CN105326755B - Additive-free mung bean anti-acne maintenance face paper and its Green production method - Google Patents

Abstract

The invention relates to an additive-free mung bean acne-removing and maintenance facial mask paper and a green production method thereof, belonging to the cosmetics processing technology. Food-grade or medicinal and edible raw materials such as mung beans, pearls, pine pollen, lily, white fungus, honeysuckle, dried roses, lemon slices, and tangerine peel are carefully processed through continuous activation, high-pressure disintegration, and supercritical extraction; the product is not Contains flavors, colorings, and preservatives. The product has good sensory quality and heat-clearing and detoxifying, anti-inflammatory and antibacterial effects. It is suitable for people who need facial maintenance care and cosmetic needs, as well as skin disease patients for the treatment or relief of acne (pimples). The production process of the product has no pollution, no waste residue, waste steam and harmful substances are produced, realizing green production; the product has a refreshing and delicate flavor, safe and non-toxic. It is a new type of food grade mask paper. The production process of the present invention does not use any chemical reagents, does not add any drugs, does not add any hormones, and is safe without any toxic and side effects.

Description

Additive-free mung bean anti-acne maintenance mask paper and its green production method

technical field

The invention belongs to the technical field of cosmetics processing, in particular to a mung bean acne-removing and maintenance facial mask paper and a production method thereof.

Background technique

Mask is a carrier of facial skin care or beauty products. It is applied or pasted on the face for a certain period of time. When the beneficial substances in the maintenance or beauty products are absorbed by the skin, or the substances harmful to skin health on the skin surface are absorbed by the mask After adsorption, it can be removed by washing or peeling to achieve the purpose of facial skin maintenance or beautification. At present, there are many types and formulations of facial mask products, such as ointment, powder, cream, emulsion, and tear-off wet tissue masks based on materials such as non-woven fabrics, silk, and biological fibers. The beauty or maintenance principle of the mask is to use it to cover the face for a certain period of time to temporarily isolate the skin from the outside air and pollution, increase the temperature of the skin, expand the pores of the skin, promote the secretion and metabolism of sweat glands, and increase the oxygen content of the skin. Exclude epidermal cell metabolism products and accumulated oily substances, and at the same time, the moisture and beneficial ingredients in the mask penetrate into the stratum corneum of the epidermis, making the skin soft, naturally bright and elastic. Generally, masks are divided into four types: mud cream type, tear type, jelly type, and wet tissue type. In particular, the wet tissue facial mask is easy to use, effective, and easy to store. It is deeply loved by beauty lovers and quickly occupies a large share in the beauty product market. Because of its convenient storage and transportation and low transportation cost, it is also highly praised by manufacturers, so its consumption is huge. Among many facial skin diseases, the incidence of acne is relatively high, also known as acne and acne. In ancient Chinese medicine, it was called facial sores. It is a common and frequently-occurring disease in dermatology. acne". According to statistics, 95% of males and 85% of females have suffered from different degrees of acne in adolescence. Untimely or blind treatment will lead to more serious facial diseases, prolong the course of the disease, and even leave scars that are difficult to eradicate, affecting health and image, and bringing psychological shadows to young people. Acne is a chronic skin disease that occurs in the pilosebaceous glands, mostly in areas rich in sebaceous glands such as the head, face, neck, chest and back. Traditional medicine believes that the main cause of acne is due to overeating, fat, sweet and greasy, which leads to warm internal heat in the spleen and stomach, or accumulation of heat in the lung meridian, external exposure to wind evil, or excessive thinking, emotional agitation, irritability, accumulation of qi and blood It is caused by heat transformation, or digestive tract dysfunction, constipation, and imbalance of Ren Chong and stagnation on the face. Western medicine believes that acne is related to high levels of androgen in the human body, excessive sebum secretion, abnormal keratinization of the sebaceous duct epidermis to block hair follicle pores, local accumulation of sebum and poor excretion, and infection of Corynebacterium acnes (also known as Propionibacterium) causing inflammation of facial skin tissue And edema and other factors.

In addition to medication and reasonable diet for acne patients, some cosmetics with anti-acne function, especially facial mask products, are also popular with acne patients and beauty lovers because of their combination of treatment and maintenance and easy use. However, at present, most of the mask products for reducing or treating acne are added with drugs such as dexamethasone, chloramphenicol, metronidazole, aspirin, clindamycin, erythromycin, chloramphenicol, and even a large amount of hormones. , antibiotics; or add imidazolidinyl urea, polyethylene glycol, zinc oxide, propylene glycol, kaolin and other additives. Moreover, almost all preservatives are added. On the one hand, the skin will become drug-dependent, and long-term use will produce drug resistance; at the same time, the body will have adverse reactions due to excessive absorption of drugs or additives by the skin.

Contents of the invention

The invention provides an additive-free mung bean anti-acne maintenance facial mask paper and its green production method. The product uses mung beans, pearls, pine pollen, lily, honeysuckle, dried roses, lemons, and tangerine peel as main raw materials. Add any chemical additives, that is, all food-grade or medicinal and edible raw materials are carefully processed by activation, high-pressure disintegration, supercritical extraction, and low-temperature immersion; the product does not contain flavors, pigments, and preservatives. With anti-inflammatory and antibacterial effects, the product is suitable for skin disease patients of all walks of life and ages who need the treatment or relief of facial acne (acne), and can also meet the beauty needs of facial skin maintenance. The production process of the product has no pollution, no waste residue, waste steam and harmful substances are produced, realizing green production, and the product has a refreshing and delicate flavor, safe and non-toxic.

