Search Results (45)

Peptides are an important class of biomolecules that perform many physiological functions and which occupy a significant and increasing share of the pharmaceutical market. Methods to determine the solid-state structures of peptides in different environments are important to help understand their biological functions and to aid the development of drug formulations. Here, a new magic-angle spinning (MAS) solid-state nuclear magnetic resonance (SSNMR) approach is described for the structural analysis of uniformly ¹³C-labeled solid peptides. Double-quantum (DQ) coherence between selective pairs of ¹³C nuclei in peptide backbone and side-chain CH₃ groups is excited to provide restraints on (i) ¹³C–¹³C internuclear distances and (ii) the relative orientations of C–H bonds. DQ coherence is selected by adjusting the MAS frequency to the difference in the resonance frequencies of selected nuclear pairs (the rotational resonance condition), which reintroduces the dipolar coupling between the nuclei. Interatomic distances are then measured using a constant time SSNMR experiment to eliminate uncertainties arising from relaxation effects. Further, the relative orientations of C–H bond vectors are determined using a DQ heteronuclear local field SSNMR experiment, employing ¹³C–¹H coupling amplification to increase sensitivity. These methods are applied to determine the molecular conformation of a uniformly ¹³C-labeled peptide, N-formyl-l-methionyl-l-leucyl-l-phenylalanine (fMLF). From just six distance and six angular restraints, two possible molecular conformations are determined, one of which is in excellent agreement with the crystal structure of a closely related peptide. The method is envisaged to a useful addition to the SSNMR repertoire for the solid-state structure determination of peptides in a variety of forms, including amyloid fibrils and pharmaceutical formulations. Full article

The rapid development of wireless power transfer (WPT) technology has provided new avenues for supplying continuous and stable power to capsule robots. In this article, we propose a two-dimensional omnidirectional wireless power transfer (OWPT) system, which enables power to be transmitted effectively in multiple spatial directions. This system features a three-dimensional transmitting structure with a Helmholtz coil and saddle coil pairs, combined with a one-dimensional receiving structure. This design provides sufficient internal space, accommodating patients of various body types. Based on the magnetic field calculation and finite element analysis, the saddle coil structure is optimized to enhance magnetic field uniformity; to achieve a two-dimensional rotating magnetic field, a phase difference control method for the excitation signal is developed through the analysis of circuit topology and quantitative synthesis of non-equivalent magnetic field vectors. Finally, an experimental prototype is built, and the experimental results show that the one-dimensional transmitting coil achieves a minimum received voltage stability of 94.5% across different positions. When the three-dimensional transmitting coils operate together, a two-dimensional rotating magnetic field in the plane is achieved at the origin, providing a minimum received power of 550 mW with a voltage fluctuation rate of 7.68%. Full article

This paper reports the successful application of a self-developed, miniaturized, low-power nano-star tracker for precise attitude measurement of a 5-m-long satellite extension boom. Such extension booms are widely used in space science missions to extend and support payloads like magnetometers. The nano-star tracker, based on a CMOS image sensor, weighs 150 g (including the baffle), has a total power consumption of approximately 0.85 W, and achieves a pointing accuracy of about 5 arcseconds. It is paired with a low-cost, commercial lens and utilizes automated calibration techniques for measurement correction of the collected data. This system has been successfully applied to the precise attitude measurement of the 5-m magnetometer boom on the Chinese Advanced Space Technology Demonstration Satellite (SATech-01). Analysis of the in-orbit measurement data shows that within shadowed regions, the extension boom remains stable relative to the satellite, with a standard deviation of 30′′ (1σ). The average Euler angles for the “X-Y-Z” rotation sequence from the extension boom to the satellite are [−89.49°, 0.08°, 90.11°]. In the transition zone from shadow to sunlight, influenced by vibrations and thermal factors during satellite attitude adjustments, the maximum angular fluctuation of the extension boom relative to the satellite is approximately ±2°. These data and the accuracy of the measurements can effectively correct magnetic field vector measurements. Full article

