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Search Results (17,792)

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20 pages, 24436 KiB  
Article
Effect of Dynamic Flexural Strength on Impact Response Analysis of AlN Substrates for Aerospace Applications
by Zhen Wang and Yan Liu
Aerospace 2025, 12(3), 221; https://doi.org/10.3390/aerospace12030221 (registering DOI) - 8 Mar 2025
Abstract
Electronic devices play an extremely important role in the aerospace field. Aluminum nitride (AlN) is a promising ceramic material for high-reliability electronic packaging structures that are subjected to impact loads during service. Quasi-static and dynamic flexural tests were conducted to determine the rate-dependent [...] Read more.
Electronic devices play an extremely important role in the aerospace field. Aluminum nitride (AlN) is a promising ceramic material for high-reliability electronic packaging structures that are subjected to impact loads during service. Quasi-static and dynamic flexural tests were conducted to determine the rate-dependent flexural strengths of AlN ceramics. The impact response of the AlN substrates was investigated using experimental tests and a smeared fixed-crack numerical model. The critical velocity of the impactor and the failure mode of the ceramic plate can be accurately predicted using the Drucker–Prager criterion with the scaled fracture-strength parameter. The radial cracks on the ceramic plate upon impact were well reproduced via the proposed novel numerical technique, showing better accuracy compared to the widely used Johnson–Holmquist II (JH-2) model. The effect of impactor nose shape and deflection angles were further investigated to better illustrate the low-velocity impact response of AlN ceramic substrates. Based on the dynamic flexural-strength testing results, this study achieves the prediction of low-speed impact response for AlN ceramic structures, thereby providing technical support for the impact reliability analysis of aerospace ceramic-packaging devices. Full article
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Figure 1
<p>(<b>a</b>) Schematic of three-point bending tests; (<b>b</b>) Instron-5948 micro-tester for quasi-static flexural tests; (<b>c</b>) modified SHPB device for dynamic flexural tests.</p>
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<p>Typical experimental results for dynamic flexural tests. (<b>a</b>) Original incident, reflected and transmitted waves; (<b>b</b>) flexural stress/loading speed–time curves.</p>
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<p>Low-velocity drop-impact device with high-speed image-recording system. The impact velocity can be calculated by the quotient of the bullet’s height difference (marked by dashed line and arrows) and interval time.</p>
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<p>(<b>a</b>) Numerical model for low-velocity impact tests; (<b>b</b>) integration points in the thickness direction of shell elements; (<b>c</b>) orthogonal cracks existing in one element for smeared fixed-crack model.</p>
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<p>Comparison of different failure criteria. (<b>a</b>) Rankine maximum stress failure criterion; (<b>b</b>) Mohr–Coulomb failure criterion; (<b>c</b>) Drucker–Prager failure criterion; (<b>d</b>) Comparison of different failure criteria at the first quadrant.</p>
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<p>Application of rate-dependent flexural strength in smeared fixed-crack model.</p>
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<p>Effects of different failure criteria and scaled strength on simulation results. The different colors represent different velocity regions as marked in the figure.</p>
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<p>Comparison of failure modes of AlN substrates between experimental observations and numerical simulations with different impact velocities.</p>
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<p>Detailed comparison for crack patterns of AlN plates. A partial enlarged image for the impacted region of AlN specimen loaded at 4.29 m/s was marked by the dashed square.</p>
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<p>Vector plot of crack direction for the AlN plate under the impact velocity of 4.29 m/s.</p>
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<p>JH-2 model.</p>
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<p>A comparison between experimental observation, the smeared fixed-crack model, and JH-2 model simulation results for the AlN plate impacted at the velocity of 4.29 m/s.</p>
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<p>(<b>a</b>) Spherical and flat-nosed projectiles with the same diameter of 9.6 mm and weight of 32.4 g; (<b>b</b>) AlN plate impacted by a spherical-nosed projectile at 4 m/s; (<b>c</b>) AlN plate impacted by a flat-nosed projectile at 4 m/s.</p>
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<p>A comparison of the ceramic plates’ maximum principal-stress-field evolution impacted by different nosed projectiles at 4 m/s. (<b>a</b>) sphere nosed projectile; (<b>b</b>) flat-nosed projectile.</p>
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<p>Effect of deflection angles for spherical (<b>left</b>) and flat (<b>right</b>)-nosed projectiles.</p>
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<p>Critical impact velocity range for spherical and flat-nosed projectiles with different deflection angles.</p>
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<p>Failure modes of AlN ceramic plates impacted by the flat-nosed projectile under different impact velocities with a deflection angle of 2°.</p>
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20 pages, 3012 KiB  
Article
Experimental Investigation and Prediction of Mechanical Properties of Carbonate Rocks Under Uniaxial and Triaxial Compressions
by Esraa Alomari, Kam Ng and Lokendra Khatri
Materials 2025, 18(6), 1211; https://doi.org/10.3390/ma18061211 (registering DOI) - 8 Mar 2025
Abstract
Compressive strength and Young’s modulus are key design parameters in rock engineering, essential for understanding the mechanical behavior of carbonate rocks. Understanding the mechanical behavior of carbonate rocks under varying load conditions is crucial for geotechnical stability analysis. In this paper, empirical relationships [...] Read more.
Compressive strength and Young’s modulus are key design parameters in rock engineering, essential for understanding the mechanical behavior of carbonate rocks. Understanding the mechanical behavior of carbonate rocks under varying load conditions is crucial for geotechnical stability analysis. In this paper, empirical relationships are developed to predict the mechanical properties of carbonate rocks. A series of uniaxial and triaxial compression experiments were conducted on carbonate rocks including limestone, dolostone, and granite from Wyoming. In addition, experimental data on different carbonate rocks from the literature are compiled and integrated into this study to evaluate the goodness of fit of our proposed empirical relationships in the prediction of compressive strength and Young’s modulus of carbonate rocks. Regression analysis was used to develop predictive models for the uniaxial compressive strength (UCS), Young’s modulus (E), and triaxial compressive strength (σ1) incorporating parameters such as the porosity (n) and confining pressure (σ3). The results indicated that the UCS and Young’s modulus showed a power relationship with porosity (n), whereas the σ1 showed a linear relationship with n and σ3. Furthermore, an analytical model expanded from the wing crack model was applied to predict the σ1 of limestone based on the coefficient of friction, the initial level of damage, the initial flaw size, and the fracture toughness of the rock. The model showed a good predictability of the σ1 with a mean bias (i.e., the ratio of the measured to the predicted strength) of 1.07, indicating its reliability in accurately predicting the rock strength. This predictability is crucial for making informed engineering decisions, design optimization, and improving safety protocols in practical applications such as structural analysis and manufacturing processes. Full article
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<p>Testing equipment GCTS Rapid Triaxial Rock (RTR-1500) for triaxial compression testing.</p>
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<p>Three deviatoric stress–strain curves of Sherman granite specimens under confining pressures of 0, 4, and 10 MPa.</p>
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<p>The negative relationship between the rock <span class="html-italic">UCS</span> and porosity, indicating how increased rock porosity can lead to strength reduction.</p>
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<p>The linear relationship between peak compressive strength, porosity, and confining pressure, highlighting a positive correlation with confining pressure and a negative correlation with porosity.</p>
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<p>Power relationship showing the decrease in mean Young’s modulus (<span class="html-italic">E</span>) as porosity (<span class="html-italic">n</span>) increases.</p>
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<p>Wing crack growth from an inclined crack under compression (adapted from Ashby and Hallam [<a href="#B17-materials-18-01211" class="html-bibr">17</a>]).</p>
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<p>Comparison of measured and predicted compressive strengths for carbonate rocks, showing a good accuracy in predicting the compressive strength.</p>
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20 pages, 5869 KiB  
Article
Research on the Long-Term Mechanical Behavior and Constitutive Model of Cemented Tailings Backfill Under Dynamic Triaxial Loading
by Yuye Tan, Jinshuo Yang, Yuchao Deng, Yunpeng Kou, Yiding Li and Weidong Song
Minerals 2025, 15(3), 276; https://doi.org/10.3390/min15030276 (registering DOI) - 8 Mar 2025
Abstract
Cemented tailings backfill (CTB) plays an important role in mine filling operations. In order to study the long-term stability of CTB under the dynamic disturbance of deep wells, ultrafine cemented tailings backfill was taken as the research object, and the true triaxial hydraulic [...] Read more.
