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23 pages, 5366 KiB  
Article
Evaluation of the Cyber-Physical System State Under Destructive Impact Conditions Based on a Comprehensive Analysis of Parameters
by Anton Mogilny, Elena Basan and Alexey Nekrasov
Robotics 2025, 14(1), 6; https://doi.org/10.3390/robotics14010006 - 8 Jan 2025
Abstract
This manuscript proposes a method for analyzing the stability of the behavior of a cyber-physical system (CPS) under conditions of potential destructive impact, considering the tasks it performs, which does not require labeled sets of abnormal data. The considered CPS has an autonomous [...] Read more.
This manuscript proposes a method for analyzing the stability of the behavior of a cyber-physical system (CPS) under conditions of potential destructive impact, considering the tasks it performs, which does not require labeled sets of abnormal data. The considered CPS has an autonomous decision-making system. The method was formalized in terms of the Markov decision-making process. Proposed metrics for assessing CPS behavior based on changes in its parameters were defined. They allowed classifying the operating mode into three classes: normal, abnormal, and uncertain. Evaluation results prove the efficiency of the proposed method. Despite the proposed method being tested on an unmanned vehicle (UV), it can also be applied to other CPSs, primarily to autonomous mobile robots (AMRs). Full article
(This article belongs to the Special Issue UAV Systems and Swarm Robotics)
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Figure 1
<p>Aerodynamic model with 3 degrees of freedom.</p>
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<p>Implementation into the CPS architecture. Purple blocks are the components of the proposed method, and yellow blocks are the components of the decision-making cycle.</p>
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<p>Workflow.</p>
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<p>Behavior of Metric 1 depending on the change in the altitude value parameter: (<b>a</b>) altitude change over time; (<b>b</b>) Metric 1 change depending on the altitude value.</p>
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<p>Behavior of Metric 2 depending on the change in the parameter of altitude value: (<b>a</b>) altitude change over time; (<b>b</b>) Metric 2 change depending on the altitude value.</p>
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<p>Workflow for calculating the third metric.</p>
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<p>Neural network architecture. The fully connected block is on the left and the architecture is on the right.</p>
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<p>AMR full-scale model.</p>
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<p>Graph of the change in training error for the parameter estimation models: (<b>a</b>) latitude, longitude, altitude; (<b>b</b>) eph, epv; (<b>c</b>) vdop, hdop; (<b>d</b>) noise; (<b>e</b>) used_satelites.</p>
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<p>An example of a simulation in the absence of destructive factors: (<b>a</b>) visualization of the simulation: the numbered markers show the waypoints of the route, markers with the letters “T” and “L” show the take-off and landing points, respectively; (<b>b</b>) probability of normal state of AMR value change in the process of completing the task.</p>
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<p>An example of a simulation under the influence of synchronous GPS substitution: (<b>a</b>) visualization of the simulation: the numbered markers show the waypoints of the route, markers with the letters “T” and “L” show the take-off and landing points, respectively; (<b>b</b>) probability of normal state of AMR value change in the process of completing the task.</p>
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16 pages, 2894 KiB  
Article
Static Analysis of Gelatin-like Simulation Mass as a Subsoil in Scale Physical Modeling
by Veronika Valašková and Jozef Vlček
Buildings 2025, 15(2), 167; https://doi.org/10.3390/buildings15020167 - 8 Jan 2025
Abstract
The investigation of wave propagation in the geological environment is warranted, and will ultimately help to provide a better understanding of the response of subsoil to excitation. Frequently utilized physical modeling represents a simplification of the global natural system for the needs of [...] Read more.
The investigation of wave propagation in the geological environment is warranted, and will ultimately help to provide a better understanding of the response of subsoil to excitation. Frequently utilized physical modeling represents a simplification of the global natural system for the needs of the investigation of static and dynamic phenomena with regard to the time domain. The determination of appropriate model materials is probably the most important task for physical model creation. Considering that subsoil represents a crucial medium for wave propagation, an evaluation of suitable model materials was carried out. A plate load test with a circular plate is a non-destructive method for determining the static bearing capacities of soils and aggregates, which are usually expressed by the deformation modulus Edef,2 (MPa) and the static modulus of elasticity E (MPa). A lightweight deflectometer test was used to characterize the impact modulus of deformation Evd (MPa), which is determined based on the pressure under the load plate due to the impact load. A representative propagation of the load–settlement curve for the PLT and the acceleration–time curve for the hammer drop test were investigated. The calculated E values were found to be in the interval between 2.6 and 5.7 kPa, and depending on the load cycle, the values of E ranged from 2.6 to 3.1 kPa. The modulus E from the hammer drop test was significantly larger than the interval between 10.6 and 40.4 kPa. The values of the dynamic multiplier, as a ratio of the hammer drop value to the PLT value, of the modulus E ranged from 4.1 to 13.0. The output of the plate load testing was utilized for the calibration of the finite element method (FEM) numerical model. Both the physical and numerical models showed practically ideal linear behavior of the mass. However, the testing of gelatin-like materials is a complex process because of their viscoelastic nonlinear behavior. Full article
(This article belongs to the Special Issue Advances in Foundation Engineering for Building Structures)
16 pages, 13899 KiB  
Article
Comprehensive Rehabilitation of the Punta del Este Shopping Center After Fire Damage
by Álvaro Leez, María Noel Pereyra and Patricia Vila
Buildings 2025, 15(2), 161; https://doi.org/10.3390/buildings15020161 - 8 Jan 2025
Abstract
On 6 August 2022, a fire devastated 80% of the Punta del Este Shopping Center in Maldonado, Uruguay. Originating in the kitchen of a supermarket, the fire ravaged the shopping center for 72 h before being brought under control. This article outlines the [...] Read more.
On 6 August 2022, a fire devastated 80% of the Punta del Este Shopping Center in Maldonado, Uruguay. Originating in the kitchen of a supermarket, the fire ravaged the shopping center for 72 h before being brought under control. This article outlines the studies conducted to assess the fire’s impact on the building’s structure, as well as the strategies and rehabilitation project aimed at ensuring its stability and performance. An in-depth analysis of the concrete, reinforcements, and foundations was carried out using destructive and non-destructive testing. In total, over 150 concrete samples were collected for analysis, and the foundations were studied using indirect methods. Based on these analyses, actions were planned for each area, including structural repairs, reinforcements, or demolition. Due to the tight deadline for resuming commercial activity, special innovative structural solutions were designed to rehabilitate large severely damaged areas with the specific feature of avoiding demolition. This involved altering the static scheme of the structure, incorporating reinforcements and using slabs of the damaged structure as formworks. Complete demolition and subsequent reconstruction would have required timelines incompatible with the clients’ expectations, while the adopted solutions enabled the project to meet its objectives. Full article
(This article belongs to the Special Issue Selected Papers from the REHABEND 2024 Congress)
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<p>Photo of the structure taken after reconstruction.</p>
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<p>The Punta del Este shopping center during and after the fire.</p>
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<p>Identification of risk zones.</p>
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<p>Column with significant deformations.</p>
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<p>Structural cracking, spalling, and deformation.</p>
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<p>Left: fire-affected concrete sample (core V7). Right: unaffected concrete sample (core V8).</p>
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<p>Construction details of the capital.</p>
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<p>Column jacketing (<b>left</b>) and construction details of the anchoring to the foundation cap (<b>right</b>).</p>
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<p>Reinforcements in the beamless slabs.</p>
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<p>Construction progress of the expanded area.</p>
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<p>Simplified version of the work schedule, highlighting in red those tasks with less than five days of float.</p>
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18 pages, 4041 KiB  
Review
Review of Drone-Based Technologies for Wind Turbine Blade Inspection
by Seong-Jun Heo and Wongi S. Na
Electronics 2025, 14(2), 227; https://doi.org/10.3390/electronics14020227 - 8 Jan 2025
Viewed by 137
Abstract
Wind energy is one of the most rapidly growing sectors in renewable energy generation, with wind turbines being central to this expansion. Regular maintenance, particularly the inspection of wind turbine blades, is critical to ensure operational efficiency and prevent catastrophic failures. Conventional methods [...] Read more.
