 MPa to 2562.1 MPa. The sizing agent acts as a bridge between the carbon fiber and polyimide resin, with anchorage and bonding at the interface between the fiber and resin, which are beneficial for enhancing the interface performance of composites. Full article
(This article belongs to the Special Issue Research on Properties of Polymers and Their Engineering Applications)
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Graphical abstract

Graphical abstract
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<p>Schematic diagram of synthesis of sizing agents and preparation of polyimide composite materials by sizing carbon fiber.</p>
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<p>Infrared spectra (<b>a</b>), TGA curve (<b>b</b>), and DSC curve (<b>c</b>) of the sizing agent and PMR-PI resin.</p>
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<p>SEM and AFM images of carbon fibers under different sizing conditions: (<b>a</b>) Desized-CF; (<b>b</b>) Epoxy-CF; (<b>c</b>) PI-CF; (<b>d</b>) PI/2%TPI-CF; (<b>e</b>) PI/4%TPI-CF; (<b>f</b>) PI/6%TPI-CF; (<b>g</b>) PI/8%TPI-CF; and (<b>h</b>) intrinsic viscosity of different sizing agents.</p>
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<p>Surface morphology of CFs after PI debonding: (<b>a</b>) Desized-CF; (<b>b</b>) Epoxy-CF; (<b>c</b>) PI-CF; (<b>d</b>) PI/4%TPI-CF; and (<b>e</b>) IFSS of CF/PI.</p>
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<p>SEM images of fracture of composites after ILSS test and flexural properties test: (<b>a1</b>–<b>a3</b>) Desized-CF; (<b>b1</b>–<b>b3</b>) Epoxy-CF; (<b>c1</b>–<b>c3</b>) PI-CF; and (<b>d1</b>–<b>d3</b>) PI/4%TPI-CF.</p>
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<p>Mechanical properties test of composites under different sizing conditions: (<b>a</b>) ILSS; (<b>b</b>) bending strength; (<b>c</b>) storage modulus in DMA; and (<b>d</b>) tan δ in DMA.</p>
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<p>Schematic diagram of interface strengthening mechanism.</p>
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15 pages, 4777 KiB  
Article
Multipoint Thermal Sensing System for Power Semiconductor Devices Utilizing Fiber Bragg Gratings
by Ridwanullahi Isa, Naveed Iqbal, Mohammad Abido, Jawad Mirza and Khurram Karim Qureshi
Appl. Sci. 2024, 14(23), 11328; https://doi.org/10.3390/app142311328 - 4 Dec 2024
Viewed by 576
Abstract
This study investigates the feasibility of using fiber Bragg grating (FBG) sensors for multipoint thermal monitoring of several power semiconductor devices (PSDs), such as insulated gate bipolar transistors (IGBTs), and rectifiers assembled on a common heatsink in a three-phase inverter. A novel approach [...] Read more.
This study investigates the feasibility of using fiber Bragg grating (FBG) sensors for multipoint thermal monitoring of several power semiconductor devices (PSDs), such as insulated gate bipolar transistors (IGBTs), and rectifiers assembled on a common heatsink in a three-phase inverter. A novel approach is proposed to integrate FBG sensors beneath the baseplates of the IGBT modules, avoiding the need for invasive modifications to the device structure. By strategically positioning multiple FBG sensors, accurate temperature profiles of critical components can be obtained. The experimental results demonstrate the effectiveness of the proposed method, with the temperature measurements from FBG sensors closely matching those obtained using thermal infrared (IR) cameras within ±1.1 °C. This research highlights the potential of FBG sensors for reliable and precise thermal management in power electronic systems, contributing to improved performance and reliability. Full article
(This article belongs to the Special Issue Recent Advances and Applications of Optical and Acoustic Measurements)
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<p>Schematic of a three-phase inverter.</p>
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<p>Thermal network of a single IGBT module referenced to FBG sensor.</p>
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<p>Thermal resistance network of multiple IGBTs.</p>
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<p>Schematic of the calibration setup.</p>
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<p>Temperature–wavelength correlation of FBG sensors.</p>
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<p>(<b>a</b>) FBG array in a single optical fiber. (<b>b</b>) Installation settings of the sensors in the inverter circuit (<b>c</b>) FIBER1; vertical sensor configuration along the rectifier/IGBT baseplate. (<b>d</b>) FIBER2; horizontal sensor configuration along the rectifier/IGBTs baseplate.</p>
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<p>(<b>a</b>) Tabletop experimental setup. (<b>b</b>) Thermal imaging of the IGBT.</p>
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<p>Observed reflection spectra for the FBG sensors on the optical spectrum analyzer.</p>
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<p>FBG temperature response to varying load power.</p>
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<p>FBG temperature response to varying load power with minimized airgap effect.</p>
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<p>(<b>a</b>) Thermal imaging of IGBT at time T1. (<b>b</b>) Thermal imaging of IGBT at time T2 (where T2 &gt; T1).</p>
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<p>Predictions of hotspots using neural networks.</p>
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12 pages, 3548 KiB  
Article
A Coaxial Triboelectric Fiber Sensor for Human Motion Recognition and Rehabilitation via Machine Learning
by Qicheng Ding, Aamir Rasheed, Haonan Zhang, Sara Ajmal, Ghulam Dastgeer, Kamoladdin Saidov, Olim Ruzimuradov, Shavkat Mamatkulov, Wen He and Peihong Wang
Nanoenergy Adv. 2024, 4(4), 355-366; https://doi.org/10.3390/nanoenergyadv4040022 - 4 Dec 2024
Viewed by 623
Abstract
This work presents the fabrication of a coaxial fiber triboelectric sensor (CFTES) designed for efficient energy harvesting and gesture detection in wearable electronics. The CFTES was fabricated using a facile one-step wet-spinning approach, with PVDF-HFP/CNTs/Carbon black as the conductive electrode and PVDF-HFP/MoS2 [...] Read more.