Among the more than 60 sources observed in the first two years of operations, IXPE addressed four magnetars, neutron stars believed to host ultra-strong magnetic fields. We report here the main implication coming from IXPE measurements for the physics of magnetars. Polarimetric observations confirmed the expectations of high polarization degrees, up to ≈$80\%$, values which have not been detected in any other source so far, providing further proof (independent from the P-$\dot{P}$ estimate) that magnetars host indeed ultra-magnetized neutron stars. Polarization measurements also indicate that softer X-rays likely come from surface regions where the overlying atmosphere underwent magnetic condensation. The agreement of the phase-dependent polarization angle with a simple rotating vector model strongly supports the presence of vacuum birefringence around the star. Full article

X-ray polarization, which now can be measured by the Imaging X-ray Polarimetry Explorer (IXPE), is a new probe of jets in the supermassive black hole systems of active galactic nuclei (AGNs). Here, we summarize IXPE observations of radio-loud AGNs that have been published thus far. Blazars with synchrotron spectral energy distributions (SEDs) that peak at X-ray energies are routinely detected. The degree of X-ray polarization is considerably higher than at longer wavelengths. This is readily explained by energy stratification of the emission regions when electrons lose energy via radiation as they propagate away from the sites of particle acceleration as predicted in shock models. However, the 2–8 keV polarization electric vector is not always aligned with the jet direction as one would expect unless the shock is oblique. Magnetic reconnection may provide an alternative explanation. The rotation of the polarization vector in Mrk421 suggests the presence of a helical magnetic field in the jet. In blazars with lower-frequency peaks and the radio galaxy Centaurus A, the non-detection of X-ray polarization by IXPE constrains the X-ray emission mechanism. Full article

This paper examines the relationship between the magnetization behavior and crystal lattice orientations of Fe–Si alloys intended for magnetic applications. A novel approach is introduced to assess anisotropy of the magnetic losses and first magnetization curves. This method links the magnetocrystalline anisotropy energy of single crystal structures to the textures of polycrystalline materials through a vectorial space description of the crystal unit cell, incorporating vectors for external applied field and saturation magnetization. This study provides a preliminary understanding of how texture influences magnetic loss rates and the first magnetization curves. Experimental results from Electron Back-Scattered Diffraction (EBSD) and Single-Sheet Tests (SSTs), combined with energy considerations and mathematical modeling, reveal the following key findings: (i) a higher density of cubic texture components, whether aligned or rotated relative to the rolling direction, decreases magnetic anisotropy, suggesting that optimizing cubic texture can enhance material performance; (ii) at high magnetic fields, there is no straightforward correlation between energy losses and polarization; and (iii) magnetization rates significantly impact magnetization loss rates, highlighting the importance of considering these rates in optimizing Fe–Si sheet manufacturing processes. These findings offer valuable insights for improving the manufacturing and performance of Fe–Si sheets, emphasizing the need for further exploration of texture effects on magnetic behavior. Full article

Radiation from X-ray pulsars (XRPs) was expected to be strongly linearly polarized owing to a large difference in their ordinary and extraordinary mode opacities. The launch of IXPE allowed us to check this prediction. IXPE observed a dozen X-ray pulsars, discovering pulse-phase dependent variation of the polarization degree (PD) and polarization angle (PA). Although the PD showed rather erratic profiles resembling flux pulse dependence, the PA in most cases showed smooth variations consistent with the rotating vector model (RVM), which can be interpreted as a combined effect of vacuum birefringence and dipole magnetic field structure at a polarization-limiting (adiabatic) radius. Application of the RVM allowed us to determine XRP geometry and to confirm the free precession of the NS in Her X-1. Deviations from RVM in two bright transients led to the discovery of an unpulsed polarized emission likely produced by scattering off the accretion disk wind. Full article

Direct current (DC) bias induced by the DC transmission and geomagnetically induced current is a critical factor in the abnormal operation of electrical equipment and is widely used in the field of power transmission and distribution system state evaluation. As the main affected component, the vector magnetization state of a transformer core under DC bias has rarely been studied, resulting in inaccurate transformer operation state estimations. In this paper, a dynamic vector hysteresis model that considers the impact of rotating and DC-biased fields is introduced into the numerical analysis to simulate the distribution of magnetic properties, iron loss and temperature of the transformer core model and a physical 110 kV single-phase autotransformer core. The maximum values of B, H and iron loss exist at the corners and T-joint of the core under rotating and DC-biased fields. The corresponding maximum value of the temperature increase is found in the main core limb area. The temperature rise of the 110 kV transformer core under various DC-biased conditions is measured and compared with the FEM (Finite Element Method) results of the proposed model and the model solely based on the magnetization curve B||H. The calculation error of the temperature rise obtained by the improved model is approximately 3.76–15.73% and is much less than the model solely based on magnetization curve B||H (approximately 50.71–66.92%). Full article

