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Search Results (2,378)

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21 pages, 5071 KiB  
Article
Experimental Determination of the Equivalent Moment of Inertia and Stresses of Aluminium Profiles with Thermal Breaks
by Dawid Rusin, Janusz Juraszek and Piotr Woźniczka
Materials 2025, 18(1), 23; https://doi.org/10.3390/ma18010023 - 25 Dec 2024
Abstract
This paper presents the results of experimental tests and computer simulations on the stiffness of composite aluminium mullions used in unitised façades. The elements analysed were subjected to bending in order to simulate the actual operating conditions of aluminium façades subjected to significant [...] Read more.
This paper presents the results of experimental tests and computer simulations on the stiffness of composite aluminium mullions used in unitised façades. The elements analysed were subjected to bending in order to simulate the actual operating conditions of aluminium façades subjected to significant wind pressure or suction loads. The basic mechanical and physical properties of the materials from which the analysed type of aluminium façade is made (Aluminium EN AW-6060 in the T66 temper and polyamide PA66 25GF), the test method, and the results obtained are described. As a result of the tests, equivalent moments of inertia of the composite profile (aluminium profile with the thermal break) were determined, which are strongly dependent on the strength of the connection between the individual elements, the asymmetry of the cross-section, and the properties of the thermal break. Strain measurements carried out using FBG (Fiber Bragg Grating) strain sensors installed in the profiles under tests allowed for determining the actual stress values of the aluminium profiles under consideration. The results obtained were compared to theoretical (numerical) values, indicating discrepancies at higher load values. The methodology presented in this article is to be used to monitor the deformation of the aluminium façade mullions of HRB (High-Rise Buildings). Full article
(This article belongs to the Special Issue Testing of Materials and Elements in Civil Engineering (4th Edition))
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Graphical abstract

Graphical abstract
Full article ">Figure 1
<p>(<b>a</b>) Method of transferring the load to the profile; (<b>b</b>) diagram of the loading of the profiles by the steel cube and placement of the measuring instruments; 1—steel block, 2—inner half of the profile with a thermal break (aluminium), 3—FBG sensor, 4—mechanical displacement sensor, 5—external half of the profile with a thermal break (aluminium), 6—the thermal break profile (PA GF25).</p>
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<p>Test bench diagram; 1—steel block, 2—profile (with or without a thermal break), 3—FBG sensor, 4—mechanical displacement sensor.</p>
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<p>View of the mechanical displacement sensor; 1—steel block, 2—inner half of the profile with a thermal break (aluminium), 3—mechanical displacement sensor, 4—external half of the profile with a thermal break (aluminium), 5—the thermal break profile (PA GF25).</p>
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<p>View of FBG sensor glued to aluminium; 1—inner half of the profile with a thermal break (aluminium), 2—FBG sensor, 3—mechanical displacement sensor.</p>
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<p>(<b>a</b>) Aluminium profile with the thermal break; (<b>b</b>) Inner half of the profile with the thermal break; 1—inner half of the profile with the thermal break (aluminium), 2—external half of the profile with the thermal break (aluminium), 3—the thermal break (PA GF25).</p>
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<p>Deflection U [mm] of inner halves of profiles with the thermal break (average value for loading and unloading of the beam). Calculated value—according to the theoretical calculation.</p>
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<p>Moment of inertia I (cm<sup>4</sup>) of inner halves of profiles with the thermal break (average value for loading and unloading of the beam). Calculated value—according to the theoretical calculation.</p>
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<p>Strain ε (με) of inner halves of profiles with the thermal break (average value for loading and unloading of the beam).</p>
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<p>Stress σ (MPa) of inner halves of profiles with the thermal break (average value for loading and unloading of the beam).</p>
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<p>Deflection U [mm] of profiles with a thermal break (average value for loading and unloading of the beam). Calculated value—according to [<a href="#B29-materials-18-00023" class="html-bibr">29</a>].</p>
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<p>Moment of inertia I (cm<sup>4</sup>) of profiles with the thermal break (average value for loading and unloading of the beam). Calculated value—according to [<a href="#B29-materials-18-00023" class="html-bibr">29</a>].</p>
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<p>Strain ε (με) of profiles with the thermal break (average value for loading and unloading of the beam).</p>
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<p>Stress σ (MPa) in profiles with the thermal break (average value for loading and unloading of the beam).</p>
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<p>Load [kN]–Deflection U (mm): summary values of inner halves of profiles and profiles with the thermal break made in single-colour (A) and two-colour technology (B).</p>
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<p>Load [kN]–Moment of inertia I (cm<sup>4</sup>): summary values of inner halves of profiles and profiles with the thermal break made in single-colour (A) and two-colour technology (B).</p>
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<p>Load [kN]–Stress σ (MPa): summary values of inner halves of profiles and profiles with the thermal break made in single-colour (A) and two-colour technology (B).</p>
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<p>Load [kN]–Strain ε (με): summary values of inner halves of profiles and profiles with the thermal break made in single-colour (A) and two-colour technology (B).</p>
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<p>Boundary conditions of the (<b>a</b>) profile with the thermal break; (<b>b</b>) inner half of profiles with the thermal break.</p>
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<p>(<b>a</b>) Comparison of FEM deflection and tests—profiles with the thermal break, (<b>b</b>) Comparison of FEM deflection and tests—inner halves of profiles with the thermal break.</p>
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<p>Deflection [mm] of profile with the thermal break for F = 10 kN.</p>
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18 pages, 6225 KiB  
Article
An Energy Modulation Interrogation Technique for Monitoring the Adhesive Joint Integrity Using the Full Spectral Response of Fiber Bragg Grating Sensors
by Chow-Shing Shin, Tzu-Chieh Lin and Shun-Hsuan Huang
Sensors 2025, 25(1), 36; https://doi.org/10.3390/s25010036 - 25 Dec 2024
Abstract
Adhesive joining has the severe limitation that damages/defects developed in the bondline are difficult to assess. Conventional non-destructive examination (NDE) techniques are adequate to reveal disbonding defects in fabrication and delamination near the end of service life but are not helpful in detecting [...] Read more.
Adhesive joining has the severe limitation that damages/defects developed in the bondline are difficult to assess. Conventional non-destructive examination (NDE) techniques are adequate to reveal disbonding defects in fabrication and delamination near the end of service life but are not helpful in detecting and monitoring in-service degradation of the joint. Several techniques suitable for long-term joint integrity monitoring are proposed. Fiber Bragg grating (FBG) sensors embedded in the joint are one of the promising candidates. It has the advantages of being close to the damage and immune to environmental attack and electromagnetic interference. Damage and disbonding inside an adhesive joint will give rise to a non-uniform strain field that may bring about peak splitting and chirping of the FBG spectrum. It is shown that the evolution of the full spectral responses can closely reveal the development of damages inside the adhesive joints during tensile and fatigue failures. However, recording and comparing the successive full spectra in the course of damage is tedious and can be subjective. An energy modulation interrogation technique is proposed using a pair of tunable optical filters. Changes in the full FBG spectral responses are modulated by the filters and converted into a conveniently measurable voltage output by photodiodes. Monitoring damage development can then be easily automated, and the technique is well-suited for practical applications. Filter spectrum width of 5 nm and initial overlap with the FBG spectrum to give 40% of the maximum output voltage is found to be optimal for measurement. The technique is tested on embedded FBGs from different adhesive lap-joint specimens and successfully reflected the severity of changes in the full spectral shapes during the course of tensile failure. Moreover, the trends in these PD outputs corroborate with the V value previously proposed to describe the qualitative change in FBG spectral shape. Full article
(This article belongs to the Special Issue Feature Papers in Physical Sensors 2024)
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Figure 1

Figure 1
<p>Schematic diagram showing the effect of complex strain field on the spectral shape reflected from an FBG.</p>
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<p>Schematic arrangement for energy modulation interrogation of FBG.</p>
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<p>Overlapping of the FBG and filter spectra resulted in the hatched area that will come through the filter.</p>
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<p>Comparison of measured filter spectrum with the quadratic fit with light intensity in (<b>a</b>) dbm; and (<b>b</b>) nW.</p>
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<p>Simulated filter spectra for full width at half maximum equals (<b>a</b>) 1 nm, (<b>b</b>) 3 nm, and (<b>c</b>) 5 nm.</p>
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<p>The evolution of FBG spectrum measured at (<b>a</b>) increasing load during a tensile test; (<b>b</b>) zero load after progressively increasing load during a tensile test (the bracketed numbers after the loading values in the figure legends indicated the loading as a percentage of the failure load).</p>
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<p>Comparison of calculated and measured energy-modulated results: (<b>a</b>) Relative positions between the filter and FBG spectra to give 0.5 of maximum voltage; (<b>b</b>) energy-modulated output spectra in dbm; (<b>c</b>) energy-modulated output spectra in nW.</p>
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<p>Comparison of calculated and measured energy-modulated results: (<b>a</b>) Relative positions between the filter and FBG spectra to give 0.1 of maximum voltage; (<b>b</b>) energy-modulated output spectra in dbm; (<b>c</b>) energy-modulated output spectra in nW.</p>
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<p>(<b>a</b>) The FBG and the two-filter spectra before the test; (<b>b</b>) evolution of the unloaded FBG spectra up to 96% of failure load.</p>
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<p>Comparison between the measured and simulated energy modulation outputs from the filter on the short wavelength side, with an initial output of 0.5 <span class="html-italic">V</span><sub>max,</sub> and on the long wavelength side, with an initial output of 0.25 <span class="html-italic">V</span><sub>max</sub>.</p>
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<p>Relative positions between the filters and FBG spectra when output equals (<b>a</b>) 0.1 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math> and (<b>b</b>) 0.9 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>.</p>
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<p>Simulated PD output compared with the <span class="html-italic">V</span> values for initial overlap corresponding to (<b>a</b>) 0.1 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>; (<b>b</b>) 0.3 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>; (<b>c</b>) 0.5 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>; and (<b>d</b>) 0.9 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>.</p>
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<p>Simulated PD output for filters with different FWHMs and initial overlap PD voltages compared with the <span class="html-italic">V</span> values: (<b>a</b>) FWHM = 3 nm, 0.4 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>; (<b>b</b>) FWHM = 3 nm, 0.9 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>; (<b>c</b>) FWHM = 5 nm, 0.4 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>; and (<b>d</b>) FWHM = 5 nm, 0.9 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math>.</p>
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<p>Evolution of the load-free spectra during tensile tests in (<b>a</b>) FBG 3; (<b>c</b>) FBG 4; and (<b>e</b>) FBG 5; and comparison of the corresponding V values and simulated PD output for filters. FWHM = 5 nm and initial overlap of 0.4 <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>V</mi> </mrow> <mrow> <mi mathvariant="normal">m</mi> <mi mathvariant="normal">a</mi> <mi mathvariant="normal">x</mi> </mrow> </msub> </mrow> </semantics></math> for (<b>b</b>) FBG 3; (<b>d</b>) FBG 4, and (<b>f</b>) FBG 5. (the bracketed numbers after the loading values in the figure legends indicated the loading as a percentage of the failure load).</p>
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18 pages, 4690 KiB  
Article
Calibration of Marine Pressure Sensors with a Combination of Temperature and Pressure: A Case Study of SBE 37-SM
by Muzi Zhang, Qingquan Sun, Xiaoxue Bai, Bo Yang, Wei Zhao and Chi Wu
J. Mar. Sci. Eng. 2024, 12(12), 2366; https://doi.org/10.3390/jmse12122366 - 23 Dec 2024
Abstract
Accurate pressure measurement is crucial for understanding ocean dynamics in marine research. However, pressure sensors based on strain measurement principles are significantly affected by temperature variations, impacting the accuracy of depth measurements. This study investigates the SBE37-SM sensor and presents an improved calibration [...] Read more.