This work presents the fabrication of a coaxial fiber triboelectric sensor (CFTES) designed for efficient energy harvesting and gesture detection in wearable electronics. The CFTES was fabricated using a facile one-step wet-spinning approach, with PVDF-HFP/CNTs/Carbon black as the conductive electrode and PVDF-HFP/MoS2 as the triboelectric layer. The incorporation of 1T phase MoS2 into the PVDF-HFP matrix significantly improves the sensor’s output owing to its electron capture capabilities. The sensor’s performance was carefully optimized by varying the weight percentage of MoS2, the thickness of the fiber core, and the CNT ratio. The optimized CFTES, with a core thickness of 156 µm and 0.6 wt% MoS2, achieved a stable output voltage of ~8.2 V at a frequency of 4 Hz and 10 N applied force, exhibiting remarkable robustness over 3600 s. Furthermore, the CFTES effectively detects human finger gestures, with machine learning algorithms further enhancing its accuracy. This innovative sensor offers a sustainable solution for energy transformation and has promising applications in smart portable power sources and wearable electronic devices. Full article
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<p>Schematic illustration of the synthesis of the composites via the wet spinning method.</p>
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<p>EDS mapping of PVDF-HFP/1T-MoS<sub>2</sub> (<b>a</b>) C, (<b>b</b>) S, (<b>c</b>) and Mo; (<b>d</b>) scanning electron microscopic image of PVDF-HFP/1T-MoS<sub>2</sub>; (<b>e</b>) high-resolution S2p XPS spectra of PVDF-HFP/1T-MoS<sub>2</sub>; (<b>f</b>) high-resolution Mo3d XPS spectra of PVDF-HFP/1T-MoS<sub>2</sub>; (<b>g</b>–<b>i</b>) flexibility test of the fabricated fiber: (<b>g</b>) straight, (<b>h</b>) bending, and (<b>i</b>) knotted.</p>
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<p>Schematic illustration showing the working principle of the CFTES device.</p>
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<p>Effect of core diameter on the electrical output performance of the CFTESL (<b>a</b>) output voltage, (<b>b</b>) short-circuit current, and (<b>c</b>) charge; effect of m<sub>CNT</sub>/m<sub>ACET</sub> ratio on the electrical output performance of the CFTES: (<b>d</b>) output voltage, (<b>e</b>) short-circuit current, and (<b>f</b>) charge; effect of % of MoS<sub>2</sub> on the electrical output performance of the CFTES: (<b>g</b>) output voltage, (<b>h</b>) short-circuit current, and (<b>i</b>) % of MoS<sub>2</sub>.</p>
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<p>Effect of operating frequency on the electrical properties of the CFTES: (<b>a</b>) output voltage, (<b>b</b>) short-circuit current, and (<b>c</b>) transferred charge; effect of external force on the electrical properties of the CFTES: (<b>d</b>) output voltage, (<b>e</b>) short-circuit current, and (<b>f</b>) transferred charge, respectively; (<b>g</b>) sensitivity of the CFTES and (<b>h</b>) voltage retention of the CFTES after operation for 3600 s.</p>
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<p>Real-time application of the CFTES device: (<b>a</b>) 3D graphs for the output voltage generation indicating the bending gestures of human fingers and (<b>b</b>) corresponding images of fingers bending at different angles. (<b>c</b>) Workflow diagram of an LSTM model for deep learning and a confusion matrix for recognizing different finger movements.</p>
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12 pages, 12255 KiB  
Article
A New Caffeine Detection Method Using a Highly Multiplexed Smartphone-Based Spectrometer
by Erhuan Zhuo, Huanxin Xia, Huan Hu and Yu Lin
Biosensors 2024, 14(12), 590; https://doi.org/10.3390/bios14120590 - 3 Dec 2024
Viewed by 685
Abstract
Smartphones equipped with highly integrated sensors are increasingly being recognized as powerful tools for rapid on-site testing. Here, we propose a low-cost, portable, and highly multiplexed smartphone-based spectrometer capable of collecting three types of spectra—transmission, reflection, and fluorescence—by simply replacing the optical fiber [...] Read more.
Smartphones equipped with highly integrated sensors are increasingly being recognized as powerful tools for rapid on-site testing. Here, we propose a low-cost, portable, and highly multiplexed smartphone-based spectrometer capable of collecting three types of spectra—transmission, reflection, and fluorescence—by simply replacing the optical fiber attached to the housing. Spectral analysis is performed directly on the smartphone using a custom-developed app. Furthermore, we introduce a high signal-to-noise ratio (SNR) caffeine detection scheme that leverages aspirin and salicylic acid as fluorescent probes, allowing for the rapid and straightforward detection of caffeine in various samples. The fluorescence quenching of the probes was found to be linearly related to the caffeine concentration (0–200 μM), and the recoveries of the commercially available caffeine-containing samples were in the range of 98.0333–105.6000%, with a limit of detection (LOD) of 2.58 μM. The reliability and stability of the on-site assay using the smartphone spectrometer were verified. More importantly, this spectrometer demonstrates great potential as a versatile device for use outside of laboratory settings by enabling different operating modes tailored to various scenarios. Full article
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<p>Light path and fabrication of the smartphone-based spectrometer. (<b>a</b>) Light path and fabrication of the spectrometer. (<b>b</b>) Smartphone spectrometer physical picture.</p>
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<p>Spectrum RGB images processing. (<b>a</b>) RGB ROI (red boxes) and peak pixel position of 532 nm and 650 nm. Resolution = (650 − 532)/(1296 − 743) ≈ 0.21 nm/pixel. (<b>b</b>–<b>e</b>) Spot and contours of 532 nm RGB image before and after correcting.</p>
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<p>Validation of spectrometer using R6G. (<b>a</b>) Absorption spectrum of R6G. (<b>b</b>) Linear fit of OD value and concentration of R6G. (<b>c</b>) 650 nm reflective intensity of diluted milk. Milk content in diluted solution is 0, 20, 40, 60, 80, 100%.</p>
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<p>(<b>a</b>) Aspirin fluorescence excited by UV LED. (<b>b</b>) Aspirin fluorescence is quenched by caffeine.</p>
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<p>Effect of the presence or absence of inhibition of aspirin hydrolysis on its fluorescence. (<b>a</b>) Experiment design under group I, II, III. M1–M7 are the specific cases of measuring spectrum. (<b>b</b>,<b>c</b>) Fluorescence spectra after 12 h reaction with caffeine under inhibited and uninhibited conditions. (<b>d</b>–<b>h</b>) Fluorescence spectrum obtained by hydrolyzing 0, 3, 6, 9, 12 h aspirin with caffeine. (<b>i</b>,<b>j</b>) Linear fit results of quenching fluorescence and caffeine concentration in <a href="#biosensors-14-00590-f005" class="html-fig">Figure 5</a> M1 and M2. (<b>k</b>) Caffeine concentration in coffee diluted at different times. The red line is the result of fitting dilution factor and caffeine concentration.</p>
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<p>The effect of the degree of aspirin hydrolysis on the linear fitting results when aspirin hydrolysis is not inhibited. (<b>a</b>) Experiment design of the effect of aspirin hydrolysis time under under group I, II, III, IV. (<b>b</b>) Linear fit results of different aspirin hydrolysis times.</p>
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<p>The original caffeine content in five samples. Data for red and green flags are from <a href="#biosensors-14-00590-t001" class="html-table">Table 1</a>.</p>
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14 pages, 1053 KiB  
Article
An Efficient pH Detector for Water Contamination Based on Mach–Zehnder Interferometer Application
by Mario Angel Rico-Mendez, Romeo Selvas, Oxana V. Kharissova, Daniel Toral-Acosta, Norma Patricia Puente-Ramirez, Ricardo Chapa-Garcia and Abraham Antonio Gonzalez-Roque
Sci 2024, 6(4), 80; https://doi.org/10.3390/sci6040080 - 2 Dec 2024
Viewed by 533
Abstract
This paper presents a pH sensor with a Mach–Zehnder Interferometer (MZI) that operates in solutions of 4.0, 7.0, and 10.0. The sensor device consists of two tapered sections with dimensions of 1 mm/1 mm/1 mm for down-taper, waist-length, and up-taper, respectively, with a [...] Read more.