The field of sensorless control of permanent magnet synchronous motor (PMSM) systems has been the subject of extensive research. The accuracy of sensorless controllers depends on the precise estimation of PMSM state quantities, including rotational speed and rotor position. In order to enhance state estimation accuracy, this paper proposes a moving horizon estimator that can be utilized in the sensorless control system of PMSM. Considering the parameter variations observed in PMSM, a nonlinear mathematical model of PMSM is established. A model reference adaptive system (MRAS) is employed to identify parameters such as resistance, inductance, and magnetic chain in real time. This approach can mitigate the impact of parameter fluctuations. Moving horizon estimation (MHE) is an estimation method based on optimization that can directly handle nonlinear system models. In order to eliminate the influence of external interference and improve the robustness of state estimation, a method based on MHE has been designed for PMSM, and a sensorless observer has been established. Considering the traditional MHE with large computation and high memory occupation, the calculation of MHE is optimized by utilizing a Hessian matrix and gradient vector. The speed and position of the PMSM are estimated within constraints during a single-step iteration. The results of the simulation demonstrate that in comparison to the traditional control structure, the estimation error of rotational speed and rotor position can be reduced by utilizing the proposed method. A more accurate estimation can be achieved with good adaptability and computational speed, which can enhance the robustness of the control system of PMSM. Full article

A mathematical model for an electric field induced by an angularly oscillating magnetic dipole was proposed with magnetic vector potential to analyze the characteristics of the electric field induced by a rotating and angularly oscillating magnetic object. This mathematical model was constructed for the electric field induced by a magnetic object oscillating at a certain angle. On this basis, the phase relationship among the three components of the induced electric field was analyzed (defining the right-hand Cartesian coordinate system). Evidently, a phase difference of π/2 always existed between the horizontal components of the electric field induced by a magnetic dipole rotating around the z-axis. The phase difference between the vertical and transverse components in the x–z plane was also π/2. A phase difference of π was observed in the y–z plane. The above theoretical analysis was verified through simulation and experiment. The results showed that the frequency of the induced electric field was related to the angular velocity and angle of rotation. The amplitude was associated with the magnetic moment and the angular velocity and angle of oscillation. The maximum amplitude did not exceed the amplitude of the electric field induced by a magnetic object angularly oscillating at the same velocity. With regard to the amplitude and phase relationship, the three components of the induced electric field measured in the experiment were consistent with the results of the theoretical analysis. Full article

The paper presents a method for estimating the inertia tensor components of a spacecraft that has expired its active life using measurement data of the Earth’s magnetic field induction vector components. The implementation of this estimation method is supposed to be carried out when cleaning up space debris in the form of a clapped-out spacecraft with the help of a space tug. It is assumed that a three-component magnetometer and a transmitting device are attached on space debris. The parameters for the rotational motion of space debris are estimated using this measuring system. Then, the known controlled action from the space tug is transferred to the space debris. Next, measurements for the rotational motion parameters are carried out once again. Based on the available measurement data and parameters of the controlled action, the space debris inertia tensor components are estimated. It is assumed that the measurements of the Earth’s magnetic field induction vector components are made in a coordinate system whose axes are parallel to the corresponding axes of the main body axis system. Such an estimation makes it possible to effectively solve the problem of cleaning up space debris by calculating the costs of the space tug working body and the parameters of the space debris removal orbit. Examples of numerical simulation using the measurement data of the Earth’s magnetic field induction vector components on the Aist-2D small spacecraft are given. Thus, the purpose of this work is to evaluate the components of the space debris inertia tensor through measurements of the Earth’s magnetic field taken using magnetometer sensors. The results of the work can be used in the development and implementation of missions to clean up space debris in the form of clapped-out spacecraft. Full article

