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WO2014023661A3 - Dualhärtende lösungsmittelfreie einkomponenten-massen und ihre verwendung - Google Patents

Dualhärtende lösungsmittelfreie einkomponenten-massen und ihre verwendung Download PDF

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Publication number
WO2014023661A3
WO2014023661A3 PCT/EP2013/066302 EP2013066302W WO2014023661A3 WO 2014023661 A3 WO2014023661 A3 WO 2014023661A3 EP 2013066302 W EP2013066302 W EP 2013066302W WO 2014023661 A3 WO2014023661 A3 WO 2014023661A3
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WIPO (PCT)
Prior art keywords
weight
free
composition
dual
containing compound
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PCT/EP2013/066302
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English (en)
French (fr)
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WO2014023661A2 (de
Inventor
Jürgen KÖBLER
Michael Stumbeck
Original Assignee
Delo Industrie Klebstoffe Gmbh & Co. Kgaa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Delo Industrie Klebstoffe Gmbh & Co. Kgaa filed Critical Delo Industrie Klebstoffe Gmbh & Co. Kgaa
Priority to DE112013003942.7T priority Critical patent/DE112013003942B4/de
Priority to US14/420,409 priority patent/US10227445B2/en
Publication of WO2014023661A2 publication Critical patent/WO2014023661A2/de
Publication of WO2014023661A3 publication Critical patent/WO2014023661A3/de

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/003—Polymeric products of isocyanates or isothiocyanates with epoxy compounds having no active hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78—Nitrogen
    • C08G18/7806—Nitrogen containing -N-C=0 groups
    • C08G18/7818—Nitrogen containing -N-C=0 groups containing ureum or ureum derivative groups
    • C08G18/7831—Nitrogen containing -N-C=0 groups containing ureum or ureum derivative groups containing biuret groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/81—Unsaturated isocyanates or isothiocyanates
    • C08G18/8141—Unsaturated isocyanates or isothiocyanates masked
    • C08G18/815—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen
    • C08G18/8158—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen with unsaturated compounds having only one group containing active hydrogen
    • C08G18/8175—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen with unsaturated compounds having only one group containing active hydrogen with esters of acrylic or alkylacrylic acid having only one group containing active hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/14—Polycondensates modified by chemical after-treatment
    • C08G59/1433—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds
    • C08G59/1477—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C08G59/4007—Curing agents not provided for by the groups C08G59/42 - C08G59/66
    • C08G59/4064—Curing agents not provided for by the groups C08G59/42 - C08G59/66 sulfur containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C08G59/50—Amines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04—Polyurethanes
    • C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
    • C09J175/04—Polyurethanes
    • C09J175/14—Polyurethanes having carbon-to-carbon unsaturated bonds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Sealing Material Composition (AREA)

Abstract

Die Erfindung betrifft eine dualhärtende, lösungsmittelfreie Einkomponenten- Masse zur Verwendung für das Verkleben, Vergießen, Abdichten und Beschichten von Substraten, insbesondere von elektronischen Bauteilen. Die Masse besteht aus (A)30 bis 60 Gew.-% einer mindestens difunktionellen epoxidhaltigen Verbindung, (B)5 bis 35 Gew.-% einer Hybridverbindung, die mindestens eine Isocyanatgruppe und zugleich mindestens eine radikalisch polymerisierbare Gruppe trägt, (C)5 bis 40 Gew.-% eines latenten Härters auf Basis von Stickstoffverbindungen, die zur Additionsvernetzung der epoxidhaltigen Verbindung geeignet sind, (D)0,2 bis 5 Gew.-% eines durch Bestrahlung mit Licht zur Radikalbildung fähigen Photoinitiators, jeweils bezogen auf das Gesamtgewicht der Komponenten (A) bis (D); sowie wahlweise (E)0bis 80 Gew.-% Modifikatoren, ausgewählt aus mindestens einer der Gruppen der Füllstoffe, Farbstoffe, Pigmente, Stabilisatoren, Feuchtigkeit bindenden Mittel, Beschleuniger, Fließverbesserer, Benetzungsmittel, Thixotropierungsmittel, Verdünnungsmittel und polymeren Verdickungsmittel, jeweils bezogen auf das Gesamtgewicht der Masse. Die Masse zeichnet sich dadurch aus, dass sie nach einer Lichthärtung durch radikalische Photopolymerisation oberflächentrocken ist.
PCT/EP2013/066302 2012-08-09 2013-08-02 Dualhärtende lösungsmittelfreie einkomponenten-massen und ihre verwendung WO2014023661A2 (de)

Priority Applications (2)

Application Number Priority Date Filing Date Title
DE112013003942.7T DE112013003942B4 (de) 2012-08-09 2013-08-02 Dualhärtende lösungsmittelfreie Einkomponenten-Massen und ihre Verwendung
US14/420,409 US10227445B2 (en) 2012-08-09 2013-08-02 Dual-curing solvent-free single-component masses and their use

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102012015729.0 2012-08-09
DE102012015729.0A DE102012015729A1 (de) 2012-08-09 2012-08-09 Dualhärtende lösungsmittelfreie Einkomponenten-Massen und ihre Verwendung