The technical scheme that the present invention takes is obtained by the raw materials and steps of the following parts by weight:

25-35 parts of mung beans, 3-5 parts of pearls, 2-3 parts of pine pollen, 1-3 parts of dried honeysuckle, 2-3 parts of dried roses, 1-2 parts of dried lilies, 1-2 parts of lemon slices, dried tangerine peel 1 to 2 parts, 0.1 to 0.5 parts of white fungus;

(1) Continuous activation and crushing of mung beans

Take the mature mung bean grains of the year and screen them to remove impurities, spray and wash them with cold water at 8-15°C, put them into a vortex scalding tank and scald them in water at 80-90°C for 3-5 seconds, and perform the first activation, then quickly remove them and put them into 29 Soak in ～35℃ water with aerobic reciprocating oscillation for 5～9 hours, then carry out the second activation treatment, the oscillation frequency is 30～80r/min, the air volume into the water is 1～3L/h, then spray and wash with flowing water, drain Dry the surface moisture, carry out the third activation treatment at 40-45°C, 3-5min microwave oscillation, then freeze-dry to a water content of 18-25%, and crush it to the active mung bean powder that can pass through a 60-100-mesh sieve. Bacteria storage, standby;

(2) Combined high-pressure disintegration of mung bean, pine pollen, and pearl powder

Crush the pearls to 80-100 mesh pearl powder for later use, then mix the pearl powder with the active mung bean powder and pine pollen obtained in step (1), adjust the water content to 24-30% by mass, and use a screw extruder at a pressure of 18 Rotary extrusion under the conditions of ~20MPa and temperature 102~120℃, so that the macromolecular substances and hard plant substances in the raw materials are disintegrated under high temperature and high pressure, which is conducive to the dissolution of active ingredients, and the extruded product is dried at low temperature to the moisture content 6-8%, pulverized to obtain a powder with a particle size of 80-100 mesh, stored aseptically, and used for later use;

(3) Activate and crush tremella, dried flowers, lemon slices and dried tangerine peel

White fungus and dried lily were soaked in cold water at 8-15°C for 5-10 hours and rehydrated, then washed, drained off the surface water, activated by microwave oscillation at 40-45°C for 5-8 minutes, and then freeze-dried to a water content of 6 ~8%, Lily is crushed to a powder that can pass through a sieve with an aperture of 60 to 100 mesh, stored aseptically, and used for later use; Tremella is crushed to a powder that can pass through a sieve with an aperture of 240 to 500 mesh, stored aseptically, and used for later use;

Dried roses, dried honeysuckle, lemon slices, and dried tangerine peel are cleaned and removed, and crushed to a powder that can pass through a 40-100 mesh aperture sieve. Add purified water to adjust the water content to 30-35%. Microwave vibration for activation treatment, then freeze-drying to a water content of 6-8%, crushing to a powder that can pass through a 60-100-mesh sieve, sterile storage, and standby;

(4) Supercritical extraction

Take the raw material powder prepared by the above steps, mix evenly, add the active ingredient extraction carrier agent, adjust the water content of the mixture to 28-40%, the carrier agent composition is purified water 96%, food grade 3° white vinegar 2%, concentration 30% 2% edible alcohol, then stir evenly, and conduct CO ₂ supercritical fluid extraction at 45-60°C, 25-45MPa, time 60-120min, CO ₂ flow rate 19-26L/h, and store the extract aseptically for later use;

(5) variable temperature extraction

Take the raffinate of step (4) out of the extraction kettle, add deionized water 5 to 15 times its mass, stir evenly, soak at 15 to 30°C for 1 to 3 days, then separate and filter to obtain The extract of the filter membrane with a pore size of 5-10 μm, aseptically stored, and used for later use; add 4-6 times the deionized water to the separated residue according to its mass ratio, stir evenly, and extract at 40-60°C for 30-60 minutes , leached at 60-90°C for 20-40 minutes, then separated and filtered to obtain an extract that can pass through a filter membrane with a pore size of 5-10 μm, stored aseptically, and used for later use;

(6) Blending, sterilization, impregnation

Mix the supercritical extract obtained in step (4) and the extract solution obtained in step (5) evenly under clean conditions, add white fungus powder, continue to stir evenly, and then sterilize at 130-135°C for 4-9s at ultra-high temperature instantaneously, Cool to 22-30°C, get the natural mung bean skin care solution for facial skin, store it in a sterile tank, put the aseptically treated natural silk mask paper into the above-mentioned mung bean care solution, and soak it under sterile conditions at 25-30°C After 2-6 hours, take it out, flatten it, and aseptically pack it in a watertight and airtight airtight packaging bag, which is the mung bean acne treatment mask paper product.

The product of the invention does not contain drugs and chemical additives, and is entirely composed of food raw materials, has the safety of food-grade products, has no toxic and side effects in long-term use, and does not produce drug dependence. Additive-free mung bean anti-acne maintenance facial mask paper, apply it on the face when using it, peel it off after 10-25 minutes, and wash the face with clean water. Long-term use has the functions of removing dirt, beautifying facial skin, anti-inflammatory and antibacterial, reducing acne, and lightening acne scars on the facial skin. At the same time, it can make the facial skin delicate and shiny.