Cemented tailings backfill (CTB) plays an important role in mine filling operations. In order to study the long-term stability of CTB under the dynamic disturbance of deep wells, ultrafine cemented tailings backfill was taken as the research object, and the true triaxial hydraulic fracturing antireflection-wetting dynamic experimental system of coal and rock was used to carry out a static true triaxial compression test, a true triaxial compression test under unidirectional disturbance, and a true triaxial compression test under bidirectional disturbance. At the same time, the acoustic emission monitoring and positioning tests of the CTB were carried out during the compression test. The evolution law of the mechanical parameters and deformation and failure characteristics of CTB under different confining pressures is analyzed, and the damage constitutive model of the filling body is established using stochastic statistical theory. The results show that the compressive strength of CTB increases with an increase in intermediate principal stress. According to the change process of the acoustic emission ringing count over time, the triaxial compression test can be divided into four stages: the initial active stage, initial calm stage, pre-peak active stage, and post-peak calm stage. When the intermediate principal stress is small, the specimen is dominated by shear failure. With an increase in the intermediate principal stress, the specimen changes from brittle failure to plastic failure. The deformation and failure strength of CTB are closely related to its loading and unloading methods. Under a certain stress intensity, compared with unidirectional unloading, bidirectional unloading produces a greater deformation of the rock mass, and the failure strength of the rock mass is higher. This study only considers the confining pressure within the compressive limit of the specimen. Future research can be directed at a wider range of stresses to improve the applicability and reliability of the research results. Full article
(This article belongs to the Special Issue Advances in Mine Backfilling Technology and Materials)
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<p>Particle size composition of ultrafine tailings.</p>
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<p>Chemical composition of ultrafine tailings.</p>
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<p>Chemical composition of cementitious materials.</p>
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<p>Loading diagram.</p>
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<p>Experimental process.</p>
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<p>Stress–strain curves of CTB specimens under different loading conditions.</p>
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<p>Loading time–energy acoustic emission curve of CTB under different loading conditions: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa.</p>
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<p>Loading time–energy acoustic emission curve of CTB under different loading conditions: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa.</p>
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<p>CTB true triaxial dynamic load disturbance test under various conditions damaging fracturing diagram: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa. (Red line: cracks on the front of the specimen, green line: cracks on other surfaces of the specimen).</p>
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<p>Complete stress–strain curves of unidirectional disturbance test of CTB: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa.</p>
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<p>Unidirectional acoustic emission energy curves of CTB: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa.</p>
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<p>Unidirectional disturbance macroscopic failure characteristics of CTB: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa. (B, U, F, L and R represent the back, up, front, left and right sides respectively. Red line: cracks on the front, upper and right sides of the specimen; green line: cracks on other surfaces of the specimen).</p>
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<p>Complete stress–strain curves of bidirectional disturbance test of CTB: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa.</p>
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<p>Bidirectional acoustic emission energy curves of CTB: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa.</p>
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<p>Macroscopic failure characteristics of bidirectional disturbance of CTB: (<b>a</b>) σ<sub>2</sub> = 0.3 MPa; (<b>b</b>) σ<sub>2</sub> = 0.5 MPa; and (<b>c</b>) σ<sub>2</sub> = 0.7 MPa.(B, U, F, L and R represent the back, up, front, left and right sides respectively. Red line: cracks on the front, upper and right sides of the specimen; green line: cracks on other surfaces of the specimen).</p>
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11 pages, 540 KiB  
Article
Cephalomedullary Nailing vs. Dynamic Hip Screw for the Treatment of Pertrochanteric Fractures: The Role of Cytokines in the Prediction of Surgical Invasiveness
by Armando Del Prete, Pasquale Sessa, Ferdinando Del Prete, Christian Carulli, Giacomo Sani, Mariangela Manfredi and Roberto Civinini
J. Clin. Med. 2025, 14(6), 1825; https://doi.org/10.3390/jcm14061825 (registering DOI) - 8 Mar 2025
Viewed by 39
Abstract
Background/Objectives: Limited surgical invasiveness is desirable in elderly patients with femur fracture. Serum cytokines have been considered as a possible marker but with inconclusive evidence. The present study aimed to assess the systemic inflammatory response to surgical trauma through the serum levels [...] Read more.
