CN107929170A - A kind of eucalyptus oil shampoo and its preparation method and application of pet - Google Patents

Abstract

The invention discloses a eucalyptus oil shampoo for pets and its preparation method and application. Sodium Sulfate, Lauryl Betaine, Diethanolamide Cocoate, Disodium EDTA, 20% Sodium Chloride Solution, Essence, Pearlescent Syrup, Carbomer, C12~13 Alcohol Lactate, Lemon Made with acid, deionized water. The eucalyptus oil shampoo for pets can effectively improve the cleaning power of pet hair, and help the traditional Chinese medicine ingredients in the shampoo to penetrate into the skin, so as to achieve the effect of sterilizing and removing mites, purifying skin and mucous membranes, and preventing hair loss. Keep the hair and skin moisturized for a long time without drying, and long-term use can also increase the skin resistance of pets.

Description

A kind of eucalyptus oil shampoo for pets and its preparation method and application

technical field

The invention relates to a eucalyptus oil shampoo for pets and its preparation method and application, in particular to a eucalyptus oil shampoo for pets, which has antibacterial, insecticidal and mite-killing properties, high cleanliness but can keep pet skin and hair moist and not dry for a long time, and can improve the quality of pets after long-term use. Shampoo for skin resistance and method for its preparation and use.

Background technique

With the rapid development of the economy, pets such as dogs and cats have become common companions in human life, and people pay more and more attention to the health of pets. In the United States, the largest pet country in the world, the largest pet food company for cats and dogs has an annual sales volume of US$5 billion. It is predicted that in the next few years, it will increase at an annual rate of more than 6%. Although my country's pet industry started only a dozen years ago, it is no longer a single pet transaction, but also includes pet grooming, pet medical treatment, pet clothing, etc. At this stage, the market potential of my country's pet economy can reach at least 15 billion yuan.

However, the health problems of pets are not optimistic, and skin diseases have become the biggest problem for owners. Clinically, there are parasitic skin diseases of dogs and cats, bacterial skin diseases, fungal skin diseases, allergic skin diseases, hormonal skin diseases, and metabolic skin diseases. After the disease develops, multiple mixed infections may occur, which may be caused by two or more pathogens. The treatment is complicated, the course of the disease is long, and the treatment effect is poor. Among the many causes of disease, parasitic dermatosis, fungal dermatosis, bacterial dermatosis and mixed dermatosis occur frequently. The common clinical parasitic skin diseases are mainly scabies, demodex and itchy ear mite; the pathogens that cause fungal skin diseases in dogs and cats include Microsporum canis, Trichophyton mentagrophytes and gypsum-like spores; bacterial 97.0% of the pathogenic bacteria of skin diseases are Staphylococcus intermedius, 2.5% are Staphylococcus aureus and Escherichia coli secondary infection, while the mixed infection is dominated by mites and fungal infections.

Traditional pet shampoos can only clean off the dirt on pets, and are difficult to kill dust mites. However, although shampoos using chemical insecticides can solve the problem of pet parasites, they cannot prevent pets from licking their skin, Drugs penetrate into the body through the skin to cause poisoning, and long-term use is also likely to cause drug resistance. CN102085163A discloses a mite-removing pet shampoo, which uses the mite-removing agent N,N-bis(3-aminopropyl) dodecylamine (Lonzabac 12.100) to act, although it can wash off the dirt and kill the pets. It can kill dust mites, but its effect is relatively single, and it cannot solve the defect of strong detergency but easy drying of pet skin and hair. CN1079776A discloses a special medicated detergent for dogs and cats. It is made from the insecticide harmless to humans and animals—Amitraz, and processed with auxiliary materials such as surfactants, fur protection agents, spices and pigments. It has the function of keeping pets The fur is clean, bright and soft. It can also kill mites, fleas and other skin parasites. It also has a certain therapeutic effect on fungal skin diseases. However, amitraz is used when the temperature is lower than 25°C. Slow, low efficacy, so it has certain limitations.

