A kind of manufacture method of glazed tile and products thereof
Technical field
The present invention relates to Ceramic Tiles manufacturing field, more particularly, to a kind of manufacture method of glazed tile and products thereof.
Background technology
Glazed tile is also Full-glazed tile, is a kind of architectural pottery product emerging in recent years, and it has gathered polished bricks, modelled after an antique
The advantage of three kinds of brick, ceramics products, product release the implicit property of glazed tile cloudy colour half-light completely, solve half throwing brick and easily hide dirt
The defects of, possess glossiness, the porcelain hardness of polished bricks, while the high imitation fruit of the glaze paint for also possessing Antique Imitation Tiles, and ceramics
The abundant printing effect of glaze paint.Existing glazed tile is that to apply on decorative layer 0.5~1.5mm after printed decoration layer in adobe saturating
After bright glaze layer is fired, formed through elastic module rubbing down.Because transparent glaze layer is very thin, and use elastic module so that glazed layer with
Modular surface contact is not complete, brick face waveform is produced, in overall paving in use, beautiful decoration and associative perception can be influenceed.
Patent No. CN201310137879.X discloses a kind of production for the super flat Full-glazed tile for adding transparent microcrystal fine powder
Technique, comprise the following steps:Make base substrate, dedusting, water spray, leaching ground-coat enamel, stamp, print protection glaze, burn till brick body, polishing, waxing,
Pack, obtain finished product, wherein, transparent microcrystal is added to brick body after the print protection glaze step and before burning till step
Fine powder;The transparent microcrystal fine powder is printed onto in the form of powdered on brick body surface, and it is thin to form transparent microcrystal on brick body surface
Bisque;Or the transparent microcrystal fine powder is mixed with glue and added in the form of starchy on brick body surface.Because glazed tile with
The main distinction of Polished crystal tile is that the transparent glaze layer on surface is formed by being fired after micro-crystal powder cloth, or is printed by transparent glaze layer
Fire and form after brush, such as use transparent microcrystal fine powder to be printed onto in the form of powdered on brick body surface, then referred to as Polished crystal tile,
It is then glazed tile not to be, mixes with glue such as by transparent microcrystal fine powder and is added in the form of starchy on brick body surface, although
It can be carried out by drenching the form of glaze, but crystallite fine powder can not be dissolved completely in water, or adobe surface is present in graininess,
Thus it is equal to Polished crystal tile.
The content of the invention
It is an object of the invention to propose a kind of manufacture method of glazed tile, it can solve the problem that glazed tile surface wave shape wave
Problem.
To use following technical scheme up to this purpose, the present invention:
A kind of manufacture method of glazed tile, step include successively:
A, ceramic powder is suppressed to form adobe, controls adobe temperature to apply bottom in the adobe at 65-75 DEG C after drying
Glaze;
B, the stamp and after drying on the ground-coat enamel, control adobe temperature applies protection glaze more than 50 DEG C;
C, the biscuiting at 800-950 DEG C;
D, the adobe temperature is controlled to apply last layer clear frit more than 70 DEG C, then dry;
E, rubbing down is carried out after firing using non-resilient module.
The glaze volume for applying ground-coat enamel in the step A is 300-400g/m2。
The stamp in the step B includes the one or more in screen printing, roller printing, inkjet printing stamp
Combination.
The softening temperature of the protection glaze is 1070-1080 DEG C, and the softening temperature of the clear frit is 1100-1120 DEG C.
