WO2012078468A2 - Extending lines through, and preventing extrusion of, seal elements of packer assemblies - Google Patents
Extending lines through, and preventing extrusion of, seal elements of packer assemblies Download PDFInfo
- Publication number
- WO2012078468A2 WO2012078468A2 PCT/US2011/063077 US2011063077W WO2012078468A2 WO 2012078468 A2 WO2012078468 A2 WO 2012078468A2 US 2011063077 W US2011063077 W US 2011063077W WO 2012078468 A2 WO2012078468 A2 WO 2012078468A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- end ring
- leaves
- seal element
- packer assembly
- ring body
- Prior art date
Links
- 238000001125 extrusion Methods 0.000 title description 9
- 230000000712 assembly Effects 0.000 title description 3
- 238000000429 assembly Methods 0.000 title description 3
- 238000000034 method Methods 0.000 claims abstract description 21
- 239000012530 fluid Substances 0.000 claims abstract description 17
- 230000004044 response Effects 0.000 claims abstract description 14
- 230000008961 swelling Effects 0.000 claims abstract description 13
- 238000007789 sealing Methods 0.000 claims abstract description 5
- 239000000463 material Substances 0.000 description 27
- 230000003213 activating effect Effects 0.000 description 8
- 239000003795 chemical substances by application Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 239000004215 Carbon black (E152) Substances 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 238000004026 adhesive bonding Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000012217 deletion Methods 0.000 description 1
- 230000037430 deletion Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000009760 electrical discharge machining Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 125000001183 hydrocarbyl group Chemical group 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B33/00—Sealing or packing boreholes or wells
- E21B33/10—Sealing or packing boreholes or wells in the borehole
- E21B33/12—Packers; Plugs
- E21B33/1208—Packers; Plugs characterised by the construction of the sealing or packing means
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B33/00—Sealing or packing boreholes or wells
- E21B33/10—Sealing or packing boreholes or wells in the borehole
- E21B33/12—Packers; Plugs
- E21B33/1208—Packers; Plugs characterised by the construction of the sealing or packing means
- E21B33/1216—Anti-extrusion means, e.g. means to prevent cold flow of rubber packing
Definitions
- This disclosure relates generally to equipment utilized and operations performed in conjunction with a subterranean well and, in an example described below, more particularly provides for extending lines through, and preventing extrusion of, packer seal elements.
- An annulus differential pressure rating of a packer assembly can be limited by extrusion of the packer
- this disclosure provides to the art a packer assembly for use in a subterranean well.
- the packer assembly can include an annular seal element and at least one end ring.
- the end ring includes leaves formed on a body of the end ring, whereby the leaves are biased radially outward when the seal element extends radially outward.
- a method of sealing an annulus in a subterranean well is provided by this disclosure.
- the method can include positioning a circumferential series of leaves radially outwardly overlying an annular seal element of a packer assembly, and the leaves pivoting radially outward in response to swelling of the seal element.
- a disclosed packer assembly for use in a subterranean well can include an annular seal element which swells in response to contact with a selected fluid in the well, and at least one end ring including an end ring body with a removable portion. The removable portion is engaged with the body of the end ring via
- FIG. 1 is a schematic partially cross-sectional view of a well system and associated method which can embody
- FIGS. 2-9 are schematic views of one example of a packer assembly which may be used in the system and method of FIG. 1.
- FIGS. 10-15 are schematic views of another example of the packer assembly.
- FIGS. 16-19 are schematic views of yet another example of the packer assembly.
- FIG. 1 Representatively illustrated in FIG. 1 is a well system 10 and associated method which can embody principles of this disclosure.
- a packer assembly 12 is used to seal off an annulus 14 formed between a tubular string 16 and a wellbore 18.
- the wellbore 18 is lined with casing 20 and cement 22, but in other examples, the wellbore could be uncased or open hole.
- the packer assembly 12 is representatively of the type known to those skilled in the art as a swellable packer, but other types of packers can incorporate the principles of this disclosure.
- a seal element 24 of the packer assembly 12 is extended radially outward into sealing contact with the wellbore 18 to seal off the annulus 14. This radial extension of the seal element 24 can be due to swelling of a swellable material in response to contact with a selected fluid.
- the term "swell” and similar terms are used herein to indicate an increase in volume of a swellable material.
- this increase in volume is due to incorporation of molecular components of an activating agent into the swellable material itself, but other swelling mechanisms or techniques may be used, if desired. Note that swelling is not the same as expanding, although a seal material may expand as a result of swelling.
- a seal element may be expanded radially outward by longitudinally compressing the seal element, or by inflating the seal element.
