CN1307082A - 长余辉无机发光材料的制备方法 - Google Patents
长余辉无机发光材料的制备方法 Download PDFInfo
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- CN1307082A CN1307082A CN 00100321 CN00100321A CN1307082A CN 1307082 A CN1307082 A CN 1307082A CN 00100321 CN00100321 CN 00100321 CN 00100321 A CN00100321 A CN 00100321A CN 1307082 A CN1307082 A CN 1307082A
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- 239000000463 material Substances 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910001868 water Inorganic materials 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 4
- 239000000126 substance Substances 0.000 claims abstract description 4
- 229910052693 Europium Inorganic materials 0.000 claims abstract description 3
- 229910052772 Samarium Inorganic materials 0.000 claims abstract description 3
- 229910052769 Ytterbium Inorganic materials 0.000 claims abstract description 3
- 238000004519 manufacturing process Methods 0.000 claims description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 4
- 238000000227 grinding Methods 0.000 claims description 4
- 229910052692 Dysprosium Inorganic materials 0.000 claims description 3
- 229910052779 Neodymium Inorganic materials 0.000 claims description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 3
- 239000004115 Sodium Silicate Substances 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 3
- -1 rare-earth ion Chemical class 0.000 claims description 3
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
- 229910052691 Erbium Inorganic materials 0.000 claims description 2
- 229910052689 Holmium Inorganic materials 0.000 claims description 2
- 239000004111 Potassium silicate Substances 0.000 claims description 2
- 229910052777 Praseodymium Inorganic materials 0.000 claims description 2
- 229910052775 Thulium Inorganic materials 0.000 claims description 2
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- 229910052796 boron Inorganic materials 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 229910052733 gallium Inorganic materials 0.000 claims description 2
- 229910052746 lanthanum Inorganic materials 0.000 claims description 2
- 229910052749 magnesium Inorganic materials 0.000 claims description 2
- 238000000643 oven drying Methods 0.000 claims description 2
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 claims description 2
- 229910052913 potassium silicate Inorganic materials 0.000 claims description 2
- 235000019353 potassium silicate Nutrition 0.000 claims description 2
- 229910052706 scandium Inorganic materials 0.000 claims description 2
- 229910052712 strontium Inorganic materials 0.000 claims description 2
- 229910052727 yttrium Inorganic materials 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 239000011593 sulfur Substances 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
- 238000002360 preparation method Methods 0.000 abstract description 8
- 230000002829 reductive effect Effects 0.000 abstract description 6
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract 1
- 229910052747 lanthanoid Inorganic materials 0.000 abstract 1
- 150000002602 lanthanoids Chemical class 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 15
- 239000000047 product Substances 0.000 description 13
- 238000001035 drying Methods 0.000 description 8
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
- 238000007873 sieving Methods 0.000 description 6
- 239000002245 particle Substances 0.000 description 5
- 238000010304 firing Methods 0.000 description 4
- 229910000018 strontium carbonate Inorganic materials 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 3
- 229910000019 calcium carbonate Inorganic materials 0.000 description 3