The glaze volume for applying protection glaze in the step B is 300-350g/m2。
The glaze volume for applying clear frit in the step D is 1000-1050g/m2。
Compared with prior art, protection glaze of the invention has the big characteristic of high temperature viscosity, and bottom gas can be prevented to arrange
Go out, so as to solve the defects of glaze paint pin hole recessed glaze, glaze is preferably absorbed by biscuiting adobe glaze paint and reduces glaze layer gas
Bubble, moisture organic matter volatilizees during biscuiting, and protection glaze softening range is 10 DEG C, relatively transparent glaze softening range 20
It is DEG C narrow, it can melt completely faster, and melted prior to clear frit, compacting is played to bottom gas in sintering procedure and is made
With, avoid base substrate gas evaporation formed stomata;And base substrate moisture is reduced, cracked even prevented also from sintering process
Fried base;Brick is more abundant in face of the absorption of glaze during leaching clear frit in addition, the recessed glaze of glaze layer can be also reduced, so as to solve serial life
Production. art stability problem, and ensure that the smooth of glaze paint, the product after firing and due to the protection glaze layer in printed layer
It is thicker and smooth with transparent glazed thickness thus non-resilient module can be used to carry out rubbing down so as to ensure that the super flat of its surface
And mirror effect.
It is another object of the present invention to propose a kind of glazed tile manufactured by the above method, it is from bottom to top wrapped successively
Include bottom base layer printed layer, protection glaze layer, transparent glaze layer.
The bottom base thickness degree is 6-9mm, and the printed layer thickness is to be less than 0.1mm, the protection glazed thickness
0.1-0.2mmmm, the transparent glazed thickness are 0.8-1.0mm.
Brief description of the drawings
Fig. 1 is the structure chart of the glazed tile of one of embodiment of the present invention.
Wherein:Bottom base layer 1, printed layer 2, protection glaze layer 3, transparent glaze layer 4.
Embodiment
Technical scheme is further illustrated below by embodiment.Its glaze of embodiments of the invention
Use commercially available Dow company glaze.
Embodiment 1
As shown in figure 1, a kind of glazed tile of the present embodiment, it from bottom to top includes bottom base layer 1, printed layer 2, protection successively
Glaze layer 3 and transparent glaze layer 4, its thickness of midsole base layer 1 are 8.5mm, and printed layer thickness is 0.05mm, and protection glazed thickness is
0.2mm, transparent glazed thickness are 0.8mm.
The glazed tile manufacture method that specification as described above is 1000*1000mm, step include successively:
A, ceramic powder is suppressed to form adobe, control adobe temperature applies 380g bottoms at 65 DEG C in the adobe after drying
Glaze forms bottom base layer 1;
B, printed layer 2 is formed after on the bottom base layer 1 after the step A by screen printing and drying, controls brick
Base temperature applies protection glaze 350g and forms protection glaze layer 3, the softening temperature for protecting glaze is 1070 DEG C, chemical composition Si at 55 DEG C:
70%, Al:13.7%, Ca:12.5%, Mg:1.24%, K:0.5%, Na:5.8%;
C, adobe enters kiln biscuiting at 900 DEG C;
D, control adobe temperature to apply the clear frit 1000g that one layer of softening temperature is 1100 DEG C again at 75 DEG C, then dry;
E, the adobe after the step D is entered after carrying out rubbing down using non-resilient module after kiln is fired at 1200 DEG C,
Packaging and storage.
Protection glaze in the present embodiment has the big characteristic of high temperature viscosity, bottom gas can be prevented to discharge, so as to solve
The defects of glaze paint pin hole recessed glaze, glaze is preferably absorbed by biscuiting adobe glaze paint and reduces glaze layer bubble, the mistake of biscuiting
Moisture organic matter is volatilized in journey, and protection glaze softening temperature is low, is first melted in sintering procedure, and compacting is played to bottom gas and is made
With, avoid base substrate gas evaporation formed stomata;And base substrate moisture is reduced, cracked even prevented also from sintering process
Fried base;Brick is more abundant in face of the absorption of glaze during leaching clear frit in addition, the recessed glaze of glaze layer can be also reduced, so as to solve serial life
Production. art stability problem, and ensure that the smooth of glaze paint, the product after firing and due to the protection glaze layer in printed layer
It is thicker and smooth with transparent glazed thickness thus non-resilient module can be used to carry out rubbing down so as to ensure that the super flat of its surface
And mirror effect.
Embodiment 2
As shown in figure 1, a kind of glazed tile of the present embodiment, it from bottom to top includes bottom base layer 1, printed layer 2, protection successively
Glaze layer 3 and transparent glaze layer 4, its thickness of midsole base layer 1 are 6mm, and printed layer thickness is 0.08mm, and protection glazed thickness is 0.1mm,
Transparent glazed thickness is 1.0mm.