Wind energy is one of the most rapidly growing sectors in renewable energy generation, with wind turbines being central to this expansion. Regular maintenance, particularly the inspection of wind turbine blades, is critical to ensure operational efficiency and prevent catastrophic failures. Conventional methods of blade inspection, including ground-based visual inspections, rope-access inspections, and cranes, are time-consuming, expensive, and often hazardous. In recent years, drone-based technologies have emerged as a promising alternative for wind turbine blade inspection. This paper provides a comprehensive review of current drone-based technologies for wind turbine blade inspection, highlighting their advantages, challenges, and future prospects. Full article
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<p>Summary of drone types [<a href="#B16-electronics-14-00227" class="html-bibr">16</a>].</p>
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<p>Example of heuristic simulated annealing for 7 targets [<a href="#B31-electronics-14-00227" class="html-bibr">31</a>].</p>
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<p>Suggestion results on the test images for the trained model [<a href="#B31-electronics-14-00227" class="html-bibr">31</a>].</p>
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<p>Passive thermography experiment setup for a blade [<a href="#B62-electronics-14-00227" class="html-bibr">62</a>].</p>
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<p>(<b>a</b>) Phase images of the passive thermograms at 0.00184 Hz and (<b>b</b>) amplitude image of the passive thermograms at 0.0165 Hz [<a href="#B62-electronics-14-00227" class="html-bibr">62</a>].</p>
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<p>Blade close inspection procedure after obtaining wind turbine model estimation [<a href="#B79-electronics-14-00227" class="html-bibr">79</a>].</p>
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<p>Wall sticking drone and its components [<a href="#B88-electronics-14-00227" class="html-bibr">88</a>].</p>
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15 pages, 6899 KiB  
Article
Influence of Potting Radius on the Structural Performance and Failure Mechanism of Inserts in Sandwich Structures
by Filippos Filippou and Alexis Τ. Kermanidis
Machines 2025, 13(1), 34; https://doi.org/10.3390/machines13010034 - 7 Jan 2025
Viewed by 140
Abstract
In this study, the mechanical performance and failure modes of cold-potted inserts within sandwich structures were examined, focusing on the influence of the potting radius, while maintaining constant insert radius and specimen characteristics. In this research, destructive testing was used to evaluate the [...] Read more.
In this study, the mechanical performance and failure modes of cold-potted inserts within sandwich structures were examined, focusing on the influence of the potting radius, while maintaining constant insert radius and specimen characteristics. In this research, destructive testing was used to evaluate the pull out, load-carrying capacity, and failure mechanisms of the inserts. The methods of stiffness degradation and acoustic emissions (AE) were employed for structural health monitoring to capture real-time data on failure progression, including core buckling, core rupture, and skin delamination. The results indicated that increasing the potting radius significantly altered the failure modes and critical failure load of the insert system. A critical potting radius was identified where maximum stiffness was achieved. Beyond this point, insert fracture became the dominant failure mode, with minimal damage to the surrounding core and CFRP skins. Larger potting radii also led to reduced displacement at failure, increased ultimate loads, and elevated stiffness, which were maintained until sudden structural failure. Through detailed isolation and observation of each failure event and with the use of AE data, precise identification of system damage in real time was allowed, offering insights into the progression and causes of failure. Full article
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<p>Potting geometry.</p>
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<p>(<b>a</b>) Initial cut; (<b>b</b>) Undercutting; (<b>c</b>) Potting of the insert; (<b>d</b>) Final potted insert system.</p>
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<p>(<b>a</b>) Insert tensile out-of-plane loading fixture front view; (<b>b</b>) Test fixture side view.</p>
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<p>Distance (e) from free edge.</p>
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<p>(<b>a</b>,<b>b</b>) Characteristic force, displacement and acoustic data diagrams for R<sub>p</sub> = 8.6 mm and R<sub>p</sub> = 9.3 mm, respectively.</p>
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<p>(<b>a</b>,<b>b</b>) Characteristic lower skin indentation for R<sub>p</sub> = 8.6 mm and R<sub>p</sub> = 9.3 mm, respectively; (<b>c</b>) Upper skin extrusion.</p>
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<p>(<b>a</b>,<b>b</b>) Characteristic cross-sections for R<sub>p</sub> = 8.6 mm and R<sub>p</sub> = 9.3 mm, respectively; (<b>c</b>) Stereoscopical observation of core buckling; (<b>d</b>) Stereoscopical observation of shear rupture and skin delamination.</p>
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<p>Characteristic force, displacement and acoustic data diagram for R<sub>p</sub> = 10 mm.</p>
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<p>(<b>a</b>) Lower skin indentation; (<b>b</b>,<b>c</b>) Insert extrusion.</p>
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<p>(<b>a</b>) Characteristic cross-sections of R<sub>p</sub> = 10 mm; (<b>b</b>) Stereoscopical observation of core buckling; (<b>c</b>) Stereoscopical observation of shear rupture; (<b>d</b>) Absence of delamination; (<b>e</b>) Stereoscopical observation of insert lower flange failure.</p>
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<p>(<b>a</b>,<b>b</b>) Characteristic force, displacement and acoustic data diagrams for R<sub>p</sub> = 11 mm and R<sub>p</sub> = 12.5 mm, respectively.</p>
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<p>(<b>a</b>,<b>b</b>) Characteristic lower skin indentation absence for R<sub>p</sub> = 11 mm and R<sub>p</sub> = 12.5 mm, respectively; (<b>c</b>,<b>d</b>) Insert extrusion.</p>
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<p>(<b>a</b>,<b>b</b>) Characteristic cross-sections for R<sub>p</sub> = 11 mm and R<sub>p</sub> = 12.5 mm, respectively; (<b>c</b>) Stereoscopical observation of insert lower flange failure; (<b>d</b>) Stereoscopical observation of core buckling.</p>
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<p>(<b>a</b>,<b>b</b>) Average experimental results for each potting radius (R<sub>p</sub>).</p>
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58 pages, 25512 KiB  
Review
The Role of Non-Destructive Testing of Composite Materials for Aerospace Applications
by Thiago Luiz Lara Oliveira, Maha Hadded, Saliha Mimouni and Renata Brandelli Schaan
NDT 2025, 3(1), 3; https://doi.org/10.3390/ndt3010003 - 3 Jan 2025
Viewed by 1082
Abstract
This review examines the essential application of non-destructive testing (NDT) techniques in assessing the integrity and damage of composite materials used in aerospace engineering, focusing on polymer matrix composites (PMCs), metal matrix composites (MMCs), and ceramic matrix composites (CMCs). As these materials increasingly [...] Read more.