This paper presents a pH sensor with a Mach–Zehnder Interferometer (MZI) that operates in solutions of 4.0, 7.0, and 10.0. The sensor device consists of two tapered sections with dimensions of 1 mm/1 mm/1 mm for down-taper, waist-length, and up-taper, respectively, with a separation of 10 mm. The diameter of the waist is 40 μm. This work includes the experimental evaluation of an MZI fiber optic pH sensor at 1559 nm, where 1559 nm represents a specific wavelength chosen for its optimal sensitivity in evaluating the sensor pH detection performance. It is not the central wavelength of the optical fiber, but one of the minimal values selected to enhance the interaction between the evanescent field and the sample, ensuring the reliable detection of pH variations. These sensor dimensions and the functionalized solution of multi-walled carbon nanotubes (MWCNTs) increase the detection of pH in dyes used in the textile industry. Alizarin is a strong anionic red dye that is part of the anthraquinone dye group. The experimental results demonstrated effective detection of pH levels in water contamination involving dye. This development could resolve the problem with Alizarin. The simple fabrication, low cost, and stability of the optical response make this sensor relevant for pH measurements in water contamination. Full article
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<p>In the geometric structure of the sensor, the regions labelled with A, B, and C are 1 mm of length, corresponding to the DT, UT, and WT, respectively, and region B has a diameter of 40 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m.</p>
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<p>Transmission spectrum of the Mach–Zehnder Interferometer (MZI), observed in the absence of an external surrounding medium.</p>
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<p>Simulated evolution of the input electromagnetic field E is highlighted in the taper regions of the optical fiber.</p>
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<p>Simulated transmission spectrum of an MZI featuring two tapers, each with a transition length of 1 mm, a waist length of 40 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m, and a separation of 10 mm between the tapers.</p>
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<p>Setup for pH optical fiber sensor.</p>
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<p>Stability of the output power of pH 4.0 in a period of 50 min; the axis output power was adjusted (shift) for better data appreciation.</p>
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<p>Comparative of the interference spectrum to dip centered at 1559 nm of transmission of MZFI for each pH sample.</p>
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<p>Output power shifting of the central response from the sensor when submerged in buffer pH values of 4 to 10 in a time of 0–50 min.</p>
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<p>Wavelength shifting of the central response from the sensor as a function of the time in a range of 50 min.</p>
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37 pages, 15018 KiB  
Review
Graphene-Based Fiber Materials for Gas Sensing Applications: State of the Art Review
by Susanna Vu, Mohamed Siaj and Ricardo Izquierdo
Materials 2024, 17(23), 5825; https://doi.org/10.3390/ma17235825 - 27 Nov 2024
Viewed by 529
Abstract
The importance of gas sensors is apparent as the detection of gases and pollutants is crucial for environmental monitoring and human safety. Gas sensing devices also hold the potential for medical applications as health monitoring and disease diagnostic tools. Gas sensors fabricated from [...] Read more.
The importance of gas sensors is apparent as the detection of gases and pollutants is crucial for environmental monitoring and human safety. Gas sensing devices also hold the potential for medical applications as health monitoring and disease diagnostic tools. Gas sensors fabricated from graphene-based fibers present a promising advancement in the field of sensing technology due to their enhanced sensitivity and selectivity. The diverse chemical and mechanical properties of graphene-based fibers—such as high surface area, flexibility, and structural stability—establish them as ideal gas-sensing materials. Most significantly, graphene fibers can be readily tuned to detect a wide range of gases, making them highly versatile in gas-sensing technologies. This review focuses on graphene-based composite fibers for gas sensors, with an emphasis on the preparation processes used to achieve these fibers and the gas sensing mechanisms involved in their sensors. Graphene fiber gas sensors are presented based on the chemical composition of their target gases, with detailed discussions on their sensitivity and performance. This review reveals that graphene-based fibers can be prepared through various methods and can be effectively integrated into gas-sensing devices for a diverse range of applications. By presenting an overview of developments in this field over the past decade, this review highlights the potential of graphene-based fiber sensors and their prospective integration into future technologies. Full article
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<p>Examples of graphene-based fiber sensors for diatomic gases: (<b>a</b>) Schematic illustration of RGO-ZnO sensing mechanism for H<sub>2</sub> gas [<a href="#B69-materials-17-05825" class="html-bibr">69</a>]; (<b>b</b>) Schematic diagram of Cd/RGO/SnO<sub>2</sub> sensing mechanism to CO gas [<a href="#B73-materials-17-05825" class="html-bibr">73</a>].</p>
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<p>Schematic illustration of graphene/PANI/PS nanofibers preparation steps [<a href="#B91-materials-17-05825" class="html-bibr">91</a>].</p>
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<p>Field-emission scanning electron microscopy images of: (<b>a</b>) Pristine CuO nanofibers, and RGO-CuO nanofibers with different amounts of RGO; (<b>b</b>) 0.05 wt% RGO, (<b>c</b>) 0.1 wt% RGO, (<b>d</b>) 0.2 wt% RGO, (<b>e</b>) 0.3 wt% RGO, (<b>f</b>) 0.5 wt% RGO, (<b>g</b>) 1 wt% RGO, and (<b>h</b>) 1.5 wt RGO% [<a href="#B93-materials-17-05825" class="html-bibr">93</a>].</p>
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<p>Schematic illustration of the fabrication process for PS-WO<sub>3</sub>/NOGR nanofibers, whereby controlled pore distribution on the nanofiber is achieved [<a href="#B95-materials-17-05825" class="html-bibr">95</a>].</p>
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<p>Schematic depicting the gas sensing mechanism of RGO-ZnFe<sub>2</sub>O<sub>4</sub> nanofibers: (<b>a</b>) Band diagram of RGO and ZFO; (<b>b</b>) At equilibrium; (<b>c</b>) In air; (<b>d</b>) H<sub>2</sub>S gas exposure [<a href="#B98-materials-17-05825" class="html-bibr">98</a>].</p>
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<p>Schematic illustration of the sensing mechanism of (<b>a</b>) In<sub>2</sub>O<sub>3</sub> compared to (<b>b</b>) RGO-In<sub>2</sub>O<sub>3</sub> towards NO<sub>2</sub> gas [<a href="#B111-materials-17-05825" class="html-bibr">111</a>].</p>
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<p>(<b>a</b>) Response of RGO-SnO<sub>2</sub> nanofibers to NO<sub>2</sub>, O<sub>2</sub>, and SO<sub>2</sub> gases, where the concentration was set to of 1, 2, and 5 ppm, respectively [<a href="#B114-materials-17-05825" class="html-bibr">114</a>]; (<b>b</b>) Response of RGO-ZnO nanofibers, with varying RGO concentrations, to 5 ppm of NO<sub>2</sub> gas [<a href="#B70-materials-17-05825" class="html-bibr">70</a>].</p>
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<p>Schematic illustration of Cu/Cu<sub>2</sub>O/graphene and Ni/NiO/graphene fiber (M/MO/GF) fabrication, involving wet-spinning and thermal treatment of fibers [<a href="#B122-materials-17-05825" class="html-bibr">122</a>].</p>