The raw materials used in the present invention are all food-grade or medicinal-edible raw materials with heat-clearing and detoxifying, anti-inflammatory, anti-inflammatory and anti-viral effects, and long-term use without any toxic and side effects, specifically as follows:

Mung bean (Vigna radiata (Linn.) Wilczek.) belongs to the leguminous family, also known as green bean. It has been cultivated in China for more than 2,000 years. Now it is widely planted in East Asian countries, and a small amount is also planted in Africa, Europe, and the United States. China is one of the major exporters of mung beans. After testing, every 100g of mung beans contains 21.6 grams of protein, 0.8 grams of fat, 55.6 grams of carbohydrates, 6.4 grams of dietary fiber, 81 mg of calcium, 6.5 mg of iron, 2.18 mg of zinc, and 10.95 mg of vitamin E. Modern studies have shown that mung beans contain bioactive components such as flavonoids, tannins, saponins, alkaloids, phytosterols, coumarins, and cardiac glycosides. According to clinical experiment reports, mung bean has anti-allergic effect, has inhibitory effect on staphylococcus and certain viruses, can clear away heat and detoxify; mung bean has the effect of protecting liver and kidney. "Kaibao Materia Medica" records: "Mung beans are sweet, cold, and non-toxic. Enter the heart and stomach." It is more powerful than it. It also benefits qi, thickens the stomach, and clears the meridians. There is no taboo to take it for a long time. Surgical treatment of carbuncle and ulcer, there is an inner support to protect the heart, which is extremely effective." It can also "relieve all kinds of metal stones, arsenic, and vegetation. poison". Traditional Chinese medicine believes that mung beans are sweet in taste and cold in nature; they enter the heart and stomach meridian;

Tangerine peel: It is the peel of various citrus (Citrus chachiensis Hort.) such as Rutaceae plant Chazhi orange or Ou orange, containing hesperidin (Hesperidin), nobiletin (Nobiletin) and volatile oil. Spicy, sweet, cold in nature, enters the spleen and stomach meridian. It has the effects of lowering Qi, regulating the middle, reducing phlegm, and detoxifying alcohol. Indications for eating disorders, stagnation of qi and dampness, fullness and oppression in the chest and diaphragm, abdominal distension and pain, alcohol injury and thirst. According to modern medical research, orange peel contains hesperidin and vitamin P, which have anti-inflammatory and anti-allergic effects.

Lemon: The fruit of the evergreen small tree lemon (Citrun Limonia Osbeck) of the Rutaceae Citrus genus. Lemons are rich in citric acid, malic acid, sugars, hesperidin, naringin, vitamin C, vitamin B1, vitamin B2, niacin, calcium, phosphorus, iron and other nutrients. Lemon tastes sour, slightly sweet, mild and cold in nature, enters the liver and stomach meridian. It has the effects of resolving phlegm and relieving cough, promoting body fluid, invigorating the spleen, benefiting the liver, anti-sclerosis, anti-corruption, antibacterial and sterilizing, and increasing immunity. Indications of bronchitis, vitamin C deficiency, polydipsia, loss of appetite, Naxia embolism. Modern medical and nutritional studies have shown that lemon is a highly alkaline food with a strong antioxidant effect, which can promote the body's metabolism, promote liver detoxification, delay aging, scavenge free radicals, and inhibit skin pigmentation.

Lily: Edible lily is the underground bulb of lily, rich in starch, protein, fat, alkaloid, calcium, phosphorus, iron and other components, as well as functional ingredients such as lily saponin, deacylated lily saponin, β-D-glucopyranoside. Lily is sweet in taste, slightly bitter, slightly cold in nature, non-toxic, and enters the heart and lung meridians. It has the effects of nourishing the lungs and relieving cough, nourishing yin and clearing away heat, clearing the heart and calming the nerves, and facilitating defecation. It is often used in the treatment of diseases such as chronic cough due to lung deficiency, hemoptysis caused by overworked cough, residual heat from febrile diseases, restlessness and palpitation due to deficiency, insomnia and dreaminess.

Pearl powder: The medicinal use of pearls has a history of more than 2,000 years in China. Ancient medical books such as "Bielu of Famous Doctors" in the Three Kingdoms period, "Compendium of Materia Medica" in Liang Dynasty, "Haiyao Materia Medica" in Tang Dynasty, "Kaibao Materia Medica" in Song Dynasty, "Compendium of Materia Medica" in Ming Dynasty, and "Fu of Lei Gong Yao Xing" in Qing Dynasty are all relevant. The healing properties of pearls are well documented. "Compendium of Materia Medica" records that "pearl tastes salty, sweet and cold, non-toxic, calms the mind; pearls paint the face, making people moisturize and good color. ------ remove facial spots, stop diarrhea; remove children's frightened fever, soothe the soul; Stop spermatorrhea and white turbidity, relieve acne and treat toxins...make luster white, etc. "Compendium of Materia Medica" also records that pearls can reduce freckles and chloasma. Modern medical research has found that pearls contain a large amount of trace elements, which have the functions of anti-oxidation, enhancing skin activity, clearing away heat and detoxification, whitening, removing acne, and lightening spots. "Pharmacopoeia of the People's Republic of China" and "Dictionary of Traditional Chinese Medicine" record that pearls have the effects of calming the nerves, calming convulsions, improving eyesight, detoxifying and promoting muscle growth. Modern medical research shows that pearl powder has unique effects in improving human immunity, delaying aging, removing freckles, whitening, and supplementing calcium.