This review examines the essential application of non-destructive testing (NDT) techniques in assessing the integrity and damage of composite materials used in aerospace engineering, focusing on polymer matrix composites (PMCs), metal matrix composites (MMCs), and ceramic matrix composites (CMCs). As these materials increasingly replace traditional metallic and alloy components due to their advantageous properties, such as light weight, high strength, and corrosion resistance, ensuring their structural integrity becomes paramount. Here, various NDT techniques were described in detail, including ultrasonic, radiographic, and acoustic emission, among others, highlighting their significance in identifying and evaluating damages that are often invisible, yet critical, to parts safety. It stresses the need for innovation in NDT technologies to keep pace with the evolving complexity of composite materials and their applications. The review underscores the ongoing challenges and developments in NDT, advocating for enhanced techniques that provide accurate, reliable, and timely assessments to ensure the safety and durability of aerospace components. This comprehensive analysis not only illustrates current capabilities but also directs future research pathways for improving NDT methodologies in aerospace material engineering. Full article
(This article belongs to the Topic Nondestructive Testing and Evaluation)
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Graphical abstract

Graphical abstract
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<p>Strength of diverse materials as a function of operational temperatures. Modified [<a href="#B35-ndt-03-00003" class="html-bibr">35</a>].</p>
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<p>Composite laminate and the evolution of damage based on the material lifetime [<a href="#B77-ndt-03-00003" class="html-bibr">77</a>].</p>
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<p>Microscopic images showing damage mechanisms of (<b>A</b>) fiber breakage due to pull-out and (<b>B</b>) interfacial debonding between the matrix and the fiber, modified from [<a href="#B89-ndt-03-00003" class="html-bibr">89</a>].</p>
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<p>High-resolution micrograph showing the damages on MMCs, (<b>A</b>) a surface fracture fiber–matrix interface in a titanium matrix composite reinforced with SiC fibers (modified from [<a href="#B90-ndt-03-00003" class="html-bibr">90</a>]), and (<b>B</b>) presence of voids due to loading in an AlSi matrix reinforced with SiC (modified from [<a href="#B92-ndt-03-00003" class="html-bibr">92</a>]).</p>
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<p>SEM images of corrosion damage in metal matrix composites: (<b>a</b>) uncoated titanium components displaying surface roughness and corrosion; (<b>b</b>) cross-sectional view highlighting the corrosion product layer formed after exposure to a corrosive environment, modified from [<a href="#B95-ndt-03-00003" class="html-bibr">95</a>].</p>
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<p>Surface (<b>a</b>) and cross-section (<b>b</b>) SEM images of the c-AlPO₄-SiCw-mullite coating with 20 wt.% c-AlPO₄ applied on SiC–C/SiC composites. The surface image (<b>a</b>) highlights the morphology of the coating, while the cross-section image (<b>b</b>) reveals cracks formed after 210 h of oxidation at 1773 K in air. Adapted from [<a href="#B100-ndt-03-00003" class="html-bibr">100</a>].</p>
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<p>Mechanisms of matrix cracking under tensile test: (<b>a</b>) typical stress–strain curve of a unidirectional CMC; (<b>b</b>) schematic representation of crack–tip and crack–wake debonding for the same material. Modified from [<a href="#B103-ndt-03-00003" class="html-bibr">103</a>].</p>
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<p>A proposed workflow for detecting and analyzing voids and cracks in a SiC [<a href="#B108-ndt-03-00003" class="html-bibr">108</a>]. The arrow indicates a magnified region of a smaller number of pores with larger sizes.</p>
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<p>Ultrasonic C-scan (<b>a</b>) and B-scan (<b>b</b>) were performed on a specimen following the application of an impact energy of 40 J. The C-scan (<b>a</b>) provides a planar view showing the lateral distribution of damage, including the impact site, delaminated areas, and manufacturing defects. The B-scan (<b>b</b>) shows a cross-sectional depth profile of the same region, illustrating the top and bottom laminas and the internal delamination. Together, the views provide a spatial representation of the impact damage. Modified from [<a href="#B135-ndt-03-00003" class="html-bibr">135</a>].</p>
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<p>Experimental setup was designed for the evaluation of capability and sensitivity, encompassing both PAUT (<b>a</b>) and SEUT (<b>b</b>). Modified from [<a href="#B136-ndt-03-00003" class="html-bibr">136</a>].</p>
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<p>Response signals for GFRP: (<b>a</b>) SEUT method and (<b>b</b>) PAUT method (the parameters used in the testing include a frequency of 1.5 MHz, a thickness of 25 mm, a hole diameter of 0.8 mm, and a hole depth of 12 mm). Modified from [<a href="#B136-ndt-03-00003" class="html-bibr">136</a>].</p>
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<p>Results from mechanical test of a CMC monitored with AE, with signal classification and damage identification. Modified from [<a href="#B101-ndt-03-00003" class="html-bibr">101</a>].</p>
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<p>Classification of damage by AE signal feature for polymer composite materials, (<b>a</b>) peak frequency, (<b>b</b>) amplitude. Modified from [<a href="#B142-ndt-03-00003" class="html-bibr">142</a>].</p>
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<p>Use of AI for classification of AE signal processing. Modified from [<a href="#B150-ndt-03-00003" class="html-bibr">150</a>].</p>
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<p>Monitoring of machining processes using AE: (<b>a</b>) drilling, modified from [<a href="#B152-ndt-03-00003" class="html-bibr">152</a>]; (<b>b</b>) milling, adapted from [<a href="#B144-ndt-03-00003" class="html-bibr">144</a>].</p>
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<p>Optical microscopy images at different magnifications illustrate (<b>a</b>) the surface and (<b>b</b>) the cross-sectional view of the sandwich panel. Modified from [<a href="#B163-ndt-03-00003" class="html-bibr">163</a>].</p>
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<p>3D renderings of the composite sample before (<b>a</b>) and after (<b>b</b>) foam masking. Modified from [<a href="#B163-ndt-03-00003" class="html-bibr">163</a>].</p>
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<p>Grayscale histograms before/after foam masking. Before masking (<b>a</b>), two peaks represent pores and combined CFRP–foam. After masking (<b>b</b>), a new peak appears for the background, with remaining peaks corresponding to pores and CFRP. Modified from [<a href="#B163-ndt-03-00003" class="html-bibr">163</a>].</p>
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<p>Typical damage maps in the X–Y plane from (<b>a</b>) the experimental ultrasonic C-scan technique, (<b>b</b>) the experimental X-ray CT technique, and (<b>c</b>) the numerical modeling predictions. Modified from [<a href="#B12-ndt-03-00003" class="html-bibr">12</a>].</p>
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<p>Comparison of interlaminar damage between blocking plies obtained from (<b>a</b>) numerical simulation and (<b>b</b>) experimental X-ray CT scan. Modified from [<a href="#B12-ndt-03-00003" class="html-bibr">12</a>].</p>
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<p>Progression of thermal response for the CMC during fatigue testing. Modified from [<a href="#B172-ndt-03-00003" class="html-bibr">172</a>].</p>
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<p>Stages of visualization of a defect in Al MMC using APIRL. Modified from [<a href="#B174-ndt-03-00003" class="html-bibr">174</a>].</p>
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<p>Detection capabilities of impact damage in CFRP of PTT and UT. Modified from [<a href="#B175-ndt-03-00003" class="html-bibr">175</a>].</p>
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<p>Thermal response of the hybrid PMC to impact damage. Modified from [<a href="#B175-ndt-03-00003" class="html-bibr">175</a>].</p>
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<p>Specimen sides and the different domains used for analyses of defects. Adapted from [<a href="#B176-ndt-03-00003" class="html-bibr">176</a>].</p>
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<p>Measurement of coating thickness by active IRT, from [<a href="#B177-ndt-03-00003" class="html-bibr">177</a>].</p>
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<p>Detection and magnification of a defect using hologram. (<b>a</b>) Wide-field hologram showing the overall fringe pattern and the location of the defect (circled in red). (<b>b</b>) Magnified-in hologram highlighting the detailed morphology of the defect [<a href="#B195-ndt-03-00003" class="html-bibr">195</a>].</p>
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<p>Phase map under large and small fields of view. (<b>a</b>) Phase map of large field of view, and (<b>b</b>) phase map of small field of view [<a href="#B195-ndt-03-00003" class="html-bibr">195</a>].</p>
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<p>(<b>a</b>) The new shearography system with a spatial light modulator; (<b>b</b>) experimental result of a thimble-loaded aluminum plate; (<b>c</b>) experimental result of a composite plate with three flaws, modified [<a href="#B197-ndt-03-00003" class="html-bibr">197</a>].</p>