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<p>Images of RGO/WO<sub>3</sub>/TCNF fibers integrated into various objects: (<b>a</b>) A wristwatch (the area highlighted in yellow is where the fiber was integrated); (<b>b</b>) A pair of safety goggles; (<b>c</b>) Sown onto Kimtech paper; (<b>d</b>) A wearable sensing module. NO<sub>2</sub> gas monitoring from the portable sensing device (<b>d</b>) is depicted in (<b>e</b>) [<a href="#B125-materials-17-05825" class="html-bibr">125</a>].</p>
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<p>(<b>a</b>) Schematic illustration depicting the multi-step fabrication of RGO/ZnO/thread sensors; (<b>b</b>) Image of sensor array network of RGO/ZnO/thread and its integration onto wearable fabric [<a href="#B128-materials-17-05825" class="html-bibr">128</a>].</p>
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<p>Examples of gas sensors using commercially available fibers: (<b>a</b>) Gas sensing performance of RGO-cotton yarn and RGO-polyester yarn exposed to 0.25 ppm and 1.25 ppm of NO<sub>2</sub> at room temperature [<a href="#B129-materials-17-05825" class="html-bibr">129</a>]; (<b>b</b>) Gas sensing performance of RGO-cotton yarn and RGO-cotton yarn with MoS<sub>2</sub> exposed to 0.45 ppm, 2.5 ppm, and 4.5 ppm NO<sub>2</sub> gas at room temperature [<a href="#B130-materials-17-05825" class="html-bibr">130</a>]; (<b>c</b>) Schematic illustration of the fabrication process for RGO-elastic yarn [<a href="#B131-materials-17-05825" class="html-bibr">131</a>]; (<b>d</b>) Schematic illustration of the fabrication process of RGO/nylon-6 [<a href="#B134-materials-17-05825" class="html-bibr">134</a>].</p>
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<p>Examples of gas sensors using commercially available fibers: (<b>a</b>) Gas sensing performance of RGO-cotton yarn and RGO-polyester yarn exposed to 0.25 ppm and 1.25 ppm of NO<sub>2</sub> at room temperature [<a href="#B129-materials-17-05825" class="html-bibr">129</a>]; (<b>b</b>) Gas sensing performance of RGO-cotton yarn and RGO-cotton yarn with MoS<sub>2</sub> exposed to 0.45 ppm, 2.5 ppm, and 4.5 ppm NO<sub>2</sub> gas at room temperature [<a href="#B130-materials-17-05825" class="html-bibr">130</a>]; (<b>c</b>) Schematic illustration of the fabrication process for RGO-elastic yarn [<a href="#B131-materials-17-05825" class="html-bibr">131</a>]; (<b>d</b>) Schematic illustration of the fabrication process of RGO/nylon-6 [<a href="#B134-materials-17-05825" class="html-bibr">134</a>].</p>
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<p>Schematic illustration of the fabrication process for RGO–Co<sub>3</sub>O<sub>4</sub> nanofibers involving electrospinning and calcination process [<a href="#B143-materials-17-05825" class="html-bibr">143</a>].</p>
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<p>Schematic illustration of (<b>a</b>) The preparation of hollow In<sub>2</sub>O<sub>3</sub> nanofibers, N-GQDs, and PANI/N-GQD/In<sub>2</sub>O<sub>3</sub> nanofibers, and (<b>b</b>) nanofiber sensor fabrication [<a href="#B147-materials-17-05825" class="html-bibr">147</a>].</p>
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<p>Schematic representation of RGO-In<sub>2</sub>O<sub>3</sub> gas sensing mechanism, depicting depletion layer in air (<b>i</b>) and in NH<sub>3</sub> gas (<b>ii</b>) [<a href="#B150-materials-17-05825" class="html-bibr">150</a>].</p>
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<p>(<b>a</b>) Schematic illustration of MXene/GO via wet-spinning; (<b>b</b>) Selectivity of RGO/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> MXene to NH<sub>3</sub> in comparison to other gases [<a href="#B153-materials-17-05825" class="html-bibr">153</a>].</p>
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<p>(<b>a</b>) Frequency shifts of G-COOH/PS QCM sensors upon exposure to increasing NH<sub>3</sub> concentrations [<a href="#B158-materials-17-05825" class="html-bibr">158</a>]; (<b>b</b>) Frequency shifts of CA/PEI/GO QCM sensors upon exposure to increasing NH<sub>3</sub> concentrations [<a href="#B162-materials-17-05825" class="html-bibr">162</a>].</p>
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<p>Schematic illustration of the preparation of RGO-ZnO nanofiber sensors [<a href="#B176-materials-17-05825" class="html-bibr">176</a>].</p>
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<p>Gas sensor on e-skin device: (<b>a</b>) Response of gas sensor to different concentrations of acetone vapor; (<b>b</b>) Response of gas sensor to increasing acetone concentrations; (<b>c</b>) Response and recovery time of gas sensor; (<b>d</b>) sensing stability of device under different bending states in 500 ppm of acetone vapor (each color on the plot represents the response for different bending states) [<a href="#B179-materials-17-05825" class="html-bibr">179</a>].</p>
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<p>Schematic depicting RGO-Cu fiber preparation illustrating the content of Cu in the fiber [<a href="#B180-materials-17-05825" class="html-bibr">180</a>].</p>
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<p>(<b>a</b>) Response of GO-SnO<sub>2</sub> nanofibers (II) and SnO<sub>2</sub> without GO (I); (<b>b</b>) Selectivity of GO-SnO<sub>2</sub> nanofibers (II) and SnO<sub>2</sub> without GO (I) to ethanol gas compared to other gases [<a href="#B182-materials-17-05825" class="html-bibr">182</a>].</p>
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<p>(<b>a</b>) Response of RGO-SnO<sub>2</sub> sensor compared to RGO with other nanocarbons to 100 ppm of formaldehyde as a function of temperature; (<b>b</b>) Response of RGO-SnO<sub>2</sub> sensor containing different RGO concentrations as a function of temperature [<a href="#B186-materials-17-05825" class="html-bibr">186</a>].</p>
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<p>Schematic illustration of the preparation of RGO-SnO<sub>2</sub> nanofiber composite [<a href="#B193-materials-17-05825" class="html-bibr">193</a>].</p>
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<p>Schematic illustration of gas sensing mechanism of RGO/(Pt or Pd)/SnO<sub>2</sub> (the change in the potential barrier is presented by the black and red curves) [<a href="#B201-materials-17-05825" class="html-bibr">201</a>].</p>
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<p>Schematic illustration of the synthesis of RGO/(Au or Pd)/ZnO [<a href="#B206-materials-17-05825" class="html-bibr">206</a>].</p>
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<p>(<b>a</b>) Schematic illustrating the gas sensing mechanism of RGO-MoS<sub>2</sub> composite fiber to (<b>a</b>) NO<sub>2</sub> and (<b>b</b>) NH<sub>3</sub> gas [<a href="#B212-materials-17-05825" class="html-bibr">212</a>].</p>
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<p>(<b>a</b>) Schematic illustration of wet-spinning of GO fiber and fiber sensor; (<b>b</b>) Schematic illustrating the sensing mechanism of RGO-ZnO fiber [<a href="#B215-materials-17-05825" class="html-bibr">215</a>].</p>
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17 pages, 11664 KiB  
Article
Self-Oscillation of Liquid Crystal Elastomer Fiber-Slide System Driven by Self-Flickering Light Source
by Dali Ge, Qingrui Hong, Xin Liu and Haiyi Liang
Polymers 2024, 16(23), 3298; https://doi.org/10.3390/polym16233298 - 26 Nov 2024
Viewed by 387
Abstract
Self-oscillation, a control approach inspired by biological systems, demonstrates an autonomous, continuous, and regular response to constant external environmental stimuli. Until now, most self-oscillation systems have relied on a static external environment that continuously supplies energy, while materials typically absorb ambient energy only [...] Read more.