Based on the above analysis, a pet with obvious sterilization and mite removal effect, soft and non-irritating, strong cleaning power, can also prevent the water evaporation on the surface of the animal skin, keep the hair and skin moist and not dry, and can improve the skin resistance of pets after long-term use Shampoo with eucalyptus oil is urgently needed in the industry at present.

Contents of the invention

In view of the above deficiencies, the purpose of the present invention is to provide a pet product that is clean and antibacterial, insecticidal and acaricidal, soft and non-irritating, strong in cleaning power, keeps hair and skin moist and not dry, and can improve the skin resistance of pets after long-term use. Eucalyptus oil shampoo has preventive and auxiliary treatment effects on common skin diseases of dogs and cats.

In order to achieve the above object, the present invention adopts the following technical solutions. The amount of each component of the present invention is also obtained through a large amount of exploration by the inventor. The eucalyptus oil shampoo for pets prepared by the amount of each component within the following weight range It has the advantages of cleaning and inhibiting bacteria, eliminating insects and mites, soft and non-irritating, strong cleaning power, keeping hair and skin moist and not dry, and long-term use can improve pet skin resistance.

A kind of eucalyptus oil shampoo for pets mainly comprises the following raw materials in proportions by weight:

Eucalyptus oil 1~3 parts, sodium lauryl polyoxyethylene ether sulfate 10~20 parts, sodium lauryl sulfate 7~15 parts, lauryl betaine 6~20 parts, coconut acid diethanolamide 1~ 3 parts, 3~5 parts of disodium edetate, 0.1~0.9 parts of 20% sodium chloride solution, 0.1~0.3 parts of essence, 1~3 parts of pearl paste, 0.2~0.4 parts of carbomer, C12~13 0.3~0.7 parts of alcohol lactate, appropriate amount of citric acid, appropriate amount of deionized water.

Further, the eucalyptus oil shampoo also includes the following raw materials in parts by weight:

0.5-1 part of eclipta extract, 0.5-1 part of geranium extract, and 0.5-1 part of brewer's yeast powder.

Further, the eucalyptus oil shampoo consists of the following raw materials in parts by weight:

2 parts of eucalyptus oil, 0.5 parts of eclipse extract, 0.5 part of geranium extract, 0.5 part of brewer's yeast powder, 15 parts of sodium lauryl polyoxyethylene ether sulfate, 11 parts of sodium lauryl sulfate, lauryl beet 13 parts of alkali, 2 parts of coconut acid diethanolamide, 5 parts of disodium edetate, 0.5 parts of 20% sodium chloride solution, 0.2 parts of essence, 2 parts of pearl paste, 0.3 parts of carbomer, C12~13 0.5 parts of alcohol lactate, appropriate amount of citric acid, and 50 parts of deionized water.

Further, the extract of Eclipta chinensis is prepared by the following method:

Rinse the dried Eclipta chinensis with running water, remove and drain, cut into pieces, add to a blender and pulverize for 3-5 minutes, add 8 times the amount of 20% ethanol, extract 4-5 times, combine the extracts and filter, and then Ethanol was recovered from the filtrate under reduced pressure in a vacuum thin film evaporator, and concentrated to a relative density of 1.05-1.08 to obtain an extract of Eclipta chinensis.

Further, the geranium extract is prepared by the following method:

Take geranium for beating, add 3 to 5 times the amount, extract with distilled water at a temperature of 55 to 65°C for 3 to 5 hours, filter, and concentrate the filtrate to a relative density of 1.01 to 1.10 to obtain a geranium extract.