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<p>(<b>a</b>) Preparation of the helicopter fuselage with random speckle patterns for DIC analysis; (<b>b</b>) Comparison of the helicopter fuselage pre-impact and post-impact conditions, without applying DIC analysis; (<b>c</b>) Deformation fields derived through DIC analysis, illustrating structural changes resulting from the impact event. Adapted from [<a href="#B213-ndt-03-00003" class="html-bibr">213</a>,<a href="#B214-ndt-03-00003" class="html-bibr">214</a>].</p>
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<p>Correlation between DIC and AE monitoring of mechanical tests. (<b>a</b>) DIC snapshot of the tensile specimen, (<b>b</b>) AE snapshot highlighting the detected events, and (<b>c</b>) Combined stress profile and corresponding AE events during the test. Adapted from [<a href="#B220-ndt-03-00003" class="html-bibr">220</a>].</p>
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<p>Multi-scale analysis of strain distribution and crack propagation in SiC/SiC composite: (<b>a</b>) Displacement field overlaid on the sectioning plane; (<b>b</b>) Optical micrograph of the sectioned area highlighting the internal structure of the CMC; (<b>c</b>) Electron micrograph zoom-in on a large central crack within the composite. Red arrows denote fiber breaks, and blue arrows denote cracks in the paint. Adapted from [<a href="#B221-ndt-03-00003" class="html-bibr">221</a>].</p>
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<p>Region-specific market demand projections are provided for the non-destructive evaluation (NDE) of composite materials spanning the years 2021–2027, accompanied by a visual representation of the trend line superimposed on the data. Modified from [<a href="#B244-ndt-03-00003" class="html-bibr">244</a>].</p>
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<p>Schematic the self-healing composite with integrated damage detection. (<b>a</b>) Initial composite structure with microcapsules and Ag nanoparticles at the fiber-matrix interface. (<b>b</b>) Damage and subsequent self-healing process, coupled with thermal release detected by infrared imaging. Modified from [<a href="#B261-ndt-03-00003" class="html-bibr">261</a>].</p>
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<p>Comparison of defect characterization using thermal data from (<b>a</b>) pulse-phase (<b>left</b>) and lock-in (<b>right</b>) thermography methods and quantitative metrics (<b>b</b>) derived from phase differences. Modified from [<a href="#B268-ndt-03-00003" class="html-bibr">268</a>].</p>
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<p>Schematic of the use of acoustic emission for quality monitoring during a powder bed additive manufacturing. The arrows indicate the process flow: (1) AE signals are generated during selective laser melting (SLM), corresponding to varying porosity levels; (2) an FBG sensor records these signals; and (3) a spectral convolutional neural network (CNN) is trained to classify part quality based on porosity levels, based on extracted acoustic features. Modified from [<a href="#B269-ndt-03-00003" class="html-bibr">269</a>].</p>
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14 pages, 11937 KiB  
Article
A Refractive Index-Based Dual-Band Metamaterial Sensor Design and Analysis for Biomedical Sensing Applications
by Lakshmi Darsi and Goutam Rana
Sensors 2025, 25(1), 232; https://doi.org/10.3390/s25010232 - 3 Jan 2025
Viewed by 250
Abstract
We propose herein a metamaterial (MM) dual-band THz sensor for various biomedical sensing applications. An MM is a material engineered to have a particular property that is rarely observed in naturally occurring materials with an aperiodic subwavelength arrangement. MM properties across a wide [...] Read more.
We propose herein a metamaterial (MM) dual-band THz sensor for various biomedical sensing applications. An MM is a material engineered to have a particular property that is rarely observed in naturally occurring materials with an aperiodic subwavelength arrangement. MM properties across a wide range of frequencies, like high sensitivity and quality factors, remain challenging to obtain. MM-based sensors are useful for the in vitro, non-destructive testing (NDT) of samples. The challenge lies in designing a narrow band resonator such that higher sensitivities can be achieved, which in turn allow for the sensing of ultra-low quantities. We propose a compact structure, consisting of a basic single-square split ring resonator (SRR) with an integrated inverted Z-shaped unit cell. The projected structure provides dual-band frequencies resonating at 0.75 THz and 1.01 THz with unity absorption at resonant peaks. The proposed structure exhibits a narrow bandwidth of 0.022 THz and 0.036 THz at resonances. The resonant frequency exhibits a shift in response to variations in the refractive index of the surrounding medium. This enables the detection of various biomolecules, including cancer cells, glucose, HIV-1, and M13 viruses. The refractive index varies between 1.35 and 1.40. Furthermore, the sensor is characterized by its performance, with an average sensitivity of 2.075 THz and a quality factor of 24.35, making it suitable for various biomedical sensing applications. Full article
(This article belongs to the Section Optical Sensors)
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<p>Different outlooks of the sensor structure: (<b>a</b>) front view, (<b>b</b>) 3D perspective view, (<b>c</b>) periodic arrangement, and (<b>d</b>) cross-sectional view.</p>
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<p>The suggested absorber’s evolution: (<b>a</b>) a basic single-square SRR, (<b>b</b>) an inverted “Z”-shape, and (<b>c</b>) a combination of a basic single-square SRR and inverted Z-shape.</p>
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<p>Distribution of electric and magnetic fields, as well as surface currents, at the resonant frequencies of 0.75 THz and 1.01 THz: (<b>a</b>,<b>b</b>) E-fields, (<b>c</b>,<b>d</b>) H-fields, and (<b>e</b>,<b>f</b>) surface current.</p>
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<p>Absorption spectrum analysis by adjusting various design structure parameters: (<b>a</b>) slit width (g) of the basic single-square SRR, (<b>b</b>) width (w) of the basic single-square SRR, (<b>c</b>) interaction (i) between the inverted Z arms and the basic single-square SRR, and (<b>d</b>) substrate height <math display="inline"><semantics> <mrow> <mo>(</mo> <msub> <mi>h</mi> <mn>2</mn> </msub> <mo>)</mo> </mrow> </semantics></math>.</p>
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<p>The sensing performance of the sensor for (<b>a</b>) analyte n = 1.35 to 1.40 and (<b>b</b>) water and glucose detection.</p>
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<p>Relationship between the refractive index and (<b>a</b>) change in resonant frequency, (<b>b</b>) quality factor, (<b>c</b>) sensitivity, and (<b>d</b>) figure of merit.</p>
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<p>Relationship between the refractive index and (<b>a</b>) change in resonant frequency, (<b>b</b>) quality factor, (<b>c</b>) sensitivity, and (<b>d</b>) figure of merit.</p>
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<p>The sensing performance of the sensor for (<b>a</b>) HIV virus detection and (<b>b</b>) M13 virus detection.</p>
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<p>The sensing performance of the design: (<b>a</b>) breast cancer detection, (<b>b</b>) skin cancer detection, (<b>c</b>) MCF-7 detection, and (<b>d</b>) PC12 detection.</p>
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<p>Proposed working setup for the recommended sensor.</p>
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4 pages, 428 KiB  
Proceeding Paper
Quality Control and Management of Nondestructive Testing Process in Aircraft Fatigue Test
by Shuang Lv and Zhiwei Peng
Eng. Proc. 2024, 80(1), 9; https://doi.org/10.3390/engproc2024080009 - 2 Jan 2025
Viewed by 137
Abstract
Aircraft fatigue test is a critical step for new aircraft models to obtain certification. The primary task of fatigue test is to detect damage promptly and gather damage data. Therefore, to ensure the timeliness and effectiveness of non-destructive testing (NDT) data, it is [...] Read more.
Aircraft fatigue test is a critical step for new aircraft models to obtain certification. The primary task of fatigue test is to detect damage promptly and gather damage data. Therefore, to ensure the timeliness and effectiveness of non-destructive testing (NDT) data, it is essential to control and manage the quality of the NDT process in aircraft fatigue test. This paper, based on the characteristics and work features of NDT in aircraft fatigue test, aims to achieve the goal of timely damage detection by focusing on the five key aspects of NDT quality control, namely: personnel, equipment, materials, methods, and environment. It elaborates on the quality control process, identifies key aspects of quality management, and enhances the quality of NDT in aircraft fatigue test. Full article
(This article belongs to the Proceedings of 2nd International Conference on Green Aviation (ICGA 2024))
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<p>The standard process for component inspection.</p>
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<p>The standard process for full-scale fatigue inspection.</p>
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30 pages, 18127 KiB  
Article
Innovative Approaches to Material Selection and Testing in Additive Manufacturing
by Alexandr Fales, Vít Černohlávek, Jan Štěrba, Milan Dian and Marcin Suszyński
Materials 2025, 18(1), 144; https://doi.org/10.3390/ma18010144 - 2 Jan 2025
Viewed by 325
Abstract
This study focuses on selecting a suitable 3D printer and defining experimental methods to gather the necessary data for determining the optimal filament material for printing components of the VEX GO and VEX IQ robotic kits. The aim is to obtain the required [...] Read more.