Self-oscillation, a control approach inspired by biological systems, demonstrates an autonomous, continuous, and regular response to constant external environmental stimuli. Until now, most self-oscillation systems have relied on a static external environment that continuously supplies energy, while materials typically absorb ambient energy only intermittently. In this article, we propose an innovative self-oscillation of liquid crystal elastomer (LCE) fiber-slide system driven by a self-flickering light source, which can efficiently regulate the energy input in sync with the self-oscillating behavior under constant voltage. This system primarily consists of a photo-responsive LCE fiber, a slider that includes a conductive segment and an insulating segment, a light source, and a conductive track. Using the dynamic LCE model, we derive the governing equation for the motion of the LCE fiber-slider system. Numerical simulations show that the LCE fiber-slide system under constant voltage exhibits two distinct motion phases, namely the stationary phase and the self-oscillation phase. The self-oscillation occurs due to the photo-induced contraction of the LCE fiber when the light source is activated. We also investigate the critical conditions required to initiate self-oscillation, and examine key system parameters influencing its frequency and amplitude. Unlike the continuous energy release from the static environmental field in most self-oscillation systems, our LCE fiber-slide self-oscillation system is driven by a self-flickering light source, which dynamically adjusts the energy input under a constant voltage to synchronize with the self-oscillating behavior. Our design features advantages such as spontaneous periodic lighting, a simple structure, energy efficiency, and ease of operation. It shows significant promise for dynamic circuit systems, monitoring devices, and optical applications. Full article
(This article belongs to the Special Issue Advances in Functional Rubber and Elastomer Composites II)
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<p>Schematic diagram of a self-oscillation of LCE fiber-slide system driven by self-flickering light source. (<b>a</b>) Reference state. (<b>b</b>) Initial state. (<b>c</b>) Current state. (<b>d</b>) State transition and force analysis.</p>
Full article ">Figure 2
<p>Temporal behavior of displacement and phase trajectory curves for two motion phases. (<b>a</b>) Displacement temporal behavior with <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0; (<b>b</b>) phase trajectory with <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0; (<b>c</b>) displacement temporal behavior with <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1; and (<b>d</b>) phase trajectory with <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1. Other parameters are <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>C</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>β</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>k</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 5.8, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>v</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 1.2, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2. Under constant voltage, the LCE fiber-slide system driven by self-flickering light source exhibits two distinct motion phases: the stationary phase and the self-oscillation phase.</p>
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<p>Mechanism of the self-oscillation of the LCE fiber-slider system driven by self-flickering light source for the typical case in <a href="#polymers-16-03298-f002" class="html-fig">Figure 2</a>c,d. (<b>a</b>) Variation of concentration of <span class="html-italic">cis</span> molecules over <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>t</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math>; (<b>b</b>) Variation of LCE fiber <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>F</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> over <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>t</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math>. (<b>c</b>) The relationship between <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>F</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>x</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math>, and (<b>d</b>) relationship between <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>F</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mi>d</mi> </mrow> </msub> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>x</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math>. The damping dissipation is balanced by the energy input from the tensile force, thereby maintaining stable self-oscillation.</p>
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<p>Influence of light intensity on self-oscillation of LCE fiber-slide system, for <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>C</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>β</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>k</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 5.8, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>v</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 1.2, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2. (<b>a</b>) Stable cycles. (<b>b</b>) <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math>. As <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> increases, the <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math> tends to rise, while the <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> remains relatively stable.</p>
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<p>Influence of contraction coefficient on self-oscillation of LCE fiber-slide system, for <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>β</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>k</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 5.8, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>v</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 1.2, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2. (<b>a</b>) Stable cycles. (<b>b</b>) <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math>. As the contraction coefficient increases, the <math display="inline"><semantics> <mrow> <mtext> </mtext> <mi>A</mi> </mrow> </semantics></math> shows a distinct increase, while the <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> stays largely unaffected.</p>
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<p>Influence of damping coefficient on self-oscillation of LCE fiber-slide system, for <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>C</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>k</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 5.8, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>v</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 1.2, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2. (<b>a</b>) Stable cycles. (<b>b</b>) <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math>. With the increase in damping coefficient, the <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math> presents a decreasing trend, while the <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> remains nearly constant.</p>
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<p>Influence of stiffness coefficient on self-oscillation of LCE fiber-slide system, for <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>C</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>β</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>v</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 1.2, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2. (<b>a</b>) Stable cycles. (<b>b</b>) <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math>. As the stiffness coefficient increases, both the a <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math> exhibit an upward trend.</p>
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<p>Influence of initial velocity on self-oscillation of LCE fiber-slide system, for <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>C</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>β</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>k</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 5.8, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 1.2, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2. (<b>a</b>) Stable cycles. (<b>b</b>) <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math>. Initial conditions do not influence the <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> of self-oscillation.</p>
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<p>Influence of gravitational acceleration on self-oscillation of LCE fiber-slide system, for <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>C</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>β</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>v</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>k</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 5.8, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2. (<b>a</b>) Stable cycles. (<b>b</b>) <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math>. As <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> increases, the <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math> initially rises and then falls, while <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> has barely changed at all.</p>
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<p>Influence of conductive track position on self-oscillation of LCE fiber-slide system, for <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>I</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>C</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.2, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>β</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>v</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> = 0.1, <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>k</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 5.8, and <math display="inline"><semantics> <mrow> <mover accent="true"> <mrow> <mi>g</mi> </mrow> <mo>¯</mo> </mover> </mrow> </semantics></math> = 1.2. (<b>a</b>) Stable cycles. (<b>b</b>) <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math>. As <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>h</mi> </mrow> <mo>¯</mo> </mover> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math> increases, the <math display="inline"><semantics> <mrow> <mi>A</mi> </mrow> </semantics></math> initially rises and then falls, while <math display="inline"><semantics> <mrow> <mi>f</mi> </mrow> </semantics></math> has barely changed at all.</p>
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11 pages, 3441 KiB  
Article
THz Polarimetric Imaging of Carbon Fiber-Reinforced Composites Using the Portable Handled Spectral Reflection (PHASR) Scanner
by Kuangyi Xu, Zachery B. Harris, Paul Vahey and M. Hassan Arbab
Sensors 2024, 24(23), 7467; https://doi.org/10.3390/s24237467 - 22 Nov 2024
Viewed by 471
Abstract
Recent advancements in novel fiber-coupled and portable terahertz (THz) spectroscopic imaging technology have accelerated applications in nondestructive testing (NDT). Although the polarization information of THz waves can play a critical role in material characterization, there are few demonstrations of polarization-resolved THz imaging as [...] Read more.