Pine pollen: Pine pollen is the sperm cells of pine stamens, also known as pine yellow, which is collected from the pure and dry pollen of Pinus massoniana Lamb. and Pinus tabulaeformis Carr., native tree species in my country. There is a record of "pine yellow" in the first pharmacopoeia "Shen Nong's Materia Medica" in Chinese history. Ancient medical books claim that pine pollen is "sweet, warm, and non-toxic", and has the functions of "moistening the heart and lungs, replenishing qi, dispelling wind and stopping bleeding, strengthening the face and benefiting the will". Ming • Li Shizhen "Compendium of Materia Medica": Songhua, sweet, warm, nontoxic. Moisten the heart and lungs, replenish qi, dispel wind and stop bleeding, and can also make wine. Pine pollen is non-toxic, has no side effects, and it has no sensitizing allergen substances, nor will it cause pollen allergic reactions. The "food therapy" recorded in the ancient book "Zhou Li" in the pre-Qin period of our country established the medical theory of "preventive treatment" of traditional Chinese medicine, and the "Diet Therapy Materia Medica" compiled by later generations used pine pollen to make soup, stuffing, steamed cakes, Brewing records. Modern medical independent research results also prove that pine pollen is non-toxic and harmless.

Pine pollen contains all the active nutrients needed by living organisms, including various proteins, amino acids, minerals, enzymes and coenzymes, nucleic acids, monosaccharides, polysaccharides, biotin, cellulose, unsaturated fatty acids, flavonoids, rutin, etc. The total content of active substances is more than 200 kinds, and the combination is reasonable, which can fully supplement and balance the nutrition needed by the human body. Pine pollen is rich in nutrients and functional ingredients, which can enhance skin metabolism, increase skin elasticity, delay skin aging, activate cells, remove free radicals, block the production of chloasma and butterfly spots, eliminate skin melanin, reduce and remove acne , making the skin white and beautiful.

Honeysuckle: Flos Lonicerae (La), Lonicera Lonicerae and the same genus of Lonicera and its dry flower buds or flowers, are native to China and distributed in various provinces. The name "Honeysuckle" comes from "Compendium of Materia Medica". Because the honeysuckle flowers are white at first and then turn yellow, it is named honeysuckle. It has been known as a good medicine for clearing away heat and detoxification since ancient times. "Shen Nong's Materia Medica" contains: "Honeysuckle is cold in nature and sweet in taste, has the effects of clearing heat and detoxification, cooling blood and removing stasis, and is mainly used for exogenous wind-heat, early blast, sore furunculosis, redness, swelling and pain, pus and blood in stool" and so on. "Compendium of Materia Medica" discusses in detail that honeysuckle has the effect of "long-term service, light body, prolong life". Honeysuckle is sweet and cold in nature and fragrant. It is sweet and cold in clearing away heat without hurting the stomach. Spots, pyretic sores, sore throat and other symptoms. Honeysuckle is cold in nature, sweet in taste, and enters the lung, heart, and stomach meridians. It has the effects of clearing heat and detoxifying, anti-inflammatory and anti-inflammatory, tonifying deficiency and treating wind, and is mainly used for swelling and lowering diseases, febrile diseases, fever, heat-toxin carbuncles, and tumors. It has a certain curative effect on enteritis, measles, pneumonia, meningitis, sepsis, skin infection, carbuncle and furuncle, erysipelas, mumps, suppurative tonsillitis and other diseases. Honeysuckle has been widely known for its medicinal value since ancient times.

Dried roses: Roses are native to China and have a long history of cultivation. They are Rosarugosa shrubs of the Rosaceae family. Roses are edible and rich in vitamin C. There are Swedish soup (Nyponsoppa), honey wine (Rhodomel). Roses contain rose essential oil, the main component of which is L-alcohol, which is used for food and cosmetics. The petals can be used to make cake fillings, rose wine, rose syrup, and can be used to make tea after drying. Roses are warm in nature, sweet in taste, slightly bitter, and return to the Liver and Spleen Channels. It has the effects of promoting qi, soothing the liver, relieving depression, harmonizing blood, and relieving pain. Indications of fullness in the chest and diaphragm, epigastric cavity, flank ribs, irregular menstruation, bruises, carbuncle and other diseases. "Food Materia Medica" said that it "mainly benefits the lungs and spleen, liver and gallbladder, and the food is fragrant and sweet, which makes people feel refreshed." Long-term consumption can reduce inflammation, eliminate fatigue, improve physical fitness, moisturize the skin, effectively remove free radicals, and eliminate pigmentation. Calmness, beauty, etc.

Tremella: alias white fungus, white ear, mulberry goose, Wudingzhi, white ear. Flat in nature, sweet in taste, light in taste, non-toxic. Return lung, stomach, kidney channel. It can nourish lung yin, relieve kidney dryness, refresh and replenish qi. It has the functions of nourishing body fluid, strengthening essence and kidney, nourishing yin, clearing heat and moistening lung, nourishing stomach, clearing intestine and moistening dryness, nourishing qi and blood, strengthening heart and body, nourishing brain and refreshing, beautifying and rejuvenating skin. Tremella also has the effects of relieving muscle fatigue, preventing radiation damage, and increasing immunity. Tremella polysaccharides and tremella spore polysaccharides contained in Tremella have anti-ulcer and anti-inflammatory effects.