Background/Objectives: Limited surgical invasiveness is desirable in elderly patients with femur fracture. Serum cytokines have been considered as a possible marker but with inconclusive evidence. The present study aimed to assess the systemic inflammatory response to surgical trauma through the serum levels of several cytokines (IL1β, IL6, IL8, and IL-10), inflammatory markers (c reactive protein—CRP), and muscular damage markers (creatinkinase—CK) at different time intervals in a consecutive series of patients affected by pertrochanteric fractures (PFs) and treated by two different surgical devices (intramedullary nailing (IM) vs. dynamic hip screw plate—DHS). Methods: A total of 60 consecutive patients (45 female and 15 male, mean age 85.6 years) with PFs (AO31A1.2-2.2) were randomly assigned to two groups according to the surgical procedure used (IM vs. DHS). Specimens of venous blood were collected 1 h preoperatively and at 24, 48, and 72 h postoperatively. Commercial ELISA kits were used. Results: In the adjusted linear mixed model, the serum levels of IL-1β, IL-8, IL-10, CRP, and CK revealed no statistically significant correlation with the type of surgical intervention performed. A significant (p < 0.001) correlation was found for IL-6 values in patients undergoing IM, showing higher serum values than patients receiving DHSs in all postoperative blood sample collections. Conclusions: The results of this study reveal that the use of DHSs may have less biological impact than IM in frail elderly due to a more limited secretion of IL-6 cytokines deriving from the preservation of the femoral medullary canal, representing a possible guide for the choice of the surgical device. Full article
(This article belongs to the Section Orthopedics)
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<p>The IL, CRP, CK, and VAS delta mean serum differences trends in the observed time intervals are shown in this figure. DHS: dynamic hip screw.</p>
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<p>The figure shows the forest plot of the crude (upper lines) and adjusted (lower lines) linear mixed model for the IL-6 delta values. In the adjusted model, a delta value of 15.69 (95%CI, 1.21–3.17) reveals a significant correlation between the variable and the performed surgical technique (cephalomedullary nail vs. dynamic hip screw—DHS).</p>
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32 pages, 2621 KiB  
Article
Mechanical Characterization of Dicyclopentadiene and Glass-Fibre-Reinforced Polymer Subjected to Low to High Strain Rate
by Rogério F. F. Lopes, Daniela Azevedo, Gonçalo P. Cipriano, Tiago M. R. M. Domingues and Pedro M. G. P. Moreira
Polymers 2025, 17(6), 715; https://doi.org/10.3390/polym17060715 - 7 Mar 2025
Viewed by 84
Abstract
This work provides a detailed description of the procedures employed to characterize the mechanical behaviour of two materials present in a coach’s exterior panels, including glass-fibre-reinforced polymer (GFRP) and neat DCPD (dicyclopentadiene)-based polymers. Tensile tests were conducted at quasi-static, intermediate 1 s-1 [...] Read more.
This work provides a detailed description of the procedures employed to characterize the mechanical behaviour of two materials present in a coach’s exterior panels, including glass-fibre-reinforced polymer (GFRP) and neat DCPD (dicyclopentadiene)-based polymers. Tensile tests were conducted at quasi-static, intermediate 1 s-1, 10 s-1, and high strain rates 150 s-1, 250 s-1 to obtain a comprehensive understanding of their behaviour. The results indicate positive and significant dependence on the strain rate. Additionally, GFRP demonstrates superior energy absorption capacity for higher strain rates, unlike DCPD, which exhibits a higher energy absorption capacity for QS tests. In the case of DCPD, raising the strain rate to 10 s-1 the maximum stress was not affected but decreased the elongation at fracture. At higher strain rates, there was an increase in maximum stress alongside greater elongation. DCPD maintained consistent stiffness across all rates ranging between 2087 MPa and 2389 MPa, and the tests disclosed a failure mode characterized by numerous surface-transverse fissures. Regarding GFRP, a more pronounced variation in stiffness is observed, decreasing from 11,005 MPa to 4532 MPa at 133 s⁻1, recovering to 7288 MPa at 252 s⁻1. In addition, the maximum stress and failure elongation tends to increase with the strain rate increase. The detailed analysis of these results provides valuable insights into the mechanical behaviour of these materials under different loading conditions. Full article
(This article belongs to the Special Issue Advances in Fracture and Failure of Polymers)
11 pages, 5951 KiB  
Article
The Osteoinductive Effect of Water-Soluble Matrix from Nano-Nacre Particles of Haliotis diversicolor (H. diversicolor) Abalone on MC3T3-E1 Osteoblasts
by Chanyatip Suwannasing, Ausanai Prapan, Piyaporn Surinlert, Chanyarak Sombutkayasith and Wattana Weerachatyanukul
Appl. Sci. 2025, 15(6), 2907; https://doi.org/10.3390/app15062907 - 7 Mar 2025
Viewed by 146
Abstract
Osteoporosis is characterized by an imbalance between osteoblastic bone formation and osteoclastic bone resorption, leading to an increased risk of fractures. The water-soluble matrix (WSM) of nacre exhibits osteoinductive properties in osteoblastic cells, both in vitro and in vivo. However, its release from [...] Read more.
Osteoporosis is characterized by an imbalance between osteoblastic bone formation and osteoclastic bone resorption, leading to an increased risk of fractures. The water-soluble matrix (WSM) of nacre exhibits osteoinductive properties in osteoblastic cells, both in vitro and in vivo. However, its release from natural nacre remains challenging due to its solid and compact surface. This study aimed to prepare nano-nacre particles with smaller diameters than intact aragonite crystals to enhance WSM release and to investigate its effects on osteoblast differentiation. Size analysis and SEM imaging showed that the nano-nacre particles had an average size of about 600 nm. Furthermore, their effects on osteoblast differentiation and mineralization were evaluated through qPCR and ARS assay. The results showed that WSM significantly upregulated key osteogenic genes, including RUNX2, ALP, and OCN, in a dose- and time-dependent manner over 14 days, with fold-changes ranging from 1.6 to 3.6. Additionally, the mineralization effects showed calcium deposition levels comparable to those of the positive group. These findings suggest that WSM may be a promising soluble factor for osteoblast differentiation and mineralization. Therefore, understanding the effects of the WSM from H. diversicolor nano-nacre particles on osteoblasts in vitro may provide evidence suggesting that it could be a promising anti-osteoporosis agent. Full article
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<p>Nano-nacre particles observed by scanning electron microscopy. Scale bars represent 5 μm (<b>a</b>) and 0.5 μm (<b>b</b>).</p>
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<p>Protein expression of BMP-2/4 in the WSM from nano-nacre particles of <span class="html-italic">H. diversicolor</span>. Western blotting of protein lysates from three tissues: WSM from nano-nacre particles (WSM) (lane 1), foot tissue (lane 2), and mantle tissue (MT) (lane 3) using a polyclonal antibody against BMP-2/4 (<b>a</b>) and its competition with HdBMP-2/4 peptide (<b>b</b>). Note the reactive band of BMP-2/4 antibody at 47 kDa.</p>
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<p>Effect of WSM from nano-nacre particles of <span class="html-italic">H. diversicolor</span> on cell viability percentage as measured by MTT assay, indicating the non-toxic nature of WSM for MC3T3-E1 cells. Each value is the mean ± SD of three independent experiments when compared with the DMEM group. * <span class="html-italic">p</span> &lt; 0.05 indicates significant differences compared with the control group.</p>
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<p>Effect of WSM from nano-nacre particles of <span class="html-italic">H. diversicolor</span> on osteogenic gene expressions (<b>a</b>–<b>c</b>) using the MC3T3-E1 pre-osteoblastic cell line as a model. The cells were incubated with WSM for 2 consecutive days and collected for mRNA analysis at days 7 and 14 post-treatment. Osteogenic markers assessed include RUNX2 (<b>a</b>), ALP (<b>b</b>), and OCN (<b>c</b>). Each value is the mean ± SE of three independent experiments when compared with the DMEM group. * <span class="html-italic">p</span> &lt; 0.05 indicates significant differences compared with the control group.</p>
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<p>Enhanced biomineralization of MC3T3-E1 pre-osteoblasts with WSM from nano-nacre particles of <span class="html-italic">H. diversicolor</span>. The cells were treated with various concentrations (0–0.1% <span class="html-italic">w</span>/<span class="html-italic">v</span> WSM) and positive control at day 7 (<b>a</b>–<b>e</b>) and day 14 (<b>f</b>–<b>j</b>), and calcium nodule formation was detected by Alizarin Red Staining (<b>a</b>) and further quantified by PCP solution and spectrophotometric absorbance at 564 nm (A564) (<b>b</b>). Each value is the mean ± SD of three independent experiments when compared with the DMEM group. * <span class="html-italic">p</span> &lt; 0.05 indicates significant differences compared with the control group.</p>
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11 pages, 4943 KiB  
Article
Study on Microstructure and Mechanical Properties of Core–Shell-Structured Ti@TixN Reinforced Al Composite Prepared by Pressure Infiltration
by Yixiao Xia, Zhiyu Sun, Ping Zhu, Juanrui Hu, Leilei Hao, Yun Liu, Boyu Ju, Guoqin Chen and Wenshu Yang
Materials 2025, 18(6), 1200; https://doi.org/10.3390/ma18061200 - 7 Mar 2025
Viewed by 146
Abstract
In this research, a nitrogenized shell layer was formed on the surface of Ti powder in a high-temperature N2 environment, resulting in core–shell-structured Ti@TixN powder. Using this as a reinforcement, Ti@TixN/Al composite was successfully designed and fabricated via [...] Read more.