Further, the preparation method of eucalyptus oil shampoo for pets comprises the following steps:

(1) Weigh the prescribed amount of deionized water and heat it to 60°C~65°C in a beaker, add the prescribed amount of disodium edetate, lower the temperature to 40°C, and add sodium laurate polyoxyethylene ether sulfate in turn , Sodium lauryl sulfate, stir until completely dissolved, keep the temperature at 40°C, add lauryl betaine and coconut acid diethanolamide, stir evenly, keep the temperature at 40°C, add pearlescent slurry, 20% sodium chloride in turn solution;

(2) When the temperature drops to normal temperature, add eucalyptus oil, eclipta extract, geranium extract, brewer's yeast powder, then add C12~13 alcohol lactate, essence, carbomer in sequence, and use 50% citric acid solution Adjust the pH to 6.5~8.5, stir until the system is uniform, and let stand to get the finished product.

The present invention has the following beneficial effects:

1. The preparation process is simple, the material is widely obtained, the cost is low, the operability is strong, the environment is friendly, and it is suitable for industrialized promotion and application.

2. Effectively soften pet skin cuticles, purify skin and mucous membranes, and allow active ingredients in eucalyptus oil, rehmannia root and geranium to quickly penetrate into the skin, achieving antibacterial, mite removal, insecticidal, and calming effects, and at the same time form a skin protective film to accelerate skin healing. Metabolism, long-term prevention of the formation of insects and mites.

3. It does not contain silicone oil, guar gum and other substances, will not clog the pores of pets, and reduce symptoms such as hair loss and depilation. Under the joint action of eucalyptus oil and brewer's yeast powder, it locks the moisture on the skin and hair surface, so that pets can keep their hair soft and not knotted after shampooing. At the same time, various nutrients in brewer's yeast powder can restore the pet's hair. Gloss.

4. The formula and process of the present invention are inseparable and mutually synergistic, and are an indispensable integral process. Only under the formula and process conditions of the present invention can each raw material be well balanced, so that the eucalyptus oil and eclipta extract , geranium extract, and brewer's yeast powder synergistically achieve strong detergency, which can not only strengthen the skin's resistance, but also keep the skin and hair moist and not dry for a long time, and long-term use can also improve pet skin resistance.

Detailed ways

Below we will further elaborate the present invention in combination with specific embodiments.

Example 1

Eucalyptus shampoo for pets

(1) Preparation of Eclipta chinensis extract: Rinse the dry Eclipta chinensis with flowing water, remove and drain, cut into pieces, add to a blender and pulverize for 4 minutes, add 8 times the amount of 20% ethanol, extract 5 times, and combine The extract was filtered, and then the filtrate was recovered to ethanol under reduced pressure in a vacuum thin film evaporator, and concentrated to a relative density of 1.06 to obtain an extract of Eclipta chinensis.

(2) Preparation of geranium extract: take geranium and beat it, add 4 times the amount, extract with distilled water at a temperature of 60° C. for 4 hours, filter, and concentrate the filtrate to a relative density of 1.05 to obtain a geranium extract.

(3) Weigh 50kg of deionized water and heat it to 62.5°C in a beaker, add 5kg of disodium edetate, lower the temperature to 40°C, add 15kg of sodium laurate polyoxyethylene ether sulfate, 11kg of dodecyl Sodium sulfate, stir until completely dissolved, keep the temperature at 40°C, add 13kg of lauryl betaine and 2kg of cocoic acid diethanolamide, stir evenly, keep the temperature at 40°C, add 2kg of pearl paste, 0.5kg of 20% sodium chloride in turn solution;

(2) When the temperature drops to room temperature, add 2kg of eucalyptus oil, 0.5kg of eclipta extract, 0.5kg of geranium extract, 0.5kg of brewer's yeast powder, and then add 0.5kg of C12~13 alcohol lactate and 0.2kg of essence , 0.3kg carbomer, adjust the pH to 7.5 with 50% citric acid solution, stir until the system is uniform, and let stand to get the finished product.