Recent advancements in novel fiber-coupled and portable terahertz (THz) spectroscopic imaging technology have accelerated applications in nondestructive testing (NDT). Although the polarization information of THz waves can play a critical role in material characterization, there are few demonstrations of polarization-resolved THz imaging as an NDT modality due to the deficiency of such polarimetric imaging devices. In this paper, we have inspected industrial carbon fiber composites using a portable and handheld imaging scanner in which the THz polarizations of two orthogonal channels are simultaneously captured by two photoconductive antennas. We observed significant polarimetric differences between the two-channel images of the same sample and the resulting THz Stokes vectors, which are attributed to the anisotropic conductivity of carbon fiber composites. Using both polarimetric channels, we can visualize the superficial and underlying interfaces of the first laminate. These results pave the way for the future applications of THz polarimetry to the assessment of coatings or surface quality on carbon fiber-reinforced substrates. Full article
(This article belongs to the Special Issue Millimeter Wave and Terahertz Source, Sensing and Imaging)
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Figure 1

Figure 1
<p>(<b>a</b>) Front surface of the first test panel from Boeing Company. (<b>b</b>) Microscopic image (10×) of the bare substrate, appearing as unidirectional CFRP.</p>
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<p>(<b>a</b>) Back surface of the second test panel from Boeing Company. (<b>b</b>) Microscopic image (2.5×) of the back surface, appearing as interwoven (plain-weaved) CFRP.</p>
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<p>(<b>a</b>) The THz signals reflected from unidirectional CFRP at the sample orientations of 0° and 90°, corresponding to the TM and TE modes of polarization, respectively. The dashed box shows the difference in the propagation of the TE and TM modes in a single CFRP ply. (<b>b</b>,<b>c</b>) are the spectra of reflectivity and impulse responses retrieved from signals in (<b>a</b>). (<b>d</b>) The impulse responses are measured at different locations of interwoven CFRP, where the fiber orientations are different.</p>
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<p>Cross-section images (B-scan) of (<b>a</b>) the unidirectional CFRP and the interwoven CFRP in the (<b>b</b>) X and (<b>c</b>) Y channels. The colors are on the same scale and have been extended to [−1, 1].</p>
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<p>(<b>a</b>) Photo of the interwoven CFRP, top view. (<b>b</b>,<b>c</b>) are the C-scanned THz images of the X channel, at the optical depths of z = 0 and z = 0.52 mm, respectively. (<b>d</b>,<b>e</b>) are the correlated images of the Y channel, at the optical depths of z = 0 and z = 0.60 mm, respectively.</p>
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<p>The spatial variation in the Stokes parameters <span class="html-italic">I</span>, <span class="html-italic">Q</span>, <span class="html-italic">U</span>, and <span class="html-italic">V</span> for the interwoven CFRP at different frequencies. <span class="html-italic">I</span> is in arbitrary units while the other Stokes parameters are normalized by <span class="html-italic">I</span>.</p>
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<p>(<b>a</b>) Two ROIs (blue and red) are selected in the C-scan images of interwoven CFRP. (<b>b</b>) The mean value and standard deviation of the reflectivity in the two ROIs. (<b>c</b>–<b>f</b>) The distribution of pixels in the 2D plane of |R<sub>x</sub>| and |R<sub>y</sub>|, indicating the separation of orthogonal fibers in the 0.4–0.6 THz range.</p>
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16 pages, 1242 KiB  
Article
Logic Gate Generation in a Monostable Optical System: Improving the Erbium-Doped Fiber Laser Reconfigurable Logic Operation
by Samuel Mardoqueo Afanador-Delgado, José Luis Echenausía-Monroy, Guillermo Huerta-Cuellar, Juan Hugo García-López, Erick Emiliano Lopez-Muñoz and Rider Jaimes-Reátegui
Photonics 2024, 11(12), 1103; https://doi.org/10.3390/photonics11121103 - 22 Nov 2024
Viewed by 411
Abstract
A logic gate is typically an electronic device with a Boolean or other type of function, e.g., adding or subtracting, including or excluding according to its logical properties. They can be used in electronic, electrical, mechanical, hydraulic, and pneumatic technology. This paper presents [...] Read more.