- the seal element is expanded without any increase in volume of the seal material of which the seal element is made.
- the seal element expands, but does not swell .
- the activating agent which causes swelling of the swellable material is in this example preferably a
- the swellable material swells when the fluid comprises the activating agent (e.g., when the fluid enters the wellbore 18 from a formation surrounding the wellbore, when the fluid is circulated to the packer assembly 12, when the fluid is released from a chamber carried with the packer assembly, etc.).
- the seal element 24 seals off the annulus 14 and can apply a gripping force to the
- the activating agent which causes swelling of the swellable material could be comprised in any type of fluid.
- the activating agent could be naturally present in the well, or it could be conveyed with the packer assembly 12,
- the swellable material may have a substantial portion of cavities therein which are
- the swellable material used in the well tool 12 swells by diffusion of hydrocarbons into the
- swellable material or in the case of a water swellable material, by the water being absorbed by a super-absorbent material (such as cellulose, clay, etc.) and/or through osmotic activity with a salt-like material.
- a super-absorbent material such as cellulose, clay, etc.
- Hydrocarbon-, water- and gas-swellable materials may be combined, if desired.
- predetermined activating agent may be used in keeping with the principles of this disclosure.
- the swellable material could also swell in response to contact with any of multiple activating agents.
- the swellable material could swell when contacted by hydrocarbon fluid and/or when contacted by water.
- one or more lines 26 extend longitudinally through the packer assembly 12.
- the lines 26 extend through the seal element 24 and end rings 28 which longitudinally straddle the seal element.
- the end rings 28 support the seal element 24 on the tubular string 16 and operate to minimize extrusion of the seal element through the annulus 14 as the seal element swells.
- the lines 26 may be electrical, hydraulic, optical, and/or any other type of lines.
- the lines 26 may be in the form of conduits, wires, cables, optic fibers (or other types of optical waveguides), flat packs, and/or in any other form.
- the lines 26 may be used for control signals, data transmission, communication, telemetry, and/or any other purpose.
- the packer assembly 12 may be used in the well system 10 and method described above, or it may be used in any other well system in keeping with the principles of this disclosure.
- FIG. 3 A cross-sectional view of the packer assembly 12 is illustrated in FIG. 3, and a further enlarged scale cross- sectional view of one of the end rings 28 is illustrated in FIG. 4. It may be seen in FIGS. 2-4 that this example of the packer assembly 12 includes the seal element 24 and end rings 28 on a base pipe 30, which is preferably provided with suitable end connections (not shown) for
- these components are aligned along a
- a flow passage 34 extends longitudinally through the base pipe 30, so that flow can be permitted through the passage, even when the seal element 24 seals off the annulus 14 surrounding the packer assembly 12.
- longitudinally extending channels 36 are provided in the seal element 24 for
- Slits 38 enable the lines 26 to be conveniently installed in the channels 36 from a side thereof (without having to feed the lines into the channels from their ends).
- channels 36 and slits 38 are provided in the example of FIGS. 2-4, and the channels are equally circumferentially spaced apart in the seal element 24.
- Each of the end rings 28 includes a body 40 which encircles and is secured to the base pipe 30.
- the body 40 could be secured to the base pipe 30 by means of fasteners (such as set screws 42 depicted in FIG. 9), or the body could be welded to the base pipe or attached thereto by other means .
- Each end ring 28 also includes one or more removable portions 44 which allow the lines 26 to be installed through the end ring from a side thereof (without having to feed the lines through openings 46 in the end ring from an end) .
- the openings 46 are aligned with the channels 36 in the seal element 24 , thereby enabling the lines 26 to be conveniently installed in the channels and openings from the side thereof as the tubular string 16 and packer assembly 12 are being run into the wellbore 18 .
- the removable portions 44 are attached to the end ring bodies 40 , thereby securing the lines to the packer assembly 12 .
- the packer assembly 12 is then positioned in the well, and the seal element 24 is swelled to seal off the annulus 14 . This swelling of the seal element 24 also causes the seal element to seal about the lines 26 in the channels 36 , thereby preventing leakage about the lines.
- the removable portions 44 are engaged with the end ring bodies 40 via longitudinally extending interlocking profiles 48 .
- the interlocking profiles are preferably created by wire-cutting (e.g., using electrical discharge machining) the removable portions 44 from the end ring bodies 40 , but other methods of forming the interlocking profiles may be used as desired.
- the interlocking profiles 48 are depicted in the drawings as having a J-shape, but other shapes may be used as desired.
