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CN106525612B - The construction method of polycarbonate sand stone concrete based on stretching and compression experiment - Google Patents

The construction method of polycarbonate sand stone concrete based on stretching and compression experiment Download PDF

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CN106525612B
CN106525612B CN201610846085.4A CN201610846085A CN106525612B CN 106525612 B CN106525612 B CN 106525612B CN 201610846085 A CN201610846085 A CN 201610846085A CN 106525612 B CN106525612 B CN 106525612B
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许英杰
高腾龙
张卫红
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Northwestern Polytechnical University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/32Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0001Type of application of the stress
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0017Tensile
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0019Compressive
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
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Abstract

The invention discloses a kind of construction methods of polycarbonate sand stone concrete based on stretching and compression experiment, and the construction method for solving existing polycarbonate constitutive model constructs the technical problem of constitutive model order of accuarcy difference.Technical solution is by the linear elasticity stage of polycarbonate, yielding stage, the description in strain softening stage and strain hardening stage, carry out a large amount of different strain rate, at a temperature of tensile and compression test and add unloading test, relevant parameter of its material model under ture stress-strain has been determined, particularly by add unloading test by the internal injury of material to mechanical property influence write-in constitutive model in;Reasonable optimization has been carried out to the parameter in model, ensure that the order of accuarcy of constitutive model while reducing number of parameters, meanwhile, also achieve the effective unified combination for stretching constitutive model and compressing constitutive model.

Description

基于拉伸及压缩实验的聚碳酸酯统一本构模型的构建方法A method for constructing a unified constitutive model of polycarbonate based on tensile and compressive experiments

技术领域technical field

本发明涉及一种聚碳酸酯本构模型的构建方法,特别涉及一种基于拉伸及压缩实验的聚碳酸酯统一本构模型的构建方法。The invention relates to a method for constructing a polycarbonate constitutive model, in particular to a method for constructing a polycarbonate unified constitutive model based on tensile and compression experiments.

背景技术Background technique

聚碳酸酯(polycarbonate,PC)作为一种典型的热塑性非晶聚合物,以其良好的耐冲击、高的比刚度和比强度以及透光性能,广泛的应用于航空航天、汽车高铁以及建筑等领域。由于航空航天以及高铁等聚碳酸酯制品的服役环境中包括了高温差,高速撞击,大的压强差等苛刻的服役条件,对聚碳酸酯的力学性能有着很高的要求,因此构建出其本构模型,更好的掌握其力学机理,不仅可以发挥其在各个领域的作用,还将会通过数值仿真来代替部分试验大幅度的减少行业的制造成本,带来更多的效益。Polycarbonate (PC), as a typical thermoplastic amorphous polymer, is widely used in aerospace, automobile, high-speed rail and construction due to its good impact resistance, high specific stiffness and specific strength, and light transmission properties. field. Since the service environment of polycarbonate products such as aerospace and high-speed rail includes harsh service conditions such as high temperature difference, high-speed impact, and large pressure difference, there are high requirements for the mechanical properties of polycarbonate. It can not only play its role in various fields, but also replace some tests through numerical simulation, which will greatly reduce the manufacturing cost of the industry and bring more benefits.

聚碳酸酯对应变率和温度具有很强的依赖性,同时,通过试验以及文献容易发现聚碳酸酯在拉伸和压缩的过程中,表现出不同的力学性能,其屈服强度,应变软化及硬化都有一定程度的不同。为了全面的表征聚碳酸酯的力学性能,有必要构建基于拉伸和压缩试验的统一本构模型。目前,国内外对聚碳酸酯统一本构模型的研究主要有以下两种:Polycarbonate has a strong dependence on strain rate and temperature. At the same time, it is easy to find through experiments and literature that polycarbonate exhibits different mechanical properties in the process of tension and compression, its yield strength, strain softening and hardening. are somewhat different. In order to comprehensively characterize the mechanical properties of polycarbonate, it is necessary to construct a unified constitutive model based on tensile and compressive tests. At present, the research on the unified constitutive model of polycarbonate at home and abroad mainly includes the following two:

文献1“Kan Cao,Yang Wang,Yu Wang.Experimental investigation andmodeling of the tension behavior of polycarbonate with temperature effectsfrom low to high strain rates,International Journal of Solids and Structures,2014,Vol.51(13),p2539-2548”中,通过不同温度、应变率下的拉伸试验,建立了基于其工程应力-应变曲线的本构模型。但是由于工程应力-应变曲线无法反应材料变形过程中的真实性能,因此在表征聚碳酸酯的应变硬化现象时显得不足。另一方面,聚碳酸酯在拉伸和压缩过程中所呈现出的不对称性,使得构建包括不同受力形式的本构模型显得尤为重要,该方法并未涉及到压缩的力学性能,因此在表征聚碳酸酯的受力过程中准确性不足。Literature 1 "Kan Cao, Yang Wang, Yu Wang. Experimental investigation and modeling of the tension behavior of polycarbonate with temperature effects from low to high strain rates, International Journal of Solids and Structures, 2014, Vol.51(13), p2539-2548" In , a constitutive model based on its engineering stress-strain curve was established through tensile tests at different temperatures and strain rates. However, because the engineering stress-strain curve cannot reflect the real properties of the material during deformation, it is insufficient in characterizing the strain hardening phenomenon of polycarbonate. On the other hand, the asymmetry exhibited by polycarbonate during tension and compression makes it particularly important to construct constitutive models including different stress forms. This method does not involve the mechanical properties of compression, so in the Insufficient accuracy in characterizing the stress process of polycarbonate.

文献2“Sai S.Sarva,Mary C.Boyce.Mechanics of Polycarbonate duringHigh-rate Tension.Journal of mechanics of materials and structures,2007,Vol.2(10),p1853-1880”进行了一系列的拉伸压缩试验,构建了聚碳酸酯包括线弹性、屈服、应变软化以及应变硬化阶段的本构模型。但是其在建模过程中涉及到众多的统计平均量,在试验确定参数过程中比较复杂,而且在运用连续介质力学解释本质的同时并没有考虑材料的内部损伤;同时,该模型使用了仿射网络理论来模拟分子网络的伸展,在模拟真实变形过程中聚合物材料链段之间的缠结与解缠现象存在一定的困难。Document 2 "Sai S.Sarva,Mary C.Boyce.Mechanics of Polycarbonate during High-rate Tension.Journal of mechanics of materials and structures, 2007, Vol.2(10), p1853-1880" carried out a series of tension-compression The constitutive model of polycarbonate including linear elasticity, yielding, strain softening and strain hardening stages is constructed. However, it involves a large number of statistical averages in the modeling process, which is more complicated in the process of determining parameters through experiments, and does not consider the internal damage of the material while using continuum mechanics to explain the essence; at the same time, the model uses affine Network theory is used to simulate the stretching of molecular networks, and it is difficult to simulate the entanglement and disentanglement between polymer material segments during the real deformation process.

以上现有的本构模型中难以准确描述聚碳酸酯变形的准确机理,因此无法高效、准确的表征其力学性能。The above existing constitutive models are difficult to accurately describe the exact mechanism of polycarbonate deformation, so its mechanical properties cannot be characterized efficiently and accurately.