The invention provides an additive-free mung bean anti-acne maintenance mask paper with heat-clearing, detoxifying, anti-inflammatory and anti-bacterial properties. The product uses mung beans, pearls, pine pollen, lilies, honeysuckle, roses, lemon slices, tangerine peel, and white fungus as raw materials without adding any medicine. , Additives, that is, all food-grade or medicinal and edible raw materials are carefully processed by activation, high-pressure disintegration, supercritical extraction and other processes; the product does not contain flavors, pigments, and preservatives. The products are suitable for skin disease patients of all walks of life and ages who need facial maintenance, beauty care, and acne (acne) treatment or relief. The production process of the product has no pollution, no waste residue, waste steam and harmful substances are produced, and green production is realized; the product has a refreshing flavor, is safe and non-toxic, and is a new type of safe food-grade mask for external application. The production process of the present invention does not use any chemical reagents, does not add any drugs, does not add any hormones, has the advantages of non-toxicity, pollution-free, convenient operation, etc., and has no toxic and side effects for long-term use.

detailed description

Example 1

Obtained by the following raw materials and steps in parts by weight:

25 parts of mung bean, 3 parts of pearl, 2 parts of pine pollen, 1 part of dried honeysuckle, 2 parts of dried rose, 1 part of dried lily, 1 part of lemon slice, 1 part of dried tangerine peel, 0.1 part of white fungus;

(1) Continuous activation and crushing of mung beans

Take the mature mung bean seeds of the year and screen to remove impurities, spray and wash them with cold water at 8°C, put them into a vortex scalding tank, soak them in 80°C water for 5 seconds, and perform the first activation, then quickly remove them and put them into 29°C water for aerobic reciprocating oscillation Soak for 9 hours, carry out the second activation treatment, the oscillation frequency is 30r/min, the amount of air introduced into the water is 1L/h, then spray and clean with running water, drain the surface water, and carry out the third activation treatment at 40°C and 5min with microwave Secondary activation treatment, freeze-drying to water content 18% then, pulverize to the active mung bean powder that can all pass through 60 mesh aperture sieves, aseptic storage, standby;

(2) Combined high-pressure disintegration of mung bean, pine pollen, and pearl powder

Pearls are crushed to 80 mesh pearl powder for later use, and then the pearl powder is evenly mixed with the active mung bean powder and pine pollen obtained in step (1), and the water content is adjusted to 24% by mass, and the screw extruder is used at a pressure of 18MPa and a temperature of 102°C Under the condition of rotary extrusion, the macromolecular substances and hard plant substances in the raw materials are disintegrated under high temperature and high pressure, which is conducive to the dissolution of active ingredients. The extruded product is dried at low temperature to a moisture content of 6%, and the particle size is 80 Purpose powder, sterile storage, standby;

(3) Activate and crush tremella, dried flowers, lemon slices and dried tangerine peel

Tremella and dried lilies were soaked in cold water at 8°C for 10 hours and rehydrated, then washed, drained off the surface water, and activated by microwave oscillation at 40°C for 8 minutes, then freeze-dried to a water content of 6%, and the lilies were crushed until they could pass through The powder of the 60-mesh aperture sieve is stored aseptically for subsequent use; the white fungus is crushed to the powder that can pass through a 240-mesh aperture sieve, and is stored aseptically for subsequent use;

Dried roses, dried honeysuckle, lemon slices, and dried tangerine peel are cleaned and removed, and crushed to a powder that can pass through a 40-mesh sieve. Add purified water to adjust the water content to 30%. Activate at 40°C for 8 minutes with microwave vibration, and then freeze Dried to a water content of 6%, crushed to a powder that can pass through a 60-mesh aperture sieve, stored aseptically, and set aside;

(4) Supercritical extraction

Take the raw material powder prepared by the above steps, mix evenly, add the active ingredient extraction carrier agent, adjust the water content of the mixture to 28%, and the carrier agent is composed of purified water 96%, food grade 3° white vinegar 2%, and a concentration of 30%. Alcohol 2%, then stir evenly, carry out CO ₂ supercritical fluid extraction at 45°C, 25MPa, time 120min, CO ₂ flow rate 19L/h, and store the extract aseptically for later use;

(5) variable temperature extraction

Take the raffinate of step (4) out of the extraction kettle, add deionized water 5 times its mass, stir evenly, soak at 15°C for 3 days, then separate and filter to obtain the extract that can pass through a filter membrane with a pore size of 5 μm. liquid, sterile storage, for use; add 4 times the deionized water to the separated residue according to its mass ratio, stir evenly, extract at 40°C for 60 minutes, and at 60°C for 40 minutes. Extraction solution, aseptic storage, standby;

(6) Blending, sterilization, impregnation

Mix the supercritical extract obtained in step (4) and the extract solution obtained in step (5) evenly under clean conditions, add white fungus powder, continue to stir evenly, then sterilize at 130°C for 9 seconds at ultra-high temperature, and cool to 22°C , the natural mung bean maintenance solution for facial skin was obtained and stored in a sterile tank, the aseptically treated natural silk mask paper was put into the above mung bean maintenance solution, immersed for 6 hours at 25°C under sterile conditions, taken out, flattened, and aseptic Packed in a water-tight and airtight airtight packaging bag, it is the mung bean anti-acne maintenance mask paper product.