- FIG. 5 a cross-sectional view of the packer assembly 12 is representatively
- one of the channels 36 has a rectangular shape, and the remaining channels have a circular shape.
- the rectangular channel 36 may be used for installation of a flat pack therein, and the other channels may be used for installation of cylindrical cables therein, but it should be understood that any combination of shapes may be used for the channels in keeping with the principles of this
- an end ring 28 is representatively illustrated apart from the remainder of the packer assembly 12.
- longitudinally extending leaves 50 are formed on the end ring body 40, and similar longitudinally extending leaves 52 are formed on the removable portions 44.
- a sleeve-shaped insert 54 is installed in the end ring body 40, radially inward from the leaves 50.
- the insert 54 also has longitudinally extending leaves 56 formed thereon.
- the leaves 50, 52, 56 radially outwardly overlie the ends of the seal element 24 (see, for example, FIG. 4).
- the leaves 50, 52, 56 are pivoted radially outward, so that they extend across the annulus 14 radially between the end ring 28 and the wellbore 18, thereby preventing extrusion of the seal element past the leaves.
- the insert leaves 56 are circumferentially offset relative to the leaves 50, 52 on the body 40 and removable portions 44, so that there are no circumferential gaps exposed between the leaves. In this manner, the leaves 50, 52, 56 form an unbroken wall to prevent extrusion of the seal element 24, even after the leaves have been pivoted radially outward by the swelling of the seal element.
- the insert 54 can be secured in the end ring 28 by adhesive bonding or other attachment means.
- the insert 54 could be a continuous cylindrical sleeve as depicted in FIG. 9 , or it could be made in multiple sections, as described for another example below. Referring additionally now to FIGS. 10-15, another example of the packer assembly 12 is representatively illustrated. In this example, the lines 26 are not equally circumferentially distributed in the seal element 24.
- the lines 26 are installed in a thickened side of the seal element 24 produced by an eccentric positioning of the seal element relative to the base pipe 30.
- FIG. 10 a cross-sectional view through the seal element 24 section of the packer assembly 12 is
- longitudinal axis 58 which is laterally offset relative to the longitudinal axis 32 of the base pipe 30 and the inner diameter of the seal element.
- This eccentric positioning of the seal element 24 outer diameter produces a thickened side 60 of the seal element.
- the lines 26 are installed in channels 36 in this thickened side 60.
- the lines 26 are not shown in FIG. 10 for clarity of illustration, but the lines would preferably be installed in the channels 36 in the manner described above for the example of FIGS. 2-9.
- FIG. 12 an isometric view of the end ring 28 with the portion 44 removed is representatively illustrated. In this view it may be seen that the insert 54 is
- the insert 54 is illustrated in FIG. 13.
- FIG. 14 the manner in which a section 54a of the insert 54 is attached to the removable portion 44 of the end ring 28 is illustrated. Note that this arrangement preserves the circumferential offset of the insert leaves 56 relative to the leaves 50, 52 on the body 40 and removable portion 44, so that no circumferential gaps are formed, even when the leaves are pivoted outward by swelling of the seal element 24.
- the section 54a of the insert 54 is depicted in FIG. 15, apart from the remainder of the end ring 28 and
- FIGS. 16-19 Another example is representatively illustrated in FIGS. 16-19.
- the openings 46 are shaped to accommodate two different sizes of flat pack lines 26.
- the lines 26 are positioned in a thickened side of the packer assembly 12 resulting from an eccentric outer diameter relative to an inner diameter of the packer
- FIG. 18 it may be seen that is example utilizes an insert 54 which has a generally cylindrical shape, but which is circumferentially split. A view of the insert 54 alone is provided in FIG. 19.
- end ring 28 examples are described above as including multiple unique features (e.g., the removable portions 44 and the leaves 50, 52, etc.), it should be clearly understood that any one or combination of these features could be included in an end ring within the scope of this disclosure, and it is not necessary for all of the unique features described above to be included in the end ring . It may now be fully appreciated that the above
- the examples of the packer assembly 12 described above have an end ring 28 which accommodates various types, numbers and spacings of lines 26, and which secures the lines using one or more removable portions 44. Extrusion of the seal element 24 in the annulus 14 is prevented by leaves 50, 52, 56 which pivot radially outward when the seal element 24 extends radially outward.
- the above disclosure provides to the art a packer assembly 12 for use in a subterranean well.
- the packer assembly 12 can include an annular seal element and at least one end ring 28 including leaves 50 formed on a body 40 of the end ring 28.
- the leaves 50 are biased radially outward when the seal element 24 extends radially outward.