The glazed tile manufacture method that specification as described above is 1000*1000mm, step include successively:
A, will feed proportioning ball milling carry out mist projection granulating after compacting form adobe, controlled after drying adobe temperature 75 DEG C
300g ground-coat enamels are applied in the adobe and form bottom base layer 1;
B, printed layer 2, control are formed by inkjet printing stamp on the bottom base layer 1 after the step A and after drying
Brickmaking base temperature applies protection glaze 300g and forms protection glaze layer 3, the chemical composition for protecting glaze is Si at 60 DEG C:58%, Al:13%,
Ca:12%, Mg:1.2%, K:0.6%, Na:6%, softening temperature is 1080 DEG C;
C, the adobe after the step B is entered into kiln biscuiting at 950 DEG C;
D, control adobe temperature to apply the clear frit 1050g that one layer of softening temperature is 1120 DEG C again at 78 degree, then dry;
E, the adobe after the step D is entered after carrying out rubbing down using non-resilient module after kiln is fired at 1200 DEG C,
Packaging and storage.
Protection glaze in the present embodiment has the big characteristic of high temperature viscosity, bottom gas can be prevented to discharge, so as to solve
The defects of glaze paint pin hole recessed glaze, glaze is preferably absorbed by biscuiting adobe glaze paint and reduces glaze layer bubble, the mistake of biscuiting
Moisture organic matter is volatilized in journey, and protection glaze softening temperature is low, is first melted in sintering procedure, and compacting is played to bottom gas and is made
With, avoid base substrate gas evaporation formed stomata;And base substrate moisture is reduced, cracked even prevented also from sintering process
Fried base;Brick is more abundant in face of the absorption of glaze during leaching clear frit in addition, the recessed glaze of glaze layer can be also reduced, so as to solve serial life
Production. art stability problem, and ensure that the smooth of glaze paint.
Embodiment 3
As shown in figure 1, a kind of glazed tile of the present embodiment, it from bottom to top includes bottom base layer 1, printed layer 2, protection successively
Glaze layer 3 and transparent glaze layer 4, its thickness of midsole base layer 1 are 9mm, and printed layer thickness is 0.06mm, and protection glazed thickness is
0.15mm, transparent glazed thickness are 0.9mm.
The glazed tile manufacture method that specification as described above is 1000*1000mm, step include successively:
A, will feed proportioning ball milling carry out mist projection granulating after compacting form adobe, controlled after drying adobe temperature 70 DEG C
400g ground-coat enamels are applied in the adobe and form bottom base layer 1;
B, printed layer 2 is formed after on the bottom base layer 1 after the step A by roller printing and drying, controls brick
Base temperature applies protection glaze 320g and forms protection glaze layer 3, the chemical composition for protecting glaze is Si at 55 DEG C:65%, Al:14%, Ca:
13%, Mg:1.3%, K:0.2%, Na:5.5%, softening temperature is 1070 DEG C;
C, the adobe after the step B is entered into kiln biscuiting at 850 DEG C;
D, control adobe temperature to apply the clear frit 1030g that one layer of softening temperature is 1110 DEG C again at 75 degree, then dry;
E, the adobe after the step D is entered after carrying out rubbing down using non-resilient module after kiln is fired at 1250 DEG C,
Packaging and storage.
Protection glaze in the present embodiment has the big characteristic of high temperature viscosity, bottom gas can be prevented to discharge, so as to solve
The defects of glaze paint pin hole recessed glaze, glaze is preferably absorbed by biscuiting adobe glaze paint and reduces glaze layer bubble, the mistake of biscuiting
Moisture organic matter is volatilized in journey, and protection glaze softening temperature is low, is first melted in sintering procedure, and compacting is played to bottom gas and is made
With, avoid base substrate gas evaporation formed stomata;And base substrate moisture is reduced, cracked even prevented also from sintering process
Fried base;Brick is more abundant in face of the absorption of glaze during leaching clear frit in addition, the recessed glaze of glaze layer can be also reduced, so as to solve serial life
Production. art stability problem, and ensure that the smooth of glaze paint.