- 230000005284 excitation Effects 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 230000001376 precipitating effect Effects 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000006228 supernatant Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 150000004645 aluminates Chemical class 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000941 radioactive substance Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 150000003568 thioethers Chemical class 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 239000005084 Strontium aluminate Substances 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 235000005811 Viola adunca Nutrition 0.000 description 1
- 240000009038 Viola odorata Species 0.000 description 1
- 235000013487 Viola odorata Nutrition 0.000 description 1
- 235000002254 Viola papilionacea Nutrition 0.000 description 1
- 244000172533 Viola sororia Species 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229910001650 dmitryivanovite Inorganic materials 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- VQCBHWLJZDBHOS-UHFFFAOYSA-N erbium(III) oxide Inorganic materials O=[Er]O[Er]=O VQCBHWLJZDBHOS-UHFFFAOYSA-N 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- QZQVBEXLDFYHSR-UHFFFAOYSA-N gallium(III) oxide Inorganic materials O=[Ga]O[Ga]=O QZQVBEXLDFYHSR-UHFFFAOYSA-N 0.000 description 1
- 238000001033 granulometry Methods 0.000 description 1
- 229910001707 krotite Inorganic materials 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000004020 luminiscence type Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- LEDMRZGFZIAGGB-UHFFFAOYSA-L strontium carbonate Chemical compound [Sr+2].[O-]C([O-])=O LEDMRZGFZIAGGB-UHFFFAOYSA-L 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Landscapes
- Luminescent Compositions (AREA)
Abstract
Description
性能指标 | 实施例3 | SrAl4O7:Eu,Dy‡ |
发光亮度发光时间颗粒度D50 | 1506010~13μm | 1004030μm以上 |
性能指标 | 实施例4 | CaAl2O4:Eu,Nd$ |
发光亮度发光时间颗粒度D50 | 1604810~13μm | 1002035μm以上 |
Claims (6)
Priority Applications (1)
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---|---|---|---|
CN 00100321 CN1117134C (zh) | 2000-01-25 | 2000-01-25 | 长余辉无机发光材料的制备方法 |
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CN 00100321 CN1117134C (zh) | 2000-01-25 | 2000-01-25 | 长余辉无机发光材料的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN1307082A true CN1307082A (zh) | 2001-08-08 |
CN1117134C CN1117134C (zh) | 2003-08-06 |
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CN 00100321 Expired - Lifetime CN1117134C (zh) | 2000-01-25 | 2000-01-25 | 长余辉无机发光材料的制备方法 |
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CN (1) | CN1117134C (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007003102A1 (fr) | 2005-07-01 | 2007-01-11 | Sichuan Sunfor Light Co. Ltd | Materiau luminescent a remanence elevee comportant des substrats composes et son procede de fabrication |
CN1301308C (zh) * | 2004-01-16 | 2007-02-21 | 北京有色金属研究总院 | 一种高亮度铝酸盐长时发光材料及其制备方法 |
CN101429432B (zh) * | 2008-12-12 | 2011-11-16 | 江苏博睿光电有限公司 | 一种超细粒径高光效长余辉荧光粉及其制造方法 |
CN109652011A (zh) * | 2019-01-21 | 2019-04-19 | 广东工业大学 | 一种紫外-近红外吸收材料及其制备方法与应用 |
-
2000
- 2000-01-25 CN CN 00100321 patent/CN1117134C/zh not_active Expired - Lifetime
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1301308C (zh) * | 2004-01-16 | 2007-02-21 | 北京有色金属研究总院 | 一种高亮度铝酸盐长时发光材料及其制备方法 |
WO2007003102A1 (fr) | 2005-07-01 | 2007-01-11 | Sichuan Sunfor Light Co. Ltd | Materiau luminescent a remanence elevee comportant des substrats composes et son procede de fabrication |
EP1900789A4 (en) * | 2005-07-01 | 2009-09-09 | Sichuan Sunfor Light Co Ltd | LONG FLOATING LUMINESCENT MATERIAL WITH PREPARED SUBSTRATES AND ITS MANUFACTURING METHOD |
US7955523B2 (en) | 2005-07-01 | 2011-06-07 | Sichuan Sunfor Light Co., Ltd. | Long afterglow luminescent material with compounded substrates and its preparation method |
CN101429432B (zh) * | 2008-12-12 | 2011-11-16 | 江苏博睿光电有限公司 | 一种超细粒径高光效长余辉荧光粉及其制造方法 |
CN109652011A (zh) * | 2019-01-21 | 2019-04-19 | 广东工业大学 | 一种紫外-近红外吸收材料及其制备方法与应用 |
Also Published As
Publication number | Publication date |
---|---|
CN1117134C (zh) | 2003-08-06 |
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