Publications (2)

Publication Number Publication Date
WO2014023661A2 WO2014023661A2 (de) 2014-02-13
WO2014023661A3 true WO2014023661A3 (de) 2014-04-24

Family

ID=48917541

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2013/066302 WO2014023661A2 (de) 2012-08-09 2013-08-02 Dualhärtende lösungsmittelfreie einkomponenten-massen und ihre verwendung

Country Status (3)

Country Link
US (1) US10227445B2 (de)
DE (2) DE102012015729A1 (de)
WO (1) WO2014023661A2 (de)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102013211047B4 (de) * 2013-06-13 2015-04-30 MTU Aero Engines AG Verfahren zum Verschließen von Kühlluftbohrungen
DE102017129780A1 (de) 2017-12-13 2019-06-13 Delo Industrie Klebstoffe Gmbh & Co. Kgaa Lichtfixierbare und warmhärtende Massen auf Basis von Epoxidharzen und Thiolen
CN108753228B (zh) * 2018-06-15 2021-11-26 浙江航通舟新材料科技有限公司 一种环氧树脂-改性丙烯酸树脂双固化体系针头胶及其制备方法
DE102018121067A1 (de) * 2018-08-29 2020-03-05 Delo Industrie Klebstoffe Gmbh & Co. Kgaa Härtbare Zweikomponentenmasse
CN109957369B (zh) * 2019-03-29 2021-12-14 东莞初创应用材料有限公司 一种紫外光固化黑色胶黏剂及其制备方法
WO2020255045A1 (en) * 2019-06-18 2020-12-24 Davies Robert Michael System and method for achieving a one component growable resin system
CN115926598A (zh) * 2022-12-31 2023-04-07 惠州市韵点新材料科技股份有限公司 一种双固化uv面漆及其应用
CN116904115B (zh) * 2023-07-17 2024-02-13 江西昊泽光学膜科技有限公司 一种热光双固化定型的涂料及其制备方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4701478A (en) * 1985-03-09 1987-10-20 Rutgerswerke Aktiengesellschaft Radiation cross-linkable binding agents
WO2000013818A1 (en) * 1998-09-02 2000-03-16 Ashland Inc. Foundry binder of epoxy resin, acrylated polyisocyanate and acrylic monomer and/or polymer; and cold-box process
US20100212830A1 (en) * 2005-07-05 2010-08-26 Michael Stumbeck Thermosetting solvent-free single-component compositions and their use
DE102009012272A1 (de) * 2009-03-11 2010-09-23 Wellmann, Stefanie, Dr. Dual härtende UV-Klebstoffe

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DE3023486A1 (de) * 1980-06-24 1982-01-07 Bayer Ag, 5090 Leverkusen Photopolymerisierbare mischungen mit aroylphosphonsaeureestern als photoinitiatoren
DE3447355A1 (de) * 1984-12-24 1986-07-03 Basf Ag, 6700 Ludwigshafen Vernetzbares harz, lichtempfindliches aufzeichnungsmaterial auf basis dieses vernetzbaren harzes sowie verfahren zur herstellung einer flachdruckplatte mittels dieses lichtempfindlichen aufzeichnungsmaterials
DE19920799A1 (de) * 1999-05-06 2000-11-16 Basf Coatings Ag Thermisch und mit aktinischer Strahlung härtbarer Beschichtungsstoff und seine Verwendung
DE19927949A1 (de) 1999-06-18 2000-12-21 Delo Industrieklebstoffe Gmbh Kationisch härtende Masse, ihre Verwendung sowie Verfahren zur Herstellung gehärteter Polymermassen
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DE10357712A1 (de) * 2003-12-09 2005-07-14 Bayer Materialscience Ag Härter
DE102010010598A1 (de) 2010-03-08 2011-09-08 Delo Industrie Klebstoffe Gmbh & Co. Kgaa Dual härtende Masse und deren Verwendung
EP2586827B1 (de) 2010-06-28 2017-12-27 Adeka Corporation Härtbare harzzusammensetzung

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4701478A (en) * 1985-03-09 1987-10-20 Rutgerswerke Aktiengesellschaft Radiation cross-linkable binding agents
WO2000013818A1 (en) * 1998-09-02 2000-03-16 Ashland Inc. Foundry binder of epoxy resin, acrylated polyisocyanate and acrylic monomer and/or polymer; and cold-box process
US20100212830A1 (en) * 2005-07-05 2010-08-26 Michael Stumbeck Thermosetting solvent-free single-component compositions and their use
DE102009012272A1 (de) * 2009-03-11 2010-09-23 Wellmann, Stefanie, Dr. Dual härtende UV-Klebstoffe

Also Published As

Publication number Publication date
US10227445B2 (en) 2019-03-12
WO2014023661A2 (de) 2014-02-13
DE102012015729A1 (de) 2014-05-15
DE112013003942A5 (de) 2015-05-28
DE112013003942B4 (de) 2017-03-16
US20150266996A1 (en) 2015-09-24

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