Embodiment 4
As shown in figure 1, a kind of glazed tile of the present embodiment, it from bottom to top includes bottom base layer 1, printed layer 2, protection successively
Glaze layer 3 and transparent glaze layer 4, its thickness of midsole base layer 1 are 7.8mm, and the thickness of printed layer 2 is 0.03mm, and the protection thickness of glaze layer 3 is
0.18mm, the transparent thickness of glaze layer 4 are 0.8mm.
The glazed tile manufacture method that specification as described above is 1000*1000mm, step include successively:
A, will feed proportioning ball milling carry out mist projection granulating after compacting form adobe, controlled after drying adobe temperature 70 DEG C
370g ground-coat enamels are applied in the adobe and form bottom base layer 1;
B, formed by inkjet printing stamp and roller printing on the bottom base layer 1 after the step A and after drying
Printed layer 2, control adobe temperature apply protection glaze 340g and form protection glaze layer 3, the chemical composition for protecting glaze is Si at 55 DEG C:
60%, Al13.6%, Ca:12.6%, Mg:1.25%, K:0.4%, Na:5.8%, softening temperature is 1075 DEG C;
C, the adobe after the step B is entered into kiln biscuiting at 880 DEG C;
D, control adobe temperature to apply the clear frit 1010g that one layer of softening temperature is 1105 DEG C again at 75 DEG C, then dry;
E, the adobe after the step D is entered after carrying out rubbing down using non-resilient module after kiln is fired at 1250 DEG C,
Packaging and storage.
Protection glaze in the present embodiment has the big characteristic of high temperature viscosity, bottom gas can be prevented to discharge, so as to solve
The defects of glaze paint pin hole recessed glaze, glaze is preferably absorbed by biscuiting adobe glaze paint and reduces glaze layer bubble, the mistake of biscuiting
Moisture organic matter is volatilized in journey, and protection glaze softening temperature is low, is first melted in sintering procedure, and compacting is played to bottom gas and is made
With, avoid base substrate gas evaporation formed stomata;And base substrate moisture is reduced, cracked even prevented also from sintering process
Fried base;Brick is more abundant in face of the absorption of glaze during leaching clear frit in addition, the recessed glaze of glaze layer can be also reduced, so as to solve serial life
Production. art stability problem, and the smooth of glaze paint is ensure that, and non-resilient module can be used to carry out rubbing down, surfacing
Degree is high.
Embodiment 5:
A kind of Ceramic Tiles of the present embodiment, it includes bottom base layer 1, printed layer 2, transparent glaze layer 4 successively from bottom to top.
The Ceramic Tiles of the present embodiment are manufactured, its step includes successively:
A, will feed proportioning ball milling carry out mist projection granulating after compacting form adobe, controlled after drying adobe temperature 70 DEG C
370g ground-coat enamels are applied in the adobe and form bottom base layer 1;
B, formed by inkjet printing stamp and roller printing on the bottom base layer 1 after the step A and after drying
Printed layer 2;
C, clear frit 1010g is applied, is then dried;
D, the adobe after the step C is entered after carrying out rubbing down using elastic module after kiln is fired at 1250 DEG C, bag
Load storehouse.
The method of the present embodiment does not apply protection glaze, and carries out rubbing down using elastic module, and its product is due in sintering procedure
Gas is produced, breaks through transparent glaze layer, thus has the defects of pin hole, brick faces the incomplete absorption of clear frit, recessed glaze occurs, and make
Rubbing down is carried out with elastic module, brick face waveform inevitably occurs.
The technical principle of the present invention is described above in association with specific embodiment.These descriptions are intended merely to explain the present invention's
Principle, and limiting the scope of the invention can not be construed in any way.Based on explanation herein, the technology of this area
Personnel would not require any inventive effort the other embodiments that can associate the present invention, and these modes are fallen within
Within protection scope of the present invention.