Example 2

Obtained by the following raw materials and steps in parts by weight:

35 parts of mung beans, 5 parts of pearls, 3 parts of pine pollen, 3 parts of dried honeysuckle, 3 parts of dried roses, 2 parts of dried lilies, 2 parts of lemon slices, 2 parts of dried tangerine peel, 0.5 parts of white fungus;

(1) Continuous activation and crushing of mung beans

Take the ripe mung bean seeds of the year and screen to remove impurities, spray and wash them with cold water at 15°C, put them into a vortex scalding tank, soak them in 90°C water for 3 seconds, and perform the first activation, then quickly remove them and put them into 35°C water for aerobic reciprocating oscillation Soak for 5 hours, carry out the second activation treatment, the oscillation frequency is 80r/min, the air flow rate into the water is 3L/h, then spray and clean with running water, drain the surface water, and carry out the third activation treatment at 45°C and 3min with microwave Secondary activation treatment, then freeze-drying to 25% water content, crushing to the active mung bean powder that can all pass through a 100-mesh aperture sieve, aseptic storage, for subsequent use;

(2) Combined high-pressure disintegration of mung bean, pine pollen, and pearl powder

Pearls are crushed to 100 mesh pearl powder for later use, and then the pearl powder is evenly mixed with the active mung bean powder and pine pollen obtained in step (1), and the mass percentage of water content is adjusted to 30%, and the screw extruder is used at a pressure of 20MPa and a temperature of 120°C Under the condition of rotary extrusion, the macromolecular substances and hard plant substances in the raw materials are disintegrated under high temperature and high pressure, which is conducive to the dissolution of active ingredients. The extruded product is dried at low temperature to a moisture content of 8%, and the particle size is 100 Purpose powder, sterile storage, standby;

(3) Activate and crush tremella, dried flowers, lemon slices and dried tangerine peel

Tremella and dried lilies were soaked in cold water at 15°C for 5 hours and rehydrated, then washed, drained off the surface water, and activated by microwave oscillation at 45°C for 5 minutes, then freeze-dried to a water content of 8%, and the lilies were crushed until they could pass through The powder of 100-mesh aperture sieve is stored aseptically for subsequent use; Tremella is crushed to the powder that can pass through a 500-mesh aperture sieve, aseptically stored for subsequent use;

Dried roses, dried honeysuckle, lemon slices, and dried tangerine peel are cleaned and removed, and crushed to a powder that can pass through a 100-mesh sieve. Add purified water to adjust the water content to 35%. Activate at 45°C and microwave for 5 minutes, and then freeze Dried to a water content of 8%, crushed to a powder that can pass through a 100-mesh aperture sieve, stored aseptically, and set aside;

(4) Supercritical extraction

Take the raw material powder prepared by the above steps, mix evenly, add the active ingredient extraction carrier agent, adjust the water content of the mixture to 40%, the carrier agent is composed of purified water 96%, food grade 3° white vinegar 2%, concentration 30% edible Alcohol 2%, then stir evenly, carry out _CO2 supercritical fluid extraction at 60°C, 45MPa, time 60min, _CO2 flow rate 26L/h, the extract is stored aseptically, and used for later use;

(5) variable temperature extraction

Take the raffinate from step (4) out of the extraction kettle, add 15 times its mass of deionized water, stir evenly, soak at 30°C for 1 day, then separate and filter to obtain the extract that can pass through a filter membrane with a pore size of 10 μm. Liquid, aseptic storage, standby; add 6 times deionized water to the separated residue according to its mass ratio, stir evenly, extract at 60°C for 30 minutes, and at 90°C for 20 minutes, then separate and filter to obtain All the extracts that can pass through the filter membrane with a pore size of 10 μm are stored aseptically for later use;

(6) Blending, sterilization, impregnation

Mix the supercritical extract obtained in step (4) and the extract solution obtained in step (5) evenly under clean conditions, add white fungus powder, continue to stir evenly, then sterilize at 135°C and 4s ultra-high temperature instantaneously, and cool to 30°C , the natural mung bean maintenance solution for facial skin was obtained and stored in a sterile tank, the aseptically treated natural silk mask paper was put into the above mung bean maintenance solution, immersed for 2 hours at 30°C under sterile conditions, taken out, flattened, and aseptic Packed in a water-tight and airtight airtight packaging bag, it is the mung bean anti-acne maintenance mask paper product.

Example 3

Obtained by the following raw materials and steps in parts by weight:

30 parts of mung beans, 4 parts of pearls, 2.5 parts of pine pollen, 2 parts of dried honeysuckle, 2.5 parts of dried roses, 1.5 parts of dried lilies, 1.5 parts of lemon slices, 1.5 parts of dried tangerine peel, 0.3 parts of white fungus;

(1) Continuous activation and crushing of mung beans

Take the ripe mung bean seeds of the year and screen to remove impurities, spray and wash them with cold water at 11°C, put them into a vortex scalding tank and scald them in 85°C water for 4 seconds for the first activation, then quickly remove them and put them into 32°C water for aerobic reciprocating oscillation Soak for 7 hours, carry out the second activation treatment, the oscillation frequency is 55r/min, the air flow rate into the water is 2L/h, then spray and clean with running water, drain the surface water, and carry out the third activation treatment at 42.5°C and 4min microwave oscillation Secondary activation treatment, freeze-drying to water content 22% then, pulverize to the active mung bean powder that can all pass through 80 mesh aperture sieves, aseptic storage, standby;

(2) Combined high-pressure disintegration of mung bean, pine pollen, and pearl powder

Pearls are crushed to 90 mesh pearl powder for later use, and then the pearl powder is evenly mixed with the active mung bean powder and pine pollen obtained in step (1), and the water content mass percentage is adjusted to 27%, and the screw extruder is used at a pressure of 19MPa and a temperature of 111°C Under the condition of rotary extrusion, the macromolecular substances and hard plant substances in the raw materials are disintegrated under high temperature and high pressure, which is conducive to the dissolution of active ingredients. The extruded product is dried at low temperature to a moisture content of 7%, and the particle size is 90 Purpose powder, sterile storage, standby;