A logic gate is typically an electronic device with a Boolean or other type of function, e.g., adding or subtracting, including or excluding according to its logical properties. They can be used in electronic, electrical, mechanical, hydraulic, and pneumatic technology. This paper presents a new method for generating logic gates based on optical systems with an emission frequency equal to that used in current telecommunications systems. It uses an erbium-doped fiber laser in its monostable operating region, in contrast to most results published in the literature, where multistable behavior is required to induce dynamic changes, and where a DC voltage signal in the laser pump current provides the control between obtaining the different logic operations. The proposed methodology facilitates the generation of the gates, since it does not require taking the optical system to critical power levels that could damage the components. It is based on using the same elements that the EDFL requires to operate. The result is a system capable of generating up to five stable and robust logic gates to disturbances validated in numerical simulation and experimental setup. This eliminates the sensitivity to the initial conditions affecting the possible logic gates generated by the system and the need to add noise to the system (as is performed in works based on stochastic logic resonance). The experimental observations confirm the numerical results and open up new aspects of using chaotic systems to generate optical logic gates without bistable states. Full article
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Figure 1
<p>EDFL bifurcation diagram. (<b>a</b>) Numerically calculated, (<b>b</b>) experimentally determined.</p>
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<p>Experimental setup. (<b>a</b>) Optical elements required to put the Erbium-Doped Fiber Laser into operation (<b>b</b>) Elements required to implement the logic gate based on the operation of the EDFL. WFG: Wave Form Generator; LDC: Laser Diode Controller; PD: Photo-Detector; WDM: Wavelength Division Multiplexing; OS: Osciloscope; FBG: Fiber Bragg Grating.</p>
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<p>Bifurcation diagram at a modulation frequency of <math display="inline"><semantics> <msub> <mi>f</mi> <mi>m</mi> </msub> </semantics></math> = 10 kHz. (<b>a</b>) Numerically calculated −1 a.u. &lt; DC &lt; 1 a.u., (<b>b</b>) experimentally determined −1 V &lt; DC &lt; 1 V.</p>
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<p>Changes observed in the behavior of laser intensity by adding a DC signal to pump modulation (Numerically calculated on the <b>left</b>, and experimentally observed on the <b>right</b>). Left axis laser amplitude (solid line) and right axis DC amplitude (dash line). Response at DC signal with amplitude (<b>a</b>,<b>b</b>) 0.5 V &lt; DC &lt; 0.9 V, (<b>c</b>,<b>d</b>) 0.1 V &lt; DC &lt; 0.4 V, (<b>e</b>,<b>f</b>) −0.5 V &lt; DC &lt; −0.1 V, (<b>g</b>,<b>h</b>) −0.9 V &lt; DC &lt; −0.6 V.</p>
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<p>Modulation signal. (<b>a</b>) Sinusoidal signal with a frequency <math display="inline"><semantics> <msub> <mi>f</mi> <mi>m</mi> </msub> </semantics></math> = 10 kHz and <math display="inline"><semantics> <msub> <mi>A</mi> <mi>m</mi> </msub> </semantics></math> = 1 a.u. (<b>b</b>) Sum of the digital signals <math display="inline"><semantics> <mrow> <msub> <mi>I</mi> <mn>1</mn> </msub> <mo>+</mo> <msub> <mi>I</mi> <mn>2</mn> </msub> </mrow> </semantics></math>, with amplitude <math display="inline"><semantics> <msub> <mi>A</mi> <mi>d</mi> </msub> </semantics></math> = 1 a.u. (<b>c</b>) Modulation signal <math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>m</mi> </msub> <mo form="prefix">sin</mo> <mrow> <mo>(</mo> <mn>2</mn> <mi>π</mi> <msub> <mi>f</mi> <mi>m</mi> </msub> <mi>t</mi> <mo>)</mo> </mrow> <mo>+</mo> <msub> <mi>A</mi> <mi>d</mi> </msub> <mrow> <mo>(</mo> <msub> <mi>I</mi> <mn>1</mn> </msub> <mo>+</mo> <msub> <mi>I</mi> <mn>2</mn> </msub> <mo>)</mo> </mrow> <mo>+</mo> <mi>DC</mi> </mrow> </semantics></math> for modulating the laser current, <math display="inline"><semantics> <msub> <mi>A</mi> <mi>m</mi> </msub> </semantics></math> = 1 a.u., <math display="inline"><semantics> <msub> <mi>f</mi> <mi>m</mi> </msub> </semantics></math> = 10 kHz, <math display="inline"><semantics> <msub> <mi>A</mi> <mi>d</mi> </msub> </semantics></math> = 0.3 a.u. and DC = −0.8 a.u.</p>
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<p>Numerical result of the laser operating as an AND logic gate for DC = −0.8 a.u., <math display="inline"><semantics> <msub> <mi>A</mi> <mi>d</mi> </msub> </semantics></math> = 0.3 a.u. (<b>a</b>) digital signals fed into the system, (<b>b</b>) temporal behavior of the system when stimulated with the digital signal, (<b>c</b>) output signal of the constructed logic gate.</p>
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<p>Numerically calculated signals of the modulated laser system responding as a logic gate. The left column shows the behavior of the EDFL responding as an OR logic gate (<math display="inline"><semantics> <mrow> <mi>DC</mi> <mo>=</mo> <mo>−</mo> </mrow> </semantics></math>0.7 a.u., <math display="inline"><semantics> <msub> <mi>A</mi> <mi>d</mi> </msub> </semantics></math> = 0.3 a.u.), while the right column shows the laser system acting as an XOR gate (<math display="inline"><semantics> <mrow> <mi>DC</mi> <mo>=</mo> <mo>−</mo> </mrow> </semantics></math>0.5 a.u., <math display="inline"><semantics> <msub> <mi>A</mi> <mi>d</mi> </msub> </semantics></math> = 0.3 a.u.). (<b>a</b>,<b>b</b>) Digital input injected into the laser system. (<b>c</b>,<b>d</b>) Laser emission of the system under stimulation of the digital input. (<b>e</b>,<b>f</b>) Response of the logic gate built with the EDFL in monostable regime.</p>
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<p>Dynamic response numerically calculated of the EDFL as a logic gate for different DC values. Left column shows the behavior of the EDFL responding as an NAND gate (<math display="inline"><semantics> <mrow> <mi>DC</mi> <mo>=</mo> <mo>−</mo> </mrow> </semantics></math>0.4 a.u., <math display="inline"><semantics> <msub> <mi>A</mi> <mi>d</mi> </msub> </semantics></math> = 0.3 a.u.), while the right column shows the laser system acting as an NOR gate (<math display="inline"><semantics> <mrow> <mi>DC</mi> <mo>=</mo> <mo>−</mo> </mrow> </semantics></math>0.3 a.u., <math display="inline"><semantics> <msub> <mi>A</mi> <mi>d</mi> </msub> </semantics></math> = 0.3 a.u.). (<b>a</b>,<b>b</b>) Digital input injected into the EDFL. (<b>c</b>,<b>d</b>) Laser emission of the system under stimulation of the digital input. (<b>e</b>,<b>f</b>) Response of the logic gate built with the EDFL in monostable regime.</p>
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<p>Experimentally obtained signals of the modulated laser system responding as an AND logic gate for <math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>d</mi> </msub> <mo>=</mo> <mn>0.5</mn> </mrow> </semantics></math> V y DC = −0.1 V. (<b>a</b>) Digital input injected into the laser system. (<b>b</b>) Laser emission of the system under stimulation of the digital input. (<b>c</b>) Response of the logic gate built with the EDFL in monostable regime.</p>
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<p>Experimental signals of the modulated laser system responding as a logic gate. The left column shows the behavior of the EDFL responding as an OR logic gate (<math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>d</mi> </msub> <mo>=</mo> <mn>0.5</mn> <mspace width="0.166667em"/> <mi mathvariant="normal">V</mi> </mrow> </semantics></math>, DC = 0 V), while the right column shows the laser system acting as an XOR gate (<math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>d</mi> </msub> <mo>=</mo> <mn>0.5</mn> <mspace width="0.166667em"/> <mi mathvariant="normal">V</mi> </mrow> </semantics></math>, DC = 0.1 V). (<b>a</b>,<b>b</b>) Digital input injected into the laser system. (<b>c</b>,<b>d</b>) Laser emission of the system under stimulation of the digital input. (<b>e</b>,<b>f</b>) Response of the logic gate built with the EDFL in monostable regime.</p>
Full article ">Figure 10 Cont.