This study focuses on selecting a suitable 3D printer and defining experimental methods to gather the necessary data for determining the optimal filament material for printing components of the VEX GO and VEX IQ robotic kits. The aim is to obtain the required data to identify an appropriate filament material and set 3D printing parameters to achieve the desired mechanical properties of the parts while maintaining cost-effectiveness. Another key objective is achieving optimal operational functionality, ensuring the required part performance with minimal printing costs. It is desirable for the modeled and printed parts to exhibit the required mechanical properties while maintaining economic efficiency. Another crucial aspect is achieving optimal functionality of the produced parts with minimal printing costs. This will be assessed by analyzing the impact of key 3D printing technology parameters, focusing in this research phase on material selection. The criteria for selecting filament materials include ease of printability under the conditions of primary and secondary schools, simplicity of printing, minimal need for post-processing, and adequate mechanical properties verified through experimental measurements and destructive tests on original parts from VEX GO and VEX IQ kits. The study analyzed various filaments regarding their mechanical properties, printability, and cost-effectiveness. The most significant practical contribution of this study is selecting a suitable filament material tested through a set of destructive tests, emphasizing maintaining the mechanical properties required for the real-life application of the parts. This includes repetitive assembly and disassembly of various robotic model constructions and their activation for demonstration purposes and applications of STEM/STEAM/STREAM methods in the educational process to achieve the properties of original components. Additionally, the study aims to set up 3D printing such that even a beginner-level operator, such as a primary or secondary school student under the supervision of their teacher or a teacher with minimal knowledge and experience in 3D printing, can successfully execute it. Further ongoing research focuses on evaluating the effects of characteristic 3D printing parameters, such as infill and perimeter, on the properties of 3D-printed parts through additional measurements and analyses. Full article
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<p>Printer Original Prusa MK4.</p>
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<p>Original part 2 × 8 Smooth Panel (228-2500-524) VEX—top side.</p>
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<p>Original part 2 × 8 Smooth Panel (228-2500-524) VEX—bottom side.</p>
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<p>Original part 2 × 12 Beam (228-2500-026) VEX—top side.</p>
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<p>Original part 2 × 12 Beam (228-2500-026) VEX—bottom side.</p>
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<p>Modified part 2 × 12 Beam (228-2500-026) VEX—top side.</p>
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<p>Modified part 2 × 12 Beam (228-2500-026) VEX—bottom side.</p>
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<p>Static tensile test—before and after the test completion.</p>
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<p>Tensile load test—multiple representations of the loading force curves—Original.</p>
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<p>Tensile load test—multiple representations of the loading force curves—PLA.</p>
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<p>Tensile load test—multiple representations of the loading force curves—PET-G1.</p>
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<p>Tensile load test—multiple representations of the loading force curves—PET-G2.</p>
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<p>Tensile load test—multiple representations of the loading force curves—ASA.</p>
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<p>Tensile load test—multiple representations of the loading force curves—ABS.</p>
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<p>Deflection test—before and after the test.</p>
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<p>Deflection test—multiple representations of the applied force curves—Original.</p>
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<p>Deflection test—multiple representations of the applied force curves—PLA.</p>
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<p>Deflection test—multiple representations of the applied force curves—PET-G1.</p>
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<p>Deflection test—multiple representations of the applied force curves—PET-G2.</p>
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<p>Deflection test—multiple representations of the applied force curves—ASA.</p>
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<p>Deflection test—multiple representations of the applied force curves—ABS.</p>
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21 pages, 7471 KiB  
Article
Monitoring the Calibration Status of a Universal Testing Machine Through the Implementation of Acoustic Methods: Development of Equipment and a Suitable Interface
by Sharath P. Subadra, Roy Skaria, Andrea Hasselmann, Eduard Mayer and Shahram Sheikhi
NDT 2025, 3(1), 2; https://doi.org/10.3390/ndt3010002 - 2 Jan 2025
Viewed by 376
Abstract
The calibration of a universal testing machine (UTM) verifies the accuracy of the system instruments responsible for obtaining force and displacement measurements. This process involves comparing the instrument to equipment that has already been calibrated to a known traceable standard. The limit of [...] Read more.
The calibration of a universal testing machine (UTM) verifies the accuracy of the system instruments responsible for obtaining force and displacement measurements. This process involves comparing the instrument to equipment that has already been calibrated to a known traceable standard. The limit of accuracy is then certified and the traceability of the measurements is determined. There are several internationally recognized standards that are used to calibrate the cross-head speed and displacement (ASTM E2658 and E2309, respectively), strain and load rate (ASTM E2309), measurement of tension, compression (ASTM E4) and dynamic force (ASTM E467). The current study aims to monitor the calibration status of UTMs through the implementation of acoustic methods. A methodology is developed whereby a reference sample is initially identified with suitable material properties, enabling it to be used continuously. The sample is used simultaneously with acoustic instruments to check its natural frequencies, which enables the monitoring of the UTM calibration status. An algorithm is developed that enables the user to interact with the system, thus forming an interface and helping the user to check the calibration status of the equipment. The entire system is validated to check if the equipment and the inbuilt algorithm can predict the calibration status of the machine. It was found that the geometric constraints imposed on the sample influence the output from the algorithm, and hence correct values should be fed to the system. Our sample never lost its elastic characteristics through continuous use, demonstrating that it can be used to continuously monitor the machine’s status. Full article
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<p>Reference sample dimensions.</p>
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<p>QASAR 200 UTM.</p>
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<p>Loading stages of reference samples.</p>
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<p>Sample constrained for acoustic excitation.</p>
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<p>Sound system used in the project: (<b>A</b>) Dytran 3225F accelerometer and (<b>B</b>) data acquisition system.</p>
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<p>Sensor integration for calibration monitoring.</p>
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<p>Overview of the system developed for calibration status check.</p>
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<p>Overview of the algorithm.</p>
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<p>Simulated modal frequencies of the reference sample (both Al6060 and M700).</p>
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<p>A sample spectrum generated for Al6060.</p>
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<p>Plots generated for Al6060 from stage 1 to 2. (<b>A</b>) Sample loaded until 0.1% strain, (<b>B</b>) same sampled loaded subsequently until 0.15% strain, (<b>C</b>) spectrum before sample was loaded and (<b>D</b>) spectrum after sample was loaded.</p>
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<p>Plots generated for Al6060 during stage 3. (<b>A</b>) Sample loaded until 0.2% strain and (<b>B</b>) spectrum obtained after test.</p>
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<p>Plots generated for M700 from stage 1 to 2. (<b>A</b>) Sample loaded until 0.1% strain, (<b>B</b>) Same sampled loaded subsequently until 0.15% strain, (<b>C</b>) spectrum before sample was loaded and (<b>D</b>) spectrum after sample was loaded.</p>
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<p>Plots generated for M700 from stage 1 to 2. (<b>A</b>) Sample loaded until 0.1% strain, (<b>B</b>) Same sampled loaded subsequently until 0.15% strain, (<b>C</b>) spectrum before sample was loaded and (<b>D</b>) spectrum after sample was loaded.</p>
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<p>Plots generated for M700 during stage 3. (<b>A</b>) Sample loaded until 0.2% strain and (<b>B</b>) spectrum obtained after test.</p>
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<p>(<b>A</b>) Code excerpt from the source code for calibration and (<b>B</b>) GUI developed for checking calibration status of machine.</p>
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21 pages, 17144 KiB  
Article
Failure and Degradation Mechanisms of Steel Pipelines: Analysis and Development of Effective Preventive Strategies
by Marcin Kowalczyk, Jakub Andruszko, Paweł Stefanek and Robert Mazur
Materials 2025, 18(1), 134; https://doi.org/10.3390/ma18010134 - 31 Dec 2024
Viewed by 410
Abstract
The increasing challenges related to the reliability and durability of steel pipeline infrastructure necessitate a detailed understanding of degradation and failure mechanisms. This study focuses on selective corrosion and erosion as critical factors, analyzing their impact on pipeline integrity using advanced methods, including [...] Read more.