(3) Activate and crush tremella, dried flowers, lemon slices and dried tangerine peel

White fungus and dried lilies were soaked in cold water at 11°C for 8 hours and rehydrated, then washed, drained off the surface water, activated by microwave oscillation at 42.5°C for 7 minutes, then freeze-dried to a water content of 7%, and the lilies were crushed until they could pass through The powder of the 80-mesh aperture sieve is stored aseptically for subsequent use; the white fungus is crushed to the powder that can pass through the 380-mesh aperture sieve, and is stored aseptically for subsequent use;

Dried roses, dried honeysuckle, lemon slices, and dried tangerine peel are cleaned and removed, and crushed to a powder that can pass through a 60-mesh sieve. Add purified water to adjust the water content to 33%. Activate at 42.5°C for 7 minutes with microwave vibration, and then freeze Dried to a water content of 7%, crushed to a powder that can pass through an 80-mesh aperture sieve, stored aseptically, and set aside;

(4) Supercritical extraction

Take the raw material powder prepared by the above steps, mix evenly, add the active ingredient extraction carrier agent, adjust the water content of the mixture to 34%, and the carrier agent is composed of purified water 96%, food grade 3° white vinegar 2%, and a concentration of 30%. Alcohol 2%, then stir evenly, carry out CO ₂ supercritical fluid extraction at 52°C, 35MPa, time 90min, CO ₂ flow rate 23L/h, and store the extract aseptically for later use;

(5) variable temperature extraction

Take the raffinate from step (4) out of the extraction kettle, add 10 times the mass of deionized water, stir evenly, soak at 23°C for 2 days, then separate and filter to obtain the extract that can pass through a filter membrane with a pore size of 8 μm. Liquid, aseptic storage, for use; add 5 times deionized water to the separated residue according to its mass ratio, stir evenly, extract at 50°C for 45 minutes, and at 75°C for 30 minutes, then separate and filter to obtain All extracts that can pass through the 8μm pore size filter membrane should be stored aseptically for later use;

(6) Blending, sterilization, impregnation

Mix the supercritical extract obtained in step (4) and the extract solution obtained in step (5) evenly under clean conditions, add white fungus powder, continue to stir evenly, then sterilize at 133°C for 6 seconds at ultra-high temperature, and cool to 26°C , the natural mung bean maintenance solution for facial skin was obtained and stored in a sterile tank, the aseptically treated natural silk mask paper was put into the above mung bean maintenance solution, immersed for 4 hours at 27°C under sterile conditions, taken out, flattened, and aseptic Packed in a water-tight and airtight airtight packaging bag, it is the mung bean anti-acne maintenance mask paper product.

The present invention has a good effect through the crowd test, and the results are as follows:

Table 1 Test results of use effect of mung bean anti-acne maintenance mask paper without additives

Claims (2)

1. a kind of additive-free mung bean anti-acne maintenance face paper, it is characterised in that obtained by the raw material and step of following parts by weight 's：

25~35 parts of mung bean, 3~5 parts of pearl, 2~3 parts of pollen pini, honeysuckle are dry 1~3 part, 2~3 parts of dried rose flower, dried lily bulb 1~2 part, 1~2 part of lemon tablet, dry 1~2 part of dried orange peel, 0.1~0.5 part of white fungus, natural silk face paper；

（One）Mung bean continuously activation and crushing

Take and remove impurity when producing the screening of ripe mung bean seed per year, 8~15 DEG C of cold water spray washings are clean, be sent into vortex scalding groove in 3~5s of scalding in 80~90 DEG C of water, first time activation is carried out, then pulls aerobic reciprocating vibration in 29~35 DEG C of water of input out rapidly 5~9h to be soaked, carries out second of activation process, frequency of oscillation is 30~80r/min, and it is 1~3L/h that air capacity is passed through into water, Then circulating water cleaning showers, surface moisture is drained, third time activation process is carried out in 40~45 DEG C, 3~5min microwave oscillations, Then it is freeze-dried to water content 18~25%, being crushed to can be sterile all by the active mung bean flour of 60~100 mesh aperture sieves Storage, it is standby；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 80~100 mesh, then by pearl powder and step（One）The active mung bean flour of acquisition and Pollen pini is well mixed, and adjustment water content mass percent is 24~30%, using screw extruder in 18~20MPa of pressure, temperature Rotary extrusion under conditions of 102~120 DEG C of degree, make macromolecular substances in raw material and hard plant material composition in HTHP It is lower to be disintegrated, be advantageous to the dissolution of active ingredient, extrudate low temperature drying to moisture 6~8%, crushing obtains granularity and is 80~100 mesh powders, aseptic storage are standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 8~15 DEG C of 5~10h of cold water soak rehydrations, are washed out totally, dripping net surface moisture, Activation process is carried out in 40~45 DEG C, 5~8min microwave oscillations, is then freeze-dried to water content 6~8%, lily is crushed to can It is all standby by the powder of 60~100 mesh aperture sieves, aseptic storage；White fungus is crushed to can be all by 240~500 mesh holes The powder of footpath sieve, aseptic storage are standby；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 40~100 mesh aperture sieve Powder, adds pure water adjustment water content 30~35%, carries out activation process in 40~45 DEG C, 5~8min microwave oscillations, then To water content 6~8%, being crushed to can be all standby by the powder of 60~100 mesh aperture sieves, aseptic storage for freeze-drying；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjustment compound is aqueous Measure as 28~40%, guide and support agent composition be pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30%, then stir Uniformly, in 45~60 DEG C, 25~45MPa, 60~120min of time, CO₂19~26L/h of flow carries out CO₂Supercritical fluid extracts Take, extract aseptic storage is standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 5~15 times of its quality, stir, in 1~3d is impregnated under the conditions of 15~30 DEG C, then separate, be filtrated to get can all by the extract solution of 5~10 μm of bore filter films, Aseptic storage, it is standby；Dregs after separation are pressed to the deionized water of 4~6 times of its mass ratio addition, stirred, in 40~60 30~60min is extracted under the conditions of DEG C, 20~40min is extracted under the conditions of 60~90 DEG C, then separates, is filtrated to get and can all pass through The leaching liquor of 5~10 μm of bore filter films, aseptic storage are standby；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed, adds under the leaching liquor cleaning condition of acquisition White fungus powder, continue to stir, then in 130~135 DEG C, 4~9s ultra high temperature short time sterilizations, be cooled to 22~30 DEG C, obtain The natural mung bean curing fluid of skin of face is deposited in aseptic tank, and the natural silk face paper through aseptic process is put into above-mentioned mung bean In curing fluid, 2~6h is impregnated under 25~30 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, air-locked close In closure pack, as mung bean anti-acne conserves facial mask paper product.