Example 2

Eucalyptus shampoo for pets

The preparation process is the same as in Example 1, except that the shampoo is made from the following raw materials in proportions by weight:

Eucalyptus Oil 1kg, Sodium Laureth Sulfate 10kg, Sodium Lauryl Sulfate 7kg, Lauryl Betaine 6kg, Diethanolamide Cocoate 1kg, Disodium EDTA 3kg, 20% Chlorine Sodium chloride solution 0.1kg, essence 0.1kg, pearl paste 1kg, carbomer 0.2kg, C12~13 alcohol lactate 0.3kg, citric acid solution to adjust pH to 6.5, deionized water 60kg.

Example 3

Eucalyptus shampoo for pets

The preparation process is the same as in Example 1, except that the shampoo is made from the following raw materials in proportions by weight:

Eucalyptus oil 3kg, eclipse extract 1kg, geranium extract 1kg, beer yeast powder 1kg, sodium lauryl polyoxyethylene ether sulfate 20kg, sodium lauryl sulfate 15kg, lauryl betaine 20kg, coconut oil acid Diethanolamide 3kg, EDTA disodium 5kg, 20% sodium chloride solution 0.9kg, essence 0.3kg, pearl paste 3kg, carbomer 0.4kg, C12~13 alcohol lactate 0.7kg, citric acid solution Adjust the pH to 8.5, 40kg of deionized water.

Test example 1

Eucalyptus shampoo for pets (compared with Example 1 without adding brewer's yeast powder)

Test example 2

Eucalyptus oil shampoo for pets (compared with Example 1 without adding eucalyptus oil)

Performance Testing

The eucalyptus oil shampoos of Example 1 and each test example were selected for performance testing. The products were packaged and placed at 30-35°C for 2 weeks at a constant temperature, and then placed at 0-10°C for 24 hours. There was no change in the product. The skin care effect test is as follows: 50 2-year-old cats and 50 2-year-old dogs were randomly selected, and 100 pets were randomly divided into 5 groups, with 10 cats and 10 dogs in each group, using Example 1, Test Example 1, 2 pet shampoo for cleaning, once every 3 days, and continued use for 3 months. Observe the hair texture, decontamination rate, hair loss, and the probability of skin diseases in each group of pets after using the shampoo for 3 months. The results are shown in Table 1 .

Table 1 Product performance test data

.

It can be seen from Table 1 that long-term use of the pet shampoos of Examples 1 and 3 has the effect of smooth, moist and easy to comb the hair of pets, and is not easy to shed hair. The probability of skin diseases in pets after 3 months of use Neither exceed 10%. In Example 2, the Eclipta extract, geranium extract and brewer's yeast powder were removed, and the detergency after use was slightly lower than that of Examples 1 and 3, while the incidence of skin diseases was higher than that of Examples 1 and 3. Test Example 1 is difficult to comb after use, easy to knot, greasy on the second day, easy to shed hair in daily life, the effect is not as good as the worst decontamination effect, and the probability of skin disease is 30%, which is significantly lower than that of Example 1 and 3. In Test Example 2, the hair was slightly knotted after washing after use, it was easier to comb, and the hair was slightly shed in daily life. The hair was not greasy on the second day after use, and the incidence of skin diseases in 3 months was 40%. Although the cleanliness reached 85%, but the incidence of skin disease was the lowest among the five trials. It shows that only the addition of eucalyptus oil, eclipta extract, geranium extract and brewer's yeast powder can maintain the fluffy, soft and moist pet hair, and at the same time, it can promote the cleaning of pet skin pores, and it is not easy to shed hair , can also reduce the chance of animals suffering from skin diseases.