In this research, a nitrogenized shell layer was formed on the surface of Ti powder in a high-temperature N2 environment, resulting in core–shell-structured Ti@TixN powder. Using this as a reinforcement, Ti@TixN/Al composite was successfully designed and fabricated via pressure infiltration method. The TixN layer consists of a double-layered spherical shell structure, with TiN as the outer layer and Ti2N as the inner layer. After the composite was fabricated, no intermetallic compounds between Ti and Al were observed at the interface, as the TixN layer effectively prevented the reaction between Ti and Al. The tensile strength, yield strength, and elongation of the Ti@TixN/Al composite were 173 ± 7.7 MPa, 115 ± 8.1 MPa, and 7.5 ± 0.55%, respectively. Both the strength and hardness were significantly improved compared to the pure Al matrix. Observations of the tensile fracture surface revealed severe interfacial debonding at the interface, and the reinforcement did not exhibit significant coordinated deformation with the matrix. This suggests that future research could focus on strengthening the matrix by adding alloying elements and improving the interfacial bonding to enhance the performance of the composite. Full article
(This article belongs to the Special Issue Study on Advanced Metal Matrix Composites (3rd Edition))
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<p>The morphology and EDS analysis of Ti powder.</p>
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<p>Schematic preparation process of Ti@Ti<sub>x</sub>N/Al composite.</p>
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<p>Dimensions of tensile sample.</p>
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<p>The XRD patterns of the Ti and Ti@Ti<sub>x</sub>N powders.</p>
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<p>(<b>a</b>) Morphology and (<b>b</b>) transversal surface of Ti@Ti<sub>x</sub>N powder by SEM.</p>
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<p>(<b>a</b>) Macroscopic morphologies and (<b>b</b>) Raman scattering spectra of powders.</p>
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<p>SEM characterization of Ti@Ti<sub>x</sub>N/Al composite; (<b>b</b>) is the local amplification of (<b>a</b>).</p>
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<p>XRD pattern of Ti@Ti<sub>x</sub>N/Al composite.</p>
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<p>Strain–stress curve of Ti@Ti<sub>x</sub>N/Al composite and matrix.</p>
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<p>Fracture surfaces of Ti@Ti<sub>x</sub>N/Al composite. (<b>a</b>,<b>b</b>) <span class="html-italic">x</span> direction, (<b>c</b>,<b>d</b>) <span class="html-italic">z</span> direction.</p>
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14 pages, 10583 KiB  
Article
Study on the Influence of Sn58Bi Alloy on Rock Perforation Plugging Performance
by Chunqing Zha, Wenhe Xia, Wei Wang, Gonghui Liu, Jun Li and Wei Liu
Materials 2025, 18(6), 1195; https://doi.org/10.3390/ma18061195 - 7 Mar 2025
Viewed by 58
Abstract
In order to solve certain issues, such as brittle fracture corrosion and easy failure, which occur under high ambient temperatures and high breakthrough pressures when conventional cement is used to plug rock perforations, a method using a Sn58Bi alloy was adopted in this [...] Read more.
In order to solve certain issues, such as brittle fracture corrosion and easy failure, which occur under high ambient temperatures and high breakthrough pressures when conventional cement is used to plug rock perforations, a method using a Sn58Bi alloy was adopted in this paper; it was utilized to melt and plug a perforation. Subsequently, the influence of the characteristics of the rock perforation (such as perforation length and diameter) on alloy plugging performance under different conditions and ambient temperatures was studied. The experimental results show that the plugging effect of the Sn58Bi alloy was affected by ambient temperature, plugging diameter, and length. When the plugging length was 100 mm and the perforation diameter was 10 mm, the mechanical plug performance decreased by 24.0% when the ambient temperature increased from 30 °C to 60 °C, and then decreased by 19.0% when the ambient temperature increased to 90 °C. At 30 °C, the mechanical plug performance decreased by 30.4% when the diameter decreased from 10 mm to 8 mm, and decreased by 28.0% when the diameter decreased to 6 mm. When the length was constant and the diameter was decreased from 10 mm to 8 mm and then to 6 mm, the hydraulic plugging effect became better, and the trend increased from 33.7% to 37.2%. Full article
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<p>A schematic diagram of heating device for molten alloy plugging perforation.</p>
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<p>A schematic diagram of alloy plugging perforation.</p>
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<p>A schematic diagram of alloy pressure plugging perforation.</p>
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<p>Rocks of different sizes used in the experiment.</p>
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<p>The schematic and physical diagram mechanical push-out experiment.</p>
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<p>Connection diagram of hydraulic plugging experimental device.</p>
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<p>The physical picture of the device in the experiment.</p>
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<p>Cement and alloy plugging rock before and after the experiment and the experimental operation interface.</p>
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<p>The actual rock surface condition.</p>
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<p>Comparison of the alloy not pushed out and pushed out, as observed by optical microscope.</p>
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<p>Effect of Sn58Bi alloy and cement on mechanical pressure of plugging rock perforation.</p>
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<p>The curve of the load change at 30 °C with time.</p>
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<p>The effect of different factors on the mechanical pressure of Sn58Bi alloy plug at 30 °C.</p>
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<p>The influence of different factors on the mechanical pressure of Sn58Bi alloy plug at 60 °C and 90 °C.</p>
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<p>The curve of the load change with time.</p>
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<p>Effect of Sn58Bi alloy plugging and cement plugging on hydraulic plugging of rock.</p>
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16 pages, 1104 KiB  
Article
Detection of Fractured Endodontic Instruments in Periapical Radiographs: A Comparative Study of YOLOv8 and Mask R-CNN
by İrem Çetinkaya, Ekin Deniz Çatmabacak and Emir Öztürk
Diagnostics 2025, 15(6), 653; https://doi.org/10.3390/diagnostics15060653 - 7 Mar 2025
Viewed by 75
Abstract
Background/Objectives: Accurate localization of fractured endodontic instruments (FEIs) in periapical radiographs (PAs) remains a significant challenge. This study aimed to evaluate the performance of YOLOv8 and Mask R-CNN in detecting FEIs and root canal treatments (RCTs) and compare their diagnostic capabilities with those [...] Read more.