Accurate pressure measurement is crucial for understanding ocean dynamics in marine research. However, pressure sensors based on strain measurement principles are significantly affected by temperature variations, impacting the accuracy of depth measurements. This study investigates the SBE37-SM sensor and presents an improved calibration method based on a constant-pressure, variable-temperature scheme that effectively addresses temperature-induced deviations in pressure measurement. Experiments were conducted across a pressure range of 2000 dbar to 6000 dbar and a temperature range of 2 °C to 35 °C, establishing a comprehensive pressure–temperature calibration grid. The results show that, at a pressure of 6000 dbar, temperature-induced variations in readings for brand new SBE37-SM sensors can reach up to 9 dbar, while, for used sensors, they exceed 12 dbar, following a U-shaped trend. After applying a polynomial regression model for calibration, these variations were reduced to within ±0.5 dbar, significantly reducing the measurement uncertainty of the sensors in complex marine environments. This method underscores the necessity of further optimizing the CTD system’s temperature compensation mechanism during calibration and highlights the importance of regular calibration to minimize measurement uncertainty. Full article
(This article belongs to the Section Ocean Engineering)
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Graphical abstract

Graphical abstract
Full article ">Figure 1
<p>Reference curve of ocean temperature versus pressure, where the horizontal axis represents temperature and the vertical axis represents the overlying seawater pressure. The blue line indicates all recorded CTD data, while the green line represents the trend of ocean temperature profile changes after averaging the temperature data [<a href="#B10-jmse-12-02366" class="html-bibr">10</a>].</p>
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<p>Traceability scheme of the oceanographic pressure sensor (NIM: National Institute of Metrology).</p>
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<p>Experimental setup, including the piston diameter and quartz resonant manometer, placed in a temperature-controlled thermotank (0–40 °C). Panel (<b>a</b>) shows a photograph of the experimental process, while panel (<b>b</b>) presents a schematic diagram of the experimental setup.</p>
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<p>Experimental results of the temperature stability of the standard pressure gauge. (<b>a</b>) The temperature readings from the temperature sensor inside the quartz resonator pressure gauge, which is used for temperature correction. (<b>b</b>) The difference of the pressure readings between the environmental temperature and the 2 °C, which demonstrates the impact of varying environmental temperatures on the pressure readings. μ and σ represent the mean pressure difference and its standard deviation, respectively.</p>
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<p>Main components and layout of the variable-temperature pressure calibration system.</p>
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<p>Preliminary test results. The red line represents the water temperature variation in the tank during the experiment, as recorded by the SBE 37-SM temperature sensor; the purple line shows the readings from the standard quartz resonator pressure gauge; and the blue line indicates the pressure readings from the SBE 37 connected to the test system.</p>
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<p>Results of the constant pressure and variable temperature test. In the upper graph, the red line represents the water temperature variation in the tank during the experiment, as measured by the SBE 37-SM temperature sensor. The middle graph shows the readings from the standard quartz resonator pressure gauge, while the lower graph displays the pressure readings from the five SBE 37-SM sensors connected to the test system.</p>
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<p>The 3D plots of pressure sensors at constant pressure and variable temperature. Figures (<b>a</b>–<b>e</b>) are brand new SBE 37-SM units with the serial numbers 24365, 24744, 24820, 24833, and 24874, respectively. Figures (<b>f</b>,<b>g</b>) represent used SBE 37-SM units with the serial numbers 25526 and 22749. Figure (<b>h</b>) shows the difference in the error between unit 25526 and unit 24365.</p>
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<p>Pressure measurement error vs. bath temperature at 2000 dbar, 4000 dbar, and 6000 dbar.</p>
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<p>Comparison of SBE 37-SM pressure readings before and after calibration with a reference quartz pressure gauge under varying temperature conditions. (<b>a</b>) The results at a constant pressure of 4000 dbar; (<b>b</b>) the results at 6000 dbar. In both figures, the data series are represented as follows: Blue line: original pressure readings from the SBE 37-SM pressure sensor. Green line: temperature-corrected pressure readings from the SBE 37-SM sensor, accounting for the influence of temperature variations on pressure. Purple line: reference pressure readings from the calibrated quartz pressure gauge. Red line: water bath temperature recorded by the SBE 37-SM temperature sensor during the experiment.</p>
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12 pages, 2112 KiB  
Article
Foliar Spraying with Endophytic Trichoderma Biostimulant Increases Drought Resilience of Maize and Sunflower
by András Csótó, György Tóth, Péter Riczu, Andrea Zabiák, Vera Tarjányi, Erzsébet Fekete, Levente Karaffa and Erzsébet Sándor
Agriculture 2024, 14(12), 2360; https://doi.org/10.3390/agriculture14122360 - 22 Dec 2024
Viewed by 305
Abstract
Microbial biostimulants that promote plant growth and abiotic stress tolerance are promising alternatives to chemical fertilizers and pesticides. Although Trichoderma fungi are known biocontrol agents, their biostimulatory potential has been scarcely studied in field conditions. Here, the mixture of two endophytic Trichoderma strains [...] Read more.
Microbial biostimulants that promote plant growth and abiotic stress tolerance are promising alternatives to chemical fertilizers and pesticides. Although Trichoderma fungi are known biocontrol agents, their biostimulatory potential has been scarcely studied in field conditions. Here, the mixture of two endophytic Trichoderma strains (Trichoderma afroharzianum TR04 and Trichoderma simmonsii TR05) was tested as biostimulant in the form of foliar spray on young (BBCH 15-16) maize (5.7 ha) and sunflower (5.7 and 11.3 ha) fields in Hungary. The stimulatory effect was characterized by changes in plant height, the number of viable leaves, and the chlorophyll content, combined with yield sensor collected harvest data. In all trials, the foliar treatment with Trichoderma spores increased photosynthetic potential: the number of viable leaves increased by up to 6.7% and the SPAD index by up to 19.1% relative to the control. In extreme drought conditions, maize yield was doubled (from 0.587 to 1.62 t/ha, p < 0.001). The moisture content of the harvested seeds, as well as sunflower height, consistently increased post-treatment. We concluded that foliar spraying of young plants with well-selected endophytic Trichoderma strains can stimulate growth, photosynthesis, and drought tolerance in both monocot maize and dicots sunflower crops in field conditions. Full article
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Figure 1

Figure 1
<p>Experimental design to study the effect of the endophytic <span class="html-italic">Trichoderma</span> formulation. Aerial view of Experimental Site 1 (<b>a</b>) and Experimental Site 2 (<b>b</b>). Blue lines indicate the borders of the Experimental Sites, red lines indicate the borders of the plots. (<b>c</b>) Experimental designs C1–4 indicate control plots; T1–4 indicate plots treated with <span class="html-italic">Trichoderma</span>.</p>
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<p>Average NDVI mean values with natural breaks coloring method, using 80% overlapping (Experimental Site I). Light blue polygon outline color shows the lower average NDVI values (below 0.8). C1–4 indicate control plots; T1–4 indicate Trichoderma-treated plots.</p>
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<p>Monthly weather data of the experimental years 2022 and 2023. (<b>a</b>) Average, minimal and maximal temperatures. (<b>b</b>) Monthly average of solar radiation and precipitation.</p>
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<p>Changes in average number of viable leaves (<b>a</b>,<b>c</b>) and chlorophyll content (<b>b</b>,<b>d</b>, measured as SPAD values) of maize (<b>a</b>,<b>b</b>) and sunflower (<b>c</b>,<b>d</b>) plants following treatment with <span class="html-italic">Trichoderma</span> spp. compared to untreated control plants. Data points represent mean values, and error bars indicate standard error. *: <span class="html-italic">t</span>-test <span class="html-italic">p</span> &lt; 0.01, **: <span class="html-italic">t</span>-test <span class="html-italic">p</span> &lt; 0.001.</p>
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<p>Average yield (<b>a</b>) and average moisture content of harvested seeds (<b>b</b>) of maize and sunflower plants treated with <span class="html-italic">Trichoderma</span> spp. compared to untreated controls. Error bars represent standard error. **: <span class="html-italic">t</span>-test <span class="html-italic">p</span> &lt; 0.001.</p>
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17 pages, 4016 KiB  
Article
Analyzing and Modeling the Dynamic Electrical Characteristics of Nanocomposite Large-Range Strain Gauges
by Alex M. Wonnacott, Anton E. Bowden, Ulrike H. Mitchell and David T. Fullwood
Sensors 2024, 24(24), 8192; https://doi.org/10.3390/s24248192 - 22 Dec 2024
Viewed by 163
Abstract
Flexible high-deflection strain gauges have been demonstrated to be cost-effective and accessible sensors for capturing human biomechanical deformations. However, the interpretation of these sensors is notably more complex compared to conventional strain gauges, particularly during dynamic motion. In addition to the non-linear viscoelastic [...] Read more.