发明内容SUMMARY OF THE INVENTION

为了克服现有聚碳酸酯本构模型的构建方法构建本构模型准确程度差的不足,本发明提供一种基于拉伸及压缩实验的聚碳酸酯统一本构模型的构建方法。该方法通过聚碳酸酯的线弹性阶段、屈服阶段、应变软化阶段以及应变硬化阶段的描述,进行大量的不同应变率、温度下的拉伸和压缩试验以及加卸载试验,确定了其材料模型在真实应力应变下的相关参数,尤其通过加卸载试验将材料的内部损伤对力学性能的影响写入本构模型中;对模型中的参数进行了合理的优化,减少参数数量的同时保证了本构模型的准确程度,同时,也实现了拉伸本构模型以及压缩本构模型的有效统一结合。In order to overcome the shortcomings of poor accuracy of the existing polycarbonate constitutive model building methods, the present invention provides a polycarbonate unified constitutive model building method based on tensile and compression experiments. Through the description of the linear elastic stage, yield stage, strain softening stage and strain hardening stage of polycarbonate, a large number of tensile and compressive tests at different strain rates and temperatures, as well as loading and unloading tests are carried out, and the material model is determined in this method. The relevant parameters under the true stress and strain, especially the influence of the internal damage of the material on the mechanical properties are written into the constitutive model through the loading and unloading test; the parameters in the model are reasonably optimized, and the number of parameters is reduced while ensuring the constitutive model. The accuracy of the model, and at the same time, it also realizes the effective and unified combination of the tensile constitutive model and the compression constitutive model.

本发明解决其技术问题所采用的技术方案:一种基于拉伸及压缩实验的聚碳酸酯统一本构模型的构建方法,其特点是包括以下步骤:The technical scheme adopted by the present invention to solve its technical problems: a method for constructing a polycarbonate unified constitutive model based on tensile and compression experiments, which is characterized by comprising the following steps:

(a)通过对聚碳酸酯进行拉伸或压缩试验得到其真实应力-应变曲线,根据其弹性阶段计算弹性模量E:(a) Obtain its true stress-strain curve by performing tensile or compressive tests on polycarbonate, and calculate the elastic modulus E according to its elastic stage:

式中,E是聚碳酸酯弹性模量,σ是试验所得的真实应力,ε是真实应变。where E is the elastic modulus of polycarbonate, σ is the true stress obtained from the test, and ε is the true strain.

(b)根据对聚碳酸酯所进行的拉伸和压缩试验数据,得到屈服应力与温度以及应变率之间的非线性关系,通过下式表示:(b) Based on the tensile and compressive test data of polycarbonate, the nonlinear relationship between yield stress and temperature and strain rate is obtained, which is expressed by the following formula:

式中,σy是聚碳酸酯的屈服应力,是试验过程中的等效应变率,Th是同系温度,K,Cr,Ct,m则是相关试验参数。where σ y is the yield stress of polycarbonate, is the equivalent strain rate during the test, Th is the homologous temperature, and K, C r , C t , and m are the relevant test parameters.

(c)根据相应的加卸载试验来确定材料内部损伤状况。并通过数据得到损伤与塑性应变之间的关系:(c) Determine the internal damage status of the material according to the corresponding loading and unloading tests. And the relationship between damage and plastic strain is obtained from the data:

其中,ω为聚碳酸酯的损伤变量,为等效塑性应变,Cω和x为试验相关参数。where ω is the damage variable of polycarbonate, is the equivalent plastic strain, and C ω and x are test-related parameters.

(d)对试验应变软化和应变硬化数据进行分析,整理可得真实应力与损伤变量、屈服应力和等效塑性应变之间的关系如下:(d) The experimental strain softening and strain hardening data are analyzed, and the relationships between the available true stress and damage variables, yield stress and equivalent plastic strain are as follows:

式中,σ为聚碳酸酯的真实应力,ω为损伤变量,σy是屈服应力,为等效塑性应变,Ch和γ则为相关参数。where σ is the true stress of polycarbonate, ω is the damage variable, σ y is the yield stress, is the equivalent plastic strain, and C h and γ are the relevant parameters.

(e)对统一本构模型中关于拉伸和压缩试验的各参数分别进行拟合求解,并将所得本构模型写入有限元软件进行模拟计算,将模拟所得应力应变曲线与试验真实应力应变曲线进行对比,验证该统一本构模型的正确性。(e) Fit and solve the parameters of the tensile and compressive tests in the unified constitutive model respectively, and write the obtained constitutive model into the finite element software for simulation calculation, and compare the stress-strain curve obtained from the simulation with the actual stress-strain of the test. The curves are compared to verify the correctness of the unified constitutive model.