Insecticidal effect test

The eucalyptus oil shampoo of embodiment 1 and each test example adopts the standard drug dipping method to test its insecticidal effect, and first determines the approximate concentration range through a pre-test, and all pet shampoos are diluted in half with distilled water. There were 10 non-blood-sucking larvae of cattle ticks, and 3 replicates per treatment. Take 1ml of the diluted shampoo solution and add it to the non-blood-sucking larvae of the small bovine tick, soak for 5s~10min, suck out the drug, wipe off the diluted shampoo solution on the body surface of the tick with filter paper, and transfer it to a drying dish with water at the bottom, room temperature, relative humidity Keep it at 80~85%. After 24 hours, the death was observed. Use the following procedures to determine whether the dead ticks are not blood-sucking larvae: first, direct observation, the limbs of the tiny tick do not move; second, under the dissecting microscope, the limbs of the tiny tick cannot move; Even with slight contact, the activities of the limbs of the tiny bovine ticks cannot be seen. Mortality calculation formula: Mortality % = (number of dead ticks / number of test ticks) × 100%. See Table 2.

Table 2 The killing effect of each group of shampoo ratios on cattle ticks

.

As can be seen from Table 2, the death rate of ticks in embodiment 1 and test example 3 can reach more than 90%, and the insecticidal effect is remarkable. In embodiment 2, no eclipta extract, geranium extract and cerevisiae cerevisiae were added The worm mortality rate drops to 76.7%, slightly lower than embodiment 1 and 3. No brewer's yeast powder was added in Test Example 1, and the death rate of ticks was 80.0%, which was significantly lower than that of Examples 1 and 3. The death rate of ticks in Test Example 2 was 60.0%, which was also slightly lower than that of Test Example 1, indicating that Eucalyptus The addition of oil plays a vital role in the insecticidal effect. At the same time, the extract of eclipta, geranium and brewer's yeast powder can promote the metabolism of the skin, soften the cutin of the skin, and enhance the absorption of the drug by the skin. Indivisible formula.

In Vitro Antibacterial Test of Eucalyptus Oil Shampoo for Pets

Pick the revived and purified bacterial colonies on MacConkey medium in nutrient broth, culture at 37°C for 18 hours, and dilute the bacterial solution with sterile saline to the equivalent of 0.5 McFarland turbidimetric standard (1×10 ⁸ CFU/part), and finally diluted 10 times in sterile nutrient broth to 2×10 ⁵ CFU·part ^~1 . Precisely weigh the drug to be tested, put it into a polypropylene centrifuge tube, and make the concentration of the eucalyptus oil shampoo 62.48 mg/part. Add 100 μL of bacterial solution to each of the 1-8 wells of a sterile 96-well plate by the micro-broth method, and add 100 μL of nutrient broth to the 8 wells without adding bacterial solution. Then add 100 μL of the corresponding drug to be tested from 1 well, and make 2-fold dilutions to 7 wells. No drug is added to the 9 wells as the control well, and cultured at 37°C 90r/min for 18-24h, and 3 replicate experiments are done for each group.

After 18 hours, 10 μL of 0.25% TTC was added to each well, and the culture was continued for 2 hours. If there were viable bacteria, it would turn red to determine the MIC. After 18 hours, inoculate the wells without growing bacteria on the plate for another 24 hours, read and observe MBC.

The test results showed that: the MIC value of eucalyptus oil shampoo to Escherichia coli was 1.95mg/part, and the MBC value was 3.91mg/part; the MIC value of eucalyptus oil shampoo to Staphylococcus aureus was 0.98mg/part, and the MBC value was 1.95mg/part.