Flexible high-deflection strain gauges have been demonstrated to be cost-effective and accessible sensors for capturing human biomechanical deformations. However, the interpretation of these sensors is notably more complex compared to conventional strain gauges, particularly during dynamic motion. In addition to the non-linear viscoelastic behavior of the strain gauge material itself, the dynamic response of the sensors is even more difficult to capture due to spikes in the resistance during strain path changes. Hence, models for extracting strain from resistance measurements of the gauges most often only work well under quasi-static conditions. The present work develops a novel model that captures the complete dynamic strain–resistance relationship of the sensors, including resistance spikes, during cyclical movements. The forward model, which converts strain to resistance, comprises the following four parts to accurately capture the different aspects of the sensor response: a quasi-static linear model, a spike magnitude model, a long-term creep decay model, and a short-term decay model. The resulting sensor-specific model accurately predicted the resistance output, with an R-squared value of 0.90. Additionally, an inverse model which predicts the strain vs. time data that would result in the observed resistance data was created. The inverse model was calibrated for a particular sensor from a small amount of cyclic data during a single test. The inverse model accurately predicted key strain characteristics with a percent error as low as 0.5%. Together, the models provide new functionality for interpreting high-deflection strain sensors during dynamic strain measurement applications, including wearables sensors used for biomechanical modeling and analysis. Full article
(This article belongs to the Special Issue Advances in Sensor Technologies for Wearable Applications)
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Figure 1

Figure 1
<p>(<b>a</b>) Strain profile for sinusoidal-type tests (<b>top</b>) used to mimic human movement during dynamic movements, with associated sensor resistance response (<b>bottom</b>). (<b>b</b>) Square-wave tests used for comparison with the smooth sinusoidal-type. Red circles indicate peaks and troughs of the resistance profile. Several of these are labeled (a–e) for later discussion. Point e indicates the top of a small ‘instantaneous’ rise in resistance during a strain decrease that is present for the square wave, but not the sinusoidal, tests.</p>
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<p>Quasi-static resistivity–strain experimental data of a typical sensor. This curve follows a shape similar to a logistic curve across the entire strain range. Adapted from data presented in [<a href="#B3-sensors-24-08192" class="html-bibr">3</a>].</p>
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<p>Resistance response (blue) to the applied strain acceleration (orange). This overlay demonstrates the precise alignment of strain acceleration peaks and resistance peaks.</p>
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<p>Data from the fourth cycle of a selected sensor from points a–b in <a href="#sensors-24-08192-f001" class="html-fig">Figure 1</a>. A first order exponential decay equation has been fitted to the data.</p>
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<p>(<b>a</b>) Correlations between <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>t</mi> </mrow> <mrow> <mi>h</mi> </mrow> </msub> </mrow> </semantics></math>, Δε, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>ε</mi> </mrow> <mrow> <mn>0</mn> </mrow> </msub> </mrow> </semantics></math>, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>ε</mi> </mrow> <mo>˙</mo> </mover> </mrow> <mrow> <mi>m</mi> <mi>a</mi> <mi>x</mi> </mrow> </msub> </mrow> </semantics></math> and spike magnitude factors, <span class="html-italic">Fi</span>. (<b>b</b>) Sample correlation between <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>ε</mi> </mrow> <mo>¨</mo> </mover> </mrow> <mrow> <mi>m</mi> <mi>a</mi> <mi>x</mi> </mrow> </msub> </mrow> </semantics></math> and <span class="html-italic">F</span><sub>2</sub>. R-squared values for all correlations are shown in <a href="#sensors-24-08192-t001" class="html-table">Table 1</a>.</p>
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<p>Example of linear correlation between the spike magnitude factors and the rate constants. (<b>a</b>) Correlation between increasing strain rate constant, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>k</mi> </mrow> <mrow> <mn>3</mn> </mrow> </msub> </mrow> </semantics></math>, and <span class="html-italic">F<sub>1</sub></span> for the 30 sensors tested. (<b>b</b>) Correlation between decreasing strain rate constant, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>k</mi> </mrow> <mrow> <mn>4</mn> </mrow> </msub> </mrow> </semantics></math>, and <span class="html-italic">F<sub>1</sub></span>. R<sup>2</sup> values are shown in <a href="#sensors-24-08192-t001" class="html-table">Table 1</a>.</p>
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<p>Complete model of resistance predicted from strain, with an R-squared value of 0.897. This model combines linear, spike magnitude, long-term creep relaxation, and short-term viscoelastic decay relaxation models into one complete resistance prediction model.</p>
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<p>(<b>a</b>) Initial and final predictions of strain curve. The strain curve predictions are created from the following predicted key strain factors: Δε, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>ε</mi> </mrow> <mo>˙</mo> </mover> </mrow> <mrow> <mi>m</mi> <mi>a</mi> <mi>x</mi> </mrow> </msub> </mrow> </semantics></math>, <math display="inline"><semantics> <mrow> <msub> <mrow> <mover accent="true"> <mrow> <mi>ε</mi> </mrow> <mo>¨</mo> </mover> </mrow> <mrow> <mi>m</mi> <mi>a</mi> <mi>x</mi> </mrow> </msub> </mrow> </semantics></math>, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>t</mi> </mrow> <mrow> <mi>h</mi> </mrow> </msub> </mrow> </semantics></math>. The initial strain curve prediction has an R<sup>2</sup> value of 0.696. (<b>b</b>) After iteration through the forward model, the final predicted strain curve has an R<sup>2</sup> value of 0.905. The iterations through the forward model improved the accuracy of the model.</p>
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13 pages, 5878 KiB  
Article
Analysis of Stability and Variability in Sensor Readings from a Vehicle Weigh-in-Motion Station
by Artur Ryguła, Krzysztof Brzozowski, Marcin Grygierek and Agnieszka Socha
Sensors 2024, 24(24), 8178; https://doi.org/10.3390/s24248178 - 21 Dec 2024
Viewed by 310
Abstract
This study presents a detailed analysis of the stability of weigh-in-motion sensors used at vehicle weighing stations. The objective of this research was a long-term assessment of reading variability, with a particular focus on the sensors’ application in automated measurement stations. These investigations [...] Read more.