本发明的有益效果是:该方法通过聚碳酸酯的线弹性阶段、屈服阶段、应变软化阶段以及应变硬化阶段的描述,进行大量的不同应变率、温度下的拉伸和压缩试验以及加卸载试验,确定了其材料模型在真实应力应变下的相关参数,尤其通过加卸载试验将材料的内部损伤对力学性能的影响写入本构模型中;对模型中的参数进行了合理的优化,减少参数数量的同时保证了本构模型的准确程度,同时,也实现了拉伸本构模型以及压缩本构模型的有效统一结合。The beneficial effects of the present invention are: the method can carry out a large number of tensile and compression tests and loading and unloading tests at different strain rates and temperatures through the description of the linear elastic stage, yield stage, strain softening stage and strain hardening stage of polycarbonate. , the relevant parameters of the material model under the true stress and strain are determined, especially the influence of the internal damage of the material on the mechanical properties is written into the constitutive model through the loading and unloading test; the parameters in the model are reasonably optimized, and the parameters are reduced. At the same time, the accuracy of the constitutive model is ensured, and the effective and unified combination of the tensile constitutive model and the compression constitutive model is also realized.

下面结合附图和具体实施方式对本发明作详细说明。The present invention will be described in detail below with reference to the accompanying drawings and specific embodiments.

附图说明Description of drawings

图1是本发明方法中屈服应力与拉伸环境温度的线性关系图。Figure 1 is a graph showing the linear relationship between yield stress and tensile ambient temperature in the method of the present invention.

图2是本发明方法中屈服应力与拉伸试验中的对数应变率间的双线性关系图。Figure 2 is a graph of the bilinear relationship between yield stress in the method of the present invention and logarithmic strain rate in a tensile test.

图3是本发明方法中拉伸试验中损伤变量同塑性应变之间的曲线图。Figure 3 is a graph of the damage variable versus plastic strain in a tensile test in the method of the present invention.

图4是本发明方法实施例中在25℃,应变率为0.1s-1的拉伸状态下统一本构模型所得曲线与真实应力应变曲线的对比图。4 is a comparison diagram of the curve obtained by the unified constitutive model and the true stress-strain curve in the tensile state at 25° C. and the strain rate of 0.1s −1 in the embodiment of the method of the present invention.

图5是本发明方法实施例中在25℃,应变率为4500s-1的拉伸状态下统一本构模型所得曲线与真实应力应变曲线的对比图。5 is a comparison diagram of the curve obtained by the unified constitutive model and the true stress-strain curve under the tensile state at 25° C. and the strain rate of 4500 s −1 in the embodiment of the method of the present invention.

具体实施方式Detailed ways

参照图1-5。本发明基于拉伸及压缩实验的聚碳酸酯统一本构模型的构建方法具体步骤如下:Refer to Figures 1-5. The specific steps of the construction method of the polycarbonate unified constitutive model based on the tensile and compression experiments of the present invention are as follows:

统一本构模型中的拉伸以及压缩参数并不相同,但是由于其试验方法和参数确定方法一致,下面仅针对聚碳酸酯在不同温度(-60-120℃)、不同应变率(0.0005s-1,0.001s-1,0.01s-1,0.1s-1,1400s-1,2000s-1,3500s-1,4500s-1)下的拉伸试验所得试验数据,进行相关参数的拟合,并将计算得到的结果与真实试验结果进行对比验证。The tensile and compressive parameters in the unified constitutive model are not the same, but due to the same test method and parameter determination method, the following is only for polycarbonate at different temperatures (-60-120°C) and different strain rates (0.0005s - 1 , 0.001s -1 , 0.01s -1 , 0.1s -1 , 1400s -1 , 2000s -1 , 3500s -1 , 4500s -1 ) under the tensile test data obtained, the relevant parameters were fitted, and The calculated results are compared with the real test results.