- the seal element 24 may swell in response to contact with a selected fluid in the well.
- a removable portion 44 of the end ring 28 may be engaged with the end ring body 40 via interlocking profiles 48.
- the leaves 50 may overlie the seal element 24.
- the end ring 28 may also include an insert 54 with leaves 56 formed thereon.
- the insert leaves 56 can be circumferentially offset relative to the end ring body leaves 50.
- At least one line 26 can extend through the seal element 24 and the end ring 28.
- the line 26 may be
- the method can include positioning a circumferential series of leaves 50, 52 radially outwardly overlying an annular seal element 24 of a packer assembly 12, and the leaves 50, 52 pivoting radially outward in response to swelling of the seal element 24.
- the method can also include installing in the end ring body 40 an insert 54 with leaves 56 formed thereon, so that the insert leaves 56 are circumferentially offset relative to the end ring body leaves 50.
- the above disclosure also describes a packer assembly 12 for use in a subterranean well, with the packer assembly 12 comprising an annular seal element 24 which swells in response to contact with a selected fluid in the well.
- At least one end ring 28 includes a removable portion 44 thereof engaged with a body 40 of the end ring 28 via interlocking profiles 48.
Landscapes
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mining & Mineral Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Fluid Mechanics (AREA)
- Physics & Mathematics (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Earth Drilling (AREA)
- Mechanical Sealing (AREA)
- Gasket Seals (AREA)
- Consolidation Of Soil By Introduction Of Solidifying Substances Into Soil (AREA)
- Laying Of Electric Cables Or Lines Outside (AREA)
Abstract
Description
Claims
Priority Applications (9)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA2818831A CA2818831C (en) | 2010-12-10 | 2011-12-02 | Extending lines through, and preventing extrusion of, seal elements of packer assemblies |
MX2013006458A MX336448B (en) | 2010-12-10 | 2011-12-02 | Extending lines through, and preventing extrusion of, seal elements of packer assemblies. |
CN201180059317.7A CN103261572B (en) | 2010-12-10 | 2011-12-02 | Through the potted component of packer assembly and the extension pipeline preventing it from extruding |
AU2011338709A AU2011338709B2 (en) | 2010-12-10 | 2011-12-02 | Extending lines through, and preventing extrusion of, seal elements of packer assemblies |
EP11846448.6A EP2649269B1 (en) | 2010-12-10 | 2011-12-02 | Extending lines through, and preventing extrusion of, seal elements of packer assemblies |
RU2013130385/03A RU2571479C2 (en) | 2010-12-10 | 2011-12-02 | Lines routing via sealing elements of packer assembly and prevention of extrusion of said sealing elements |
DK11846448.6T DK2649269T3 (en) | 2010-12-10 | 2011-12-02 | EXTENDING LINES THROUGH, AND PREVENTING EXTRUSION OF, SEAL ELEMENTS OF PACKER ASSEMBLIES |
JP2013543225A JP5710780B2 (en) | 2010-12-10 | 2011-12-02 | Insertion of the line into the seal element of the packer assembly and prevention of extrusion of the line from the seal element of the packer assembly |
BR112013014212-0A BR112013014212B1 (en) | 2010-12-10 | 2011-12-02 | SHUTTER SET FOR USE IN AN UNDERGROUND WELL AND METHOD FOR SEALING A TUBULAR RING IN AN UNDERGROUND WELL |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12/965,513 US8596369B2 (en) | 2010-12-10 | 2010-12-10 | Extending lines through, and preventing extrusion of, seal elements of packer assemblies |
US12/965,513 | 2010-12-10 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2012078468A2 true WO2012078468A2 (en) | 2012-06-14 |
WO2012078468A3 WO2012078468A3 (en) | 2012-08-23 |
Family
ID=46198159
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2011/063077 WO2012078468A2 (en) | 2010-12-10 | 2011-12-02 | Extending lines through, and preventing extrusion of, seal elements of packer assemblies |