This article, or essay, addresses the anisotropic structure and the dynamics of quasi-homogeneous, incompressible turbulence. Modal projection and expansions in terms of spherical harmonics in three-dimensional Fourier space are in line with a seminal study by Jack Herring, around the so-called Craya–Herring frame of reference, with a large review of the related approaches to date. The research part is focused on structure and dynamics of rotating sheared turbulence, including a description of both directional and polarization anisotropy with a minimal number of modes. Effort is made to generalize expansions in terms of scalar spherical harmonics (SSHs) to vector spherical harmonics (VSHs). Looking at stochastic fields, for possibly intermittent vector fields, some directions are explored to reconcile modal projection, firstly used for smooth vector fields, and multifractal approaches for internal intermittency but far beyond scalar correlations, such as structure functions. In order to illustrate turbulence from Earth to planets, stars, and galaxies, applications to geophysics and astrophysics are touched upon, with generalization to coupled vector fields (for kinetic, magnetic, and potential energies), possibly dominated by waves (Coriolis, gravity, and Alfvén). Full article

Interior Permanent Magnet Synchronous Motor (IPMSM) motion-sensorless speed control necessitates precise knowledge of rotor flux, speed, and position. Due to numerous non-ideal aspects, such as converter nonlinearities, detection errors, integral initial value, and parameter mismatches, the conventional first-order integrator’s estimated rotor flux experiences a DC offset (Doff). Low-pass filters (LPF) with a constant cut-off frequency yield accurate estimates only in the medium- and high-speed range; however, at the low-speed area, both magnitude and phase estimates are inaccurate. The presented technique resolves the aforementioned issue for a broad speed range. In order to achieve precise flux estimation, this article presents an improved technique of flux estimator with two distinct drift mitigation strategies for the motion-sensorless field-oriented control (FOC) system of IPMSM. Using the orthogonality of the $\mathrm{\alpha }\text{-}$ and $\mathrm{\beta }$-axes, the proposed drift elimination system can estimate drift in different situations while maintaining a high level of dynamic performance. The stator flux linkage (SFL) computation in the synchronous coordinate is established from the estimation of the rotating shaft’s permanent magnetic flux linkage orientation and the statistical equations model of the SFL. By comparing the calculated SFL vector to the SFL vector derived from the stator winding voltage and currents integral model with a drift PI compensation loop, a feedback loop is formed to neutralize integral drift, and the rotational speed and position of an IPMSM is estimated utilizing the vector product of the two flux linkages in a phase-locked loop. Theoretical interpretation is presented, and Matlab Simulink simulations, as well as experimental outcomes, consistently demonstrate that the suggested estimation techniques can eliminate the phenomenon of flux drift. Full article

CubeSats require accurate determination of their orientation relative to the Sun, Earth, and other celestial bodies to operate successfully and collect scientific data. This paper presents an orientation system based on solar and magnetic sensors that offers a cost-effective and reliable solution for CubeSat navigation. Solar sensors analyze the illumination on each face to measure the satellite’s orientation relative to the Sun, while magnetic sensors determine the Earth’s magnetic field vector in the satellite’s reference frame. By combining the measured data with the known ephemeris of the satellite, the satellite–Sun vector and the magnetic field orientation can be reconstructed. The orientation is expressed using quaternions, representing the rotation from the internal reference system of the satellite to the selected reference system. The proposed system demonstrates the ability to accurately determine the orientation of a CubeSat using only two sensors, making it suitable for installations where more complex and expensive instruments are impractical. Additionally, the paper presents a mathematical model of a low-cost CubeSat orientation system and a hardware implementation of the sensor. The technology, using solar and magnetic sensors, provides a reliable and affordable solution for CubeSat navigation, supporting the increasing sophistication of miniature payloads and enabling accurate satellite positioning in space missions. Full article

The results of the asymmetric magneto-optical rotation in the magnetoplasmonic nanocomposite study are presented. The asymmetry is observed in spectra of magneto-optical rotation when a magneto-optical medium with a plasmonic subsystem is magnetized along or against the radiation wave vector. The asymmetry is observed as vertical displacement of a magneto-optical hysteresis loop too. Such asymmetry is detected in magnetoplasmonic nanocomposite, which consists of a magneto-optical layer of Bi substituted iron-garnet intercalated with a plasmonic subsystem of gold self-assembled nanoparticles. It is shown that the physical reason for the asymmetric magneto-optical rotation is the manifestation of the Cotton–Mouton birefringence effect when the normal magnetization of the sample to a radiation wave vector appears due to the magnetic component of the electromagnetic field of resonating nanoparticles. This effect is additive to the basic magneto-optical Faraday Effect. Full article