步骤1:通过准静态单轴拉伸试验,得出当前条件(25℃,0.01s-1)下聚碳酸酯的真实应力应变曲线,根据其线弹性阶段的数据计算其弹性模量:Step 1: Obtain the true stress-strain curve of polycarbonate under the current conditions (25°C, 0.01s -1 ) through a quasi-static uniaxial tensile test, and calculate its elastic modulus according to the data in its linear elastic stage:

式中,E是聚碳酸酯弹性模量,σ是试验所得的真实应力,ε是真实应变。where E is the elastic modulus of polycarbonate, σ is the true stress obtained from the test, and ε is the true strain.

步骤2:根据不同温度、应变率下拉伸试验数据,得到屈服应力与温度以及应变率之间的非线性关系,通过下式表示:Step 2: According to the tensile test data at different temperatures and strain rates, the nonlinear relationship between yield stress, temperature and strain rate is obtained, which is expressed by the following formula:

式中,σy是聚碳酸酯的屈服应力,是试验过程中的等效应变率,Th是同系温度,K,Cr,Ct,m则是相关试验参数,等效应变率以及同系温度Th通过下式来表示:where σ y is the yield stress of polycarbonate, is the equivalent strain rate during the test, Th is the homologous temperature, K, C r , C t , m are the relevant test parameters, and the equivalent strain rate And the homologous temperature T h is represented by the following formula:

其中,是应变增量的偏张量,T是试验中的环境温度,Tr是室温25℃,Tg则代表了聚碳酸酯的玻璃化转变温度,取值为150℃。图1和图2分别显示了拉伸状态下温度和应变率同屈服应力之间的关系,拉伸状态下,屈服应力随着温度的增加呈现出线性减小的趋势;同时,屈服应力随着应变率的增加展现出了双线性增加的规律。in, is the deviator of the strain increment, T is the ambient temperature in the test, Tr is the room temperature of 25°C, and Tg represents the glass transition temperature of polycarbonate, which is 150°C. Figures 1 and 2 show the relationship between temperature, strain rate and yield stress in tensile state, respectively. In tensile state, yield stress shows a linear decreasing trend with the increase of temperature; at the same time, yield stress increases with temperature. The increase in strain rate exhibits a bilinear increase.

步骤3:通过多次拉伸加卸载试验确定材料内部损伤状况。对于离散试验数据,损伤变量得以根据下式求得:Step 3: Determine the internal damage of the material through multiple tensile loading and unloading tests. For discrete test data, the damage variable can be derived from:

式中,ω为聚碳酸酯的损伤变量,E0是最初弹性模量,是加卸载过程中弹性模量的值。将计算得到的离散损伤变量数据进行整合,得到损伤与塑性应变之间的关系:where ω is the damage variable of polycarbonate, E 0 is the initial elastic modulus, is the value of the elastic modulus during loading and unloading. The calculated discrete damage variable data are integrated to obtain the relationship between damage and plastic strain:

其中,ω为聚碳酸酯的损伤变量,为等效塑性应变,Cω和x为试验相关参数。图3显示了损伤变量同塑性应变之间的关系,损伤变量与材料的塑性应变成指数函数的规律,起始阶段随塑性应变快速增加,而后趋势渐渐变的平缓。where ω is the damage variable of polycarbonate, is the equivalent plastic strain, and C ω and x are test-related parameters. Figure 3 shows the relationship between the damage variable and the plastic strain. The damage variable and the plastic strain of the material become an exponential function. The initial stage increases rapidly with the plastic strain, and then the trend gradually becomes gentle.

步骤4:对拉伸试验应力应变曲线中的应变软化和应变硬化数据进行分析,整理可得真实应力与损伤变量、屈服应力和等效塑性应变之间的关系如下:Step 4: Analyze the strain softening and strain hardening data in the stress-strain curve of the tensile test, and sort out the relationship between the true stress and damage variables, yield stress and equivalent plastic strain as follows:

式中,σ为聚碳酸酯的真实应力,ω为损伤变量,σy是屈服应力,为等效塑性应变,Ch和γ则为相关参数。where σ is the true stress of polycarbonate, ω is the damage variable, σ y is the yield stress, is the equivalent plastic strain, and C h and γ are the relevant parameters.