This study presents a detailed analysis of the stability of weigh-in-motion sensors used at vehicle weighing stations. The objective of this research was a long-term assessment of reading variability, with a particular focus on the sensors’ application in automated measurement stations. These investigations constitute a critical component of modern traffic management systems and vehicle overload control. The analysis covered the period from 2022 to 2024, incorporating data from vehicles participating in regular traffic as well as dedicated control runs using vehicles with known wheel and axle load distributions. The study also considered changes in road surface conditions, particularly rut depth, and their variations over the examined period. The findings revealed that, despite the lack of station calibration over the three-year period, the observed parameters exhibited only minor changes. These results confirm the high stability of the applied measurement system and its ability to maintain measurement accuracy over extended operational periods, which is essential for its practical application in real-world traffic conditions. Full article
(This article belongs to the Section Vehicular Sensing)
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<p>The layout of the WIM station. The size of sensors W1 and W2 is 1.75 × 0.07 m, with a sensitivity of 0.825 mV/V at 3000 kg [<a href="#B32-sensors-24-08178" class="html-bibr">32</a>]. Loop L1’s dimensions are 2.8 × 1 m.</p>
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<p>The road pavement construction at the WIM station.</p>
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<p>The distribution of the gross vehicle weight of the vehicles with GVW &gt; 3500 kg in the period 2022–2024.</p>
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<p>Static wheel load assessment using Intercomp LP788 scales.</p>
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<p>The increasing average rut depth for the entire section, with a breakdown by wheel path, from 2018 to 2024.</p>
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<p>The distribution of the rut depth difference between the right and left wheel paths in the years 2022 and 2024.</p>
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<p>The distribution of depth in the left and right wheel paths according to measurements in 2024.</p>
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<p>Total weight distribution for reference vehicle category.</p>
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<p>Gross vehicle weight spectra for vehicles in the reference category obtained from data recorded in each year in May.</p>
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<p>Steering axle load spectra for the reference vehicle category, obtained based on data recorded in each year, specifically in the month of May.</p>
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<p>Wheel load spectra for the steering axle of the reference vehicle category, obtained based on data recorded in each year in May: (<b>a</b>) left wheel load; (<b>b</b>) right wheel load.</p>
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<p>Comparison of wheel loads recorded in the 2023 in relation to the values determined on static scales: (<b>a</b>) left side; (<b>b</b>) right side. Dots represent measurement points, while the line represents the result of linear approximation.</p>
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<p>The percentage error in determining the wheel load for the reference category vehicle in the control tests of 2023 (box boundaries correspond to the IQR; whiskers—quartile 1 − 1.5 IQR and quartile 3 + 1.5 IQR, respectively; the dash inside the box represents the median, while the green triangle indicates the mean value).</p>
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<p>Comparison of wheel loads recorded in the 2024 in relation to the values determined on static scales: (<b>a</b>) left side; (<b>b</b>) right side. Dots represent measurement points, while the line represents the result of linear approximation.</p>
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<p>The percentage error in determining the wheel load for the reference category vehicle in the control tests of 2024 (box boundaries correspond to the IQR; whiskers—quartile 1 − 1.5 IQR and quartile 3 + 1.5 IQR, respectively; the dash inside the box represents the median, while the green triangle indicates the mean value).</p>
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19 pages, 15802 KiB  
Article
Preparation and Characterization of Highly Conductive PVDF/PAN Conjugate Electrospun Fibrous Membranes with Embedded Silver Nanoparticles
by Siyang Wu, Luyu Zhang, Xiaochun Qiu, Yuntai Guo, Liangliang Dong, Mingzhuo Guo and Jiale Zhao
Polymers 2024, 16(24), 3540; https://doi.org/10.3390/polym16243540 - 19 Dec 2024
Viewed by 321
Abstract
This study reports the development of highly conductive and stretchable fibrous membranes based on PVDF/PAN conjugate electrospinning with embedded silver nanoparticles (AgNPs) for wearable sensing applications. The fabrication process integrated conjugate electrospinning of PVDF/PAN, selective dissolution of polyvinylpyrrolidone (PVP) to create porous networks, [...] Read more.
This study reports the development of highly conductive and stretchable fibrous membranes based on PVDF/PAN conjugate electrospinning with embedded silver nanoparticles (AgNPs) for wearable sensing applications. The fabrication process integrated conjugate electrospinning of PVDF/PAN, selective dissolution of polyvinylpyrrolidone (PVP) to create porous networks, and uniform AgNP incorporation via adsorption-reduction. Systematic optimization revealed that 10 wt.% PVP content and 1.2 mol/L AgNO3 concentration yielded membranes with superior electrical conductivity (874.93 S/m) and mechanical strength (2.34 MPa). The membranes demonstrated excellent strain sensing performance with a gauge factor of 12.64 within 0–30% strain and location-specific sensing capabilities: moderate movements at wrist (ΔR/R0: 98.90–287.25%), elbow (124.65–300.24%), and fingers (177.01–483.20%) generated stable signals, while knee articulation exhibited higher sensitivity (459.60–1316.48%) but significant signal fluctuations. These results demonstrate the potential of the developed conductive porous PVDF/PAN composite fibrous membranes for applications in wearable sensors, flexible electronics, and human-machine interfaces, particularly in scenarios requiring moderate-range motion detection with high reliability and stability. The findings suggest promising opportunities for developing next-generation wearable sensing devices through the optimization of conjugate electrospun fibrous membranes. Full article
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<p>Schematic illustration of the fabrication process for the conductive porous PVDF/PAN composite fibrous membrane.</p>
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<p>SEM microstructures of porous PVDF/PAN composite membranes with PVP contents of (<b>a</b>) 5 wt.%, (<b>b</b>) 10 wt.%, (<b>c</b>) 15 wt.%, and (<b>d</b>) high-magnification image of the membrane with 10 wt% PVP content showing detailed porous structure.</p>
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<p>The porosity of porous PVDF/PAN composite membranes with different PVP contents.</p>
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<p>(<b>a</b>) Stress and (<b>b</b>) strain values of porous PVDF/PAN composite membranes with different PVP mass fractions, (<b>c</b>) residual strain of PCM-2 with 5 wt.%, 10 wt.% and 15 wt.% PVP contents, (<b>d</b>) Overlaid FTIR spectra of PVDF/PVP/PAN composite membrane before and after PVP dissolution.</p>
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<p>Morphological and compositional characterization of PVDF/PAN composite membrane: (<b>a</b>) interwoven network structure, (<b>b</b>) AgNPs distribution on different fibers, (<b>c</b>) abundant AgNPs on PVDF fiber surface, and (<b>d</b>) EDX spectrum of the composite.</p>
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<p>Effect of AgNO<sub>3</sub> concentration on the electrical (<b>a</b>) conductivity and (<b>b</b>) stress of conductive porous PVDF/PAN composite fibrous membranes.</p>
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<p>Tensile test results of the Conductive Porous PVDF/PAN Composite Fibrous Membrane: (<b>a</b>) linearity of the Conductive Porous PVDF/PAN Composite Fibrous Membrane, (<b>b</b>) linearity change at 10% strain, (<b>c</b>) linearity change at 20% strain, (<b>d</b>) linearity change at 30% strain.</p>
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<p>Physical appearance, sensing principle and human motion sensing performance of the conductive porous PVDF/PAN composite fibrous membrane.</p>
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19 pages, 8015 KiB  
Article
Signal Detection by Sensors and Determination of Friction Coefficient During Brake Lining Movement
by Leopold Hrabovský, Vieroslav Molnár, Gabriel Fedorko, Nikoleta Mikusova, Jan Blata, Jiří Fries and Tomasz Jachowicz
Sensors 2024, 24(24), 8078; https://doi.org/10.3390/s24248078 - 18 Dec 2024
Viewed by 275
Abstract
This article presents a laboratory device by which the course of two signals can be detected using two types of sensors—strain gauges and the DEWESoft DS-NET measuring apparatus. The values of the coefficient of friction of the brake lining when moving against the [...] Read more.
This article presents a laboratory device by which the course of two signals can be detected using two types of sensors—strain gauges and the DEWESoft DS-NET measuring apparatus. The values of the coefficient of friction of the brake lining when moving against the rotating shell of the brake drum were determined from the physical quantities sensed by tensometric sensors and transformed into electrical quantities. The friction coefficient of the brake lining on the circumference of the rotating brake disc shell can be calculated from the known values measured by the sensors, the design dimensions of the brake, and the revolutions of the rotating parts system. The values of the friction coefficient were measured during brake lining movement. A woven asbestos-free material, Beral 1126, which contained brass fibers and resin additives, showed slightly higher values when rotating at previously tested speeds compared to the friction coefficient values obtained when the brake drum rotation was uniformly delayed. The methodology for determining the friction coefficient of the brake lining allowed the laboratory device to verify its magnitude for different friction materials under various operating conditions. Full article
(This article belongs to the Special Issue Sensors and Systems for Automotive and Road Safety (Volume 2))
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<p>Laboratory device detecting the friction coefficient of the brake lining. 1—steel structure; 2—electric motor; 3—flywheel; 4—double-jaw brake; 5—weights; 6—torque sensor [<a href="#B35-sensors-24-08078" class="html-bibr">35</a>]; 7—force sensor [<a href="#B38-sensors-24-08078" class="html-bibr">38</a>]; 8—shaft; 9—plummer block [<a href="#B36-sensors-24-08078" class="html-bibr">36</a>]; 10—Jäckl 60 × 40.</p>
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<p>Two-dimensional laboratory device sketch. 1—steel structure; 2—electric motor; 3—flywheel; 4—double-jaw brake; 5—weights; 6—torque sensor [<a href="#B35-sensors-24-08078" class="html-bibr">35</a>]; 7—force sensor [<a href="#B38-sensors-24-08078" class="html-bibr">38</a>]; 8—shaft; 9—plummer block [<a href="#B36-sensors-24-08078" class="html-bibr">36</a>].</p>
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<p>(<b>a</b>) Plummer block SN 507 [<a href="#B36-sensors-24-08078" class="html-bibr">36</a>], (<b>b</b>) clamping sleeve A207X [<a href="#B41-sensors-24-08078" class="html-bibr">41</a>]. 1—plummer block; 2—clamping sleeve; 3—KM nut KM7 [<a href="#B42-sensors-24-08078" class="html-bibr">42</a>]; 4—MB washer MB7; 5—tilting ball bearing 1207 K.</p>
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<p>Two-jaw disc brake. (<b>a</b>) Basic dimensions of the brake, (<b>b</b>) forces acting in the brake pins, (<b>c</b>) tensile force acting in the threaded rod. 1—brake arm; 2—brake lever; 3—brake shoes; 4—brake drum; 5—force sensor [<a href="#B38-sensors-24-08078" class="html-bibr">38</a>]; 6—threaded rod; 7—weight.</p>
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<p>Calibration of (<b>a</b>) T4WA-S3 torque sensor, (<b>b</b>) AST-250 kg force sensor. 1—sensor T4WA-S3; 2—bench vice; 3—head of assembly sliding rod socket adapter socket wrench; 4—steel pipe; 5—suspension nut; 6—weight; 7—sensor AST-250 kg; 8—hinge; 9—weight.</p>