Background/Objectives: Accurate localization of fractured endodontic instruments (FEIs) in periapical radiographs (PAs) remains a significant challenge. This study aimed to evaluate the performance of YOLOv8 and Mask R-CNN in detecting FEIs and root canal treatments (RCTs) and compare their diagnostic capabilities with those of experienced endodontists. Methods: A data set of 1050 annotated PAs was used. Mask R-CNN and YOLOv8 models were trained and evaluated for FEI and RCT detection. Metrics including accuracy, intersection over union (IoU), mean average precision at 0.5 IoU (mAP50), and inference time were analyzed. Observer agreement was assessed using inter-class correlation (ICC), and comparisons were made between AI predictions and human annotations. Results: YOLOv8 achieved an accuracy of 97.40%, a mAP50 of 98.9%, and an inference time of 14.6 ms, outperforming Mask R-CNN in speed and mAP50. Mask R-CNN demonstrated an accuracy of 98.21%, a mAP50 of 95%, and an inference time of 88.7 ms, excelling in detailed segmentation tasks. Comparative analysis revealed no statistically significant differences in diagnostic performance between the models and experienced endodontists. Conclusions: Both YOLOv8 and Mask R-CNN demonstrated high diagnostic accuracy and reliability, comparable to experienced endodontists. YOLOv8’s rapid detection capabilities make it particularly suitable for real-time clinical applications, while Mask R-CNN excels in precise segmentation. This study establishes a strong foundation for integrating AI into dental diagnostics, offering innovative solutions to improve clinical outcomes. Future research should address data diversity and explore multimodal imaging for enhanced diagnostic capabilities. Full article
(This article belongs to the Special Issue Advances in Medical Image Processing, Segmentation and Classification)
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<p>Representative examples of Mask R-CNN’s performance on periapical radiographs (PAs) for detecting fractured endodontic instruments (FEI) and root canal treatments (RCT). The bounding boxes and associated confidence scores highlight the model’s ability to accurately identify and localize objects. Panels (<b>A1</b>–<b>E1</b>) represent the ground truth annotations marked with blue boxes for FEI and red boxes for RCT, while panels (<b>A2</b>–<b>E2</b>) depict the segmentations generated by the Mask R-CNN model, where FEI is marked with red boxes and RCT with pink boxes.</p>
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<p>Flowchart of Mask R-CNN architecture. CNN extracts feature maps from the input image. The Region Proposal Network generates candidate regions, which are processed through RoI (Region of Interest) Align to ensure accurate spatial alignment. The extracted features are passed through FC (Fully Connected) layers for classification and bounding box regression. Additionally, Conv (Convolutional) layers are used for mask prediction.</p>
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<p>Flowchart of YOLO architecture.</p>
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<p>Saliency map outputs for FEI and RCT detection using YOLO and Mask R-CNN. (<b>A1</b>–<b>D1</b>) Raw periapical radiographs, (<b>A2</b>–<b>D2</b>) corresponding saliency maps. (<b>A</b>) YOLO-based saliency map for FEI detection, (<b>B</b>) YOLO-based saliency map for RCT detection, (<b>C</b>) Mask R-CNN-based saliency map for FEI detection, and (<b>D</b>) Mask R-CNN-based saliency map for RCT detection. The red boxes indicate the regions identified by the models as containing FEI or RCT, highlighting the areas of interest detected by the respective deep learning approaches.</p>
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<p>Comparison of training and validation losses for YOLOv8 (top) and Mask R-CNN (bottom) models. The YOLOv8 graphs depict box loss (<b>A</b>) and class loss (<b>B</b>), illustrating a steady decrease in both training and validation losses with minimal divergence, indicating strong generalization and effective performance in object localization and classification. In contrast, the Mask R-CNN graph (<b>C</b>) shows the total loss across training and validation, with training loss decreasing rapidly and validation loss stabilizing with slight fluctuations, reflecting its ability to perform detailed segmentation tasks. Overall, YOLOv8 demonstrates faster convergence and smoother loss reduction, while Mask R-CNN exhibits robustness in tasks requiring precise segmentation.</p>
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15 pages, 3971 KiB  
Article
Impact Resistance of Yttria- and Ceria-Doped Zirconia Ceramics in Relation to Their Tetragonal-to-Monoclinic Transformation Ability
by Mohamed Imariouane, Malika Saâdaoui, Norberto Labrador, Helen Reveron and Jérôme Chevalier
Ceramics 2025, 8(1), 26; https://doi.org/10.3390/ceramics8010026 - 7 Mar 2025
Viewed by 85
Abstract
In this work, the impact resistance of three zirconia ceramics was investigated: two yttria-stabilized zirconia (3Y-TZP and 1.5Y-TZP) and a ceria-stabilized-zirconia (Ce-TZP) composite. The impact resistance was evaluated through drop-ball impact tests on disk-shaped samples. The results are discussed in terms of the [...] Read more.