步骤5:将统一本构模型写入非线性有限元软件Ls-dyna中的子程序模块,建立与试验相同条件下的模型、约束及载荷。对模型进行数值模拟计算,将所得应力应变曲线与试验真实应力应变曲线进行对比,验证该统一本构模型的正确性。图4和图5分别显示了聚碳酸酯拉伸试样在应变率分别为0.1s-1,4500s-1,温度为25℃环境中的真实应力应变曲线的试验数据和仿真数据,应力应变曲线展现了明显的弹性、屈服、应变软化以及应变硬化阶段,计算结果与试验结果吻合良好,进一步证实了该统一本构模型的准确性。Step 5: Write the unified constitutive model into the subroutine module in the nonlinear finite element software Ls-dyna, and establish the model, constraints and loads under the same conditions as the test. The model is numerically simulated, and the obtained stress-strain curve is compared with the actual stress-strain curve of the test to verify the correctness of the unified constitutive model. Figures 4 and 5 show the experimental data and simulation data of the true stress-strain curves of polycarbonate tensile specimens at strain rates of 0.1s -1 , 4500s -1 , and temperature of 25°C, respectively, and stress-strain curves It shows obvious elastic, yielding, strain softening and strain hardening stages. The calculated results are in good agreement with the experimental results, which further confirms the accuracy of the unified constitutive model.

表1给出了在拉伸状态下,聚碳酸酯本构模型中的相关参数值。Table 1 gives the relevant parameter values in the polycarbonate constitutive model in the tensile state.

Claims (1)

1. A method for constructing a polycarbonate unified constitutive model based on a tensile or compression experiment is characterized by comprising the following steps:
(a) the actual stress-strain curve of the polycarbonate is obtained by carrying out a tensile or compression test on the polycarbonate, and the elastic modulus E is calculated according to the elastic stage:
wherein E is the elastic modulus of the polycarbonate, sigma is the real stress obtained by the test, and epsilon is the real strain;
(b) according to the tensile or compressive test data of the polycarbonate at different temperatures and strain rates, the nonlinear relation between the yield stress and the temperature and strain rate is obtained and is represented by the following formula:
in the formula, σyIs the yield stress of the polycarbonate,is the equivalent strain rate, T, in the course of the testhIs the temperature of the same system,
homologous temperature ThIs represented by the following formula
K,Cr,CtM is the relevant test parameter, where T is the test temperature, TrIs a reference temperature, TgIs the glass transition temperature of the polycarbonate;
(c) determining the internal damage condition of the material through a plurality of times of stretching or compressing loading and unloading tests; for discrete test data, the damage variable was found according to the following formula:
in the formula, ω is the damage variable of the polycarbonate, E0Is the initial modulus of elasticity of the polymer,is the value of the modulus of elasticity during loading and unloading; integrating the calculated discrete damage variable data to obtain the relation between the damage and the plastic strain:
wherein ω is a damage variable of the polycarbonate,for equivalent plastic strain, CωAnd x is a test-related parameter;
(d) the strain softening and strain hardening data in the tensile or compressive test stress-strain curve are analyzed and the relationship between the real stress and the damage variable, the yield stress and the equivalent plastic strain are obtained by sorting as follows:
wherein σ is the true stress of the polycarbonate, ω is the damage variable, σyIs the yield stress of the steel, and,for equivalent plastic strain, ChAnd gamma is the relevant parameter;
(e) and respectively carrying out fitting solution on each parameter related to a tensile test or a compression test in the unified constitutive model, writing the obtained constitutive model into finite element software for simulation calculation, comparing a stress-strain curve obtained by simulation with a real stress-strain curve of the test, and verifying the correctness of the unified constitutive model.
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