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<p>A measuring chain is a sequence of interconnected devices and equipment that enables the detection and processing of measured signals.</p>
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<p>The time course of torque M<sub>ri</sub> [N·m], expressing the system resistance against rotation, was measured on a laboratory device. (<b>a</b>) M<sub>r1</sub> = 2.32 N·m, (<b>b</b>) M<sub>r2</sub> = 2.76 N·m, (<b>c</b>) M<sub>r4</sub> = 2.56 N·m, (<b>d</b>) M<sub>r6</sub> = 2.67 N·m.</p>
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<p>A laboratory device was created to determine the friction coefficient f<sub>1i</sub> [-] of the brake lining in motion and the friction coefficient f<sub>2i</sub> [-] of the brake lining when the rotating parts of the laboratory device are braked. 1—electric motor; 2—driven shaft; 3—torque sensor; 4—speed sensor; 5—force sensor; 6—hexagonal nut.</p>
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<p>Time recording of tensile force F<sub>Mi</sub> [N] and torque M<sub>Mi</sub> [N·m] measured on a laboratory device for f<sub>c</sub> [Hz] (<b>a</b>,<b>b</b>) 10, (<b>c</b>,<b>d</b>) 20.</p>
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<p>Tensile force F<sub>Mi</sub> [N] and torque M<sub>Mi</sub> [N·m] course, measured on a laboratory device for f<sub>c</sub> [Hz] (<b>a</b>,<b>b</b>) 30, (<b>c</b>,<b>d</b>) 40.</p>
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<p>Tensile force F<sub>Mi</sub> [N] and torque M<sub>Mi</sub> [N·m] course, measured on laboratory device for f<sub>c</sub> = 50 Hz. (<b>a</b>) F<sub>M1</sub> = 88.9 N, M<sub>M1</sub> = 16.60 N·m; (<b>b</b>) F<sub>M2</sub> = 72.3 N, M<sub>M2</sub> = 13.50 N·m; (<b>c</b>) F<sub>M3</sub> = 83.2 N, M<sub>M3</sub> = 12.89 N·m; (<b>d</b>) F<sub>M4</sub> = 85.3 N, M<sub>M4</sub> = 12.50 N·m.</p>
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<p>Tensile force F<sub>Mi</sub> [N] and torque M<sub>Mi</sub> [N·m] course measured on the laboratory device during the braking of the rotating parts system. (<b>a</b>) f<sub>c</sub> = 10 Hz, t<sub>11</sub> = 18.53 s; (<b>b</b>) f<sub>c</sub> = 10 Hz, t<sub>21</sub> = 19.57 s; (<b>c</b>) f<sub>c</sub> = 20 Hz, t<sub>11</sub> = 17.39 s; (<b>d</b>) f<sub>c</sub> = 20 Hz, t<sub>21</sub> = 18.44 s.</p>
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<p>Tensile force F<sub>Mi</sub> [N] and torque M<sub>Mi</sub> [N·m] course measured on the laboratory device during braking of the rotating parts system. (<b>a</b>) f<sub>c</sub> = 30 Hz, t<sub>11</sub> = 24.18 s; (<b>b</b>) f<sub>c</sub> = 30 Hz, t<sub>21</sub> = 26.13 s; (<b>c</b>) f<sub>c</sub> = 40 Hz, t<sub>11</sub> = 24.06 s; (<b>d</b>) f<sub>c</sub> = 40 Hz, t<sub>21</sub> = 26.43 s.</p>
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<p>Tensile force F<sub>Mi</sub> [N] and torque M<sub>Mi</sub> [N·m] course, measured on the laboratory device during braking of the rotating parts system of the laboratory device at f<sub>c</sub> = 50 Hz. (<b>a</b>) t<sub>11</sub> = 20.82 s, (<b>b</b>) t<sub>21</sub> = 23.63 s, (<b>c</b>) t<sub>12</sub> = 29.63 s, (<b>d</b>) t<sub>22</sub> = 32.61 s.</p>
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24 pages, 8709 KiB  
Article
Residual Stress Analysis at the Conductor–Insulator Interface During the Curing Process of Hair-Pin Motors
by Mingze Ma, Hongyi Gan, Xiao Shang, Linsen Song, Yiwen Zhang, Jingru Liu, Chunbai Liu, Yanzhong Hao and Xinming Zhang
Polymers 2024, 16(24), 3514; https://doi.org/10.3390/polym16243514 - 17 Dec 2024
Viewed by 335
Abstract
The curing process of hair-pin motor stator insulation is critical, as residual stress increases the risk of partial discharge and shortens a motor’s lifespan. However, studies on the stress-induced defects during insulation varnish curing remain limited. This research integrates three-dimensional numerical simulations and [...] Read more.
The curing process of hair-pin motor stator insulation is critical, as residual stress increases the risk of partial discharge and shortens a motor’s lifespan. However, studies on the stress-induced defects during insulation varnish curing remain limited. This research integrates three-dimensional numerical simulations and experimental analysis to develop a curing model based on unsaturated polyester imide resin, aiming to explore the mechanisms of residual stress formation and optimization strategies. A dual fiber Bragg grating (FBG) sensor system is employed for simultaneous temperature and strain monitoring, while curing kinetics tests confirm the self-catalytic nature of the process and yield the corresponding kinetic equations. The multi-physics simulation model demonstrates strong agreement with the experimental data. The results show that optimizing the curing process reduces the maximum stress from 45.1 MPa to 38.6 MPa, effectively alleviating the stress concentration. These findings highlight the significant influence of the post-curing temperature phase on residual stress. The proposed model offers a reliable tool for stress prediction and process optimization in various insulating materials, providing valuable insights for motor insulation system design. Full article
(This article belongs to the Special Issue Application and Characterization of Polymer Composites)
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<p>Flowchart of the experimental and simulation process.</p>
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<p>FBG in situ measurement. (<b>a</b>) Test equipment; (<b>b</b>) curing test model; (<b>c</b>) curing procedure.</p>
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<p>Curing strain test results of insulating varnish.</p>
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<p>Coupling relationship.</p>
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<p>DSC data analysis. (<b>a</b>) Heat flow–temperature curves; (<b>b</b>) degree of cure–temperature curves; (<b>c</b>) rate of curing at different degrees of cure; (<b>d</b>) fitting curves of the Starink equation; (<b>e</b>) reaction activation energy <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>E</mi> </mrow> <mrow> <mi>a</mi> </mrow> </msub> </mrow> </semantics></math> at different degrees of cure; (<b>f</b>) model validation curves.</p>
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<p>Fitting curve of the DiBenedetto equation.</p>
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<p>Thermal expansion coefficient curve of cured insulating varnish.</p>
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<p>DMA test results.</p>
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<p>Finite element mesh for the simplified curing module.</p>
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<p>Comparison of strain and temperature simulation curves with experimental data.</p>
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<p>Stress distribution in the cross-section of copper wire and insulating varnish.</p>
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<p>Degree of cure distribution in the cross-section of copper wire and insulating varnish.</p>
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<p>Temperature distribution in the cross-section of copper wire and insulating varnish.</p>
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<p>(<b>a</b>) Stress distribution; (<b>b</b>) strain curve of measurement points.</p>
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13 pages, 2944 KiB  
Article
Development of a Wearable Electromyographic Sensor with Aerosol Jet Printing Technology
by Stefano Perilli, Massimo Di Pietro, Emanuele Mantini, Martina Regazzetti, Pawel Kiper, Francesco Galliani, Massimo Panella and Dante Mantini
Bioengineering 2024, 11(12), 1283; https://doi.org/10.3390/bioengineering11121283 - 17 Dec 2024
Viewed by 491
Abstract
Electromyographic (EMG) sensors are essential tools for analyzing muscle activity, but traditional designs often face challenges such as motion artifacts, signal variability, and limited wearability. This study introduces a novel EMG sensor fabricated using Aerosol Jet Printing (AJP) technology that addresses these limitations [...] Read more.
Electromyographic (EMG) sensors are essential tools for analyzing muscle activity, but traditional designs often face challenges such as motion artifacts, signal variability, and limited wearability. This study introduces a novel EMG sensor fabricated using Aerosol Jet Printing (AJP) technology that addresses these limitations with a focus on precision, flexibility, and stability. The innovative sensor design minimizes air interposition at the skin–electrode interface, thereby reducing variability and improving signal quality. AJP enables the precise deposition of conductive materials onto flexible substrates, achieving a thinner and more conformable sensor that enhances user comfort and wearability. Performance testing compared the novel sensor to commercially available alternatives, highlighting its superior impedance stability across frequencies, even under mechanical stress. Physiological validation on a human participant confirmed the sensor’s ability to accurately capture muscle activity during rest and voluntary contractions, with clear differentiation between low and high activity states. The findings highlight the sensor’s potential for diverse applications, such as clinical diagnostics, rehabilitation, and sports performance monitoring. This work establishes AJP technology as a novel approach for designing wearable EMG sensors, providing a pathway for further advancements in miniaturization, strain-insensitive designs, and real-world deployment. Future research will explore optimization for broader applications and larger populations. Full article
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<p>Design solutions chosen for the creation of the sensor with <span class="html-italic">AJP</span> technology: (<b>a</b>) eight-pole sensor in plane view; (<b>b</b>) eight-pole sensor in 3D view.</p>
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<p>Sensor deposed with AJPs onto a Kapton<sup>®</sup> sheet.</p>
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<p>Frequency–impedance trend for the CALLIBRI<sup>®</sup> sensor with conductive gel. The average and standard deviation for each set of measurements are shown.</p>
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<p>Frequency–impedance trend for the AJP sensor without conductive gel. The average and standard deviation for each set of measurements are shown.</p>
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<p>Experimental setup for analyzing the deformation/impedance properties for the sensor realized with the AJP technique.</p>
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<p>The impedance–frequency trend for the AJP sensor with the <span class="html-italic">X</span>-axis oriented parallel to the long side of the plate and glued to an aluminum bar. (<b>a</b>) Trend of the sensor in undeformed bar condition; (<b>b</b>) trend of the sensor in deformed bar condition.</p>
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<p>Impedance–frequency trend for the AJP sensor with the <span class="html-italic">Y</span>-axis oriented orthogonal to the long side of the plate and glued to an aluminum bar. (<b>a</b>) Trend of the sensor in undeformed bar condition; (<b>b</b>) trend of the sensor in deformed bar condition.</p>
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<p>EMG signal throught the Callibri and AJP printed sensor; (<b>A</b>) Callibri resting state timecourse; (<b>B</b>) Callibri resting state power spectrum; (<b>C</b>) Callibri MVC timecourse; (<b>D</b>) Callibri MVC power spectrum; (<b>E</b>) AJP sensor resting state; (<b>F</b>) AJP sensor power spectrum; (<b>G</b>) AJP sensor MVC resting state; (<b>H</b>) AJP sensor power spectrum.</p>
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16 pages, 4022 KiB  
Article
Effectiveness of Differentiating Mold Levels in Soybeans with Electronic Nose Detection Technology
by Xuejian Song, Lili Qian, Dongjie Zhang, Xinhui Wang, Lixue Fu and Mingming Chen
Foods 2024, 13(24), 4064; https://doi.org/10.3390/foods13244064 - 17 Dec 2024
Viewed by 404
Abstract
This study employed electronic nose technology to assess the mold levels in soybeans, conducting analyses on artificially inoculated soybeans with five strains of fungi and distinguishing them from naturally moldy soybeans. Principal component analysis (PCA) and linear discriminant analysis (LDA) were used to [...] Read more.