In this work, the impact resistance of three zirconia ceramics was investigated: two yttria-stabilized zirconia (3Y-TZP and 1.5Y-TZP) and a ceria-stabilized-zirconia (Ce-TZP) composite. The impact resistance was evaluated through drop-ball impact tests on disk-shaped samples. The results are discussed in terms of the materials’ transformability, which was correlated to the size of tetragonal-to-monoclinic (t-m) transformation zones observed after the impact tests and to the volume fraction of the monoclinic content on fractured surfaces. The findings show that impact resistance increases with the ability of the material to undergo t-m transformation. The Ce-TZP composite exhibited the highest transformability and consequently the highest impact resistance, followed by 1.5Y-TZP, and then 3Y-TZP. Full article
(This article belongs to the Special Issue Mechanical Behavior and Reliability of Engineering Ceramics)
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<p>Schematic representation of the impact resistance testing device.</p>
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<p>SEM micrographs of fractured surfaces of tested samples for each material.</p>
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<p>Fracture probability versus drop height for the three materials.</p>
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<p>Critical drop heights (H<sub>C</sub>) for the three materials.</p>
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<p>Absorbed energy (E<sub>a</sub>) during impact testing at drop heights of 10, 15, 20, and 25 cm.</p>
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<p>Optical micrographs (Nomarski contrast) of t-m transformation zones observed in 1.5Y-TZP and Ce-TZP composite after impact tests at drop heights of 20, 25, and 30 cm.</p>
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<p>Evolution of the impact-induced t-m transformation zone size with the drop height.</p>
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<p>3D confocal images of the transformation zones developed under impact testing for 1.5Y-TZP and Ce-TZP composite samples with drop heights of 15 and 25 cm, along with their radial topography profile curves as a function of the distance, r.</p>
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<p>XRD patterns of polished (<b>a</b>) and fractured (<b>b</b>) surfaces of the studied materials.</p>
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<p>Variation of the critical drop high, H<sub>C</sub>, with toughness, K<sub>IC</sub>, (<b>a</b>), and with strength, σ<sub>R</sub>, (<b>b</b>) for the studied materials.</p>
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50 pages, 5064 KiB  
Systematic Review
Design, Algorithms, and Applications of Microstrip Antennas for Image Acquisition: Systematic Review
by Luis Fernando Guerrero-Vásquez, Nathalia Alexandra Chacón-Reino, Byron Steven Sigüenza-Jiménez, Felipe Tomas Zeas-Loja, Jorge Osmani Ordoñez-Ordoñez and Paúl Andrés Chasi-Pesantez
Electronics 2025, 14(6), 1063; https://doi.org/10.3390/electronics14061063 - 7 Mar 2025
Viewed by 152
Abstract
This systematic literature review investigates microstrip antenna applications in image acquisition, focusing on their design characteristics, reconstruction algorithms, and application areas. We applied the PRISMA methodology for article selection. From selected studies, classifications were identified based on antenna patch geometry, substrate types, and [...] Read more.
This systematic literature review investigates microstrip antenna applications in image acquisition, focusing on their design characteristics, reconstruction algorithms, and application areas. We applied the PRISMA methodology for article selection. From selected studies, classifications were identified based on antenna patch geometry, substrate types, and image reconstruction algorithms. According to inclusion criteria, a significant increase in publications on this topic has been observed since 2013. Considering this trend, our study focuses on a 10-year publication range, including articles up to 2023. Results indicate that medical applications, particularly breast cancer detection, dominate this field. However, emerging areas are gaining attention, including stroke detection, bone fracture monitoring, security surveillance, avalanche radars, and weather monitoring. Our study highlights the need for more efficient algorithms, system miniaturization, and improved models to achieve precise medical imaging. Visual tools such as heatmaps and box plots are used to provide a deeper analysis, identify knowledge gaps, and offer valuable insights for future research and development in this versatile technology. Full article
(This article belongs to the Section Microwave and Wireless Communications)
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<p>PRISMA method scheme.</p>
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<p>Publication scheme of articles by year.</p>
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<p>Distribution of studies by countries.</p>
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<p>Article classification by geometry design.</p>
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<p>Types of antenna designs, including (<b>a</b>) Slot insertion, (<b>b</b>) Basic geometry, (<b>c</b>) Array antenna, (<b>d</b>) Slit insertion, (<b>e</b>) Vivaldi geometry, (<b>f</b>) Bowtie slot, (<b>g</b>) Fractal slot (<b>h</b>) Fractal array (<b>i</b>) Spiral (<b>j</b>) Bowtie Array. Each design has unique characteristics related to image adquisition applications. These are representative figures of antennas, intended as a visual reference for the design type, but not necessarily functional with the current dimensions.</p>
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<p>Article classification by substrates used in microstrip antennas.</p>
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<p>Article classification by image reconstruction algorithms.</p>
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<p>Article classification by application type.</p>
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<p>Article classification by application type and antenna bandwidth.</p>
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<p>Article classification by application type and antenna operating frequency.</p>
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<p>Article classification by application type and antenna size.</p>
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<p>Article classification by reconstruction algorithms and antenna bandwidth.</p>
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<p>Article classification by reconstruction algorithms and antenna operating frequency.</p>
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<p>Article classification by reconstruction algorithm and antenna area.</p>
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<p>Standard deviation values of different dimensions of our review.</p>
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<p>Article classification by application and image reconstruction algorithm.</p>
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<p>Article classification by applications and frequency bands.</p>
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<p>Article classification by applications and antenna geometry.</p>
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<p>Article classification by application and substrate.</p>
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<p>Classification of frequency bands and image reconstruction algorithms.</p>
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<p>Article classification by antenna geometry and frequency band.</p>
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<p>Article classification by antenna geometry and substrate.</p>
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<p>Article classification by substrate and image reconstruction algorithms.</p>
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<p>Article classification by substrate and frequency band.</p>
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<p>Article classification by antenna geometry and image reconstruction algorithm.</p>
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12 pages, 18338 KiB  
Article
Effect of Heat Treatment on Microstructures and Mechanical Properties of a Ti-Al-V-Cr-Fe-Based Alloy
by Honglin Fang, Shewei Xin, Huan Wang, Xingyang Tu, Fei Qiang, Zhiwei Lian and Ping Guo
Crystals 2025, 15(3), 250; https://doi.org/10.3390/cryst15030250 - 7 Mar 2025
Viewed by 100
Abstract
The effects of different processes for heat treatment on microstructures and mechanical properties of a Ti-Al-V-Cr-Fe-based alloy (TLC002) were investigated based on the Ti-6411 alloy designed by Northwest Institute for Nonferrous Metals Research. The results show that the TLC002 alloy treated with solid [...] Read more.