<p>Experimental signals of the modulated laser system responding as a logic gate. The left column shows the behavior of the EDFL responding as an OR logic gate (<math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>d</mi> </msub> <mo>=</mo> <mn>0.5</mn> <mspace width="0.166667em"/> <mi mathvariant="normal">V</mi> </mrow> </semantics></math>, DC = 0 V), while the right column shows the laser system acting as an XOR gate (<math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>d</mi> </msub> <mo>=</mo> <mn>0.5</mn> <mspace width="0.166667em"/> <mi mathvariant="normal">V</mi> </mrow> </semantics></math>, DC = 0.1 V). (<b>a</b>,<b>b</b>) Digital input injected into the laser system. (<b>c</b>,<b>d</b>) Laser emission of the system under stimulation of the digital input. (<b>e</b>,<b>f</b>) Response of the logic gate built with the EDFL in monostable regime.</p>
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<p>Experimental behavior of the modulated EDFL responding as a logic gate. The left column shows the behavior of the EDFL responding as an NAND logic gate (<math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>d</mi> </msub> <mo>=</mo> <mn>0.5</mn> <mspace width="0.166667em"/> <mi mathvariant="normal">V</mi> </mrow> </semantics></math> y DC = 0.2 V), while the right column shows the laser system acting as an NOR gate (<math display="inline"><semantics> <mrow> <msub> <mi>A</mi> <mi>d</mi> </msub> <mo>=</mo> <mn>0.5</mn> <mspace width="0.166667em"/> <mi mathvariant="normal">V</mi> </mrow> </semantics></math> y DC = 0.3 V). (<b>a</b>,<b>b</b>) Digital input injected into the laser system. (<b>c</b>,<b>d</b>) Laser emission of the system under stimulation of the digital input. (<b>e</b>,<b>f</b>) Response of the logic gate built with the EDFL.</p>
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12 pages, 4480 KiB  
Article
He-Kr Gas-Discharge Laser Based on Hollow-Core Fiber
by Igor Bufetov, Dmitry Komissarov, Sergey Nefedov, Alexey Kosolapov, Vladimir Velmiskin, Alexander Mineev and Alexey Gladyshev
Photonics 2024, 11(12), 1102; https://doi.org/10.3390/photonics11121102 - 22 Nov 2024
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Abstract
Recently, two completely different types of lasers—a fiber laser and a gas-discharge laser—were combined into a single device by demonstrating 2.03 µm laser generation in He-Xe plasma that was produced by a microwave discharge directly inside a hollow-core fiber. This new type of [...] Read more.
Recently, two completely different types of lasers—a fiber laser and a gas-discharge laser—were combined into a single device by demonstrating 2.03 µm laser generation in He-Xe plasma that was produced by a microwave discharge directly inside a hollow-core fiber. This new type of laser—a gas-discharge fiber laser—provides excellent opportunities to greatly enrich the wavelength range of the operation of fiber lasers. In this work, we investigate a He-Kr gas mixture as an active medium of this new type of laser. As a result, a He-Kr gas-discharge fiber laser is demonstrated for the first time. The laser was pumped by a microwave discharge in a He:Kr (40:1) mixture that was filled into a revolver fiber with the hollow-core diameter of 130 µm. The total gas pressure was about 100 torr. With broadband mirrors of the laser resonator, generation was observed simultaneously at wavelengths of 2190 and 2523 nm. The output power of the He-Kr gas-discharge fiber laser was about 1 mW. Full article
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Figure 1

Figure 1
<p>(<b>a</b>) The scheme of experimental setup. 1—Revolver-type hollow-core fiber; 2—small vacuum chambers; 3—a section of a microwave waveguide; 4—a slit in the side surface of the waveguide. Red arrows illustrate direction and intensity of the microwave electric field E<sub>0</sub> in the slit. HR—high-reflection mirror; OC—output coupler; UV—mercury lamp for the discharge ignition. The inset PH shows a real photograph of microwave discharge luminescence in the hollow-core fiber placed in the slit. (<b>b</b>) Microphotograph of the hollow-core fiber cross-section.</p>
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<p>Transmission spectrum of the hollow-core fiber used in the experiments. Red dashed lines point out the wavelengths, at which lasing of the He-Kr GDFL is observed in this work.</p>
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<p>Reflection spectra of the mirrors that formed the cavity of He-Kr gas-discharge fiber laser. Blue dashed lines point out the wavelengths, at which lasing of the He-Kr GDFL was observed.</p>
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<p>Relative peak output power of the He-Kr GDFL as a function of mole fraction of Kr atoms. Total pressure of the He-Kr gas mixture was 105 torr.</p>
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<p>Typical waveforms measured by a photoresistor at the output of He-Kr GDFL for different values of a microwave electric field E<sub>0</sub> that is applied across the hollow-core fiber. The E<sub>0</sub> amplitudes are shown in the figure legend. The microwave pump pulse (curves 2) and the waveform of plasma discharge registered from the side surface of the fiber (curves 1) are also shown. The duration of pump pulses was (<b>a</b>) 20 µs and (<b>b</b>) 80 µs. Total pressure of the He-Kr mixture was 105 torr with Kr mole fraction of 2.5%.</p>
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<p>Peak power generated by He-Kr GDFL as a function of total gas pressure. The mole fraction of Kr was 2.5%. The amplitude of the microwave field E<sub>0</sub> was 3.6 kV/cm (red dots) and 5.3 kV/cm (black squares).</p>
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<p>Typical output spectra generated by He-Kr GDFL based on He-Kr mixture at a total pressure of 105 torr and Kr mole fraction of 2.5%. The spectra were measured (<b>a</b>,<b>b</b>) by optical spectrum analyzer AQ6375B (Yokogawa) in 1200–2400 nm range and (<b>c</b>) by grating-based monochromator MS2004 (SOLAR TII) in 1600–3700 nm range.</p>
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<p>Typical waveforms generated by He-Kr GDFL and measured separately for the line at 2190 nm (curves 1) and the line at 2523 nm (curves 2). The data were obtained in the He-Kr mixture with a 2.5% mole fraction of Kr and at total pressure of (<b>a</b>) 105 torr and (<b>b</b>) 81 torr.</p>
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<p>The scheme of krypton energy levels involved in the He-Kr laser generation. A transition responsible for luminescence at 760 nm is also shown, since it serves as an indicator of population of lower laser level for both laser transitions observed in this work.</p>
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<p>Plasma luminescence spectra measured from the side surface of the fiber for different concentrations of He in the He-Kr mixture. The amplitude of the microwave excitation was E<sub>0</sub> = 5.3 kV/cm. The following gas mixtures were studied: (<b>a</b>) pure Kr at pressure of 30 torr, (<b>b</b>) He:Kr = 20:1 at total pressure of 105 torr, (<b>c</b>) He:Kr = 40:1 at total pressure of 105 torr, (<b>d</b>) He:Kr = 100:1 at total pressure of 105 torr. The wavelengths of lines (1–10) and their relation to He or Kr are explained in <a href="#photonics-11-01102-f011" class="html-fig">Figure 11</a>.</p>
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<p>Intensities of He I and Kr I luminescence lines as a function of the microwave pump field E<sub>0</sub> applied across the hollow-core fiber. The measurements were performed with a He-Kr mixture at a total pressure of 105 torr and Kr mole fraction of 2.5%.</p>
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