This study employed electronic nose technology to assess the mold levels in soybeans, conducting analyses on artificially inoculated soybeans with five strains of fungi and distinguishing them from naturally moldy soybeans. Principal component analysis (PCA) and linear discriminant analysis (LDA) were used to evaluate inoculated and naturally moldy samples. The results revealed that the most influential sensor was W2W, which is sensitive to organic sulfur compounds, followed by W1W (primarily responsive to inorganic sulfur compounds), W5S (sensitive to small molecular nitrogen oxides), W1S (responsive to short-chain alkanes such as methane), and W2S (sensitive to alcohols, ethers, aldehydes, and ketones). These findings highlight that variations in volatile substances among the moldy soybean samples were predominantly attributed to organic sulfur compounds, with significant distinctions noted in inorganic sulfur, nitrogen compounds, short-chain alkanes, and alcohols/ethers/aldehydes/ketones. The results of the PCA and LDA analyses indicated that while both methods demonstrated moderate effectiveness in distinguishing between different dominant fungal inoculations and naturally moldy soybeans, they were more successful in differentiating various levels of moldiness, achieving a discriminative accuracy rate of 82.72% in LDA. Overall, the findings suggest that electronic nose detection technology can effectively identify mold levels in soybeans. Full article
(This article belongs to the Section Food Analytical Methods)
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<p>Analysis of the response value of sensors for each mildew degree. (<b>A</b>) No mildew; (<b>B</b>) <span class="html-italic">Aspergillus niger</span>; (<b>C</b>) <span class="html-italic">Penicillium rubens</span>; (<b>D</b>) <span class="html-italic">Rhizopus microsporus</span>; (<b>E</b>) <span class="html-italic">Penicillium oxalicum</span>; (<b>F</b>) <span class="html-italic">Aspergillus versicolor</span>; (<b>G</b>) Naturally mildewed soybean.</p>
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<p>Analysis of the response value of sensors for each mildew degree. (<b>A</b>) No mildew; (<b>B</b>) <span class="html-italic">Aspergillus niger</span>; (<b>C</b>) <span class="html-italic">Penicillium rubens</span>; (<b>D</b>) <span class="html-italic">Rhizopus microsporus</span>; (<b>E</b>) <span class="html-italic">Penicillium oxalicum</span>; (<b>F</b>) <span class="html-italic">Aspergillus versicolor</span>; (<b>G</b>) Naturally mildewed soybean.</p>
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<p>Analysis of the response value of sensors for each mildew degree. (<b>A</b>) No mildew; (<b>B</b>) <span class="html-italic">Aspergillus niger</span>; (<b>C</b>) <span class="html-italic">Penicillium rubens</span>; (<b>D</b>) <span class="html-italic">Rhizopus microsporus</span>; (<b>E</b>) <span class="html-italic">Penicillium oxalicum</span>; (<b>F</b>) <span class="html-italic">Aspergillus versicolor</span>; (<b>G</b>) Naturally mildewed soybean.</p>
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<p>Comparative analysis of response values of soybean sensors with different molds. (<b>A</b>) No mildew; (<b>B</b>) Mild mildew; (<b>C</b>) Moderate mildew; (<b>D</b>) Severe mildew.</p>
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<p>Sensor contribution: PCA and LDA score plots. (<b>A</b>) Analysis chart of the sensor contribution rate. (<b>B</b>) PCA scores of five dominant molds inoculated and naturally mildewed soybeans. (<b>C</b>) LDA scores of five dominant molds inoculated and naturally mildewed soybeans. Note: A–E are <span class="html-italic">Aspergillus niger</span>, <span class="html-italic">Penicillium rubrum</span>, <span class="html-italic">Rhizopus microsporioides</span>, <span class="html-italic">Penicillium oxalicum</span>, and <span class="html-italic">Aspergillus versicolor</span> inoculated soybeans, and F is naturally mildewed soybeans; 1–3 represent mild, moderate, and severe mildew respectively.</p>
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<p>Sensor contribution: PCA and LDA score plots. (<b>A</b>) Analysis chart of the sensor contribution rate. (<b>B</b>) PCA scores of five dominant molds inoculated and naturally mildewed soybeans. (<b>C</b>) LDA scores of five dominant molds inoculated and naturally mildewed soybeans. Note: A–E are <span class="html-italic">Aspergillus niger</span>, <span class="html-italic">Penicillium rubrum</span>, <span class="html-italic">Rhizopus microsporioides</span>, <span class="html-italic">Penicillium oxalicum</span>, and <span class="html-italic">Aspergillus versicolor</span> inoculated soybeans, and F is naturally mildewed soybeans; 1–3 represent mild, moderate, and severe mildew respectively.</p>
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<p>Sensor contribution: PCA and LDA score plots. (<b>A</b>) Analysis chart of the sensor contribution rate. (<b>B</b>) PCA scores of five dominant molds inoculated and naturally mildewed soybeans. (<b>C</b>) LDA scores of five dominant molds inoculated and naturally mildewed soybeans. Note: A–E are <span class="html-italic">Aspergillus niger</span>, <span class="html-italic">Penicillium rubrum</span>, <span class="html-italic">Rhizopus microsporioides</span>, <span class="html-italic">Penicillium oxalicum</span>, and <span class="html-italic">Aspergillus versicolor</span> inoculated soybeans, and F is naturally mildewed soybeans; 1–3 represent mild, moderate, and severe mildew respectively.</p>
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<p>PCA and LDA scores of different moldy soybean grades. (<b>A</b>) PCA score map; (<b>B</b>) LDA score map.</p>
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<p>PCA and LDA scores of different moldy soybean grades. (<b>A</b>) PCA score map; (<b>B</b>) LDA score map.</p>
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25 pages, 17344 KiB  
Review
Wearable Electrospun Nanofibrous Sensors for Health Monitoring
by Nonsikelelo Sheron Mpofu, Tomasz Blachowicz, Andrea Ehrmann and Guido Ehrmann
Micro 2024, 4(4), 798-822; https://doi.org/10.3390/micro4040049 - 16 Dec 2024
Viewed by 371
Abstract
Various electrospinning techniques can be used to produce nanofiber mats with randomly oriented or aligned nanofibers made of different materials and material mixtures. Such nanofibers have a high specific surface area, making them sensitive as sensors for health monitoring. The entire nanofiber mats [...] Read more.