The effects of different processes for heat treatment on microstructures and mechanical properties of a Ti-Al-V-Cr-Fe-based alloy (TLC002) were investigated based on the Ti-6411 alloy designed by Northwest Institute for Nonferrous Metals Research. The results show that the TLC002 alloy treated with solid solution and aging has high strength and low impact toughness. For the annealed specimens, both strength and impact toughness are high. With the rising annealing temperature from 800 °C to 880 °C, the tensile strength (UTS), yield strength (YS), and impact toughness (αu2) increase, especially for the αu2 from 48.7 J/cm2 to 86.0 J/cm2. The tensile and impact specimens treated with both solid solution and aging and annealing are all typical ductile fractures. Both the size dimension and depth of the dimples for the equiaxed structures are greater than those of the bimodal structures, indicating that the plasticity of the equiaxed structures is superior to that of the bimodal structures. The heat treatment that annealing at 880 °C for 1.5 h and then air cooling leads to qualified mechanical properties and a good match of the strength and plasticity of the TLC002 alloy. Full article
(This article belongs to the Special Issue Microstructural Characterization and Property Analysis of Alloys)
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<p>Diagram of forging for the TLC002 alloy.</p>
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<p>The forged microstructure of the TLC002 alloy.</p>
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<p>Optical metallographs of the TLC002 alloy under solid solution and aging (<b>a</b>) 900 °C/1 h, AC + 500 °C/4 h, AC; (<b>b</b>) 920 °C/1 h, AC + 500 °C/4 h, AC; and (<b>c</b>) 940 °C/1 h, AC + 500 °C/4 h, AC; together with specimens under annealing; (<b>d</b>) 800 °C/1.5 h, AC; (<b>e</b>) 840 °C/1.5 h, AC; and (<b>f</b>) 880 °C/1.5 h, AC.</p>
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<p>Microstructures of the TLC002 alloy under (<b>a</b>) solid solution and aging (920 °C/1 h, AC + 500 °C/4 h, AC), and (<b>b</b>) annealing (840 °C/1.5 h, AC). The blue arrows stand for the α<sub>s</sub>.</p>
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<p>The (<b>a</b>) bimodal microstructures and concentration distributions of alloying elements (<b>b</b>) V, (<b>c</b>) Al, (<b>d</b>) Cr, (<b>e</b>) Fe, and (<b>f</b>) O of the TLC002 alloy under solid solution and aging (900 °C/1 h, AC + 500 °C/4 h, AC) and (<b>g</b>) equiaxed microstructures and concentration distributions of alloying elements (<b>h</b>) V, (<b>i</b>) Al, (<b>j</b>) Cr, (<b>k</b>) Fe, and (<b>l</b>) O of the TLC002 alloy under annealing (840 °C/1.5 h, AC).</p>
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<p>The representative stress–strain curves of the TLC002 alloy under (<b>a</b>) solid solution and aging (1) 900 °C/1 h, AC + 500 °C/4 h, AC; (2) 920 °C/1 h, AC + 500 °C/4 h, AC; (3) 940 °C/1 h, AC + 500 °C/4 h, AC, as well as (<b>b</b>) annealing (4) 800 °C/1.5 h, AC; (5) 840 °C/1.5 h, AC; (6) 880 °C/1.5 h, AC. The tensile strength (UTS), yield strength (YS), and impact toughness (α<sub>u2</sub>) of the TLC002 alloy treated with (<b>c</b>) solid solution and aging, and (<b>d</b>) annealing. For comparison, the previous data and available experimental results [<a href="#B38-crystals-15-00250" class="html-bibr">38</a>,<a href="#B39-crystals-15-00250" class="html-bibr">39</a>] are also displayed.</p>
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<p>Tensile fracture morphologies of the TLC002 alloy with different solid solution and aging temperatures: (<b>a</b>) 900 °C/1 h, AC + 500 °C/4 h, AC; (<b>b</b>) 920 °C/1 h, AC + 500 °C/4 h, AC; (<b>c</b>) 940 °C/1 h, AC + 500 °C/4 h, AC, as well as annealing temperatures: (<b>d</b>) 800 °C/1.5 h, AC; (<b>e</b>) 840 °C/1.5 h, AC; (<b>f</b>) 880 °C/1.5 h, AC.</p>
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<p>Impact fracture morphologies of the TLC002 alloy with different solid solution and aging temperatures: (<b>a1</b>–<b>a3</b>) 900 °C/1 h, AC + 500 °C/4 h, AC; (<b>b1</b>–<b>b3</b>) 920 °C/1 h, AC + 500 °C/4 h, AC; (<b>c1</b>–<b>c3</b>), 940 °C/1 h, AC + 500 °C/4 h, AC, as well as annealing temperatures: (<b>d1</b>–<b>d3</b>) 800 °C/1.5 h, AC; (<b>e1</b>–<b>e3</b>) 840 °C/1.5 h, AC; (<b>f1</b>–<b>f3</b>) 880 °C/1.5 h, AC.</p>
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<p>Impact fracture morphologies of the TLC002 alloy under different heat treatments: (<b>a</b>) 900 °C/1 h, AC + 500 °C/4 h, AC; (<b>b</b>) 880 °C/1.5 h, AC.</p>
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11 pages, 588 KiB  
Article
Health Professional Support for Friends and Family Members of Older People Discharged from Hospital After a Fracture: A Survey Study
by Toby O. Smith, Susanne Arnold and Mark Baxter
Geriatrics 2025, 10(2), 36; https://doi.org/10.3390/geriatrics10020036 - 7 Mar 2025
Viewed by 174
Abstract
Background/Objectives: Friends and family members of people who are discharged from hospital after a fracture often take on caring roles, since these patients have reduced independence during recovery. Previous literature suggests that these individuals are rarely supported in their adoption of these roles. [...] Read more.
Background/Objectives: Friends and family members of people who are discharged from hospital after a fracture often take on caring roles, since these patients have reduced independence during recovery. Previous literature suggests that these individuals are rarely supported in their adoption of these roles. No studies have previously explored the use of carer training interventions to support friends/family members by health professionals in this setting. This survey study aimed to address this. Methods: A cross-sectional online survey was conducted among health professionals who treat people in hospital following fractures. Respondents were asked about the use of care training for friends/family members of people discharged from hospital after fracture, and whether a clinical trial would be useful to test such carer training interventions. Results: A total of 114 health professionals accessed the survey. Fifty respondents (44%) reported that carer training was not offered in their practice. When it was offered, respondents reported this was not consistently provided. Less than 12% of respondents reported offering carer training to most of their patients following a fracture. What was offered in these instances was largely based on education provision (69%), practical skills in exercise prescription (55%) and manual handling (51%). Ninety-eight percent of respondents reported that a clinical trial would be, or would potentially be, valuable to aid a change in practice to include carer training in routine clinical care. Conclusions: Carer training programmes are not routinely provided in clinical practice for people following a fracture. The results indicate that health professionals see a potential value in these programmes, but further research is recommended to provide an evidence base for these interventions. Full article
(This article belongs to the Section Geriatric Rehabilitation)
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<p>Country of origin for respondents (<span class="html-italic">n</span> = 87).</p>
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<p>Bar chart illustrating the percentage of older people that the respondents reported as treating at home following a bone fracture.</p>
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12 pages, 7645 KiB  
Article
Dynamic Mechanical and Failure Properties of Grouted Fractured Rock Based on Nano-Grouting Material
by Yuhao Jin, Shuo Yang, Hui Guo, Lijun Han, Pengcheng Huang, Miao Chen, Hao Shan, Lanying Huang, Shanjie Su, Shengcheng Wang, Peitao Qiu, Xiaoxi Bi and Zu-an Liu
Processes 2025, 13(3), 765; https://doi.org/10.3390/pr13030765 - 6 Mar 2025
Viewed by 188
Abstract
Fractured rock masses are extremely common in geological engineering. In order to improve the stability of surrounding rock under dynamic conditions, new grouting materials and their reinforcement characteristics were studied. In this paper, split Hopkinson pressure bar (SHPB) tests were employed to analyze [...] Read more.
