CN217139229U - Device for purifying diisopropyl ether - Google Patents
Device for purifying diisopropyl ether Download PDFInfo
- Publication number
- CN217139229U CN217139229U CN202123242162.0U CN202123242162U CN217139229U CN 217139229 U CN217139229 U CN 217139229U CN 202123242162 U CN202123242162 U CN 202123242162U CN 217139229 U CN217139229 U CN 217139229U
- Authority
- CN
- China
- Prior art keywords
- filter
- distillation
- diisopropyl ether
- collecting bottle
- connecting sleeve
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 238000004821 distillation Methods 0.000 claims abstract description 26
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- 238000001179 sorption measurement Methods 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 6
- 238000007789 sealing Methods 0.000 claims description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 238000005485 electric heating Methods 0.000 claims description 5
- 239000002574 poison Substances 0.000 claims description 2
- 238000000746 purification Methods 0.000 abstract description 11
- 230000001147 anti-toxic effect Effects 0.000 abstract description 5
- 238000009833 condensation Methods 0.000 abstract description 5
- 230000005494 condensation Effects 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 5
- 238000001914 filtration Methods 0.000 abstract description 5
- 239000003610 charcoal Substances 0.000 abstract description 2
- 239000007789 gas Substances 0.000 description 9
- 239000000126 substance Substances 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000002341 toxic gas Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a device for purifying diisopropyl ether, which comprises a distillation flask and a connecting sleeve, wherein a heating frame is arranged below the outer side of the distillation flask, and the connecting sleeve is arranged on the right side of the distillation flask; a collecting bottle is arranged on the right side of the connecting sleeve; and a filter is arranged at the top of the collecting bottle. The utility model discloses an install the filter, when the device is in the use, inside diisopropyl ether is in carrying out the distillation, through the condensation purification, gas after the purification will directly get into in the filter at collecting bottle top, under the effect on adsorption plate and antitoxic charcoal layer, directly filters the harmful gas in the gas, waits for gaseous complete filtration back after the processing is accomplished, again with liquid discharge, the effectual harmful gas who has solved traditional device and produce influences the healthy problem of staff.
Description
Technical Field
The utility model relates to a chemical purification technical field specifically is a be used for diisopropyl ether purification device.
Background
Diisopropyl ether belongs to toxic and harmful chemicals, and in view of the chemical property that the diisopropyl ether can be used for recovering individual chemicals and can be used as a solvent, the chemicals are generally poor in purity after synthesis, usually contain a plurality of impurities or can be mixed, and the chemicals can only be purified by a purifying device, so that the defects of the traditional purifying device are needed to be improved.
The diisopropyl ether purification device in the prior art has the following defects:
1. the existing purification device usually directly uses a flask lamp device to evaporate and purify diisopropyl ether through combustion of alcohol, and because the diisopropyl ether has toxicity due to chemical properties, exhausted gas can directly harm the health of workers during heating, and the device is not beneficial to the distillation and purification of the workers.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a be used for diisopropyl ether purification device to solve the problem that proposes among the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: a device for purifying diisopropyl ether comprises a distillation flask and a connecting sleeve, wherein a heating frame is arranged below the outer side of the distillation flask, and the connecting sleeve is arranged on the right side of the distillation flask;
a collecting bottle is arranged on the right side of the connecting sleeve;
the top of the collecting bottle is provided with a filter;
the bottom of the inner side of the filter is provided with a bearing net, the top of the bearing net is provided with an adsorption plate, the top of the adsorption plate is provided with an anti-poison carbon layer, and the top of the filter is provided with a net cover.
Preferably, the top of the distillation bottle is provided with a sealing cover.
Preferably, the condenser pipe is installed to the inboard of adapter sleeve, and the inlet outlet is installed at the both ends of condenser pipe, and two sets of sealing washers are installed to the outside of condenser pipe, and the sealing washer is located the outside of distillation flask and receiving flask.
Preferably, the front surface of the collecting bottle is provided with a liquid outlet, and the bottom of the collecting bottle is provided with a lifting seat.
Preferably, the inner side of the heating frame is embedded with an electric heating piece, the front of the heating frame is provided with a heater, the right side of the heater is provided with a connecting wire, and the front of the heater is provided with a control panel.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the utility model discloses an install the filter, when the device is in use, inside diisopropyl ether is when carrying out the distillation, through the condensation purification, gas after the purification will directly get into in the filter at collecting bottle top, under the effect on adsorption plate and antitoxic carbon layer, directly filter the harmful gas in the gas, wait for gaseous after filtering completely after processing is accomplished, again with liquid discharge, the effectual harmful gas who has solved traditional device and produce when using influences the problem that the staff is healthy.
2. The utility model discloses an install the condenser pipe, traditional device is when using, and direct through the glass tube structure install in the inboard as the condensation structure usually, and its condensation effect itself is relatively poor, and it is inside to add the condenser pipe with external comdenstion water through the inlet outlet to the quick diisopropyl ether with the vaporization condenses and is collected by the receiving flask on right side, has promoted the purification efficiency of device greatly.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention;
fig. 2 is a schematic view of the structure of the condenser tube of the present invention;
FIG. 3 is a schematic cross-sectional view of a filter according to the present invention;
fig. 4 is a schematic structural diagram of the heater of the present invention.