Various electrospinning techniques can be used to produce nanofiber mats with randomly oriented or aligned nanofibers made of different materials and material mixtures. Such nanofibers have a high specific surface area, making them sensitive as sensors for health monitoring. The entire nanofiber mats are very thin and lightweight and, therefore, can be easily integrated into wearables such as textile fabrics or even patches. Nanofibrous sensors can be used not only to analyze sweat but also to detect physical parameters such as ECG or heartbeat, movements, or environmental parameters such as temperature, humidity, etc., making them an interesting alternative to other wearables for continuous health monitoring. This paper provides an overview of various nanofibrous sensors made of different materials that are used in health monitoring. Both the advantages of electrospun nanofiber mats and their potential problems, such as inhomogeneities between different nanofiber mats or even within one electrospun specimen, are discussed. Full article
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<p>Needle-based electrospinning in a (<b>a</b>) vertical and (<b>b</b>) horizontal setup. Reprinted from [<a href="#B20-micro-04-00049" class="html-bibr">20</a>], with permission from Elsevier.</p>
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<p>Needle-based electrospinning in a (<b>a</b>) vertical and (<b>b</b>) horizontal setup. Reprinted from [<a href="#B20-micro-04-00049" class="html-bibr">20</a>], with permission from Elsevier.</p>
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<p>Diagrams of (<b>a</b>) a roller electrospinning machine; (<b>b</b>) a wire electrospinning machine. From [<a href="#B27-micro-04-00049" class="html-bibr">27</a>], originally published under a CC BY license.</p>
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<p>Schematic electrospinning setup for collecting continuous aligned fibers: (<b>a</b>) fast-rotating cylindrical collector (reprinted from [<a href="#B33-micro-04-00049" class="html-bibr">33</a>], with permission from Elsevier); (<b>b</b>) collector from two conductive silicon (Si) stripes separated by a gap (reprinted (adapted) with permission from [<a href="#B34-micro-04-00049" class="html-bibr">34</a>]). Copyright 2003 American Chemical Society.</p>
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<p>(<b>a</b>) Yarn-spinning setup with water bath-grounded collector electrode; (<b>b</b>) the top view of the yarn formation process. (<b>a</b>,<b>b</b>) Reprinted from [<a href="#B39-micro-04-00049" class="html-bibr">39</a>], with permission from Elsevier.</p>
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<p>(<b>a</b>–<b>c</b>) Scanning electron microscopy (SEM) images of the gelatin fibers produced at 20% (<span class="html-italic">w</span>/<span class="html-italic">v</span>) in formic acid at various conditions. The distance between the tip and the metal collector was 15 cm, and the applied voltage was set to 15 kV. The flow rate varied between 2.5 and 10 μL per min. (<b>d</b>–<b>f</b>) The applied voltage varied from 10 to 20 kV, keeping the distance between the tip and metal plate at a constant value of 15 cm, along with a constant flow rate of 5 μL/min. Reprinted from [<a href="#B49-micro-04-00049" class="html-bibr">49</a>], with permission from Elsevier.</p>
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<p>(<b>a</b>) Free-surface electrospinning from wire electrodes, illustrated for a single liquid. The liquid bath (gold) is charged to a high voltage. As the spindle of wires rotates counterclockwise (as viewed here), the entrained solution first forms a film, as shown on the first (leftmost) wire, which then breaks up into droplets, as shown on the second (middle) wire. As the spindle rotates, the electric field at the wire increases so that each droplet emits a fluid jet, as shown on the third (rightmost) wire. Evaporation of solvent results in the formation of dry fibers. (<b>b</b>) Evolution of the surface profiles of the two immiscible liquids as the wire (viewed end on) travels through the liquid interfaces. Reprinted from [<a href="#B55-micro-04-00049" class="html-bibr">55</a>], with permission from Elsevier.</p>
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<p>Nanofiber yarn-based fabrics manufactured by traditional textile-forming processes: (<b>A</b>) a simple closed chain stitch structure and a relatively complex weft plain stitch tubing structure by knitting technique; (<b>B</b>) three nanofiber yarn-based braided constructs; (<b>C</b>) “Nano” pattern formed on polyester plain woven fabric by embroidering. Reprinted from [<a href="#B98-micro-04-00049" class="html-bibr">98</a>], with permission from Elsevier.</p>
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<p>(<b>a</b>) Schematic of the fabrication process for the stretchable AM temperature sensor array. TFT: thin film transistor; PET: poly(ethylene terephthalate); (<b>b</b>) assembly of prepared layers, liquid metal injection, and formation of electrical contacts with the Ag NW sticker; SWCNT: walled carbon nanotube; Ag NW: silver nanowires; (<b>c</b>) circuit diagram of the stretchable active-matrix temperature sensor array. Reprinted from [<a href="#B114-micro-04-00049" class="html-bibr">114</a>], with permission from Wiley.</p>
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<p>Schematic diagram of the handheld electrospinning device for skin in situ coating with a nanofiber mat. Reprinted from [<a href="#B123-micro-04-00049" class="html-bibr">123</a>], with permission from Elsevier.</p>
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<p>(<b>a</b>) The figure of five auscultation points on the human skeleton. A: aortic; P: pulmonic; E: Erb’s point; T: tricuspid; M: mitral. (<b>b</b>) The image of the experimental setup for heart sound; (<b>c</b>) the image of the heart sound device worn by the subject on (<b>b</b>); the heart sound waveform measured on-site in five auscultation points including (<b>d</b>) aortic point, (<b>e</b>) pulmonic point, (<b>f</b>) Erb’s point, (<b>g</b>) tricuspid point, and (<b>h</b>) mitral valve point; comparison between (<b>i</b>) ECG signal and (<b>j</b>) heart sound signal; (<b>k</b>) captured signal and (<b>l</b>) source signal of aortic insufficiency heart sound recording; (<b>m</b>) captured signal and (<b>n</b>) source signal of atrial septal defect heart sound recording. Reprinted from [<a href="#B130-micro-04-00049" class="html-bibr">130</a>], originally published under a CC BY-NC-ND license.</p>
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<p>Respiration response curves during continuous different motion states and magnified response curves in the black frame regions. Reprinted from [<a href="#B140-micro-04-00049" class="html-bibr">140</a>], originally published under a CC BY license.</p>
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<p>(<b>a</b>) Response of the sensor to various wrist bending angles; (<b>b</b>) response of the sensor to sideways wrist flicking; (<b>c</b>,<b>d</b>) response of the sensor to deep and normal breathing, respectively; (<b>e</b>,<b>f</b>) response of the sensor to walking in a straight line and spot jogging, respectively. Reprinted from [<a href="#B151-micro-04-00049" class="html-bibr">151</a>], originally published under a CC BY license.</p>
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<p>Schematics of (<b>a</b>,<b>b</b>) the fabrication process of microstructured electrodes, (<b>c</b>) the assembled array as a capacitive pressure sensor, and (<b>d</b>) the performance measurement setup of the sensor. PI: polyimide, PDMS: polydimethylsiloxane, DMF: dimethylformamide, PVDF: polyvinylidene difluoride. Reprinted from [<a href="#B161-micro-04-00049" class="html-bibr">161</a>], with permission from Elsevier.</p>
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<p>Temperature sensing behavior and application of a graphite nanosheet/PA66 nanofiber mat: (<b>a</b>) resistance–temperature curve from 30 °C to 130 °C; (<b>b</b>) resistance response vs. temperature under repeated heating/cooling cycles (between 30 °C and 100 °C); (<b>c</b>) sensing behavior of monitoring the hot wind blown out by a commercial blower and (<b>d</b>) touching a cup filled with hot water. Reprinted from [<a href="#B128-micro-04-00049" class="html-bibr">128</a>], with permission from Elsevier.</p>
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<p>(<b>a</b>) Resistance of the MXene, poly(vinyl alcohol) (PVA), and PVA/MXene film sensor exposed to various relative humidities; (<b>b</b>) dynamic resistance changes of PVA/MXene film sensor exposed to various relative humidities; (<b>c</b>) repeatability of PVA/MXene film sensor; (<b>d</b>) time-dependent resistance response and recovery curves of the PVA/MXene sensor between 11 and 97% rH; (<b>e</b>) resistance of sensor with increasing and decreasing humidity; (<b>f</b>) humidity hysteresis curves of the PVA/MXene nanofibers film sensor. Reprinted from [<a href="#B179-micro-04-00049" class="html-bibr">179</a>], originally published under a CC BY license.</p>
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14 pages, 7499 KiB  
Article
Smart Concrete Using Optical Sensors Based on Bragg Gratings Embedded in a Cementitious Mixture: Cure Monitoring and Beam Test
by Edson Souza, Pâmela Pinheiro, Felipe Coutinho, João Dias, Ronaldo Pilar, Maria José Pontes and Arnaldo Leal-Junior
Sensors 2024, 24(24), 7998; https://doi.org/10.3390/s24247998 - 14 Dec 2024
Viewed by 323
Abstract
Smart concrete is a structural element that can combine both sensing and structural capabilities. In addition, smart concrete can monitor the curing of concrete, positively impacting design and construction approaches. In concrete, if the curing process is not well developed, the structural element [...] Read more.
Smart concrete is a structural element that can combine both sensing and structural capabilities. In addition, smart concrete can monitor the curing of concrete, positively impacting design and construction approaches. In concrete, if the curing process is not well developed, the structural element may develop cracks in this early stage due to shrinkage, decreasing structural mechanical strength. In this paper, a system of measurement using fiber Bragg grating (FBG) sensors for monitoring the curing of concrete was developed to evaluate autogenous shrinkage strain, temperature, and relative humidity (RH) in a single system. Furthermore, K-type thermocouples were used as reference temperature sensors. The results presented maximum autogenous shrinkage strains of 213.64 με, 125.44 με, and 173.33 με for FBG4, FBG5, and FBG6, respectively. Regarding humidity, the measured maximum relative humidity was 98.20 %RH, which was reached before 10 h. In this case, the recorded maximum temperature was 63.65 °C and 61.85 °C by FBG2 and the thermocouple, respectively. Subsequently, the concrete specimen with the FBG strain sensor embedded underwent a bend test simulating beam behavior. The measurement system can transform a simple structure like a beam into a smart concrete structure, in which the FBG sensors’ signal was maintained by the entire applied load cycles and compared with FBG strain sensors superficially positioned. In this test, the maximum strain measurements were 85.65 με, 123.71 με, and 56.38 με on FBG7, FBG8, and FBG3, respectively, with FBG3 also monitoring autogenous shrinkage strain. Therefore, the results confirm that the proposed system of measurement can monitor the cited parameters throughout the entire process of curing concrete. Full article
(This article belongs to the Section Optical Sensors)
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<p>FBG Hygrometer Sensor. The zoomed-in view shows details of the FBGs.</p>
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<p>The curing concrete setup photo is presented in (<b>A</b>). The experimental components are identified in the schematic drawing (<b>B</b>).</p>
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<p>The photo (<b>A</b>) presents the shrinkage bench, where the autogenous shrinkage strain was measured. The distribution of the FBG strain sensors is identified in the schematic drawing (<b>B</b>).</p>
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<p>The bend test using three-point bending. (<b>A</b>) presents a photo of the positioning of smart concrete and (<b>B</b>) presents a schematic representation using two supports and one loading point, highlighted in red.</p>
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<p>Temperature sensitivity calibration for FBG2 for relative humidities of 60 %RH, 70 %RH, 80 %RH, 90 %RH, and 95 %RH.</p>
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<p>Temperature sensitivity calibration for FBG1 for relative humidities of 60 %RH, 70 %RH, 80 %RH, 90 %RH, and 95 %RH.</p>
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<p>Relative humidity sensitivity calibration for FBG1 for temperatures of 30 °C, 40 °C, and 45 °C.</p>
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<p>Comparison between the temperature curves obtained by the thermocouple and FBG2.</p>
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<p>Relative humidity variation versus the test time, monitored by FBG1.</p>
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<p>Monitored temperature by thermocouple versus time in the concrete specimen of shrinkage bench.</p>
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<p>Monitored strain by the FBG4, FBG5, and FBG6 strain sensors versus time. For FBG3, the Bragg wavelength shift during the test is presented.</p>
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<p>Monitored autogenous shrinkage strain by FBG4, FBG5, and FBG6 versus test time.</p>
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<p>FBG7, FBG8, and FBG3 strain responses to applied bend load cycles.</p>
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19 pages, 7232 KiB  
Article
Finite Element Simulation of Acoustic Emissions from Different Failure Mechanisms in Composite Materials
by Manoj Rijal, David Amoateng-Mensah and Mannur J. Sundaresan
Materials 2024, 17(24), 6085; https://doi.org/10.3390/ma17246085 - 12 Dec 2024
Viewed by 565
Abstract
Damage in composite laminates evolves through complex interactions of different failure modes, influenced by load type, environment, and initial damage, such as from transverse impact. This paper investigates damage growth in cross-ply polymeric matrix laminates under tensile load, focusing on three primary failure [...] Read more.