The increasing challenges related to the reliability and durability of steel pipeline infrastructure necessitate a detailed understanding of degradation and failure mechanisms. This study focuses on selective corrosion and erosion as critical factors, analyzing their impact on pipeline integrity using advanced methods, including macroscopic analysis, corrosion testing, microscopic examination, tensile strength testing, and finite element method (FEM) modeling. Selective corrosion in the heat-affected zones (HAZs) of longitudinal welds was identified as the dominant degradation mechanism, with pit depths reaching up to 6 mm, leading to tensile strength reductions of 30%. FEM analysis showed that material loss exceeding 8 mm in weld areas under standard operating pressure (16 bar) induces critical stress levels, risking pipeline failure. Erosion was found to exacerbate selective corrosion, accelerating degradation in high-stress zones. Practical recommendations include the use of corrosion-resistant materials, such as duplex steels, and implementing integrated monitoring strategies combining non-destructive testing with FEM-based predictive modeling. These insights contribute to developing robust preventive measures to ensure the safety and longevity of pipeline infrastructure. Full article
(This article belongs to the Special Issue Advances in Corrosion and Protection of Metallic Materials)
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<p>Example segments of the analyzed pipes.</p>
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<p>Example of a damaged water pipeline segment—longitudinal seam rupture: (<b>a</b>) General view along the crack and (<b>b</b>) close-up view of the seam rupture location.</p>
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<p>Weld from the inside of the pipe on the unruptured section after cleaning.</p>
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<p>Hard, compact, subsurface permeable corrosion product coatings that separate the pipe material from the water flow inside the pipe: (<b>a</b>) Start of the pipe seam and (<b>b</b>) mechanical separation of the crust.</p>
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<p>Pipe after the removal of corrosion products, showing characteristic pits that degrade the longitudinal weld of the pipe.</p>
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<p>Pipe with a spiral SAWH seam: Longitudinal seam rupture in pipe P1, with visible defects in the weld: (<b>a</b>) Seam with visible corrosion products and (<b>b</b>) seam after cleaning off the corrosion products.</p>
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<p>Water pipe with longitudinal seam—mechanism of selective corrosion formation: 1—steel pipe shell of the pipeline; 2—trapped water layer between the pipe material and the layer of corrosion products; 3—compact, semi-permeable layer of corrosion products and contaminants; 4—external protective layer; 5—areas of selective corrosion development along the HAZ of the longitudinal weld; 6—local pits as a result of selective corrosion. σr—circumferential stresses in the pipe; p—network pressure.</p>
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<p>View of the remaining weld remnants at the edge of the joint with the longitudinal weld of the fractured pipe.</p>
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<p>View of the internal surface of the pipe segment illustrating the degree of weld degradation for water transport pipes.</p>
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<p>Division of the pipe segment into samples for macroscopic analysis (1–8) and mechanical testing (SP1–SP3).</p>
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<p>Macrostuctures of welded joint samples: (<b>a</b>) Sample 1, (<b>b</b>) Sample 2, (<b>c</b>) Sample 6, (<b>d</b>) Sample 8 from <a href="#materials-18-00134-f010" class="html-fig">Figure 10</a>.</p>
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<p>Anodic areas (<b>blue</b>) and cathodic areas (<b>pink</b>) in the welded joints of the pipe: (<b>a</b>) Sample 6, (<b>b</b>) Sample 8 from <a href="#materials-18-00134-f010" class="html-fig">Figure 10</a>.</p>
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<p>Potential profile: (<b>a</b>) Base material; (<b>b</b>) heat affected zone (HAZ) area; (<b>c</b>) weld area.</p>
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<p>Microscopic analysis—Pits in HAZ: (<b>a</b>) Sample 1, (<b>b</b>) Sample 2, (<b>c</b>) Sample 6, (<b>d</b>) Sample 8 from <a href="#materials-18-00134-f010" class="html-fig">Figure 10</a>.</p>
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<p>Samples after strength testing: (<b>a</b>)—SP1; (<b>b</b>)—SP2; (<b>c</b>)—SP3.</p>
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<p>Tensile curves: (<b>a</b>)—SP1; (<b>b</b>)—SP2; (<b>c</b>)—SP3 where: green—Test 1, blue—Test 2, red—Test 3.</p>
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<p>Schematics for modeling the pipe section and example model dimensions: (<b>a</b>) base weld cross-section dimensions; (<b>b</b>) schematic of weld material loss.</p>
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<p>Circumferential normal stresses [MPa] at a pressure of 16 bar at various levels of longitudinal weld degradation.</p>
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<p>Equivalent plastic strains in the material at a pressure of 16 bar at various levels of longitudinal weld degradation.</p>
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<p>Sharp termination of the notch bottom in the pit caused by selective corrosion: (<b>a</b>) Dimensions of the model in the second stage of numerical analysis and (<b>b</b>) discrete model in the pit area during the second stage of numerical analysis.</p>
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<p>Results of the numerical analyses for the second stage: (<b>a</b>) Circumferential normal stress in [MPa] at a pressure of 30 bar and a degradation depth of 6 mm and (<b>b</b>) equivalent plastic strain at a pressure of 30 bar and a degradation depth of 6 mm.</p>
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<p>Plastic deformation as a function of pressure at the bottom of the hole in the longitudinal weld of the pipe depending on the depth of loss of material.</p>
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15 pages, 5533 KiB  
Article
Measurement of Soil–Water Characteristic Curve of Vegetative Soil Using Polymer-Based Tensiometer for Maintaining Environmental Sustainability
by Widjojo Adi Prakoso, Abdul Halim Hamdany, Martin Wijaya, Rabbani Isya Ramadhan, Aldo Wirastana Adinegara, Alfrendo Satyanaga, Glenn Adriel Adiguna and Jong Kim
Sustainability 2025, 17(1), 218; https://doi.org/10.3390/su17010218 - 31 Dec 2024
Viewed by 456
Abstract
The interaction between moisture content and soil suction is commonly represented by a soil–water characteristic curve (SWCC). The direct measurement of water content can be easily achieved, but it usually requires a destructive method where the soil sample needs to be oven-dried. Hence, [...] Read more.
The interaction between moisture content and soil suction is commonly represented by a soil–water characteristic curve (SWCC). The direct measurement of water content can be easily achieved, but it usually requires a destructive method where the soil sample needs to be oven-dried. Hence, indirect measurement is commonly employed for monitoring purposes. The limitation of this approach is the variability in water content at the wilting point, particularly for plants in different types of soil. While the moisture content at the wilting point varies greatly, suction at the wilting point is typically around 1500 kPa despite varying slightly depending on the type of plant. However, suction measurement using a normal tensiometer is limited to 100 kPa due to cavitation. Hence, it is not sufficient to cover up to the wilting point. The focus of this paper is the establishment of a polymer-based tensiometer utilizing a 15 bar ceramic disc for the measurement of high suction. The suitability of the polymer-based tensiometer in measuring the soil suction of vegetative soil is conducted by performing a soil–water characteristic curve test on vegetative soil. The SWCC produced from the polymer-based tensiometer is verified using SWCC produced from a centrifuge test. The results show that the SWCCs from both polymer-based tensiometer and centrifuge tests are comparable. Hence, suction measurement using a polymer-based tensiometer is deemed reliable. This advancement in suction measurement technology is crucial for improving irrigation practices, optimizing water use, and enhancing agricultural productivity, which in turn contributes to environmental sustainability by minimizing water waste and ensuring efficient soil management. Full article
(This article belongs to the Section Soil Conservation and Sustainability)
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<p>Vegetative soil specimen. (<b>a</b>) Original soil. (<b>b</b>) Reconstituted soil.</p>
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<p>Compaction curve of vegetative soil.</p>
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<p>Grain size distribution of vegetative soil.</p>
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<p>PBT design modified from Hamdany et al. (2022) [<a href="#B15-sustainability-17-00218" class="html-bibr">15</a>].</p>
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<p>Synthesis process of PAM polymer.</p>
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<p>SWCC test by using PBT.</p>
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<p>Specimen for centrifuge test.</p>
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<p>Change in polymer pressure and temperature over time.</p>
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<p>Temperature correction.</p>
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<p>Evaporation test results.</p>
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<p>Maximum polymer pressure.</p>
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<p>Shrinkage curve of vegetative soil [<a href="#B30-sustainability-17-00218" class="html-bibr">30</a>].</p>
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<p>Monitoring of soil suction and volumetric water content for 20 days.</p>
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<p>SWCC-w of vegetative soil [<a href="#B29-sustainability-17-00218" class="html-bibr">29</a>].</p>
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<p>SWCC-θ<sub>w</sub> of vegetative soil [<a href="#B29-sustainability-17-00218" class="html-bibr">29</a>].</p>
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24 pages, 6819 KiB  
Article
Three-Dimensional Reconstruction of Road Structural Defects Using GPR Investigation and Back-Projection Algorithm
by Lutai Wang, Zhen Liu, Xingyu Gu and Danyu Wang
Sensors 2025, 25(1), 162; https://doi.org/10.3390/s25010162 - 30 Dec 2024
Viewed by 374
Abstract
Ground-Penetrating Radar (GPR) has demonstrated significant advantages in the non-destructive detection of road structural defects due to its speed, safety, and efficiency. This paper proposes a three-dimensional (3D) reconstruction method for GPR images, integrating the back-projection (BP) imaging algorithm to accurately determine the [...] Read more.
