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HomeJournal of Nano ResearchJournal of Nano Research Vol. 80Stabilized Bare Superparamagnetic Iron Oxide...

Stabilized Bare Superparamagnetic Iron Oxide Nanoparticles: Synthesis and Characterization

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Abstract:

Iron is a ubiquitous element found on Earth's crust, existing in various forms, such as Magnetite (Fe₃O₄) and Hematite (α-Fe₂O₃). Magnetic iron oxide nanoparticles (MIONPs) have become increasingly popular because they possess unique properties such as high surface area to volume ratio, super-paramagnetic properties, photocatalytic properties, and economical synthesis methods. This study produced MIONPs using the co-precipitation method, stabilized by a molybdenum magnet. Two soluble iron salts (FeCl₃.6H₂O and FeSO₄.7H₂O) were reacted with 5N NH₄OH solution at 80 °C in a nitrogen atmosphere. The MIONPs had a high saturation magnetization of 74.2emu/g, good crystallinity with crystalline spinel structured magnetite phase of iron oxide, high thermal stability depicted by 2.09 wt. % weight loss, and small particle sizes (6-25 nm). FTIR revealed a high-intensity peak at 546.28 cm^-1, attributed to the Fe-O stretching bond. Furthermore, the study showed that the co-precipitation method could be used to produce nanoparticles with a wide range of properties that could be used for various applications. It is a promising solution for producing stabilized magnetic nanoparticles since it uses non-toxic reagents and a straightforward, secure technique. Therefore, it may be used to synthesize nanoparticles for targeted treatment, magnetic resonance imaging, drug delivery, water treatment purposes and environmental remediation.

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Journal of Nano Research Vol. 80

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Periodical:

Journal of Nano Research (Volume 80)

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81-96

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https://doi.org/10.4028/p-f1ygDS

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Online since:

September 2023

Authors:

Evans K. Suter*, H.L. Rutto, Omwoyo N. Wesley, Musamba Banza

Keywords:

Co-Precipitation, Iron Oxide, Magnetic, Nanoparticles, Stabilized

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© 2023 Trans Tech Publications Ltd. All Rights Reserved

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