Damage in composite laminates evolves through complex interactions of different failure modes, influenced by load type, environment, and initial damage, such as from transverse impact. This paper investigates damage growth in cross-ply polymeric matrix laminates under tensile load, focusing on three primary failure modes: transverse matrix cracks, delaminations, and fiber breaks in the primary loadbearing 0-degree laminae. Acoustic emission (AE) techniques can monitor and quantify damage in real time, provided the signals from these failure modes can be distinguished. However, directly observing crack growth and related AE signals is challenging, making numerical simulations a useful alternative. AE signals generated by the three failure modes were simulated using modified step impulses of appropriate durations based on incremental crack growth. Linear elastic finite element analysis (FEA) was applied to model the AE signal propagating as Lamb waves. Experimental attenuation data were used to modify the simulated AE waveforms by designing arbitrary magnitude response filters. The propagating waves can be detected as surface displacements or surface strains depending upon the type of sensor employed. This paper presents the signals corresponding to surface strains measured by surface-bonded piezoelectric sensors. Fiber break events showed higher-order Lamb wave modes with frequencies over 2 MHz, while matrix cracks primarily exhibited the fundamental S0 and A0 modes with frequencies ranging up to 650 kHz, with delaminations having a dominant A0 mode and frequency content less than 250 kHz. The amplitude and frequency content of signals from these failure modes are seen to change significantly with source–sensor distance, hence requiring an array of dense sensors to acquire the signals effectively. Furthermore, the reasonable correlation between the simulated waveforms and experimental acoustic emission signals obtained during quasi-static tensile test highlights the effectiveness of FEA in accurately modeling these failure modes in composite materials. Full article
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<p>Schematic showing sensor position for carbon/epoxy cross-ply tensile coupons.</p>
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<p>Micrograph of a cross-section of composite laminate showing different failure modes.</p>
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<p>Fiber break event obtained during the experiment: (<b>a</b>) Waveform. (<b>b</b>) Wavelet transform.</p>
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<p>Matrix crack event obtained during the experiment: (<b>a</b>) Waveform. (<b>b</b>) Wavelet transform.</p>
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<p>Delamination event obtained during the experiment: (<b>a</b>) Waveform. (<b>b</b>) Wavelet transform.</p>
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<p>Source time functions and their FFTs used for simulating various failure modes: (<b>a</b>) Fiber break. (<b>b</b>) Matrix crack. (<b>c</b>) Delamination.</p>
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<p>Source time functions and their FFTs used for simulating various failure modes: (<b>a</b>) Fiber break. (<b>b</b>) Matrix crack. (<b>c</b>) Delamination.</p>
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<p>Schematics for various impulse loading showing locations of fiber break and matrix crack events.</p>
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<p>Schematics of couple loading for simulation of delamination events.</p>
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<p>Percentage change in maximum axial stress in consecutive models with increasing number of elements in each lamina for (<b>a</b>) symmetric mode (<b>b</b>) anti-symmetric mode.</p>
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<p>Experimental and extrapolated attenuation values along 0<sup>0</sup> for (<b>a</b>) symmetric and (<b>b</b>) anti-symmetric modes.</p>
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<p>Attenuation values and the response of arbitrary amplitude filters along 0<sup>0</sup> at 100 mm for (<b>a</b>) symmetric and (<b>b</b>) anti-symmetric modes.</p>
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<p>Dispersion curve showing group velocity for [0/90]<sub>3s</sub> laminate used obtained from post-processing the results from GUIGUW software (ver-2.2) [<a href="#B29-materials-17-06085" class="html-bibr">29</a>].</p>
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<p>Simulated FB event obtained at 25 mm from the source at impulse location FB<sub>2</sub>: (<b>a</b>) Axial strain. (<b>b</b>) Wavelet fitted with dispersion curve.</p>
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<p>Simulated MC event obtained at 50 mm from the source at impulse location MC<sub>2</sub>: (<b>a</b>) Axial strain. (<b>b</b>) Wavelet fitted with dispersion curve.</p>
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<p>Simulated delamination event obtained at 50 mm from the source: (<b>a</b>) Axial strain. (<b>b</b>) Wavelet fitted with dispersion curve.</p>
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<p>Waveforms for matrix crack at increasing source to sensor distance for different impulse locations in thermoset cross-ply composite.</p>
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<p>Waveforms for fiber break at increasing source to sensor distance for impulse located at FB<sub>2</sub> in thermoset cross-ply composite.</p>
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<p>Variation of total attenuated energy with distance from the source for different impulse locations for fiber break.</p>
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<p>Variation of total attenuated energy with distance from the source for different impulse locations for matrix crack.</p>
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<p>Comparison of waveforms from FEM and experiments for delamination: (<b>a</b>) FEM. (<b>b</b>) Experimental waveform (C.C 86%).</p>
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<p>Comparison of waveforms from FEM and experiments for fiber break: (<b>a</b>) FEM. (<b>b</b>) Experimental waveform (C.C. 85%).</p>
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<p>Comparison of waveforms from FEM and experiments for matrix crack: (<b>a</b>) FEM. (<b>b</b>) Experimental waveform (C.C 84%).</p>
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15 pages, 6123 KiB  
Article
Impact of Moisture Absorption on Optical Fiber Sensors: New Bragg Law Formulation for Monitoring Composite Structures
by Pietro Aceti and Giuseppe Sala
J. Compos. Sci. 2024, 8(12), 518; https://doi.org/10.3390/jcs8120518 - 9 Dec 2024
Viewed by 490
Abstract
In recent decades, the aviation industry has increasingly adopted composite materials for various aircraft components, due to their high strength-to-weight ratio and durability. To ensure the safety and reliability of these structures, Health and Usage Monitoring Systems (HUMSs) based on fiber optics (FO), [...] Read more.
In recent decades, the aviation industry has increasingly adopted composite materials for various aircraft components, due to their high strength-to-weight ratio and durability. To ensure the safety and reliability of these structures, Health and Usage Monitoring Systems (HUMSs) based on fiber optics (FO), particularly Fiber Bragg Grating (FBG) sensors, have been developed. However, both composite materials and optical fibers are susceptible to environmental factors such as moisture, in addition to the well-known effects of mechanical stress and thermal loads. Moisture absorption can lead to the degradation of mechanical properties, posing a risk to the structural integrity of aircraft components. This research aims to quantify and monitor the impact of moisture on composite materials. A new formulation of the Bragg equation is introduced, incorporating mechanical strain, thermal expansion, and hygroscopic swelling to accurately measure Bragg wavelength variations. Experimental validation was performed using both uncoated and polyimide-coated optical fibers subjected to controlled hygrothermal conditions in a climate chamber. The results demonstrate that uncoated fibers are insensitive to humidity, whereas coated fibers exhibit measurable wavelength shifts due to moisture absorption. The proposed model effectively predicts these shifts, with errors consistently below 2.6%. This approach is crucial for improving the performance and reliability of HUMSs in monitoring composite structures, ensuring long-term safety in extreme environmental conditions. Full article
(This article belongs to the Section Composites Manufacturing and Processing)
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<p>Accidents due to hygrothermal effects.</p>
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<p>Coated optical fiber scheme.</p>
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<p>Experimental setup.</p>
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<p>Wavelength trend in time for an uncoated fiber.</p>
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<p>Linear interpolation and sensitivities, uncoated fiber.</p>
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<p>Coated fiber response.</p>
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<p>Linear interpolation and sensitivities. (<b>a</b>) Linear interpolation for temperature sensitivities. (<b>b</b>) Linear interpolation for humidity sensitivities.</p>
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<p>Comparison between theoretical and experimental wavelengths at each constant temperature.</p>
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<p>Comparison between theoretical and experimental wavelengths at each constant temperature and relative humidity.</p>
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