In Vitro Antifungal Test of Eucalyptus Oil Shampoo for Pets

Pick l pieces of Microsporum canis, Gypsumoidosporum and Trichomonas trichomonas colonies (approximately 1mm×1mm) from the preserved strain tube, put them into a sterilized mortar, add 0.5 parts of normal saline, and grind them into a fungal mixture. suspension, and then adjust the density of the bacterial solution to 1×10 ⁵ /part to 1×10 ⁶ /part with physiological saline. Each tube of the control tube and the test tube was inoculated with 1 platinum ear by streaking method, cultured in an incubator at 28°C, and the experimental results were observed every day. After 7 days of observation, use the presence or absence of bacterial growth as the judgment standard. Compared with the control group (normal colony growth), those with visible colony growth have no antibacterial effect, and the lowest concentration of the drug for those without colony growth is the minimum inhibitory concentration of the drug. (MIC). Inoculate the ungrown colony in the above culture into the liquid medium, continue to incubate for 12 days, and observe the experimental results every day. After observing for 12 days, if the liquid medium is turbid, it means that there is fungal growth, and the liquid medium is clear, which means that there is no fungal growth, and the concentration of still no fungal growth in the liquid medium is judged as the MFC of the drug.

The test results show that the eucalyptus oil shampoo for pets has a good inhibitory effect on three common fungal pathogens of skin diseases. 1.95mg/serving, 0.98mg/serving, MFC values are 1.95mg/serving, 3.91mg/serving, 1.95mg/serving respectively.

In Vitro Acaricidal Test of Eucalyptus Oil Shampoo for Pets

The eucalyptus oil shampoo for pets was prepared with deionized water to a concentration of 500 mg/part, and then diluted to 5 concentrations (500 to 31.25 mg/part, r = 2) in equal proportions, and distilled water was used as a control group. Pick itchy mite larvae and place them in small petri dishes (diameter 5cm), and randomly divide them into 6 groups, 20 in each group, with 3 repetitions. The experiment refers to the method of in vitro dipping and killing by Fichi et al., adding 10 µL of liquid medicine to each petri dish , and then culture all plates at 25°C and 75% relative humidity, and check for death by microscope after 12 hours.

The eucalyptus oil shampoo was diluted with distilled water to three concentrations of 500mg/part, 250mg/part, and 125mg/part, and distilled water was used as a control group. Pick itchy mite larvae and place them in small petri dishes (5 cm in diameter), and divide them into 4 groups randomly, 20 larvae in each group, with 3 repetitions, and then add 10 μL of each concentration of medicinal solution. Then all the plates were cultured at 25°C and 75% relative humidity, and the death of itchy mites was observed and recorded at regular intervals until all tested itchy mites died.

The test results show that: in the in vitro acaricidal activity test of eucalyptus oil shampoo for pets on rabbit itchy mite, the LC ₅₀ of eucalyptus oil shampoo on itchy mite for 12 hours is 75.86mg/part, and at the shampoo concentration of 500mg/part, it can be killed by dipping. When measuring its in vitro acaricidal activity against the larvae of the rabbit itch mite, the median lethal time is 5.23h for the LT ₅₀ . The eucalyptus oil shampoo for pets has a certain inhibitory and killing effect on isolated mites, and can be used for the prevention and treatment of mite diseases in dogs and cats.

Through the above tests, it is known that the eucalyptus oil shampoo for pets has obvious antibacterial effects on E. It has a certain inhibitory and killing effect, and can be used for the prevention and treatment of mite diseases in dogs and cats.

To sum up, the formula and process of the present invention are inseparable and mutually synergistic, and are an indispensable overall process. Only with the formula of the present invention, the pet shampoo can better soften pet skin cuticles, purify skin and mucous membranes, and let The active ingredients in eucalyptus oil, eclipta, and geranium quickly penetrate into the skin to achieve antibacterial, mite-removing, insecticidal, and calming effects. At the same time, it forms a skin protective film, accelerates skin metabolism, and prevents the formation of insects and mites for a long time. It should be understood that those skilled in the art can make improvements or changes based on the above description, and all these improvements and changes should belong to the protection scope of the appended claims of the present invention.