In the figure: 1. a distillation flask; 101. a sealing cover; 2. a condenser tube; 201. connecting sleeves; 202. a water inlet and outlet; 203. a seal ring; 3. a collection bottle; 301. a liquid discharge port; 302. a lifting seat; 4. a filter; 401. A carrying net; 402. an adsorption plate; 403. a poison-proof charcoal layer; 404. a net cover; 5. a heater; 501. a heating frame; 502. an electric heating sheet; 503. a connecting wire; 504. a control panel.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all, embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts belong to the protection scope of the present invention.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "connected" are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1, 2 and 4, the present invention provides an embodiment: a device for purifying diisopropyl ether;
the first embodiment is as follows: the device comprises a distillation bottle 1, a sealing cover 101 is installed at the top of the distillation bottle 1, a heating frame 501 is installed below the outer side of the distillation bottle 1, an electric heating sheet 502 is installed on the inner side of the heating frame 501 in an embedded mode, a heater 5 is installed on the front side of the heating frame 501, a connecting wire 503 is installed on the right side of the heater 5, a control panel 504 is installed on the front side of the heater 5, a connecting sleeve 201 is installed on the right side of the distillation bottle 1, a condenser pipe 2 is installed on the inner side of the connecting sleeve 201, water inlets and water outlets 202 are installed at two ends of the condenser pipe 2, two groups of sealing rings 203 are installed on the outer side of the condenser pipe 2, the sealing rings 203 are located on the outer sides of the distillation bottle 1 and the collecting bottle 3, the distillation bottle 1 is of a main body structure of the device, chemicals to be distilled are added into the interior through the sealing cover 101 at the top, the front heater 5 is connected with an external power supply through the connecting wire 503 on the right side, the electric heating sheet 502 which is electrified to drive to output heats the interior of the distillation bottle 1, the right side of the distillation flask 1 is connected with a collecting device through a connecting sleeve 201, the outside condensed water is heated in the condensing pipe 2 through the water inlet and outlet 202, and the outside sealing ring 203 can greatly increase the sealing effect of the device when the device is installed.
Referring to FIG. 1, a device for purifying diisopropyl ether;
example two: including adapter sleeve 201, receiving flask 3 is installed on adapter sleeve 201's right side, and leakage fluid dram 301 is installed in the front of receiving flask 3, and promotion seat 302 is installed to the bottom of receiving flask 3, and receiving flask 3 collects the liquid after the condensation with condenser pipe 2, can discharge through positive leakage fluid dram 301, and the promotion seat 302 of bottom can promote the height of receiving flask 3.
Referring to FIG. 3, a device for purifying diisopropyl ether;
example three: including adapter sleeve 201, filter 4 is installed at the top of receiving flask 3, carrier net 401 is installed to the bottom of filter 4 inboard, adsorption plate 402 is installed at carrier net 401's top, antitoxic carbon layer 403 is installed at adsorption plate 402's top, net lid 404 is installed at filter 4's top, the gas that produces after the distillation is accomplished will directly get into filter 4's inside, adsorb the toxic gas through adsorption plate 402 and antitoxic carbon layer 403 and filter, net lid 404 at rethread top after the filtration is with gas outgoing, the carrier net 401 of bottom can prevent that the material at top from droing.
The working principle is as follows: the utility model discloses when using, inside will need the distillated chemicals to add of sealed lid 101 at top, positive heater 5 is connected with external power supply through connecting wire 503 on right side, the circular telegram drives the electric heat piece 502 of output and heats retort 1 inside under the effect of heating frame 501, retort 1's right side is passed through adapter sleeve 201 and is connected with collection device, through inlet outlet 202 with external comdenstion water heating condenser pipe 2's inboard, the gas that produces after the distillation is accomplished will directly get into filter 4's inside, adsorb the filtration with toxic gas through adsorption plate 402 and antitoxic carbon layer 403, the net lid 404 at rethread top after the filtration is with gas outgoing.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein, and any reference signs in the claims are not intended to be construed as limiting the claim concerned.
Claims (5)
1. A device for purifying diisopropyl ether comprises a distillation flask (1) and a connecting sleeve (201), and is characterized in that: a heating frame (501) is arranged below the outer side of the distillation bottle (1), and a connecting sleeve (201) is arranged on the right side of the distillation bottle (1);
a collecting bottle (3) is arranged on the right side of the connecting sleeve (201);
the top of the collecting bottle (3) is provided with a filter (4)
The bottom of the inner side of the filter (4) is provided with a bearing net (401), the top of the bearing net (401) is provided with an adsorption plate (402), the top of the adsorption plate (402) is provided with an anti-poison carbon layer (403), and the top of the filter (4) is provided with a net cover (404).
2. The apparatus according to claim 1, wherein: and a sealing cover (101) is arranged at the top of the distillation flask (1).
3. The apparatus according to claim 1, wherein: condenser pipe (2) are installed to the inboard of adapter sleeve (201), and inlet outlet (202) are installed at the both ends of condenser pipe (2), and two sets of sealing washer (203) are installed in the outside of condenser pipe (2), and sealing washer (203) are located the outside of retort (1) and receiving flask (3).
4. The apparatus according to claim 1, wherein: the front surface of the collecting bottle (3) is provided with a liquid outlet (301), and the bottom of the collecting bottle (3) is provided with a lifting seat (302).
5. The apparatus according to claim 1, wherein: the electric heating piece (502) is installed in the inboard embedding of heating frame (501), and heater (5) are installed in the front of heating frame (501), and connecting wire (503) are installed on the right side of heater (5), and control panel (504) are installed in the front of heater (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123242162.0U CN217139229U (en) | 2021-12-22 | 2021-12-22 | Device for purifying diisopropyl ether |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123242162.0U CN217139229U (en) | 2021-12-22 | 2021-12-22 | Device for purifying diisopropyl ether |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN217139229U true CN217139229U (en) | 2022-08-09 |
Family
ID=82686412
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202123242162.0U Expired - Fee Related CN217139229U (en) | 2021-12-22 | 2021-12-22 | Device for purifying diisopropyl ether |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN217139229U (en) |
-
2021
- 2021-12-22 CN CN202123242162.0U patent/CN217139229U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20220809 |