2. a kind of Green production method of additive-free mung bean anti-acne maintenance face paper as claimed in claim 1, its feature exist Then obtained by the raw material and step of following parts by weight：

25~35 parts of mung bean, 3~5 parts of pearl, 2~3 parts of pollen pini, honeysuckle are dry 1~3 part, 2~3 parts of dried rose flower, dried lily bulb 1~2 part, 1~2 part of lemon tablet, dry 1~2 part of dried orange peel, 0.1~0.5 part of white fungus, natural silk face paper；

（One）Mung bean continuously activation and crushing

Take and remove impurity when producing the screening of ripe mung bean seed per year, 8~15 DEG C of cold water spray washings are clean, be sent into vortex scalding groove in 3~5s of scalding in 80~90 DEG C of water, first time activation is carried out, then pulls aerobic reciprocating vibration in 29~35 DEG C of water of input out rapidly 5~9h to be soaked, carries out second of activation process, frequency of oscillation is 30~80r/min, and it is 1~3L/h that air capacity is passed through into water, Then circulating water cleaning showers, surface moisture is drained, third time activation process is carried out in 40~45 DEG C, 3~5min microwave oscillations, Then it is freeze-dried to water content 18~25%, being crushed to can be sterile all by the active mung bean flour of 60~100 mesh aperture sieves Storage, it is standby；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 80~100 mesh, then by pearl powder and step（One）The active mung bean flour of acquisition and Pollen pini is well mixed, and adjustment water content mass percent is 24~30%, using screw extruder in 18~20MPa of pressure, temperature Rotary extrusion under conditions of 102~120 DEG C of degree, make macromolecular substances in raw material and hard plant material composition in HTHP It is lower to be disintegrated, be advantageous to the dissolution of active ingredient, extrudate low temperature drying to moisture 6~8%, crushing obtains granularity and is 80~100 mesh powders, aseptic storage are standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 8~15 DEG C of 5~10h of cold water soak rehydrations, are washed out totally, dripping net surface moisture, Activation process is carried out in 40~45 DEG C, 5~8min microwave oscillations, is then freeze-dried to water content 6~8%, lily is crushed to can It is all standby by the powder of 60~100 mesh aperture sieves, aseptic storage；White fungus is crushed to can be all by 240~500 mesh holes The powder of footpath sieve, aseptic storage are standby；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 40~100 mesh aperture sieve Powder, adds pure water adjustment water content 30~35%, carries out activation process in 40~45 DEG C, 5~8min microwave oscillations, then To water content 6~8%, being crushed to can be all standby by the powder of 60~100 mesh aperture sieves, aseptic storage for freeze-drying；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjustment compound is aqueous Measure as 28~40%, guide and support agent composition be pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30%, then stir Uniformly, in 45~60 DEG C, 25~45MPa, 60~120min of time, CO₂19~26L/h of flow carries out CO₂Supercritical fluid extracts Take, extract aseptic storage is standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 5~15 times of its quality, stir, in 1~3d is impregnated under the conditions of 15~30 DEG C, then separate, be filtrated to get can all by the extract solution of 5~10 μm of bore filter films, Aseptic storage, it is standby；Dregs after separation are pressed to the deionized water of 4~6 times of its mass ratio addition, stirred, in 40~60 30~60min is extracted under the conditions of DEG C, 20~40min is extracted under the conditions of 60~90 DEG C, then separates, is filtrated to get and can all pass through The leaching liquor of 5~10 μm of bore filter films, aseptic storage are standby；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed, adds under the leaching liquor cleaning condition of acquisition White fungus powder, continue to stir, then in 130~135 DEG C, 4~9s ultra high temperature short time sterilizations, be cooled to 22~30 DEG C, obtain The natural mung bean curing fluid of skin of face is deposited in aseptic tank, and the natural silk face paper through aseptic process is put into above-mentioned mung bean In curing fluid, 2~6h is impregnated under 25~30 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, air-locked close In closure pack, as mung bean anti-acne conserves facial mask paper product.