Ground-Penetrating Radar (GPR) has demonstrated significant advantages in the non-destructive detection of road structural defects due to its speed, safety, and efficiency. This paper proposes a three-dimensional (3D) reconstruction method for GPR images, integrating the back-projection (BP) imaging algorithm to accurately determine the size, location, and other parameters of road structural defects. Initially, GPR detection images were preprocessed, including direct wave removal and wavelet denoising, followed by the application of the BP algorithm to effectively restore the defect’s location and size. Subsequently, a 3D data set was constructed through interpolation, and the effective reflection data were extracted by using a clustering algorithm. This algorithm distinguished the effective reflection data from the background data by determining the distance threshold between the data points. The 3D imaging of the defect was then performed in MATLAB. The proposed method was validated using both gprMax simulations and laboratory test models. The experimental results indicate that the correlation between the reconstructed and actual defects was approximately 0.67, demonstrating the method’s efficacy in accurately achieving the 3D reconstruction of road structural defects. Full article
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<p>Three-dimensional reconstruction process for road structural defects.</p>
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<p>Principle of GPR detection.</p>
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<p>Three-level wavelet decomposition.</p>
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<p>GPR image of the underground cavity model.</p>
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<p>Principle of BP algorithm imaging.</p>
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<p>BP imaging.</p>
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<p>Basic flow of K-means clustering algorithm.</p>
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<p>Defect model.</p>
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<p>B-Scan images.</p>
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<p>B-Scan images.</p>
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<p>Results of BP imaging.</p>
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<p>Results of BP imaging.</p>
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<p>Results of 3D reconstruction.</p>
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<p>Laboratory test model.</p>
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<p>IDS-RIS GPR.</p>
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<p>B-Scan images and processing results of laboratory test.</p>
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<p>B-Scan images and processing results of laboratory test.</p>
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<p>Radar used in detection.</p>
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<p>Result of 3D reconstruction on the actual road.</p>
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<p>Core sample.</p>
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24 pages, 13851 KiB  
Article
Analysis of the Influence of Manufacturing Technology on Selected Static, Fatigue and Morphological Properties of CFRP Composites
by Andrzej Kubit, Kishore Debnath, Ján Slota, Filip Dominik, Ankit Dhar Dubey, Gorrepotu Surya Rao and Krzysztof Żaba
Materials 2025, 18(1), 102; https://doi.org/10.3390/ma18010102 - 30 Dec 2024
Viewed by 350
Abstract
The aim of this study was to compare the mechanical properties of carbon-fiber-reinforced polymer (CFRP) composites produced using three popular technologies. The tests were performed on composites produced from prepregs in an autoclave, the next variant is composites produced using the infusion method, [...] Read more.
The aim of this study was to compare the mechanical properties of carbon-fiber-reinforced polymer (CFRP) composites produced using three popular technologies. The tests were performed on composites produced from prepregs in an autoclave, the next variant is composites produced using the infusion method, and the third variant concerns composites produced using the vacuum-assisted hand lay-up method. For each variant, flat plates with dimensions of 1000 mm × 1000 mm were produced while maintaining similar material properties and fabric arrangement configuration. Samples for testing were cut using a plotter in the 0° and 45° directions. Non-destructive tests (NDTs) were carried out using the active thermography method, demonstrating the correctness of the composites, i.e., the absence of structural defects for all variants. Static peel strength tests were carried out for samples with different directional orientations. The tests were carried out at temperatures of +25 °C and +80 °C. At room temperature, similar strengths were demonstrated, which for the 0° orientation were 619 MPa, 599 MPa and 536 MPa for the autoclave, vacuum and infusion variants, respectively. However, at a temperature of +80 °C, only the composite produced in the autoclave maintained the stability of its properties, showing a strength of 668 MPa. Meanwhile, in the case of the composite produced by the infusion method, a decrease in strength at an elevated temperature of 46.5% was demonstrated, while for the composite produced by the hand lay-up method, there was a decrease of 46.2%. For the last two variants, differential scanning calorimetry (DSC) analysis of epoxy resins constituting the composite matrices was carried out, showing a glass transition temperature value of 49.91 °C for the infusion variant and 56.07 °C for the vacuum variant. In the three-point static bending test, the highest strength was also demonstrated for the 0ᵒ orientation, and the bending strength was 1088 MPa for the autoclave variant, 634 MPa for the infusion variant and 547 MPa for the vacuum variant. The fatigue strength tests in tension at 80% of the static strength for the infusion variant showed an average fatigue life of 678.788 × 103 cycles for the autoclave variant, 176.620 × 103 cycles for the vacuum variant and 159.539 × 103 cycles for the infusion variant. Full article
(This article belongs to the Special Issue Advances in Carbon Fiber/Resin Matrix Polymer Composites)
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<p>Schematic diagram showing three technologies of fabrication process used for composite specimens; (1) hand layup, (2) vacuum infusion and (3) autoclave process</p>
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<p>Samples produced with three different technologies during testing by active thermography method.</p>
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<p>Results of tests conducted using active thermography for composites produced using three different technologies.</p>
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<p>Results of the velocity of sound wave propagation in composite samples fabricated with: hand lay-up (<b>a</b>), vacuum infusion (<b>b</b>) and autoclave (<b>c</b>).</p>
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<p>Results of the velocity of sound wave propagation in composite samples fabricated with: hand lay-up (<b>a</b>), vacuum infusion (<b>b</b>) and autoclave (<b>c</b>).</p>
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<p>View of the composite surface at different magnifications for the variants: autoclave (<b>a</b>), infusion (<b>b</b>) and vacuum (<b>c</b>).</p>
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<p>Results of static strength and Young’s modulus obtained in tensile test for sample orientation 0° (<b>a</b>,<b>b</b>) and 45° (<b>c</b>,<b>d</b>) and 3-point bending test (<b>e</b>,<b>f</b>) carried out at room and elevated temperature.</p>
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<p>Comparison of curves obtained in the static tensile test of samples with an orientation of 0° carried out at 25 °C (<b>a</b>) and at 80 °C (<b>b</b>), with an orientation of 45° carried out at 25 °C (<b>c</b>) and at 80 °C (<b>d</b>) and bending test of samples carried out at 25 °C (<b>e</b>) and at 80 °C (<b>f</b>).</p>
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<p>Different areas of delamination due to the failure of samples oriented at an angle of 45° and subjected to static tensile test.</p>
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<p>Different areas of delamination due to the failure of samples oriented at an angle of 45° and subjected to bending test.</p>
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<p>EDX analysis of composite specimen.</p>
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<p>SEM images of mechanically tested specimen showing different modes of failure: fiber breakage in stress concentration areas (<b>a)</b>; parallel cracking of both fibers and matrix (<b>b)</b>; cracked surface with fiber pull-out (<b>c</b>); Fiber pull-out from the matrix and their breakage in various planes (<b>d</b>); fibers partially embedded in the matrix, with visible matrix breaking and delamination (<b>e</b>); matrix cracking and fiber fracture simultaneously (<b>f</b>).</p>
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<p>DSC analysis results of epoxy resins constituting the matrix of composites produced by hand lay-up (<b>a</b>) and infusion (<b>b</b>) methods.</p>
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<p>Comparative fatigue diagram for the tested composite variants.</p>
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<p>Fatigue fractures for samples of the following variants: autoclave (<b>a</b>), infusion (<b>b</b>) and vacuum at different magnifications (<b>c</b>,<b>d</b>).</p>
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21 pages, 14395 KiB  
Article
Efficacy of Trichoderma longibrachiatum SC5 Fermentation Filtrate in Inhibiting the Sclerotinia sclerotiorum Growth and Development in Sunflower
by Enchen Li, Na Zhu, Shuwu Zhang, Bingliang Xu, Lilong Liu and Aiqin Zhang
Int. J. Mol. Sci. 2025, 26(1), 201; https://doi.org/10.3390/ijms26010201 - 29 Dec 2024
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Abstract
Sclerotinia sclerotiorum is a destructive pathogen responsible for sunflower sclerotinia rot, resulting in substantial yield and economic losses worldwide. Trichoderma species have demonstrated the capacity to inhibit plant pathogen growth through the production of secondary metabolites. However, there are fewer recent studies focusing [...] Read more.