Claims (6)

1. a kind of pet eucalyptus oil shampoo, it is characterised in that the eucalyptus oil shampoo mainly includes the raw material of following weight：Eucalyptus 1 ~ 3 part of oil, 10 ~ 20 parts of sodium laureth sulfate, 7 ~ 15 parts of lauryl sodium sulfate, empgen BB 6 ~ 20 parts, 1 ~ 3 part of lauric acid amide of ethanol, 3 ~ 5 parts of disodium ethylene diamine tetraacetate, 0.1 ~ 0.9 part of 20% sodium chloride solution, essence 0.1 ~ 0.3 part, 1 ~ 3 part of pearlite slurry, 0.2 ~ 0.4 part of carbomer, C12 ~ 0.3 ~ 0.7 part of 13 alcohol lactate, appropriate citric acid, go from Sub- appropriate amount of water.

2. pet according to claim 1 eucalyptus oil shampoo, it is characterised in that the eucalyptus oil shampoo further includes following parts by weight Raw material：0.5 ~ 1 part of Eclipta prostrata extracting solution, 0.5 ~ 1 part of fish pelargonium extracting solution, 0.5 ~ 1 part of beer yeast powder.

3. pet according to claim 2 eucalyptus oil shampoo, it is characterised in that the eucalyptus oil shampoo by following parts by weight original Material composition：2 parts of eucalyptus oil, 0.5 part of Eclipta prostrata extracting solution, 0.5 part of fish pelargonium extracting solution, 0.5 part of beer yeast powder, lauryl polyoxy 15 parts of ethene ether sodium sulfate, 11 parts of lauryl sodium sulfate, 13 parts of empgen BB, 2 parts of lauric acid amide of ethanol, 5 parts of disodium ethylene diamine tetraacetate, 0.5 part of 20% sodium chloride solution, 0.2 part of essence, 2 parts of pearlite slurry, 0.3 part of carbomer, C12 ~ 13 0.5 part of alcohol lactate, appropriate citric acid, 50 parts of deionized water.

4. the pet eucalyptus oil shampoo according to Claims 2 or 3, it is characterised in that the Eclipta prostrata extracting solution is by as follows Method is made：Eclipta prostrata dry product is rinsed well with flowing clear water, pulls out and drains, stripping and slicing, adds and 3 ~ 5 points are crushed in mixer Clock, adds 8 times of 20% ethanol of amount, extracts 4 ~ 5 times, merge extracting solution and filter, then subtract filtrate in Vacuum film evaporation instrument Receipts ethanol is pushed back, it is 1.05 ~ 1.08 to be concentrated into relative density, obtains Eclipta prostrata extracting solution.

5. the pet eucalyptus oil shampoo according to Claims 2 or 3, it is characterised in that the fish pelargonium extracting solution is by as follows Method is made：Take fish pelargonium to be beaten, add 3 ~ 5 times of amounts, when temperature is that 55 ~ 65 DEG C of distillation flooding 3 ~ 5 is small, filter, filtrate is dense It is 1.01 ~ 1.10 to be reduced to relative density, and fish pelargonium extracting solution is made.

A kind of 6. preparation method according to any pet eucalyptus oil shampoo of claim 1 ~ 4, it is characterised in that the preparation Method comprises the following steps：

（1）The deionized water for weighing recipe quantity is heated to 60 DEG C ~ 65 DEG C in beaker, adds the ethylenediamine tetra-acetic acid two of recipe quantity Sodium, reduces temperature to 40 DEG C, sequentially adds laurate polyethenoxy ether sodium sulfate, lauryl sodium sulfate, stirs to completely molten Xie Hou, keeps 40 DEG C of temperature to add empgen BBs and lauric acid amide of ethanol, stirs evenly, keep 40 DEG C of temperature according to Secondary addition pearlite slurry, 20% sodium chloride solution；

（2）Treat that temperature is down to room temperature, add eucalyptus oil, Eclipta prostrata extracting solution, fish pelargonium extracting solution, beer yeast powder, then add successively Enter the alcohol lactate of C12 ~ 13, essence, carbomer, pH to 6.5 ~ 8.5 adjusted with 50% citric acid solution, stir it is uniform to system, it is quiet Finished product can be obtained by putting.