Fractured rock masses are extremely common in geological engineering. In order to improve the stability of surrounding rock under dynamic conditions, new grouting materials and their reinforcement characteristics were studied. In this paper, split Hopkinson pressure bar (SHPB) tests were employed to analyze the dynamic mechanical and failure characteristics of grouted fractured rock with nano-grouting material (nano-grouted fractured rock). Simultaneously, high-speed camera tests were utilized to examine the macroscopic dynamic deformation and failure processes. The following was found: (1) Under a relatively low impact air pressure of 0.1 MPa, the mechanical properties of nano-grouted fractured rock are considerably better than those of traditional cement-based grouted rock. However, when the impact air pressure is increased to 0.3 MPa, the superiority of nano-grouting material diminishes, the possible cause of which is explained from the microscopic point of view. This means the nano-grouting material is more suitable for low-engineering-disturbance conditions (e.g., shield construction). (2) Both for the nano- and superfine cement grouting material, the impact fractures initially emerge at the two ends of the original grouted fracture and form a pair of parallel lines. (3) In comparison with 0.1 MPa, the impact pressure of 0.3 MPa leads to more severe damage to the rock specimen. These findings contribute to a deeper understanding of the behavior of nano-grouted fractured rock under dynamic loading and provide valuable insights for relevant engineering applications in the field of rock mechanics and grouting technology. Full article
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<p>Fractured rock masses.</p>
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<p>Preparation of nano-grouting material.</p>
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<p>Fractured rock specimen and sealing treatment.</p>
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<p>Production of grouted fractured specimens.</p>
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<p>Hopkinson experimental system with high-speed camera.</p>
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<p>Dynamic stress–strain curves of grouted fractured rock specimens with impact air pressure of (<b>a</b>) 0.1 and (<b>b</b>) 0.3 MPa.</p>
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<p>Dynamic peak strength of grouted fractured rock specimens.</p>
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<p>SEM pictures of 0.3 MPa nano-grouting material in the fracture (<b>a</b>,<b>b</b>).</p>
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<p>Dynamic deformation and failure processes of grouted fractured rock under impact air pressure of 0.1 MPa.</p>
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<p>Dynamic deformation and failure processes of grouted fractured rock under impact air pressure of 0.1 MPa.</p>
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<p>Dynamic deformation and failure processes of grouted fractured rock under impact air pressure of 0.3 MPa.</p>
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15 pages, 10121 KiB  
Article
A Study on Microstructure-Property Relationships and Notch-Sensitive Fracture Behavior of X80 Steel Welds
by Yangfan Zou, Lifeng Li, Shuxin Zhang, Xiangzhen Yan and Shuyi Xie
Processes 2025, 13(3), 763; https://doi.org/10.3390/pr13030763 - 6 Mar 2025
Viewed by 199
Abstract
X80 steel pipelines are widely used in oil and gas transportation, and the quality and fracture behavior of the girth weld have an important influence on the safety and performance of the pipeline. This study presents a comprehensive investigation into the microstructure, mechanical [...] Read more.
X80 steel pipelines are widely used in oil and gas transportation, and the quality and fracture behavior of the girth weld have an important influence on the safety and performance of the pipeline. This study presents a comprehensive investigation into the microstructure, mechanical properties, and fracture characteristics of X80 steel welded joints. Through microstructure analysis and mechanical testing, the hardness, impact, and tensile properties of the base metal, heat-affected zone, and weld zone are evaluated. Digital Image Correlation (DIC) technology is employed to scrutinize the strain behavior under quasi-static tensile tests for both smooth and notched round bar specimens, providing a detailed strain distribution analysis. The findings indicate that, while X80 welded joints are well-formed without significant defects, the hardness and impact properties vary across different zones, with the base metal exhibiting the highest impact toughness and the weld zone the lowest. Notched tensile tests reveal that the presence and geometry of notches significantly alter the stress state and deformation characteristics, influencing the fracture mode. The DIC analysis further elucidates the strain concentration and localization behavior in the weld zone, highlighting the importance of notch size in determining the load-bearing capacity and ductility of the welded joints. This study contributes to a deeper understanding of the fracture mechanics in X80 pipeline girth welds and offers valuable insights for the optimization of welding practices and the assessment of pipeline integrity. Full article
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<p>Microstructure characteristics of X80 (BM): (<b>a</b>) 500× magnification, (<b>b</b>) 1000× magnification.</p>
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<p>Dimensions of the full weld specimens: (<b>a</b>) smooth, (<b>b</b>) notched.</p>
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<p>Tensile testing equipment and DIC measuring system: (<b>a</b>) tensile machine and camera system, (<b>b</b>) testing process, (<b>c</b>) prepared specimen.</p>
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<p>Microstructures of different zones in the cross-section of welded joint: (<b>a</b>) overall microstructure of the joint, (<b>b</b>) enlarged view of area b, (<b>c</b>) enlarged view of area c, (<b>d</b>) enlarged view of area d, (<b>e</b>) enlarged view of area e, (<b>f</b>) enlarged view of area f, (<b>g</b>) enlarged view of area g, (<b>h</b>) enlarged view of area h, (<b>i</b>) enlarged view of area i.</p>
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<p>Hardness distribution at different locations (upper, middle, lower).</p>
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<p>Impact properties of welded joints in different characteristic zones.</p>
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<p>The load–displacement curve.</p>
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<p>True stress–strain curve (R represents the direction of diameter, L represents the axial direction).</p>
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<p>Strain contours of smooth round bar specimens in different stages (axial direction): (<b>a</b>) initial, (<b>b</b>) elastic stage, (<b>c</b>) local necking, (<b>d</b>) near fracture.</p>
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<p>Strain contours of R4 notched specimens in different stages (axial direction): (<b>a</b>) initial, (<b>b</b>) elastic stage, (<b>c</b>) onset of local necking, (<b>d</b>) near fracture.</p>
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<p>Strain contours of R8 notched specimens in different stages (axial direction): (<b>a</b>) initial, (<b>b</b>) elastic stage, (<b>c</b>) onset of local necking, (<b>d</b>) near fracture.</p>
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<p>Strain contours of R12 notched specimens in different stages (axial direction): (<b>a</b>) initial, (<b>b</b>) elastic stage, (<b>c</b>) onset of local necking, (<b>d</b>) near fracture.</p>
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<p>Macroscopic fracture of different welded joints.</p>
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<p>Morphologies of welded joints: (<b>a</b>–<b>d</b>) normal joint, (<b>e</b>–<b>h</b>) R4-notched joint, (<b>i</b>–<b>l</b>) R8-notched joint, (<b>m</b>–<b>p</b>) R12-notched joint.</p>
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