Sclerotinia sclerotiorum is a destructive pathogen responsible for sunflower sclerotinia rot, resulting in substantial yield and economic losses worldwide. Trichoderma species have demonstrated the capacity to inhibit plant pathogen growth through the production of secondary metabolites. However, there are fewer recent studies focusing on the application of Trichoderma metabolites in inhibiting S. sclerotiorum growth and development and controlling sunflower sclerotinia rot disease. Our results showed that five Trichoderma strains (SC5, T6, TN, P6, and TS3) exhibited mycelial growth inhibition higher than 60% in dual culture assays out of the 11 tested strains. The Trichoderma SC5 fermentation filtrate exhibited superior efficacy compared to other strains, achieving a 94.65% inhibition rate of mycelial growth on S. sclerotiorum, 96% inhibition of myceliogenic germination of sclerotia, and 81.05% reduction in the oxalic acid content of S. sclerotiorum, while significantly increasing the cell membrane permeability. In addition, the Trichoderma SC5 fermentation filtrate significantly decreased the activities of polygalacturonase and pectin methyl-galacturonic enzymes and even caused S. sclerotiorum hyphae to swell, branch, twist, lyse, and inhibited the production and development of sclerotia. Moreover, the Trichoderma SC5 fermentation filtrate downregulated genes expression that associated with the growth and infection of S. sclerotiorum. The control efficacies of the protective and curative activities of the Trichoderma SC5 fermentation filtrate were 95.45% and 75.36%, respectively, on detached sunflower leaves at a concentration of 8 mg/mL. Finally, the Trichoderma SC5 was identified as Trichoderma longibrachiatum through morphological and phylogenetic analysis. Our research indicates that the T. longibrachiatum SC5 can be considered a promising biological control candidate against S. sclerotiorum and controlling the sunflower sclerotinia rot disease, both in vitro and in vivo. Full article
(This article belongs to the Section Molecular Microbiology)
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Graphical abstract

Graphical abstract
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<p>Inhibitory effect (<b>A</b>) and antagonistic activity (<b>B</b>) of <span class="html-italic">Trichoderma</span> strains on <span class="html-italic">S. sclerotiorum</span> at 7 days after incubation, where CK is the control of <span class="html-italic">S. sclerotiorum</span> without confrontation. Means with different letters are significantly different at <span class="html-italic">p</span> &lt; 0.05 according to Duncan’s multiple range test.</p>
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<p>The inhibitory effect of different <span class="html-italic">Trichoderma</span> spp. fermentation filtrate on <span class="html-italic">S. sclerotiorum</span>. (<b>A</b>): Effects of different <span class="html-italic">Trichoderma</span> spp. fermentation filtrate on the mycelial growth of <span class="html-italic">S. sclerotiorum</span> on PDA plates at 5 days. (<b>B</b>): Effect of SC5 fermentation filtrate on hyphal morphology of <span class="html-italic">S. sclerotiorum</span> at 5 days after inoculation. (<b>a</b>) Healthy hyphae of <span class="html-italic">S. sclerotiorum</span>; (<b>b</b>) hyphae to branch; (<b>c</b>) treated hyphae with twisted; (<b>d</b>) hyphae lysis. (<b>C</b>): The effect of <span class="html-italic">Trichoderma</span> spp. fermentation filtrate on the mycelial growth and sclerotial formation of <span class="html-italic">S. sclerotiorum</span> at 20 days after incubation.</p>
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<p>Effect of different <span class="html-italic">Trichoderma</span> spp. fermentation filtrate on myceliogenic germination of sclerotia on PDA at 5 days.</p>
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<p>Standard curve for calculating oxalic acid content (<b>A</b>) and oxalic acid content of <span class="html-italic">S. sclerotiorum</span> after being treated with five <span class="html-italic">Trichoderma</span> strains fermentation filtrate (<b>B</b>). Bars represent the standard deviations of the means. According to Duncan’s multiple range test, there are significant differences (<span class="html-italic">p</span> &lt; 0.05) between the mean values in columns labeled with the different letters.</p>
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<p>Effect of <span class="html-italic">Trichoderma</span> spp. fermentation filtrate on the relative conductivity of <span class="html-italic">S. sclerotiorum</span> mycelium. Bars represent the standard deviations of the means. Means labeled with the different letters for each time period indicate significant differences (<span class="html-italic">p</span> &lt; 0.05) according to Duncan’s multiple range test.</p>
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<p>Effect of <span class="html-italic">Trichoderma</span> spp. fermentation filtrate on the cell wall degrading enzymes (<b>A</b>) PG and (<b>B</b>) PMG activities of <span class="html-italic">S. sclerotiorum</span>. Bars represent the standard deviations of the means. Means labeled with the different letters for each time period indicate significant differences (<span class="html-italic">p</span> &lt; 0.05) according to Duncan’s multiple range test.</p>
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<p>Relative expression levels of 14 genes of <span class="html-italic">S. sclerotiorum</span> after treatment with the <span class="html-italic">Trichoderma</span> SC5 fermentation filtrate at 5 days. Bars indicate the standard deviation, and asterisks (*) indicate the significant differences (one-way ANOVA): * <span class="html-italic">p</span> &lt; 0.05 and ** <span class="html-italic">p</span> &lt; 0.01.</p>
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<p>Curative (<b>A</b>) and protective activities (<b>B</b>) of <span class="html-italic">Trichoderma</span> SC5 fermentation filtrate on sunflower leaves after inoculation.</p>
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<p>Morphological characteristics of <span class="html-italic">Trichoderma</span> SC5 that cultured on PDA medium. (<b>A</b>) front colony; (<b>B</b>) reverse colony; (<b>C</b>) conidia; (<b>D</b>) conidiophores. Photographs were taken at 5 days post-inoculation.</p>
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<p>Multi-locus phylogram of the present <span class="html-italic">Trichoderma</span> SC5 (red words) based on the combination of ITS, <span class="html-italic">EF-1α1,</span> and <span class="html-italic">RPB2</span> genes sequence. <span class="html-italic">Protocrea farinose</span> (CBS 121551) was selected as outgroup. Bootstrap values at the nodes are based on 2000 replicates. The colors represent clades shown on the concatenated phylogram of the three loci.</p>
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