Country Status (12)
Country | Link |
---|---|
US (1) | US8596369B2 (en) |
EP (1) | EP2649269B1 (en) |
JP (1) | JP5710780B2 (en) |
CN (1) | CN103261572B (en) |
AU (1) | AU2011338709B2 (en) |
BR (1) | BR112013014212B1 (en) |
CA (1) | CA2818831C (en) |
DK (1) | DK2649269T3 (en) |
MX (1) | MX336448B (en) |
MY (1) | MY157015A (en) |
RU (1) | RU2571479C2 (en) |
WO (1) | WO2012078468A2 (en) |
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GB2504322B (en) * | 2012-07-26 | 2018-08-01 | Rubberatkins Ltd | Sealing apparatus and method therefore |
US8640770B1 (en) * | 2012-09-12 | 2014-02-04 | LB Enterprises, LLC | End ring for use with swell packers |
BR112015010755B1 (en) | 2013-02-06 | 2021-06-01 | Halliburton Energy Services, Inc | WELL PLUG, METHOD OF CONSTRUCTION OF A WELL PLUG FOR USE IN CEMENTING A PIPE IN A WELL AND METHOD OF CEMENTING A PIPE IN A WELL |
US9476281B2 (en) | 2013-06-20 | 2016-10-25 | Halliburton Energy Services, Inc. | High pressure swell seal |
CN105612309B (en) | 2013-11-14 | 2019-01-01 | 哈利伯顿能源服务公司 | window assembly with bypass limiter |
GB201400975D0 (en) * | 2014-01-21 | 2014-03-05 | Swellfix Bv | Downhole packer and associated methods |
US9303478B2 (en) | 2014-02-11 | 2016-04-05 | Weatherford Technology Holdings, Llc | Downhole tool and method for passing control line through tool |
US20180023366A1 (en) * | 2016-01-06 | 2018-01-25 | Baker Hughes, A Ge Company, Llc | Slotted Backup Ring Assembly |
US10364619B2 (en) | 2016-05-20 | 2019-07-30 | Alaskan Energy Resources, Inc. | Integral electrically isolated centralizer and swell packer system |
US10513921B2 (en) | 2016-11-29 | 2019-12-24 | Weatherford Technology Holdings, Llc | Control line retainer for a downhole tool |
US10689942B2 (en) | 2017-09-11 | 2020-06-23 | Baker Hughes, A Ge Company, Llc | Multi-layer packer backup ring with closed extrusion gaps |
US10907438B2 (en) | 2017-09-11 | 2021-02-02 | Baker Hughes, A Ge Company, Llc | Multi-layer backup ring |
US10907437B2 (en) | 2019-03-28 | 2021-02-02 | Baker Hughes Oilfield Operations Llc | Multi-layer backup ring |
US11142978B2 (en) | 2019-12-12 | 2021-10-12 | Baker Hughes Oilfield Operations Llc | Packer assembly including an interlock feature |
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-
2010
- 2010-12-10 US US12/965,513 patent/US8596369B2/en active Active
-
2011
- 2011-12-02 DK DK11846448.6T patent/DK2649269T3/en active
- 2011-12-02 JP JP2013543225A patent/JP5710780B2/en active Active
- 2011-12-02 BR BR112013014212-0A patent/BR112013014212B1/en active IP Right Grant
- 2011-12-02 MY MYPI2013001780A patent/MY157015A/en unknown
- 2011-12-02 EP EP11846448.6A patent/EP2649269B1/en active Active
- 2011-12-02 CA CA2818831A patent/CA2818831C/en active Active
- 2011-12-02 RU RU2013130385/03A patent/RU2571479C2/en active
- 2011-12-02 CN CN201180059317.7A patent/CN103261572B/en active Active
- 2011-12-02 AU AU2011338709A patent/AU2011338709B2/en active Active
- 2011-12-02 MX MX2013006458A patent/MX336448B/en unknown
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Title |
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See also references of EP2649269A4 |
Also Published As
Publication number | Publication date |
---|---|
MX2013006458A (en) | 2013-12-06 |
EP2649269A4 (en) | 2018-01-17 |
EP2649269B1 (en) | 2023-12-27 |
CA2818831C (en) | 2015-11-24 |
CN103261572B (en) | 2016-03-16 |
AU2011338709A1 (en) | 2013-06-06 |
JP2014502323A (en) | 2014-01-30 |
BR112013014212A2 (en) | 2016-09-13 |
RU2571479C2 (en) | 2015-12-20 |
WO2012078468A3 (en) | 2012-08-23 |
RU2013130385A (en) | 2015-01-20 |
JP5710780B2 (en) | 2015-04-30 |
MX336448B (en) | 2016-01-20 |
EP2649269A2 (en) | 2013-10-16 |
AU2011338709B2 (en) | 2014-06-12 |
US20120145412A1 (en) | 2012-06-14 |
MY157015A (en) | 2016-04-15 |
DK2649269T3 (en) | 2024-02-12 |
CA2818831A1 (en) | 2012-06-14 |
US8596369B2 (en) | 2013-12-03 |
BR112013014212B1 (en) | 2020-05-26 |
CN103261572A (en) | 2013-08-21 |
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